Coil 110 reaction heat treatment analysis

E. Takala

2019November

Figure 1: The temperature reading of every thermo-couple as a function of hours from the beginning of the reaction cycle.

Figure 2: The temperature reading of the accepted thermo-couple as a function of hours from the beginning of the reactioncycle.

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Figure 3: The temperature reading of the accepted thermo-couple as a function of hours from the beginning of the reactioncycle.

Figure 4: The temperature reading of the accepted thermo-couple as a function of hours from the beginning of the reactioncycle.

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Figure 5: Dwell plot

Figure 6: Homogenity of the fixture according to the accepted thermo-couples.

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Figure 7: Argon flow inside the retort and the tooling as a function of time.

Figure 8: Heating rate as a function of time.

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Figure 9: The temperature according to the accepted thermo-couples as a function of time and fixture fixture block number.

Figure 10: The mid-range temperature deviation according to the accepted thermo-couples as a function of time and fixtureblock number.

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Figure 11: The mid-range deviation of the accepted thermo-couples in the dwells as a function of time and fixture blocknumber.

Figure 12: heater power as a function of time.

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Figure 13: None

Figure 14: None

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Figure 15: None

Table 1: Dwell summary

Dwell 1 2 3File 110.csv 110.csv 110.csvduration 49.9 50.7 48.7Target T 210.0 400.0 665.0Tmeanmean 212.0 396.7 665.3Tmid 210.0 395.1 664.8Tmid dev 0.0 -4.9 -0.2Tmidmean 211.2 396.5 665.9Tmidmean dev 1.2 -3.5 0.9Tmeanmid 210.4 395.5 664.3Tmeanmid dev 0.4 -4.5 -0.7Hmax/2 3.5 5.9 3.6Hmean/2 3.2 3.7 3.4Hasmax/2 3.2 4.0 3.6Hasmin/2 3.1 3.7 3.4Hasmean/2 3.2 3.8 3.5

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Table 2: Dwell 1 comparison summary for all analyzed files.

Dwell 1 1 1 1 1 1 1 1 1File 110.csv 003 1.csv 003 2.csv 104.csv 105.csv 107.csv 108 1.csv 108 2.csv 109.csvHasmax/2 3.2 3.2 NaN 4.1 4.2 4.1 NaN 3.5 3.7Hasmean/2 3.2 3.1 NaN 4.0 4.0 4.0 NaN 3.4 3.6Hasmin/2 3.1 3.0 NaN 3.9 3.8 3.8 NaN 3.3 3.6Hmax/2 3.5 3.4 NaN 4.2 4.2 4.5 NaN 4.7 4.4Hmean/2 3.2 3.2 NaN 4.0 3.9 4.1 NaN 3.6 3.8Target T 210.0 210.0 NaN 210.0 210.0 210.0 NaN 210.0 210.0Tmeanmean 212.0 211.6 NaN 212.0 211.7 211.8 NaN 211.3 212.1Tmeanmid 210.4 210.3 NaN 211.0 210.9 210.3 NaN 210.2 210.4Tmeanmid dev 0.4 0.3 NaN 1.0 0.9 0.3 NaN 0.2 0.4Tmid 210.0 210.0 NaN 210.0 210.0 210.0 NaN 210.0 210.0Tmid dev 0.0 0.0 NaN 0.0 0.0 0.0 NaN 0.0 0.0Tmidmean 211.2 211.1 NaN 210.8 210.6 211.0 NaN 210.6 211.4Tmidmean dev 1.2 1.1 NaN 0.8 0.6 1.0 NaN 0.6 1.4duration 49.9 25.0 NaN 45.7 46.5 46.3 NaN 54.7 52.6

Table 3: Dwell 2 comparison summary for all analyzed files.

Dwell 2 2 2 2 2 2 2 2 2File 110.csv 003 1.csv 003 2.csv 104.csv 105.csv 107.csv 108 1.csv 108 2.csv 109.csvHasmax/2 4.0 3.7 3.8 4.9 4.9 4.8 NaN 4.5 4.7Hasmean/2 3.8 3.6 3.7 4.8 4.7 4.7 NaN 4.3 4.6Hasmin/2 3.7 3.5 3.6 4.8 4.6 4.7 NaN 4.1 4.5Hmax/2 5.9 4.3 4.1 4.9 4.9 4.8 NaN 4.5 4.7Hmean/2 3.7 3.5 3.6 4.8 4.6 4.6 NaN 4.1 4.5Target T 400.0 400.0 400.0 400.0 400.0 400.0 NaN 400.0 400.0Tmeanmean 396.7 402.9 403.3 402.0 402.5 402.5 NaN 402.3 402.6Tmeanmid 395.5 401.8 402.1 402.7 402.3 402.1 NaN 401.8 402.1Tmeanmid dev -4.5 1.8 2.1 2.7 2.3 2.1 NaN 1.8 2.1Tmid 395.1 401.6 402.0 402.0 402.0 402.0 NaN 402.0 402.0Tmid dev -4.9 1.6 2.0 2.0 2.0 2.0 NaN 2.0 2.0Tmidmean 396.5 402.9 403.2 401.3 401.8 401.9 NaN 401.6 402.0Tmidmean dev -3.5 2.9 3.2 1.3 1.8 1.9 NaN 1.6 2.0duration 50.7 19.5 28.7 40.1 45.1 43.8 NaN 55.8 54.0

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Table 4: Dwell 3 comparison summary for all analyzed files.

Dwell 3 3 3 3 3 3 3 3 3File 110.csv 003 1.csv 003 2.csv 104.csv 105.csv 107.csv 108 1.csv 108 2.csv 109.csvHasmax/2 3.6 NaN 3.6 4.1 4.1 4.1 NaN 3.9 4.4Hasmean/2 3.5 NaN 3.5 4.0 4.1 4.1 NaN 3.9 4.4Hasmin/2 3.4 NaN 3.4 4.0 4.1 4.1 NaN 3.8 4.4Hmax/2 3.6 NaN 3.6 4.1 4.1 4.2 NaN 3.9 4.4Hmean/2 3.4 NaN 3.4 4.0 4.0 4.1 NaN 3.8 4.3Target T 665.0 NaN 665.0 665.0 665.0 665.0 NaN 665.0 665.0Tmeanmean 665.3 NaN 665.4 664.7 665.0 665.0 NaN 665.2 665.0Tmeanmid 664.3 NaN 664.4 663.9 664.4 664.3 NaN 664.4 664.6Tmeanmid dev -0.7 NaN -0.6 -1.1 -0.6 -0.7 NaN -0.6 -0.4Tmid 664.8 NaN 664.9 665.0 665.0 665.0 NaN 664.8 665.0Tmid dev -0.2 NaN -0.1 0.0 0.0 0.0 NaN -0.2 0.0Tmidmean 665.9 NaN 666.0 665.8 665.6 665.7 NaN 665.5 665.4Tmidmean dev 0.9 NaN 1.0 0.8 0.6 0.7 NaN 0.5 0.4duration 48.7 NaN 52.2 71.4 71.1 67.3 NaN 72.0 27.3

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