client name: mountain view regional water com. site …€¦ · should you require any information...

CLIENT NAME: MOUNTAIN VIEW REGIONAL WATER COM.SITE 22 BOX 1 RR1INNISFAIL, AB T4E 1T6 (403) 227-5828

2910 12TH STREET NECALGARY, ALBERTA

CANADA T2E 7P7TEL (403)735-2005FAX (403)735-2771

http://www.agatlabs.com

Inga Kuzmina, Organic Laboratory SupervisorTRACE ORGANICS REVIEWED BY:

Irina Gankovsky, Senior AnalystWATER ANALYSIS REVIEWED BY:

DATE REPORTED:

PAGES (INCLUDING COVER): 29

Mar 08, 2013

VERSION*: 1

Should you require any information regarding this analysis please contact your client services representative at (403) 735-2005

13C692827AGAT WORK ORDER:

ATTENTION TO: Wes Olstad

PROJECT NO:

Laboratories (V1) of 29

All samples will be disposed of within 30 days following analysis. Please contact the lab if you require additional sample storage time.

AGAT Laboratories is accredited to ISO/IEC 17025 by the Canadian Association for Laboratory Accreditation Inc. (CALA) and/or Standards Council of Canada (SCC) for specific tests listed on the scope of accreditation. AGAT Laboratories (Mississauga) is also accredited by the Canadian Association for Laboratory Accreditation Inc. (CALA) for specific drinking water tests. Accreditations are location and parameter specific. A complete listing of parameters for each location is available from www.cala.ca and/or www.scc.ca. The tests in this report may not necessarily be included in the scope of accreditation.

Association of Professional Engineers, Geologists and Geophysicists of Alberta (APEGGA)Western Enviro-Agricultural Laboratory Association (WEALA)Environmental Services Association of Alberta (ESAA)

Member of:

*NOTES

Results relate only to the items tested and to all the items tested

TreatedSAMPLE DESCRIPTION:WaterSAMPLE TYPE:

2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter<0.0005Benzene 0.00050.005mg/L<0.0005Toluene 0.00050.024mg/L<0.0005Ethylbenzene 0.00050.0024mg/L<0.0005Xylenes 0.00050.3mg/L

Acceptable LimitsUnitSurrogate91Toluene-d8 (BTEX) % 50-150

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to CCME (D Water)Comments:


DATE RECEIVED: 2013-02-27

Certificate of Analysis

ATTENTION TO: Wes OlstadCLIENT NAME: MOUNTAIN VIEW REGIONAL WATER COM.

AGAT WORK ORDER: 13C692827

DATE REPORTED: 2013-03-08

PROJECT NO:

BTEX Analysis - Water




CERTIFICATE OF ANALYSIS (V1)

Certified By: of 29


2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter

<2.0Aldicarb 2.0µg/L<2Bendiocarb 2µg/L<5Carbofuran 5µg/L<5Carbaryl 5µg/L<10Diuron 10µg/L<1Triallate 1µg/L

<10Temephos 10µg/L

RDL - Reported Detection Limit; G / S - Guideline / StandardComments:4162089 Results relate only to the items tested.







PROJECT NO:

Carbamate Pesticides in Water





Certified By: of 29



20.2Total Haloacetic Acids 4.0ug/L20.2HAA5 4.0ug /L<1.7Chloroacetic Acid 1.7ug/L<0.2Bromoacetic Acid 0.2ug/L11Dichloroacetic Acid 0.2ug/L

<0.1Dibromoacetic Acid 0.1ug/L9.2Trichloroacetic Acid 0.2ug/L

<0.3Bromochloroacetic Acid 0.3ug/LAcceptable LimitsUnitSurrogate

1142-Bromobutanoic acid % 70-130

RDL - Reported Detection Limit; G / S - Guideline / StandardComments:4162089 Sample received in incorrect sample container, with no preservative. Ice present in sample upon receipt.







PROJECT NO:

Haloacetic Acids (water)





Certified By: of 29



<0.52,4-D 0.5µg/L<0.52,4,5-T 0.5µg/L<0.52,4,5-TP 0.5µg/L<0.5Dicamba 0.5µg/L<0.5Dichlorprop 0.5µg/L<0.5Dinoseb 0.5µg/L<0.5Picloram 0.5µg/L<0.5Diclofop-methyl 0.5µg/L

Acceptable LimitsUnitSurrogate90DCAA % 50-130

RDL - Reported Detection Limit; G / S - Guideline / StandardComments:







PROJECT NO:

Herbicides (water)





Certified By: of 29



<0.01Gamma-Hexachlorocyclohexane 0.01µg/L<0.01Heptachlor 0.01µg/L<0.01Aldrin 0.01µg/L<0.01Heptachlor Epoxide 0.01µg/L<0.05Endosulfan 0.05µg/L<0.04Chlordane 0.04µg/L<0.01DDE 0.01µg/L<0.05DDD 0.05µg/L<0.04DDT 0.04µg/L<0.02Dieldrin 0.02µg/L<0.05Endrin 0.05µg/L<0.04Methoxychlor 0.04µg/L<0.01Hexachlorobenzene 0.01ug/L<0.01Hexachlorobutadiene 0.01ug/L<0.01Hexachloroethane 0.01ug/L<0.2Aroclor 1242 0.2µg/L<0.2Aroclor 1248 0.2µg/L<0.2Aroclor 1254 0.2µg/L<0.2Aroclor 1260 0.2µg/L<0.2Polychlorinated Biphenyls 0.2µg/L

Acceptable LimitsUnitSurrogate95TCMX % 50-14097Decachlorobiphenyl % 60-140

RDL - Reported Detection Limit; G / S - Guideline / StandardComments:4162089 Note: DDT applies to the total of op'DDT and pp'DDT, DDD applies to the total of op'DDD and pp'DDD and DDE applies to the total of op'DDE and pp'DDE. Endosulfan applies to the total of Endosulfan I

and Endosulfan II.Chlordane applies to the total of Alpha-Chlordane and Gamma-Chlordane.







PROJECT NO:

O. Reg. 153(511) - OC Pesticides + PCBs (Water)





Certified By: of 29



<0.5Phorate 0.5µg/L<2.5Dimethoate 2.5µg/L<0.5Terbufos 0.5µg/L<1Diazinon 1µg/L<5Malathion 5µg/L<1Chlorpyrifos 1µg/L<1Parathion 1µg/L<2Azinphos-methyl 2µg/L

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to ODWS - Table DComments:4162089 Results relate only to the items tested.







