combechem elab book ui draft proposed by m.c. schraefel, june 15 ‘03 revised, june 19, ‘03 based...

29
CombeChem elab book UI • Draft proposed by m.c. schraefel, june 15 ‘03 • Revised, June 19, ‘03 • Based on tea experiment runs 1 and 2

Post on 19-Dec-2015

214 views

Category:

Documents


0 download

TRANSCRIPT

CombeChem elab book UI

• Draft proposed by m.c. schraefel, june 15 ‘03

• Revised, June 19, ‘03

• Based on tea experiment runs 1 and 2

Lab Bench Station

Chemist:

Date:

PLEASE ENTER YOUR ID(iButton) to begin logging

for your experiment(s)

PLEASE ENTER YOUR ID(iButton) to begin logging

for your experiment(s)

LogBench Station ActiveChemist: Graham

Experiment Selected: (Tea 1a)

Date: Friday, July 13, 2003

Tea 1aWater 1Light 4

(screen 2a)

CancelPause

LogBench Station ActiveChemist: Graham

Experiment Selected: (Tea 1a)

Date: Friday, July 13, 2003

Tea 1aWater 1Light 4

(screen 2a1)

CancelPause

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | ____

(screen 2b)

ProcessOverview

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Record

Yield: _______% Tea _______mlID:Location:

CancelPause Log Out

LogBench Station Active

DataOverview

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 10_|ml

(screen 3)

ProcessOverview

Yield: Tea _______%

Record

Yield: _______% Tea _______mlID: Location:

CancelPause Log Out

LogBench Station Active

DataOverview

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 4)

ProcessOverview

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Measure Set

Yield: _______% Tea _______mlID: Location:

CancelPause

DataOverview

TLC captures (link)

Log Out

LogBench Station Active

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 5)

ProcessOverview

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion ______ Record

Sample at ______ (min). State is _________% Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%

Record Done

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6)

ProcessOverview

- Phase 1: Make Tea [+- Phase 2: Decant Tea[+

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion ______ Record

TLC captures (link)

Sample at __|__ (min). State is _________% Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%

Record Done

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6b)

ProcessOverview

- Phase 1: Make Tea [+- Phase 2: Decant Tea [-

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion ______ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __|____% Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%

Record Done

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6c)

ProcessOverview

- Phase 1: Make Tea [+- Phase 2: Decant Tea[-

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion ______ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __30____% Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%Sample at ______ (min). State is _________%

Set

Record Done

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6d)

ProcessOverview

- Phase 1: Make Tea [+- Phase 2: Decant Tea [-

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion __4min_ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __30____% Sample at __2.5_ (min). State is __60_____%Sample at __4___ (min). State is _100____%

Set

Complete

Set

Set

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6e - alternate)

ProcessOverview

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion __4min_ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __30____% Sample at __2.5_ (min). State is __60_____%Sample at __4___ (min). State is _100____%

Set

Complete

Set

Set

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6e - alternate)

ProcessOverview

- Phase 1: Make Tea [+][-]- Phase 2: Decant Tea [+][-]

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion __4min_ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __30____% Sample at __2.5_ (min). State is __60_____%Sample at __4___ (min). State is _100____%

Set

Complete

Set

Set

CancelPause

DataOverview

Log Out

LogBench Station Active

Apparatus_

Method _

Phase Name

Process Template Selection ListProcess…………….something somethingProcess…………….something somethingProcess…………….something somethingProcess…………….something somethingProcess…………….something something

X

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 6e)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [+

Measure Set

Make TeaApparatus: -boiling thingy-Round bottomed thing for water-Flute that goes into round thing-Syringe-TLC

Method:-bring water to boil-Add tea-Reflux for 5 mins-Sample 1/min-Assess by color and aroma-decant

Actual time for completion __4min_ Record

TLC captures (link)

Sample at __1.2|_ (min). State is __30____% Sample at __2.5_ (min). State is __60_____%Sample at __4___ (min). State is _100____%

Set

Complete

Set

Set

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [-

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Record

Record Yield ________%Amount of material:_______ml

Note

Note

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7b)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [-

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Yield ________%Amount of material:_______ml

Note

Note

Record

Record

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7c)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [+

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Yield 90 %Amount of material:_______ml

Note

Note

Set

Record

Yield Note (1)Date: Friday, July 13, 2003, 14:45 GMT

Due to failure with filtration paper, we were unable to derive more than 90% yield of the material. Next time, I’d like to use a different method for decanting - one that avoids filter paper.

