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4 U.S. Gownmeat Rlntlns offtco: laataos-O~OAIOI 2.1

REPORT # 71

LABORATORY ANALYSIS ON

NAVAL SAMPLES

(A/E CONTRACT N 6 2 4 7 0 - 8 4 - B - 6 9 3 2 ) - - .- .P .,- -

J T C REPORT # 85-208

PREPARED FOR:

DEPARTMENT O F THE NAVY

ATLANTIC D I V I S I O N

NAVAL F A C I L I T I E S ENGINEERING COMMAND

NORFOLK, VA 2 3 5 1 1

PREPARED BY:

JTC ENVIRONMENTAL CONSULTANTS, INC.

4 RESEARCH PLACE, S U I T E L - 1 0

ROCKVILLE, MARYLAND 2 0 8 5 0

MAY 28, 1985

Ann E. R o s e c r a n c e / L a b o r a t o r y D i r e c t o r ' CLW

0 0 ~ 0 0 0 0 5 1 5 7

C t W ~ 0 0 0 0 0 5 1 5 8

JTC E n v i r o n m e n t a l C o n s u l t a n t s , Inc.

~a r s 3 - ~ $ - $ 5 ~ e ~ o r t NO . 7 1 t o N a v a l Facilities E n g i n e e r i n g Command, N o r f o l k , Virginia

J T C D a t a R e p o r t No. 85-208 Table / Date o f Sample R e c e i p t 5-17-85

N A V Y

SAMPLE

I D

JTC

SAMPLE

ID 4 ~ 0 & A

0

484 8% (2-520 B Cattu Phnacr

486 U-6572. A 11

B 11 3

12-08-73 A JI

fie& TL . 6 I! J 3 ,

-. ANALYSIS PARAMETER

see a h c~edl

S htct

I!

I!

I r

I I

I \

2%. this %I.

- f.

0

4 '3 3

0 0 0 0 0 0 5 1 5 9 J T C ENVXRONMENTU CONSULTI\NTS, I N C .

P R I O R I T Y POLLUTI\NT ANALYSIS DATA SHEET

VOLATILE FRnCTXON

-

JK SWPLE # 1 ; r - u 8 ( ~ q A PROJECT NO. NF-12

NAVY SAMPLE # 4 8 3 w DATE RECEIVED 51 \) \ 85 METHOD NO. 624 DETECTION ~AIMXT 10 u g / l i t :

-- - - - .7,43iL - -

PZ$RAME!I!ER RESULT PARAMETER RESULT ug/li t . ugIlXt

2V acrdrein N . D . 32V 1,2-dichloropropane N-D.

3V acrylonitrile N . D.

4v. benzene N . D .

6V carbon tetrachloride NiD.

7V chlorobenzwe N. D.

' 10V 1 r 2-dichloroethane N.D.

LlV 1, I., 1- tz ich lo~- ethane N - D .

13V 1, 1-dichloroethrtne N.D.

14V 1,1,2-trichloro- ethane N.D.

1 S V 1,1,2,2-tetra- chloroethane N.D.

16V c h l o r o e t h a n e N . D .

19V 2-chloroethylvinyl ether N . D .

2 3 V c h l o r o f o r m Lf c 6'-

33V 1,3-dichloropro- pylene N . D ,

38V ethylbenzene N.D. C

44v m e t h v l e n e chloride N . D ,

45V m e t h y l chloride N-D. '

.46V methyl bromide N.D.

4 8V dichlorobromo- , g.2 * m e t h a n e m.

49V trichlorof luoro- m e t h a n e N . D .

50V dichlorodi f luoro- m e t h a n e N . D .

.-' a I 51V c h l o r o d i b r o m o m e t h a n e

BSV tetrachloxoethylene N.D.

86V to luenc N. D.

30V 1 , 2 - t r a n s - d i c h l o r o - 88v vinyl chloride N. D.

c t h y l c n e N.D.

, 0 ~ 0 0 0 0 5 1 6 0 YTC E N V I R O N M E N T A L CONSULTWTS, XNC.

? R I O R I T Y POLLUTMT I\NALYSIS DATA S N G E T

VOLATILE FRACTION

-

JTC SAMPLE # PROJECT NO. NF-12 - NAW SAMPLE # 4 8 3 w /O DATE RECEIVED 51131 85

METHOD NO, 624 DETECTION ~ I M I T 10 ug/lit

PqRAMETER RESULT ug/lit

2~ acrolein N.D.