PROJECT NO:

OP pesticides [water]





Certified By: of 29


2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter<0.002Phenol 0.002mg/L<0.0054-Nitrophenol 0.005mg/L

<0.0005m&p-Cresol (3&4-methylphenol) 0.0005mg/L<0.0005o-Cresol (2-methylphenol) 0.0005mg/L<0.00052-Chlorophenol 0.0005mg/L<0.0052,4-Dinitrophenol 0.005mg/L<0.0052-Nitrophenol 0.005mg/L

<0.00052,4-Dimethylphenol 0.0005mg/L<0.00012,6-Dichlorophenol 0.0001mg/L<0.00054-Chloro-3-methylphenol 0.0005mg/L<0.00012,4-Dichlorophenol 0.0001mg/L<0.0054,6-Dinitro-2-methylphenol 0.005mg/L

<0.00052,3,6-Trichlorophenol 0.0005mg/L<0.00052,3,4-Trichlorophenol 0.0005mg/L<0.00052,4,6-Trichlorophenol 0.0005mg/L<0.00052,4,5-Trichlorophenol 0.0005mg/L<0.00052,3,5-Trichlorophenol 0.0005mg/L<0.00053,4,5-Trichlorophenol 0.0005mg/L<0.00052,3,4,6-Tetrachlorophenol 0.0005mg/L<0.00052,3,5,6-Tetrachlorophenol 0.0005mg/L<0.00052,3,4,5-Tetrachlorophenol 0.0005mg/L

<0.005Dinoseb (2-sec-butyl-4,6-dinitrophenol) 0.005mg/L

<0.0005Pentachlorophenol 0.0005mg/LAcceptable LimitsUnitSurrogate

1012-Fluorophenol % 50-150952,4,6-Tribromophenol % 50-150

RDL - Reported Detection Limit; G / S - Guideline / StandardComments:4162089 Results relate only to the items tested.







PROJECT NO:

Phenolic Compounds in Water





Certified By: of 29


2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter<0.0001Acridine 0.00010.0044mg/L<0.0001Quinoline 0.00010.0034mg/L0.000022-Methylnaphthalene 0.00001mg/L0.00021Naphthalene 0.000010.0011mg/L

<0.00001Acenaphthylene 0.00001mg/L<0.00001Acenaphthene 0.000010.0058mg/L<0.00001Fluorene 0.000010.003mg/L0.00002Phenanthrene 0.000010.00004mg/L

<0.00001Anthracene 0.000010.000012mg/L<0.00001Fluoranthene 0.000010.00004mg/L<0.00001Pyrene 0.000010.000025mg/L<0.00001Benzo[a]anthracene 0.000010.000018mg/L<0.00001Chrysene 0.00001mg/L<0.00001Benzo[b+j]fluoranthene 0.00001mg/L<0.00001Benzo[k]fluoranthene 0.00001mg/L<0.00001Benzo[a]pyrene 0.00001mg/L<0.00001Indeno[1,2,3-cd]pyrene 0.00001mg/L<0.00001Benzo[ghi]perylene 0.00001mg/L<0.00001Dibenzo[ah]anthracene 0.00001mg/L

Acceptable LimitsUnitSurrogate742-Fluorobiphenyl (PAH) % 50-15068p-Terphenyl-d14 (PAH) % 50-150

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to CCME (D Water)Comments:4162089 Based on GC/MS target ion analysis.

Isomers Benzo(b)fluoranthene and Benzo(j)fluoranthene have the same GC retention time and are reported as the sum based on the Benzo(b)fluoranthene response.







PROJECT NO:

Polyaromatic Hydrocarbon Analysis - Water FWAL





Certified By: of 29



<1.0Trifluralin 1.0µg/L<1.0Simazine 1.0µg/L<0.5Atrazine 0.5µg/L<0.25Metribuzin 0.25µg/L<0.25Prometryne 0.25µg/L<0.11Metolachlor 0.11µg/L<0.5Alachlor 0.5µg/L<1.0Cyanazine 1.0µg/L

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to ODWS - Table DComments:4162089 Results relate only to the items tested.







PROJECT NO:

Triazine Pesticides [water]





Certified By: of 29

MPR-InfluentTreated MPR-Effluent PlantSAMPLE DESCRIPTION:WaterWaterWater WaterSAMPLE TYPE:

2/27/2013 2/27/2013 2/27/20132/27/2013DATE SAMPLED:4162089 4162091 4162092 4162093G / S RDLUnitParameter

0.027 0.018 0.024 0.014Chloroform 0.0010.0018mg/L<0.001 <0.001 0.001 <0.001Bromodichloromethane 0.001mg/L<0.001 <0.001 <0.001 <0.001Dibromochloromethane 0.001mg/L<0.001 <0.001 <0.001 <0.001Bromoform 0.001mg/L0.027 0.018 0.025 0.014Total Trihalomethanes 0.001mg/L

Acceptable LimitsUnitSurrogate92 94 94 93Toluene-d8 (BTEX) % 50-150








PROJECT NO:

Trihalomethane Analysis - Water





Certified By: of 29


2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter<0.001Chloromethane 0.001mg/L<0.001Vinyl Chloride 0.001mg/L<0.001Bromomethane 0.001mg/L<0.001Chloroethane 0.001mg/L<0.001Trichlorofluoromethane 0.001mg/L<0.01Acetone 0.01mg/L<0.0011,1-Dichloroethylene 0.001mg/L<0.001Methylene Chloride 0.001mg/L<0.001Methyl tert-butyl ether 0.001mg/L<0.01Methyl Ethyl Ketone 0.01mg/L<0.001trans- 1,2-dichloroethylene 0.001mg/L<0.0011,1-Dichloroethane 0.001mg/L<0.001cis- 1,2-Dichloroethylene 0.001mg/L0.027Chloroform 0.001mg/L<0.0011,2-Dichloroethane 0.001mg/L<0.0011,1,1-Trichloroethane 0.001mg/L

<0.0005Carbon Tetrachloride 0.0005mg/L<0.0005Benzene 0.0005mg/L<0.0011,2-Dichloropropane 0.001mg/L<0.001Trichloroethylene 0.001mg/L<0.001Bromodichloromethane 0.001mg/L<0.001trans-1,3-Dichloropropene 0.001mg/L<0.01Methyl Isobutyl Ketone 0.01mg/L<0.001cis-1,3-Dichloropropene 0.001mg/L<0.0011,1,2-Trichloroethane 0.001mg/L

<0.0005Toluene 0.0005mg/L<0.012-Hexanone 0.01mg/L<0.001Dibromochloromethane 0.001mg/L<0.001Ethylene Dibromide 0.001mg/L<0.001Tetrachloroethene 0.001mg/L<0.0011,1,1,2-Tetrachloroethane 0.001mg/L







PROJECT NO:

Volatile Organic Compounds in Water





Certified By: of 29


2/27/2013DATE SAMPLED:4162089G / S RDLUnitParameter<0.001Chlorobenzene 0.001mg/L

<0.0005Ethylbenzene 0.0005mg/L<0.0005m & p-Xylene 0.0005mg/L<0.001Bromoform 0.001mg/L<0.001Styrene 0.001mg/L<0.0011,1,2,2-Tetrachloroethane 0.001mg/L

<0.0005o-Xylene 0.0005mg/L<0.00051,3-Dichlorobenzene 0.0005mg/L<0.00051,4-Dichlorobenzene 0.0005mg/L<0.00051,2-Dichlorobenzene 0.0005mg/L<0.0011,2,4-Trichlorobenzene 0.001mg/L

<0.0005Total Xylenes 0.0005mg/LAcceptable LimitsUnitSurrogate

92Toluene-d8 (BTEX) % 50-150








PROJECT NO:

Volatile Organic Compounds in Water





Certified By: of 29



8.38pH NA6.5-8.5pH Units<5p - Alkalinity (as CaCO3) 5mg/L213T - Alkalinity (as CaCO3) 5mg/L250Bicarbonate 5mg/L<5Carbonate 5mg/L<5Hydroxide 5mg/L451Electrical Conductivity 5uS/cm

3Chloride 1250mg/L0.15Fluoride 0.051.5mg/L<0.5Nitrate 0.545mg/L44Sulfate 1500mg/L

66.9Dissolved Calcium 0.3mg/L18.7Dissolved Magnesium 0.2mg/L7.7Dissolved Sodium 0.6200mg/L1.3Dissolved Potassium 0.6mg/L

<0.1Dissolved Iron 0.10.3mg/L<0.005Dissolved Manganese 0.0050.05mg/L

270Calculated TDS 1mg/L244Hardness 1mg CaCO3/L103Ion Balance %

<0.01Nitrate + Nitrite-N 0.01mg/L<0.113Nitrate-N 0.113mg/L<0.015Nitrite-N 0.015mg/L0.214SAR N/A

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to CCME (D Water)Comments:4162089 < - Values refer to Report Detection Limits.







