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     This project has received funding from the European Union’s Horizon 2020 research and innovationprogrammeunder grant agreement N° 636!2

    Integrated Control and Sensingfor Sustainable Operation of

    Flexible Intensied Processes

     June 29, 201

    Prof! "r! Sebastian #ngell

    $% "ort&und

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    2

    $'e Partners in t'e Consortiu&

    Universit"deg#i $tudidi %ag#iari

    $upp#ier forinstrumentation& $'Es

    (esearch institutes& academia)rocess industr*

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

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    /dvance the production of high-va#ue products thatmeet high ua#it* demands in (exible intensiedcontinuous plants 1* introducing nove# on#ine

    sensors & c#osed-#oop contro# methods

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      3

    )ission

    'iniaturizedeuipment

    ntensi4edheat & mass

    transfer

    )ossi1#*modu#ar

    setup

    )roductuniformit*

    $ustaina1i#it*

    5ast adaption tomaret demand

    nnovativeproducts

    C'aracteristics *enets

    Containerized modular plant from F³ Factory project 

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    Co&pared to batc' processes7 there are signicant benets of 8e9i1#e intensi4ed continuous processes in man* cases

    $peci4c cha##enges:

    • $ma## dimensions  fast sensors & c#osed-#oop contro# needed

    • Higher ua#it* #eve#s  more accurate sensors needed

    %omp#e9 phenomena   )/T and mode#-1ased contro# necessar*• nnovative products  fast design7 engineering and optimization

    • 5ou#ing and c#ogging  needs specia# attention

    ntegrated )/T-1ased )rocess %ontro# copes ;ith these cha##enges:

    • 5ast and accurate on#ine sensing of e* product and process

    parameters• )/T and mode# 1ased c#osed-#oop contro# and on#ine optimization

    •  Too#s for design7 monitoring7 and optimization of the process and of itscontro# s*stem

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      4

    )oti+ation

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    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      5

    pproac'

    "e+elop ne- tec'nologies for Integrated ProcessControl

    ,n#ine $ensors%#osed-#oop

    %ontro#$oft;are Too#s

    ntegrated va#idation in8e9i1#e intensi4ed continuous

    p#ants

    High quality products

    Sustainabl

    e processes

    Competitiv 

    e prices Flexibility 

    %ross-sectoria#

    dissemination & e9p#oitation

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    Intensied

    s.nt'esisof organicco&pounds

    Intensied

    production of'ig'/+iscouspol.&ers

    Continuous

    for&ulationof co&plex liuids

    Setup

     Tu1u#ar reactor cu#t to contro# =isruptions ? ;aste

    o+el

    sensors

    on#ine N'( sensor

    on#ine fou#ing sensor

    on#ine rheo#og*

    sensor for po#*merme#ts

    on#ine rheo#og*

    sensor ;ith air-1u11#e detection+enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      6

    Case Studies o+el $ec'nologies

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    Online r'eolog.

    sensors

    Online fouling

    sensor

    Online )3

    sensor

    )rocessparameter

    @iscosit* vs shearrate7 non-Ne;tonian 8uids7po#*mer me#ts

     Thicness offou#ing #a*er in atu1u#ar reactor

    %ompositions andratios of su1stances

    5eatures n#ine7 non-invasive7 measureacross pipe7mu#ti-phase-use7fast

    n#ine7 non-invasive7 possi1#*space-reso#ved

    /t-#ine7 fast7accurate7 possi1#*ca#i1ration free7high #inearit*

    )rincip#e U#trasoundAacross pipeB

    U#trasoundAa#ong pipeB

    '(-N'(spectroscop*ApermanentmagnetB

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      7

    o+el sensing tec'nologies

    $

    N

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    $ec'nolog. Features

    'ode#-1ased c#osed-#oopcontro# -

    Using simp#e rigorous mode#s ;ithon#ine adaptation of parameters

    - terative optimization- )#ant-;ide contro#

    =ata-1ased c#osed-#oopcontro#

    - =ata-1ased mode#s for comp#e9phenomena

    -%#osed-#oop contro# 1ased upon thesemode#s

     Too# for sensor fai#uredetection

    - nterna# mode# is trained using processdata

    - ,n#ine correction of fa#se sensor data

     Too# for data-mining-

    Using Cdata cu1esD ;hich com1ineprocess7 contro#7 and design data

    - denti4es #ong-term deviations- Ena1#es process optimization

     Too# for design eva#uation - Eva#uation of the integrated contro#s*stem in an ear#* design stage

    -Using rea#istic production scenarios+enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -

    20.6-06-2!  8

    o+el Control $ec'nologies $ools

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    Integrated 4alidation of $ec'nologies

    ProcessA8e9i1#e7 intensi4ed7

    continuousB

    d+anced P$5composition ? rheo#og* ? fou#ing

    6 sensors a+ailable on t'e &ar7 

    )onitoring$ensor fai#ures ? performance

    $ based adapti+e control(igorous and data-1ased contro#

    )#ant-;ide contro#

    Design valuation

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

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    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

      10

    #xa&ple for integrated +alidation5

    Intensied s.nt'esis of organic co&pounds 

    'i9ing

    (eactorsection .

    (eactorsection 2

    =os

    =os/2

    =os/.=os

    N'(

    5ou#ing$ensor

    Sensors

    ,n#ine state& parameter

    estimation

    'ode#-1asedcontro#

    Control 

    ,ther sensors

    $ensor fai#uredetection &

    correction

    ,n#ineperformancemonitoring

    Monitoring

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    %,N$EN$ focuses on 8e9i1#e intensi4ed continuousprocesses

    Nove# on#ine-sensors7 advanced contro# methodsand monitoring too#s are deve#oped and integrated

    to ena1#e to e9p#oit the 1ene4ts of these processes

     The sensing and contro# techno#ogies can a#so 1eused for conventiona# processes

    %ross-sectoria# dissemination and e9p#oitation ;i##;iden the impact of %,N$EN$ on the processindustries

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

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    Conclusions

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    $'an7 .ou8

    12

    Emai#: manue#reme#heF1a*ercom

    Coordinator5 )anuel Pereira 3e&el'e

    +enera# %,N$EN$ )resentation - 'anue# )ereira (eme#he - %ag#iari -20.6-06-2!

    mailto:[email protected]:[email protected]