client sample 13 ,:r;,/~pd qegani,s anal.fsis .alpha-bhc beta-zhc delta-bhc gamma-bhc (lindane)...

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  • CLIENT SAMPLE 13 ,:r;,/~pD QEGANi",S ANAL.fSiS T)ATA SHEET ,____----______-____

    I CP?55-06SV3-2 I

    Lab sxn~: ,?,T siC'IJ?H ENVIRONMENTAL LAEORATORY Contract: NA

    La.0 :: ,> d p : ::; T-1 L 7 t:ace No. : ?lA SAS No.: NA SDCi No.: NA

    sat+::: ?:;I> Lab Sample ID: DLK 06

    ieve: : >:;w Lab File ID: L:A522114

    Sample wr, : ,:::j g ?H: ___ Date Received: 2-7-9u

    2 r, 1 5 3': r 5 : r: c, T. -1% c : 6; ":. dec: - "4 Date Extracted: Z-14-90

    E; ,j _ .~. .; _ :, Tstraet~~:dithropyrcphosph ! 71 1u I , I rdisu;coton i 71 IU I " ('/ - 5 1 _ = : Eimethoste 71 IU I -s3-p-:y,3-c / Parathion 71 1u I ?C-?E-' I Famphur 71 : IJ I _----___---_________-----------------------------------------------,

    ) T,srpet '?;mpound List C:\NELSON\ASNPDS.TCL - ,

    10:41:06 02-22-1990 FRMlXE30

  • 1 CLIENT SAMPLE ID r.r /VP? cRGAN:CS A!!ALYSIS 3ATA .."I IvI SHEET ,------------------;

    : CP?55-06 SV-3-2 , ,_______---_______-.

    La.3 Name: (GULF SOUT!! ENVIRONMENTAL LABORATORY Contract: GOLDER

    La.3 !:ode: (GULF Case No.: - SAS No.: SDG No.:

    Matrix : SOIL Lab Sample ID: DLK-06

    Level : LOW Lab File ID: H:A212011

    Sample wt : 50 .g PH: - Date Received: 02-07-90 S*Y M,.ier,rr-. ,.^C ;.a-. rT% Aa*. r\=+a v"+r%r+nA~ CL LIv-- IL.&i. IAVI VI&. -, .'.z Yb_. -04 IYIW Ic.I.bI-1-1. CL?-,. of3

    Extraction : SONC Date Analyzed: 02-22-90

    Cle?r.Up (i/N - Type!: N - NONE Dilution Factor: 1.0

    CONCENTRATION I ,,A$ N::. CCM?'3UMD ug:/Kg I , 9.

    gJ-TE-7 1 2.1-I.! 260 I u S?-7"-' - - I 2,4.5-TP (Silvex) 37 : u gz-75-5 ',4 ,5-T 43 1 u --~~~~~~--------------------~~~~~~-------~~~~~~~~~~~~~~~~~---------

    1 Targez Compound List C:\NELSON\HERBS.TCL --3 _ / _^_.. - --

    10:5?:4Q 02-23-199 FRMlXE3

  • l,r:,i:,-i_-~---------5t~,rpnr 1-::_!.:~-_,,~-~-7-------y,., i anc3 , --,.- ( +ot>, 1 ! ___,

    7:,-,:t:s-,3 -------- -Acetonitrile-- 1 ,::> -- -I' -- .--.a--------Acr,=iein --,-- :c,7-1~-l--------Acrylonltr;le

  • ,I k zj ~ !-, p ; z : ,.ii,

    ,----------------

    i. -.

    : ^.