PROJECT NO:

Routine Chemistry Water Analysis





Certified By: of 29



0.008Total Aluminum 0.0020.1mg/L<0.001Total Antimony 0.0010.006mg/L<0.001Total Arsenic 0.0010.010mg/L

0.08Total Barium 0.051mg/L<0.01Total Boron 0.015mg/L

<0.000025Total Cadmium 0.0000250.005mg/L<0.001Total Chromium 0.0010.05mg/L0.018Total Copper 0.0021mg/L<0.1Total Iron 0.10.3mg/L

<0.001Total Lead 0.0010.01mg/L<0.005Total Manganese 0.0050.05mg/L

<0.000025Total Mercury 0.0000250.001mg/L<0.001Total Selenium 0.0010.01mg/L

<0.0001Total Silver 0.0001mg/L<0.001Total Uranium 0.0010.02mg/L0.005Total Zinc 0.0035mg/L

RDL - Reported Detection Limit; G / S - Guideline / Standard: Refers to CCME (D Water)Comments:4162089 < - Values refer to Method Detection Limit.







PROJECT NO:

Total Metals Scan in Water + Hg (mg/L)





Certified By: of 29



0.08Ammonia, Total (as N) 0.05mg/L<0.05Bromate 0.05mg/L<0.1Chlorate 0.1mg/L<0.1Chlorite 0.1mg/L

5Colour 515Colour Units<0.002Total Cyanide 0.002mg/L

255Total Dissolved Solids 5500mg/L2Total Organic Carbon 1mg/L








PROJECT NO:

Water Analysis





Certified By: of 29



<0.01Sulphide 0.01mg/L








PROJECT NO:

Water Analysis - Sulphide





Certified By: of 29

Trihalomethane Analysis - WaterChloroform 3767 4164414 0.003 0.002 NA < 0.001 86% 70% 130% 101% 70% 130%Bromodichloromethane 3767 4164414 <0.001 <0.001 NA < 0.001 86% 70% 130% 100% 70% 130%Dibromochloromethane 3767 4164414 <0.001 <0.001 NA < 0.001 83% 70% 130% 97% 70% 130%Bromoform 3767 4164414 <0.001 <0.001 NA < 0.001 87% 70% 130% 97% 70% 130% Volatile Organic Compounds in WaterChloromethane 3767 4164414 <0.001 <0.001 NA < 0.001 62% 60% 140% 107% 60% 140% 89% 60% 140%Vinyl Chloride 3767 4164414 <0.001 <0.001 NA < 0.001 61% 60% 140% 78% 60% 140% 69% 60% 140%Bromomethane 3767 4164414 <0.001 <0.001 NA < 0.001 63% 60% 140% 91% 60% 140% 75% 60% 140%Chloroethane 3767 4164414 <0.001 <0.001 NA < 0.001 96% 60% 140% 138% 60% 140% 135% 60% 140%Trichlorofluoromethane

3767 4164414 <0.001 <0.001 NA < 0.001 70% 60% 140% 90% 60% 140% 77% 60% 140%

Acetone 3767 4164414 0.15 0.15 0.0% < 0.01 124% 60% 140% 124% 60% 140% 136% 60% 140%1,1-Dichloroethylene 3767 4164414 <0.001 <0.001 NA < 0.001 73% 60% 140% 95% 60% 140% 79% 60% 140%Methylene Chloride 3767 4164414 <0.001 <0.001 NA < 0.001 77% 60% 140% 104% 60% 140% 95% 60% 140%Methyl tert-butyl ether 3767 4164414 <0.001 <0.001 NA < 0.001 98% 60% 140% 98% 60% 140% 86% 60% 140%Methyl Ethyl Ketone

3767 4164414 0.05 0.05 0.0% < 0.01 127% 60% 140% 127% 60% 140% 74% 60% 140%

trans- 1,2-dichloroethylene 3767 4164414 <0.001 <0.001 NA < 0.001 82% 60% 140% 104% 60% 140% 90% 60% 140%1,1-Dichloroethane 3767 4164414 <0.001 <0.001 NA < 0.001 86% 60% 140% 107% 60% 140% 90% 60% 140%cis- 1,2-Dichloroethylene 3767 4164414 <0.001 <0.001 NA < 0.001 82% 60% 140% 105% 60% 140% 88% 60% 140%Chloroform 3767 4164414 0.003 0.002 NA < 0.001 86% 60% 140% 101% 60% 140% 86% 60% 140%1,2-Dichloroethane

3767 4164414 <0.001 <0.001 NA < 0.001 90% 60% 140% 112% 60% 140% 99% 60% 140%

1,1,1-Trichloroethane 3767 4164414 <0.001 <0.001 NA < 0.001 83% 60% 140% 97% 60% 140% 84% 60% 140%Carbon Tetrachloride 3767 4164414 <0.0005 <0.0005 NA < 0.0005 77% 60% 140% 90% 60% 140% 78% 60% 140%Benzene 3767 4164414 0.0276 0.0279 1.1% < 0.0005 80% 60% 140% 104% 60% 140% 80% 60% 140%1,2-Dichloropropane 3767 4164414 <0.001 <0.001 NA < 0.001 87% 60% 140% 106% 60% 140% 100% 60% 140%Trichloroethylene

3767 4164414 <0.001 <0.001 NA < 0.001 82% 60% 140% 100% 60% 140% 90% 60% 140%

Bromodichloromethane 3767 4164414 <0.001 <0.001 NA < 0.001 86% 60% 140% 100% 60% 140% 97% 60% 140%trans-1,3-Dichloropropene 3767 4164414 <0.001 <0.001 NA < 0.001 77% 60% 140% 99% 60% 140% 91% 60% 140%Methyl Isobutyl Ketone 3767 4164414 <0.01 <0.01 NA < 0.01 135% 60% 140% 135% 60% 140% 103% 60% 140%cis-1,3-Dichloropropene 3767 4164414 <0.001 <0.001 NA < 0.001 80% 60% 140% 107% 60% 140% 97% 60% 140%1,1,2-Trichloroethane

3767 4164414 <0.001 <0.001 NA < 0.001 88% 60% 140% 103% 60% 140% 104% 60% 140%

Toluene 3767 4164414 0.0272 0.0282 3.6% < 0.0005 81% 60% 140% 99% 60% 140% 60% 60% 140%2-Hexanone 3767 4164414 <0.01 <0.01 NA < 0.01 139% 60% 140% 139% 60% 140% 76% 60% 140%Dibromochloromethane 3767 4164414 <0.001 <0.001 NA < 0.001 83% 60% 140% 97% 60% 140% 95% 60% 140%Ethylene Dibromide 3767 4164414 <0.001 <0.001 NA < 0.001 86% 60% 140% 111% 60% 140% 106% 60% 140%Tetrachloroethene