--------------------------Yield Note (2)Date: Friday, July 13, 2003, 14:48 GMTAn earnest student, attempting to help “clean up” has just destroyed the filter papers.

Cancel | Save | X

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7d)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [-

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Yield 90 %Amount of material:_900_ml

Note

Note

Set

Record

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7d)

ProcessOverview

- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [+

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Yield 90 %Amount of material:_900_ml

Note

Note

Set

Set

Decant Tea complete additional

CancelPause

DataOverview

Log Out

LogBench Station Active

Yield: Tea _______%

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 7e)

ProcessOverview- Phase 1: Make Tea [+ (complete)- Phase 2: Decant Tea [+

-(complete)

Measure Set

Decant TeaApparatus: -Big flask-funnel-Filter paper

Method:-Cool tea liquid-Pour through filter paper-Measure resulting yield-Store result

TLC captures (link)

Yield 90 %Amount of material:_900_ml

Note

Note

Set

Set

Decant Tea: Complete

CancelPause

DataOverview

DataOverview

Log Out

LogBench Station Active

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 8 )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: (Select Field and Scan code)

Location: (Select Location)

Measure Set

DataOverview

TLC captures (use scan station)

CancelPause Log Out

LogBench Station Active

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 9 )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: (Select Field and Scan code)

Location: (Select Location)

Measure Set

DataOverview

TLC captures (use scan station)

CancelPause Log Out

LogBench Station Active

TLC captures (use scan station)

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 10 )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: | ||| || |||| | | |||| (689 4893 485)

Location:

Measure Set

DataOverview

TLC captures (link)

CancelPause

Freezer 1, Room 290Freezer 2, Room 290Freezer 3, Room 245

Log Out

LogBench Station Active

TLC captures (use scanner)

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 11 )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: | ||| || |||| | | |||| (689 4893 485)

Location:

Measure Set

DataOverview

CancelPause

Freezer 1, Room 290

Log Out

LogBench Station Active

TLC captures: Tea1 TLC link

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 12 )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: | ||| || |||| | | |||| (689 4893 485)

Location:

Measure Set

DataOverview

CancelPause

Freezer 1, Room 290

Exp Tea1 Data Capture Concluded at

Time StampTime StampLog Out

LogBench Station Active

TLC captures: Tea1 TLC link

Chemist: Graham

Experiment Selected: (Tea 1)

Date: Friday, July 13, 2003

Tea 1Water 1Light 4

Weights: Planned | ActualTea 20g | 20.50g

Measures: Planned | ActualWater 1000ml | 1001|ml

(screen 12b )

ProcessOverview

- Phase 1: Make Tea [+][-]-(complete)

- Phase 2: Decant Tea [+][-] (complete)

Yield: 90% Tea 900 mlID: | ||| || |||| | | |||| (689 4893 485)

Location:

Measure Set

DataOverview

CancelPause

Freezer 1, Room 290

Exp Tea1 Data Capture Concluded at

Time Stamp

Log OutLog Out

LogBench Station Active

LogBook Station

Chemist:

Date:

PLEASE ENTER YOUR ID(iButton) to begin logging

for your experiment(s)

PLEASE ENTER YOUR ID(iButton) to begin logging

for your experiment(s)

LogBook StationChemist:Date:

(screen 13 - alternate )

CancelPause Log Out

You have been successfully logged out of the LogBookstation, Graham.

TLC and Compound ID remain to be done for Tea1; A note has been mailed to your logbook as a reminder.