  • -I-~:-i---------Isonhorune aY-7s----------T-Nitrophenol iLi5-67-9--------:, 4-Uimethyl phPncj1 65-85-t:)--------- Eienzoic Acid Il:-l-i--------bis(-Uhlornetno::vlMethC::~~~~~~t,~r,e-:

    ,~ - -. ? 1-I~-~,..----------~.4-Dichlornphrno? iz:I:?-sz-1-.-- ----- i,=, 3-Trichlorebenzenc 91-Xi----------Naohthalene I-~---------~. +.A-Trlchlorophenol sS-c~,--3---------~,4.S-T~~~~l~rophenol 91-58-7---------2-Chloronaphthalene SP-74-4---------T-Nitr~~~ilie .-. I_,;-ii-T--------Dlmetnyi phthaiate Ilf-s,-~--------acenaphthvlene &,:,Q--(:-~-------- _ _.6-Dinrtrbtoluene

    FOF:M i S?-1 l/R7 Rev.

  • hJ-,:,U-z -________ ~-i~iprJh+nilir,e

    31-l-----------!~~ren~~,h.th~e ~,l-~:~-~ :_____-_-- ~.J-jYinitj-go&no~ 1 ,)(:;-,:]~-y? ---- ---- G-i:ll~tropher~Oi l-=-,~3-o--------Dib~~~~~,-,r~~

    ;=I- li-_--------~;:.?-i;-ni=.rotoiLIEne.

    :S4-mm-Z---------Eiatnylohtal+te ,:,,:~5-T~~-1------- -i-2iiiorooi,ecl:,i-:,rienv1ethEr__: :~,~-71----------Cluorcne 11:1:,-1:~1-~--------4-l!i trnanl 1 ine 51j-C,T-1--------~.6-Dini,~ro-~-~~~~yloen~l-I P5-ICI-6---------N-Nitrosodiohenylamine (1 )-I llS-74-1--------Hexachlorobenzrne 27-R&,------.---- fentachlornohenol Sf,-f.:il-e---------Phenanthrer -: l-ii-12-7--------Athracene aj-74-2 --------- iii--n-ailiyrp,,L,,Olatc I..,-LA__/

    =i:)6-j3--1:~--------Fluor~ntnene i~~-,:,i,-i:--------~~,r~~~ ,-- 89-~8----------ButyIben-viphthalate 1-;-1---------~,3 -Dichlorobenzid~nep : f-,b-:4:E--:--~-------Be~o(a;~Athrecene 13-rii-9--------Chrysrne :17-Z:-7--------bis(Z-Ethylhe::yl)Phthaiate~: 117-S4-*.:I--------Di-n4ctvl Phthalate T,~i5-90-=--------Ben~~( b jFluor*nthene :Q7-1:jS-Q--------Benxoi. 1:. )Fluoranthene 5f.l-:2-8---------E-renzo (a )Pyrene i?l-I9-9--------Indeno(l.=.3-cdiPyrene :,l-70-:---------Diben-(a.h)knthracenr 1c2;-:4-=-------- Henzo(y.h.i)Perylene S-S6-~---------Acetophenone S;-s6-;---------2-Acetylain~iofl~uoree

  • I l.~,:i_-~a-~-------~fl.~,to:.:ins. Total r,z-,i.-- :---------a-~,,nnbiohenvl

    ; 1r:,72-,; --------s-!Amlnomethyl j-.y-iso;,:azfJlo!-: : jz-f;-~ -,---------&ni 1 lne ; 1-11:~-s::7-:~--------ATimite_ : +s=-:~,,;j- 8--------AlUr&Tlne. ; ==5-91-~--------Pen~o(~jacrid~n~

    J.,:''J-;s-)-- ----- -,Il-Cresn; ! l~l-ay-5--------'-Crclnhe::yl-4~~-d~nltr~phena~ : ""5-lt-E--------Dibenzo!a,h)acridine ; ="4-4Z-(:~--------Diben~o(~~j )acridine : 1CZ-65-4--------Dibenzo(a!e)pyrene : 159-55-s--------Dibenzo(a.i)pyrene s 1$4-59-I--------iH-Dibenzoic.yjcarbnzoie f 112-"7-7--------;,z-Dimethylbenrijine : 9W;7-7---------Dzchloromethylben=enzene : S7-55-!:I---------2,5-Dichiorophenol ! hc5-~fi-6--------0ichlorophenylarsine~ : 94-58-5---------Dihydrosafrole I ?s5-?l-4---------Diisopropvlf lunrophuspnate-: : hi:i-:1-7---------p-Dimethyl'aminoa~oben~ene-:

    :

    il) - Cannot be ,zeparated from DiPhenyiamlne FOFiM I SV-:

  • my----*---------, l~Dimrthvlben~nia,anthracen I 7-1;----------I, l--Dlmetny;hydra-lne ,1CI--S-~--------l ,=-Dimethvlhvdra-inr ~~~-~:,-~--------a-a-Dimethvlphrnett,~~lam~ne_: ----?2- ,--------- Dimethyl SC!+ fat.? _: o,~-,E-rl---------m-Ui~,~i,t~~b~~:~~~ l~-~~-;--------0iph~n,~~,l~m~n~-, iZ:Z-rj-, --------A .~-Diphcnylh~draz;ne 41-,1-:--------=,4-Dithiobiuret l,Jc,-,----- -____ Endrjtj,al 97--,:-?---------Ethyl Methacrylate 6Z-E8+I.+--------E~thyl Mrthanesulfnnatr 54,-1S-=---------Fnrmic Acid I~!-;--~---------fiel:achlorophene 1s3-:3-: l-7-------He:.:achloroproprOp~ne 757-~~-~--------He;.:aethyltetraphesphatetrap~,~~ph~te

    : lr;~-ll-j--------Maleic Anhydrtde : 14&-92-:--------Melphalan : 91-8~-~---------rl~thyapyrllene : 5$-49-S---------;-Methylcholanthrenr : Fj,j-o~-a--------- Methyl Methacrylatr : iC)l-14-4--------4,4-Methylrnbis(Z-chlor~anil): : 75-95-5---------2-Methyllactonitrilr

    .I-LL___.. : 66-y-z --------- pjethyi ,.,~~,,~,,~c,::Oiicit= : 5,51-~->-~--------- N-Methyl-N-nitrosn~-N-nltrogu : 6,6-26-G--------Methyl thlouraci 1

    ;I) - r, -,nnor be zeparated ,irom Diphenvlamlne FORM I w-4

    ,I.

  • ll! - Cannot be sendrated Yrom Dlphenylamlne

  • - _ _ _. _ _ _ _ _ _ _ _ _ _ _. _ _ ._

    -. . _- _. _ _. _ _ _ _ _ __ -. __ .- _..

  • FOF(M x SV-TIC l/S7 Rev.

  • CLIENT SAMPLE ID GC,'ECD ORGANICS AN:LYSIS DATA SHEET .------------------.

    : CPP55-06-SV-5-3 I ,---------------___~

    Lab Name: GULF SOUTH ENVIRONMENTAL LABORATORY Contract: G OLOGR

    Lab Code: GULF Case No. : SAS No.: "se . . am.5 NO.: -

    Matrix: SOIL Lab Sample ID: DLK-09 i*vpl: LOW Lab File ID: G:A122058

    Sample wt : 30 g pH: ci.l Date Received: 2-7-90

    Zxtraction: SONC Date Extracted: 2-14-90

    Mcisture: not dec: 15% dec: -% Date Analyzed: 02-20-90

    Cleanup iYiN - Type): N - NONE Dilution Factor: 1.0 ,--______----___________________________----------------------------,