3767 4164414 0.187 0.195 4.2% < 0.001 73% 60% 140% 90% 60% 140% 60% 60% 140%

1,1,1,2-Tetrachloroethane 3767 4164414 <0.001 <0.001 NA < 0.001 83% 60% 140% 78% 60% 140% 91% 60% 140%Chlorobenzene 3767 4164414 <0.001 <0.001 NA < 0.001 83% 60% 140% 99% 60% 140% 94% 60% 140%Ethylbenzene 3767 4164414 0.0018 0.0019 NA < 0.0005 90% 60% 140% 106% 60% 140% 99% 60% 140%m & p-Xylene 3767 4164414 0.0072 0.0077 6.7% < 0.0005 88% 60% 140% 107% 60% 140% 90% 60% 140%



Dup #1 RPD MeasuredValue Recovery Recovery

Quality AssuranceATTENTION TO: Wes Olstad

CLIENT NAME: MOUNTAIN VIEW REGIONAL WATER COM.PROJECT NO:

Trace Organics Analysis

UpperLower

AcceptableLimitsBatchPARAMETER Sample

Id Dup #2UpperLower

AcceptableLimits

UpperLower

AcceptableLimits

MATRIX SPIKEMETHOD BLANK SPIKEDUPLICATERPT Date: Mar 08, 2013 REFERENCE MATERIAL

MethodBlank




QUALITY ASSURANCE REPORT (V1) of 29AGAT Laboratories is accredited to ISO/IEC 17025 by the Canadian Association for Laboratory Accreditation Inc. (CALA) and/or Standards Council of Canada (SCC) for specific tests listed on the scope of accreditation. AGAT Laboratories (Mississauga) is also accredited by the Canadian Association for Laboratory Accreditation Inc. (CALA) for specific drinking water tests. Accreditations are location and parameter specific. A complete listing of parameters for each location is available from www.cala.ca and/or www.scc.ca. The tests in this report may not necessarily be included in the scope of accreditation.

Bromoform

3767 4164414 <0.001 <0.001 NA < 0.001 87% 60% 140% 97% 60% 140% 94% 60% 140%

Styrene 3767 4164414 <0.001 <0.001 NA < 0.001 78% 60% 140% 92% 60% 140% 84% 60% 140%1,1,2,2-Tetrachloroethane 3767 4164414 <0.001 <0.001 NA < 0.001 85% 60% 140% 85% 60% 140% 85% 60% 140%o-Xylene 3767 4164414 0.0029 0.0033 12.9% < 0.0005 90% 60% 140% 107% 60% 140% 94% 60% 140%1,3-Dichlorobenzene 3767 4164414 <0.0005 <0.0005 NA < 0.0005 83% 60% 140% 90% 60% 140% 92% 60% 140%1,4-Dichlorobenzene

3767 4164414 <0.0005 <0.0005 NA < 0.0005 84% 60% 140% 91% 60% 140% 92% 60% 140%

1,2-Dichlorobenzene 3767 4164414 <0.0005 <0.0005 NA < 0.0005 85% 60% 140% 93% 60% 140% 94% 60% 140%1,2,4-Trichlorobenzene 3767 4164414 <0.001 <0.001 NA < 0.001 76% 60% 140% 84% 60% 140% 95% 60% 140% BTEX Analysis - WaterBenzene 773 4161216 <0.0005 <0.0005 NA < 0.0005 87% 80% 120% 83% 80% 120% 80% 70% 130%Toluene 773 4161216 <0.0005 <0.0005 NA < 0.0005 90% 80% 120% 86% 80% 120% 84% 70% 130%Ethylbenzene 773 4161216 <0.0005 <0.0005 NA < 0.0005 89% 80% 120% 88% 80% 120% 83% 70% 130%Xylenes 773 4161216 0.0037 0.0037 NA < 0.0005 98% 80% 120% 92% 80% 120% 89% 70% 130% Phenolic Compounds in WaterPhenol 208 4159755 <0.002 <0.002 NA < 0.002 88% 80% 120% 109% 70% 130% 109% 60% 140%4-Nitrophenol 208 4159755 <0.005 <0.005 NA < 0.005 85% 80% 120% 109% 70% 130% 110% 60% 140%m&p-Cresol (3&4-methylphenol) 208 4159755 <0.0005 <0.0005 NA < 0.0005 109% 70% 130% 110% 60% 140%o-Cresol (2-methylphenol) 208 4159755 <0.0005 <0.0005 NA < 0.0005 106% 70% 130% 109% 60% 140%2-Chlorophenol

208 4159755 <0.0005 <0.0005 NA < 0.0005 83% 80% 120% 108% 70% 130% 103% 60% 140%

2,4-Dinitrophenol 208 4159755 <0.005 <0.005 NA < 0.005 87% 80% 120% 107% 70% 130% 104% 60% 140%2-Nitrophenol 208 4159755 <0.005 <0.005 NA < 0.005 86% 80% 120% 108% 70% 130% 109% 60% 140%2,4-Dimethylphenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 82% 80% 120% 107% 70% 130% 112% 60% 140%2,6-Dichlorophenol 208 4159755 <0.0001 <0.0001 NA < 0.0001 107% 70% 130% 108% 60% 140%4-Chloro-3-methylphenol

208 4159755 <0.0005 <0.0005 NA < 0.0005 83% 80% 120% 108% 70% 130% 110% 60% 140%

2,4-Dichlorophenol 208 4159755 <0.0001 <0.0001 NA < 0.0001 87% 80% 120% 104% 70% 130% 103% 60% 140%4,6-Dinitro-2-methylphenol 208 4159755 <0.005 <0.005 NA < 0.005 94% 80% 120% 108% 70% 130% 111% 60% 140%2,3,6-Trichlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 108% 70% 130% 105% 60% 140%2,3,4-Trichlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 108% 70% 130% 109% 60% 140%2,4,6-Trichlorophenol

208 4159755 <0.0005 <0.0005 NA < 0.0005 85% 80% 120% 108% 70% 130% 108% 60% 140%

2,4,5-Trichlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 108% 70% 130% 111% 60% 140%2,3,5-Trichlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 109% 70% 130% 96% 60% 140%3,4,5-Trichlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 109% 70% 130% 111% 60% 140%2,3,4,6-Tetrachlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 109% 70% 130% 110% 60% 140%2,3,5,6-Tetrachlorophenol

208 4159755 <0.0005 <0.0005 NA < 0.0005 105% 70% 130% 108% 60% 140%

2,3,4,5-Tetrachlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 102% 70% 130% 109% 60% 140%Dinoseb (2-sec-butyl-4,6-dinitrophenol)

208 4159755 <0.005 <0.005 NA < 0.005 108% 70% 130% 107% 60% 140%

Pentachlorophenol 208 4159755 <0.0005 <0.0005 NA < 0.0005 88% 80% 120% 109% 70% 130% 102% 60% 140%






Trace Organics Analysis (Continued)

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Polyaromatic Hydrocarbon Analysis - Water FWALAcridine 20 4156591 <0.0001 <0.0001 NA < 0.0001 75% 70% 130% 107% 70% 130% 113% 70% 130%Quinoline 20 4156591 <0.0001 <0.0001 NA < 0.0001 76% 70% 130% 127% 70% 130% 120% 70% 130%2-Methylnaphthalene 20 4156591 <0.00001 <0.00001 NA < 0.00001 83% 70% 130% 120% 70% 130% 109% 70% 130%Naphthalene 20 4156591 0.00001 0.00001 NA < 0.00001 86% 70% 130% 126% 70% 130% 115% 70% 130%Acenaphthylene

20 4156591 <0.00001 <0.00001 NA < 0.00001 72% 70% 130% 106% 70% 130% 91% 70% 130%

Acenaphthene 20 4156591 <0.00001 <0.00001 NA < 0.00001 86% 70% 130% 127% 70% 130% 117% 70% 130%Fluorene 20 4156591 <0.00001 <0.00001 NA < 0.00001 79% 70% 130% 119% 70% 130% 105% 70% 130%Phenanthrene 20 4156591 <0.00001 <0.00001 NA < 0.00001 86% 70% 130% 124% 70% 130% 113% 70% 130%Anthracene 20 4156591 <0.00001 <0.00001 NA < 0.00001 70% 70% 130% 106% 70% 130% 90% 70% 130%Fluoranthene

20 4156591 <0.00001 <0.00001 NA < 0.00001 75% 70% 130% 115% 70% 130% 109% 70% 130%

Pyrene 20 4156591 <0.00001 <0.00001 NA < 0.00001 93% 70% 130% 128% 70% 130% 121% 70% 130%Benzo[a]anthracene 20 4156591 <0.00001 <0.00001 NA < 0.00001 80% 70% 130% 107% 70% 130% 90% 70% 130%Chrysene 20 4156591 <0.00001 <0.00001 NA < 0.00001 109% 70% 130% 119% 70% 130% 129% 70% 130%Benzo[b+j]fluoranthene 20 4156591 <0.00001 <0.00001 NA < 0.00001 96% 70% 130% 119% 70% 130% 127% 70% 130%Benzo[k]fluoranthene

20 4156591 <0.00001 <0.00001 NA < 0.00001 102% 70% 130% 127% 70% 130% 128% 70% 130%

Benzo[a]pyrene 20 4156591 <0.00001 <0.00001 NA < 0.00001 77% 70% 130% 99% 70% 130% 94% 70% 130%Indeno[1,2,3-cd]pyrene 20 4156591 <0.00001 <0.00001 NA < 0.00001 71% 70% 130% 106% 70% 130% 106% 70% 130%Benzo[ghi]perylene 20 4156591 <0.00001 <0.00001 NA < 0.00001 88% 70% 130% 116% 70% 130% 123% 70% 130%Dibenzo[ah]anthracene 20 4156591 <0.00001 <0.00001 NA < 0.00001 89% 70% 130% 126% 70% 130% 129% 70% 130% Carbamate Pesticides in Water Aldicarb 1 < 2.0 < 2.0 0.0% < 2.0 98% 60% 130% 84% 60% 130% NA 60% 130%Bendiocarb 1 < 2 < 2 0.0% < 2 91% 60% 130% 102% 60% 130% NA 60% 130%Carbofuran 1 < 5 < 5 0.0% < 5 91% 60% 130% 102% 60% 130% NA 60% 130%Carbaryl 1 < 5 < 5 0.0% < 5 62% 60% 130% 106% 60% 130% NA 60% 130%Diuron

1 < 10 < 10 0.0% < 10 116% 60% 130% 105% 60% 130% NA 60% 130%

Triallate 1 < 1 < 1 0.0% < 1 99% 60% 130% 84% 60% 130% NA 60% 130%Temephos 1 < 10 < 10 0.0% < 10 107% 60% 130% 95% 60% 130% NA 60% 130% Herbicides (water)2,4-D 1 < 0.5 < 0.5 0.0% < 0.5 82% 60% 130% 88% 60% 130% NA 60% 130%2,4,5-T 1 < 0.5 < 0.5 0.0% < 0.5 108% 60% 130% 94% 60% 130% NA 60% 130%2,4,5-TP 1 < 0.5 < 0.5 0.0% < 0.5 120% 60% 130% 104% 60% 130% NA 60% 130%Dicamba 1 < 0.5 < 0.5 0.0% < 0.5 117% 60% 130% 98% 60% 130% NA 60% 130%Dichlorprop

1 < 0.5 < 0.5 0.0% < 0.5 130% 60% 130% 90% 60% 130% NA 60% 130%

Dinoseb 1 < 0.5 < 0.5 0.0% < 0.5 75% 60% 130% 60% 60% 130% NA 60% 130%Picloram 1 < 0.5 < 0.5 0.0% < 0.5 75% 60% 130% 90% 60% 130% NA 60% 130%Diclofop-methyl 1 < 0.5 < 0.5 0.0% < 0.5 130% 60% 130% 93% 60% 130% NA 60% 130% Triazine Pesticides [water]Trifluralin 1 < 2.0 < 2.0 0.0% < 1.0 80% 50% 130% 65% 50% 130% 63% 50% 130%







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Simazine 1 < 1.0 < 1.0 0.0% < 1.0 64% 50% 130% 64% 50% 130% 65% 50% 130%Atrazine 1 < 0.5 < 0.5 0.0% < 0.5 112% 50% 130% 94% 50% 130% 88% 50% 130%Metribuzin 1 < 2.0 < 2.0 0.0% < 0.25 82% 50% 130% 74% 50% 130% 69% 50% 130%Prometryne

1 < 0.25 < 0.25 0.0% < 0.25 122% 50% 130% 107% 50% 130% 86% 50% 130%

Metolachlor 1 < 2.0 < 2.0 0.0% < 0.11 107% 50% 130% 93% 50% 130% 99% 50% 130%Alachlor 1 < 0.5 < 0.5 0.0% < 0.5 108% 50% 130% 93% 50% 130% 98% 50% 130%Cyanazine 1 < 1.0 < 1.0 0.0% < 1.0 89% 50% 130% 82% 50% 130% 82% 50% 130% O. Reg. 153(511) - OC Pesticides + PCBs (Water)Gamma-Hexachlorocyclohexane 1 < 0.01 < 0.01 0.0% < 0.01 130% 50% 140% 91% 50% 140% 91% 50% 140%Heptachlor 1 < 0.01 < 0.01 0.0% < 0.01 120% 50% 140% 93% 50% 140% 81% 50% 140%Aldrin 1 < 0.01 < 0.01 0.0% < 0.01 130% 50% 140% 116% 50% 140% 105% 50% 140%Heptachlor Epoxide 1 < 0.01 < 0.01 0.0% < 0.01 130% 50% 140% 107% 50% 140% 98% 50% 140%Endosulfan

1 < 0.05 < 0.05 0.0% < 0.05 120% 50% 140% 92% 50% 140% 91% 50% 140%

Chlordane 1 < 0.04 < 0.04 0.0% < 0.04 120% 50% 140% 90% 50% 140% 90% 50% 140%DDE 1 < 0.01 < 0.01 0.0% < 0.01 114% 50% 140% 92% 50% 140% 96% 50% 140%DDD 1 < 0.05 < 0.05 0.0% < 0.05 105% 50% 140% 96% 50% 140% 97% 50% 140%DDT 1 < 0.04 < 0.04 0.0% < 0.04 130% 50% 140% 90% 50% 140% 96% 50% 140%Dieldrin