    CONCENTRATION I CAS No. COMPOUND ug/Kg I Q, I I________--_____j_-_____________________----- !_____-________-__!____I

    319-84-6 319-25-7 319-86-a 58-89-9 76-d,4-$ 309-00-Z 1024-57-3 959-98-8 60-57-l 72-55-9 72-20-e 33213-65-9 72-54-8 ;031-07-g 50-29-3 72-43-5 7421-93-4 53494-70-5 57-74-g 8001-35-2 12674-11-2 11104-28-2 l~l4~-~6-C 53469-21-G 12672-29-6 11097-69-6 11096-82-5

    alpha-BHC beta-ZHC delta-BHC gamma-BHC (Lindane) U,ants,-.hl AV .-c "--...."* Aldrin Heptachlor epoxide Endosulfan I Dieldrin 4.4.-DDE Endrin Endosulfan II 4.4'-DDD i;p.doslLlfap* sulfate 4,4'-DDT Met.hoxychlor Endrin aldehyde Endrin ketone Chlordane Toxaphene Aroclor 1016 Aroclor 1221 drhrl hv. ,717 2*vI*v* *-..," Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260

    9.4 9.4 9.4 9.4 9;4 9.4 9.4 9.4

    19 i9 19 19 19

    ~19 19 94 19 19

    1:: 94 1 94 94 94 94 I 190

    190

  • CLIENT SAMPLE ID GC/ECD ORGANICS AN;LYSIS DATA SHEET .------------------.

    : CPP55-06-SV-5-3 : ,____--___-___-____.

    Lab Name: GULF SOUTH ENVIRONMENTAL LABORATORY Contract: G~LOER.

    Lab Code: GULF Case No. : SAS No.: SDG Nol:

    Matrix: SOIL Lab Sample ID: DLK-09

    Level: LOW Lab File ID: G:A122058

    Sample wt : 30 g pH: a Date Received: 2-7-90

    Extraction: SONG Date Extracted: 2-14-90

    Moisture: not dec: 15% dec: -% Date Analyzed: 02-20-90

    Cleanup (Y/N - Type): N - NONE Dilution Factor: 1.0

    CAS No. ; CONCENTRATION I i

    COMPOUND w/Kg IQ I I_-___---____--_ 1__________-_________________I__________-------~----' 510-15-6 I Chlorobenzilate 80 ;ct j 2303-16-4 : Diallate 94 IU : 465-73-6 I Isodrin 19 'U : 143-50-o : Kepone 940 jLl I

    ~__--__-_-----____--____________________----------------------------,

    Target Compound List C:\NELSON\ASECDL.TCL

    paie 1s of x FORM I GC-8000

    09:01:48 02-26-1990 FRMlXE32 8/89 rev.

  • - 5 : Tetrarthy?dit~~r'pyrophosp~ / 79 I 'J L! ! Disulfrjtcn 79 :I!

    Dimethoste 7 9 7;

    ' u I Methyl parathion I u

    5, 6 - , ;s - : Parathion 79 / ?J 5 T; _ ::a 5. _ 7 Famphur ?9 I rJ ________________________________________---------------------------

    Tar.g:?t ;X,r~mp~und List C:\NELSON\ASNPDS.TCL

    FORM I GC-enno - -

  • 1 CLIENT SAMPLE ID GC,'ECD ORGANICS ANALYSIS DATA SHEET .------------------

    j Cppjj-06 S'j-j-j .-------__________-

    Lab Name: GULF SOUTH ENVIRONMENTAL LABORATORY Contract: GOLDER

    Lab Code: GULF [Case No. : - SAS No.: SDG No.: -

    Mztr1x : SOI!, Lab Sample ID: DLK-09

    Levei: LtL>j La.0 File 19: .^A^^-^ H:Azl~ulL

    lampie ;rt : 50 g pH: - Date Received: 02-07-90

    Moisture: not dec: 16% dec: Y -,o Date Extracted: 02-9~90

    Ex-,rricticr. : S!,7NC Date Analyzed: 02-22-90

    Cleanu; rY,/N - Tj'FS): N - NONE Dilution Factor: 1.0 ---------_-_--_-________________________~~~~~~~~~~~~~~~~~~~~