1 < 0.02 < 0.02 0.0% < 0.02 120% 50% 140% 80% 50% 140% 68% 50% 140%

Endrin 1 < 0.05 < 0.05 0.0% < 0.05 120% 50% 140% 75% 50% 140% 78% 50% 140%Methoxychlor 1 < 0.04 < 0.04 0.0% < 0.04 114% 50% 140% 75% 50% 140% 86% 50% 140%Hexachlorobenzene 1 < 0.01 < 0.01 0.0% < 0.01 120% 50% 140% 102% 50% 140% 92% 50% 140%Hexachlorobutadiene 1 < 0.01 < 0.01 0.0% < 0.01 116% 50% 140% 101% 50% 140% 91% 50% 140%Hexachloroethane

1 < 0.01 < 0.01 0.0% < 0.01 114% 50% 140% 98% 50% 140% 90% 50% 140%

Aroclor 1242 1 < 0.2 < 0.2 0.0% < 0.2 NA 60% 140% NA 60% 140% NA 60% 140%Aroclor 1248 1 < 0.2 < 0.2 0.0% < 0.2 NA 60% 140% NA 60% 140% NA 60% 140%Aroclor 1254 1 < 0.2 < 0.2 0.0% < 0.2 NA 60% 140% NA 60% 140% NA 60% 140%Aroclor 1260 1 < 0.2 < 0.2 0.0% < 0.2 NA 60% 140% NA 60% 140% NA 60% 140%Polychlorinated Biphenyls

1 < 0.2 < 0.2 0.0% < 0.2 112% 60% 140% 98% 60% 140% 96% 60% 140%

OP pesticides [water]Phorate 1 < 0.5 < 0.5 0.0% < 0.5 92% 60% 140% 95% 60% 140% 101% 60% 140%Dimethoate 1 < 2.5 < 2.5 0.0% < 2.5 84% 60% 140% 95% 60% 140% 95% 60% 140%Terbufos 1 < 0.5 < 0.5 0.0% < 0.5 96% 60% 140% 82% 60% 140% 89% 60% 140%Diazinon 1 < 1.0 < 1.0 0.0% < 1 95% 60% 140% 98% 60% 140% 97% 60% 140%Malathion

1 < 5.0 < 5.0 0.0% < 5 81% 60% 140% 90% 60% 140% 86% 60% 140%

Chlorpyrifos 1 < 1.0 < 1.0 0.0% < 1 94% 60% 140% 90% 60% 140% 100% 60% 140%Parathion 1 < 1.0 < 1.0 0.0% < 1 88% 60% 140% 73% 60% 140% 67% 60% 140%Azinphos-methyl 1 < 2.0 < 2.0 0.0% < 2 96% 60% 140% 90% 60% 140% 83% 60% 140% Haloacetic Acids (water)Chloroacetic Acid 1 4162089 < 1.7 < 1.7 0.0% < 1.7 74% 70% 130% 93% 60% 130% NA 70% 130%







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Bromoacetic Acid 1 4162089 < 0.2 < 0.2 0.0% < 0.2 97% 70% 130% 76% 60% 130% NA 70% 130%Dichloroacetic Acid 1 4162089 11 11 0.0% < 0.2 79% 70% 130% 110% 60% 130% NA 70% 130%Dibromoacetic Acid 1 4162089 < 0.1 < 0.1 0.0% < 0.1 97% 70% 130% 80% 60% 130% NA 70% 130%Trichloroacetic Acid

1 4162089 9.2 8.2 11.5% < 0.2 99% 70% 130% 76% 60% 130% NA 70% 130%

Bromochloroacetic Acid 1 4162089 < 0.3 < 0.3 0.0% < 0.3 91% 70% 130% 105% 60% 130% NA 70% 130% Comments: Matrix Spike Not Available (NA); results based on Blank Spike recovery.

Certified By:







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Routine Chemistry Water AnalysispH 4163727 4163727 8.03 8.16 1.6% 104% 90% 110%T - Alkalinity (as CaCO3) 4163727 4163727 389 392 0.9% < 5 96% 80% 120%Electrical Conductivity 4163727 4163727 816 822 0.7% < 5 101% 80% 120%Chloride 4360 4162089 3 3 0.0% < 1 92% 80% 120% 94% 80% 120%Fluoride

4360 4162089 0.15 0.15 0.0% < 0.05 98% 80% 120% 105% 80% 120%

Nitrate 4360 4162089 <0.5 <0.5 NA < 0.5 95% 80% 120% 96% 80% 120%Nitrite 4360 4162089 <0.05 <0.05 NA < 0.05 95% 80% 120% 92% 80% 120%Sulfate 4360 4162089 44 44 0.0% < 1 93% 80% 120% 98% 80% 120%Dissolved Calcium 770 529 12.6 13.0 3.0% < 0.3 102% 80% 120% 100% 80% 120%Dissolved Magnesium

770 529 7.4 7.5 1.6% < 0.2 99% 80% 120% 98% 80% 120%

Dissolved Sodium 770 529 8.8 9.1 2.8% < 0.6 98% 80% 120% 97% 80% 120%Dissolved Potassium 770 529 6.2 6.4 2.2% < 0.6 92% 80% 120% 93% 80% 120%Dissolved Iron 770 529 1.4 1.5 2.3% < 0.1 94% 80% 120% 95% 80% 120%Dissolved Manganese 770 529 0.740 0.761 2.9% < 0.005 99% 80% 120% 97% 80% 120% Comments: N/A - Not Available. Water AnalysisAmmonia, Total (as N) 53 577 2.08 2.07 0.5% < 0.05 102% 80% 120% 107% 80% 120% 101% 80% 120%Bromate 4360 4162089 <0.05 <0.05 NA < 0.05 102% 80% 120% NA 80% 120% 106% 80% 120%Chlorate 4360 4162089 <0.1 <0.1 NA < 0.1 106% 80% 120% NA 80% 120% 95% 80% 120%Chlorite 4360 4162089 <0.1 <0.1 NA < 0.1 94% 80% 120% NA 80% 120% 110% 80% 120%Colour

6150 2089 5 5 0.0% < 5 80% 120% 0% 0% 0% 0%

Total Cyanide 213 841 0.971 1.166 18.2% < 0.002 101% 80% 120% 105% 80% 120% 101% 80% 120%Total Dissolved Solids 6727 2089 255 260 1.9% < 5 98% 80% 120% 0% 0% 0% 0%Total Organic Carbon 329 8089 2 2 0.0% < 1 99% 80% 120% 101% 80% 120% 101% 80% 120% Water Analysis - SulphideSulphide 5962 2089 < 0.01 < 0.01 NA < 0.01 97% 80% 120% 85% 80% 120% Total Metals Scan in Water + Hg (mg/L)Total Aluminum 2067 464 0.394 0.416 5.5% < 0.002 102% 80% 120% 101% 80% 120%Total Antimony 905 464 0.001 0.001 0.0% < 0.001 84% 80% 120% 105% 80% 120%Total Arsenic 905 464 0.006 0.006 0.0% < 0.001 88% 80% 120% 104% 80% 120%Total Barium 905 464 0.24 0.24 0.0% < 0.05 89% 80% 120% 99% 80% 120%Total Boron

2067 464 0.03 0.03 2.1% < 0.01 96% 80% 120% 103% 80% 120%

Total Cadmium 905 464 0.000020 <0. NA < 0.000025 85% 80% 120% 103% 80% 120%Total Chromium 905 464 0.001 0.001 0.0% < 0.001 90% 80% 120% 109% 80% 120%Total Copper 905 464 0.002 0.002 0.0% < 0.002 88% 80% 120% 99% 80% 120%Total Iron 2067 464 <0.1 <0.1 NA < 0.1 100% 80% 120% 103% 80% 120%Total Lead

905 464 <0.001 <0.001 NA < 0.001 89% 80% 120% 101% 80% 120%






Water Analysis

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Total Manganese 2067 464 0.011 0.012 0.9% < 0.005 102% 80% 120% 102% 80% 120%Total Mercury 1359 4618 < 0.000025 < 0.000025 NA < 0.000025 108% 90% 110% 100% 90% 110% 99% 80% 120%Total Selenium 905 464 0.001 0.001 0.0% < 0.001 90% 80% 120% 109% 80% 120%Total Silver 905 464 0.0017 0.0019 11.1% < 0.0001 93% 80% 120% 109% 80% 120%Total Uranium

905 464 <0.001 <0.001 NA < 0.001 88% 80% 120% 105% 80% 120%

Total Zinc 905 464 0.009 0.010 10.5% < 0.003 86% 80% 120% 96% 80% 120%

Certified By:






Water Analysis (Continued)

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Trace Organics AnalysisBenzene TO 0332 EPA 624 & SW-846 5030 GC/MSToluene TO 0332 EPA 624 & SW-846 5030 GC/MSEthylbenzene TO 0332 EPA 624 & SW-846 5030 GC/MSXylenes TO 0332 EPA 624 & SW-846 5030 GC/MSToluene-d8 (BTEX) TO 0330 EPA 624 & SW-846 5030 GC/FIDAldicarb ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCBendiocarb ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCCarbofuran ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCCarbaryl ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCDiuron ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCTriallate ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCTemephos ORG-91-5101 EPA 632 531.1 & MOE E3158 HPLCTotal Haloacetic Acids ORG-120-5110 EPA 552.3 GC/ECDHAA5 ORG-120-5110 EPA 552.3 GC/ECDChloroacetic Acid ORG-120-5110 EPA 552.3 GC/ECDBromoacetic Acid ORG-120-5110 EPA 552.3 GC/ECDDichloroacetic Acid ORG-120-5110 EPA 552.3 GC/ECDDibromoacetic Acid ORG-120-5110 EPA 552.3 GC/ECDTrichloroacetic Acid ORG-120-5110 EPA 552.3 GC/ECDBromochloroacetic Acid ORG-120-5110 EPA 552.3 GC/ECD2-Bromobutanoic acid ORG-120-5110 EPA 552.3 GC/ECD2,4-D ORG-91-5110 EPA SW-846 8151A GC/ECD2,4,5-T ORG-91-5110 EPA SW-846 8151A GC/ECD2,4,5-TP ORG-91-5110 EPA SW-846 8151A GC/ECDDicamba ORG-91-5110 EPA SW-846 8151A GC/ECDDichlorprop ORG-91-5110 EPA SW-846 8151A GC/ECDDinoseb ORG-91-5110 EPA SW-846 8151A GC/ECDPicloram ORG-91-5110 EPA SW-846 8151A GC/ECDDiclofop-methyl ORG-91-5110 EPA SW-846 8151A GC/ECDDCAA ORG-91-5110 EPA SW-846 8151 GC/ECDGamma-Hexachlorocyclohexane ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDHeptachlor ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDAldrin ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDHeptachlor Epoxide ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDEndosulfan ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDChlordane ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDDDE ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDDDD ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDDDT ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDDieldrin ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDEndrin ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDMethoxychlor ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDHexachlorobenzene ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDHexachlorobutadiene ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDHexachloroethane ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDAroclor 1242 ORG-91-5112 EPA SW-846 3510 & 8082 GC/ECDAroclor 1248 ORG-91-5112 EPA SW-846 3510 & 8082 GC/ECDAroclor 1254 ORG-91-5112 EPA SW-846 3510 & 8082 GC/ECDAroclor 1260 ORG-91-5112 EPA SW-846 3510 & 8082 GC/ECD



Method SummaryATTENTION TO: Wes Olstad


AGAT S.O.P ANALYTICAL TECHNIQUELITERATURE REFERENCEPARAMETER




METHOD SUMMARY (V1) of 29

Polychlorinated Biphenyls ORG-91-5112 EPA SW-846 3510 & 8082 GC/ECDTCMX ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDDecachlorobiphenyl ORG-91-5112 EPA SW-846 3510 & 8081 GC/ECDPhorate ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSDimethoate ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSTerbufos ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSDiazinon ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSMalathion ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSChlorpyrifos ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSParathion ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSAzinphos-methyl ORG-91-5103 EPA SW-846 3510C & 8270 & 8141A GC/MSPhenol TO 1200 EPA SW-846 8321 HPLC/UV4-Nitrophenol TO 1200 EPA SW-846 8321 HPLC/UVm&p-Cresol (3&4-methylphenol) TO 1200 EPA SW-846 8321 HPLC/UVo-Cresol (2-methylphenol) TO 1200 EPA SW-846 8321 HPLC/UV2-Chlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,4-Dinitrophenol TO 1200 EPA SW-846 8321 HPLC/UV2-Nitrophenol TO 1200 EPA SW-846 8321 HPLC/UV2,4-Dimethylphenol TO 1200 EPA SW-846 8321 HPLC/UV2,6-Dichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV4-Chloro-3-methylphenol TO 1200 EPA SW-846 8321 HPLC/UV2,4-Dichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV4,6-Dinitro-2-methylphenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,6-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,4-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,4,6-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,4,5-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,5-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV3,4,5-Trichlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,4,6-Tetrachlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,5,6-Tetrachlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,3,4,5-Tetrachlorophenol TO 1200 EPA SW-846 8321 HPLC/UVDinoseb (2-sec-butyl-4,6-dinitrophenol) TO 1200 EPA SW-846 8321 HPLC/UVPentachlorophenol TO 1200 EPA SW-846 8321 HPLC/UV2-Fluorophenol TO 1200 EPA SW-846 8321 HPLC/UV2,4,6-Tribromophenol TO 1200 EPA SW-846 8321 HPLC/UVAcridine TO 0200 EPA 8270 GC/MSQuinoline TO 0200 EPA 8270 GC/MS2-Methylnaphthalene TO 0200 EPA 8270 GC/MSNaphthalene TO 0200 EPA 8270 GC/MSAcenaphthylene TO 0200 EPA 8270 GC/MSAcenaphthene TO 0200 EPA 8270 GC/MSFluorene TO 0200 EPA 8270 GC/MSPhenanthrene TO 0200 EPA 8270 GC/MSAnthracene TO 0200 EPA 8270 GC/MSFluoranthene TO 0200 EPA 8270 GC/MSPyrene TO 0200 EPA 8270 GC/MSBenzo[a]anthracene TO 0200 EPA 8270 GC/MSChrysene TO 0200 EPA 8270 GC/MSBenzo[b+j]fluoranthene TO 0200 EPA 8270 GC/MS










Benzo[k]fluoranthene TO 0200 EPA 8270 GC/MSBenzo[a]pyrene TO 0200 EPA 8270 GC/MSIndeno[1,2,3-cd]pyrene TO 0200 EPA 8270 GC/MSBenzo[ghi]perylene TO 0200 EPA 8270 GC/MSDibenzo[ah]anthracene TO 0200 EPA 8270 GC/MS2-Fluorobiphenyl (PAH) TO 0200 EPA 8270 GC/MSp-Terphenyl-d14 (PAH) TO 0200 EPA 8270 GC/MS

Trifluralin ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Simazine ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Atrazine ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Metribuzin ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Prometryne ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Metolachlor ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Alachlor ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Cyanazine ORG-91-5104 EPA SW-846 3510 & 8270 & MOE E3121 GC/MS

Chloroform TO 0300 EPA SW-846 8260 GC/MSBromodichloromethane TO 0300 EPA SW-846 8260 GC/MSDibromochloromethane TO 0300 EPA SW-846 8260 GC/MSBromoform TO 0300 EPA SW-846 8260 GC/MSToluene-d8 (BTEX) TO 0300 EPA SW-846 8260 GC/FIDChloromethane TO 0330 EPA SW-846 8260 GC/MSVinyl Chloride TO 0330 EPA SW-846 8260 GC/MSBromomethane TO 0330 EPA SW-846 8260 GC/MSChloroethane TO 0330 EPA SW-846 8260 GC/MSTrichlorofluoromethane TO 0330 EPA SW-846 8260 GC/MSAcetone TO 0330 EPA SW-846 8260 GC/MS1,1-Dichloroethylene TO 0330 EPA SW-846 8260 GC/MSMethylene Chloride TO 0330 EPA SW-846 8260 GC/MSMethyl tert-butyl ether TO 0330 EPA SW-846 8260 GC/MSMethyl Ethyl Ketone TO 0330 EPA SW-846 8260 GC/MStrans- 1,2-dichloroethylene TO 0330 EPA SW-846 8260 GC/MS1,1-Dichloroethane TO 0330 EPA SW-846 8260 GC/MScis- 1,2-Dichloroethylene TO 0330 EPA SW-846 8260 GC/MSChloroform TO 0330 EPA SW-846 8260 GC/MS1,2-Dichloroethane TO 0330 EPA SW-846 8260 GC/MS1,1,1-Trichloroethane TO 0330 EPA SW-846 8260 GC/MSCarbon Tetrachloride TO 0330 EPA SW-846 8260 GC/MSBenzene TO 0330 EPA SW-846 8260 GC/MS1,2-Dichloropropane TO 0330 EPA SW-846 8260 GC/MSTrichloroethylene TO 0330 EPA SW-846 8260 GC/MSBromodichloromethane TO 0330 EPA SW-846 8260 GC/MStrans-1,3-Dichloropropene TO 0330 EPA SW-846 8260 GC/MSMethyl Isobutyl Ketone TO 0330 EPA SW-846 8260 GC/MScis-1,3-Dichloropropene TO 0330 EPA SW-846 8260 GC/MS










1,1,2-Trichloroethane TO 0330 EPA SW-846 8260 GC/MSToluene TO 0330 EPA SW-846 8260 GC/MS2-Hexanone TO 0330 EPA SW-846 8260 GC/MSDibromochloromethane TO 0330 EPA SW-846 8260 GC/MSEthylene Dibromide TO 0330 EPA SW-846 8260 GC/MSTetrachloroethene TO 0330 EPA SW-846 8260 GC/MS1,1,1,2-Tetrachloroethane TO 0330 EPA SW-846 8260 GC/MSChlorobenzene TO 0330 EPA SW-846 8260 GC/MSEthylbenzene TO 0330 EPA SW-846 8260 GC/MSm & p-Xylene TO 0330 EPA SW-846 8260 GC/MSBromoform TO 0330 EPA SW-846 8260 GC/MSStyrene TO 0330 EPA SW-846 8260 GC/MS1,1,2,2-Tetrachloroethane TO 0330 EPA SW-846 8260 GC/MSo-Xylene TO 0330 EPA SW-846 8260 GC/MS1,3-Dichlorobenzene TO 0330 EPA SW-846 8260 GC/MS1,4-Dichlorobenzene TO 0330 EPA SW-846 8260 GC/MS1,2-Dichlorobenzene TO 0330 EPA SW-846 8260 GC/MS1,2,4-Trichlorobenzene TO 0330 EPA SW-846 8260 GC/MSTotal Xylenes TO 0330 EPA SW-846 8260 GC/MSToluene-d8 (BTEX) TO 0330 EPA SW-846 8260 GC/FID










Water AnalysispH INST 0101 SM 4500 H+ pH METERp - Alkalinity (as CaCO3) INST 0101 SM 2320 B TITRATIONT - Alkalinity (as CaCO3) INST 0101 SM 2320 B TITRATIONBicarbonate INST 0101 SM 2320 B TITRATIONCarbonate INST 0101 SM 2320 B TITRATIONHydroxide INST 0101 SM 2320 B TITRATIONElectrical Conductivity INST 0101 SM 2510 B CONDUCTIVITY METERChloride INST 0150 SM 4110 B ION CHROMATOGRAPHFluoride INST 0150 SM 4110 B ION CHROMATOGRAPHNitrate INST 0150 SM 4110 B ION CHROMATOGRAPHSulfate INST 0150 SM 4110 B ION CHROMATOGRAPHDissolved Calcium INST 0140 SM 3120 B ICP/OESDissolved Magnesium INST 0140 SM 3120 B ICP/OESDissolved Sodium INST 0140 SM 3120 B ICP/OESDissolved Potassium INST 0140 SM 3120 B ICP/OESDissolved Iron INST 0140 SM 3120 B ICP/OESDissolved Manganese INST 0140 SM 3120 B ICP/OESTotal Aluminum WATR 0200; INST 0140 SM 3030 E; SM 3120 B ICP/OESTotal Antimony WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Arsenic WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Barium WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Boron WATR 0200; INST 0140 SM 3030 E; SM 3120 B ICP/OESTotal Cadmium WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Chromium WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Copper WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Iron WATR 0200; INST 0140 SM 3030 E; SM 3120 B ICP/OESTotal Lead WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Manganese WATR 0200; INST 0140 SM 3030 E; SM 3120 B ICP/OESTotal Mercury WATR 0200; INST 0160 SM 3030 E; SM 3112 B CV/AATotal Selenium WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Silver WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Uranium WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSTotal Zinc WATR 0200; INST 0141 SM 3030 E; SM 3125 B ICP-MSAmmonia, Total (as N) INST 0340 SM 4500-NH3 G CONTINUOUS FLOW ANALYZERBromate INST 0150 SM 4110 B ION CHROMATOGRAPHChlorate INST 0150 SM 4110 B ION CHROMATOGRAPHChlorite INST 0150 SM 4110 B ION CHROMATOGRAPHColour WATR 0500 SM 2120 B VISUALTotal Cyanide INST 0310 SM 335.3 CONTINUOUS FLOW ANALYZERTotal Dissolved Solids WATR 0610 SM 2540 C GRAVIMETRICTotal Organic Carbon INST 0170 SM 5310 B COMBUSTIONSulphide WAT 0100 SM 4500 S2- D SPECTROPHOTOMETER










Wesley Olstad

Wesley Olstad

Wesley Olstad

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