4 V . benzene N.D.

6V carbon tetrachloride NiD.

7V chloxobenzqe N.D.

t ' 10V I, 2-dichloroethane N O D o

IIv l,l, 1-trichloA- 5+ 8 * ethane 4kB.

13V 1,l-dichloroethane N.D.

14V 1,1,2-trichloro- ethane N.D.

1SV 1,1,2,2-tetra- chloroethane N.D.

16V chloroethane N.D.

19V 2-chloroethylvinyl ether N.D,

23V chloroform I + xnr.

30V 1,2-trans-dichloro- ethylene N.D.

-- - - .- - -

PARAMETER RESULT . ug71i.t

32V 1,2-dichloropropane N.D.

38V ethylbenzene N,D, *

44V methylene chloride NOD-

4SV methyl chloride N.D.'

. 4 6V methyl bromide N.D.

4 8V dichlorobromo- 37 methane *

49V trichlorofluoro- methane N . D .

50V dichlorodifluoro- methane N . D .

51V chlorodibromomethane

8SV tetrachloroethylene N.D.

06V toluene N.D.

U7v trichloroethylene N. D.

08V vinyl chloride N.D.

CLW 0 0 0 0 0 0 5 1 6 1

J T C E N V I R O N M E N T A L , cONSULTWTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA S ~ ~ E E T

VOLATILE FiWCTXON

JTC SAMPLE # /a-0870 f l PROJECT NO. NF-12

NAVY SAMPLE # 2-J Lf bd DATE RECEIVED- 51 131 5

METKOD NO. 624 DETECTION ~ I M I T 10 u g / l i t

PaRAMETER RES U LT ug/lit:

2V a c m l e i n N.D.

3V a c r y l o n i t r i l e N.D-

4 V . benzene N-D.

6 V carbon t e t rach lor ide N : D.

7 V chlorobenzwe . N.D.

IlV 1,1, l-hichlok- 6 a b * ethane M.

1 3 V 1,l-dichloroethrzne N.D.

1 4 V 1 0 112-tr ichloro- ethane N . D .

15V 1,1 ,2 ,2-tetra- chloroethane N . D .

1 6 V chloroethane N. D.

19V 2-chloroethylvinyl e ther N.D.

2 3 V chloroform (4.5 &.

.-m - - - --- .

PARAMETER RESULT . ug11Lt

32V 1,2-dichloropropane N.D.

3 3 V 103-dichloropro- pylene N.D,

3 8 V ethvlbenzene N , D ,

44V methylene ch lor ide N.D.

4SV methyl chloride N.D.'

. 4 6V methyl bxotd.de N.D.

48V dichlorobromo- methane I7 M.

49V t r i c h l o r o f luoro- methane N.D.

50V dichlorodi f luoro- methane N . D .

5lV chlorodibromomethaneY am-.

85V te trachloroethylene N . D .

86v to luene N . D .

B 7 V trichloroethylene N.D.

30V 1,2-trans-dichloro- 88v vinyl c h l o r i d e N. D .

e t t ly l ene N.D.

CLW 0 0 0 0 0 0 5 1 6 2

JTC E N V X R O N M E N T ~ C . CONSULTWTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA S ~ ~ E E T

VOLATILE FRACTION

JTC SAMPLE # PROJECT NO, NF-12 - - NAVY SAMPLE # Y8U DATE RECEIVED 5//3/ 8s

' i

METLIOD NO. 624 DETECTION GIMIT 10 ug/lit:

.-* - PARAMETER - =Y.C -,-

PbRAMETER RESULT RESULT ug/lit . ug7li.t

3V acrylonitrile N-D.

4~ . benzene N-D.

6V carbon tetrachloride NID,

7V chlorobenzeqe . N, D.

' LOV I, 2-dichloroethane N.D.

11V 1,1,l-trichlom- ethane N.D.

14V 1,1,2-trichloro- ethane N . D ,

1SV 1,1,2,2-tetra- chloroethane N.D.

16V chloroethane N.D.

19V 2-chloroethylvinyl ether N.D.

33V 1,3-dichloropro- pylene N.D.

38V ethylbenzene N,D. C

44V methylene chloride N.D.

4SV methyl chloride N.D.'

4 6V methyl bromide N, D,

47v bromoform 67-. 48V dichlorobmmo- 3 3

methane -a

4 9V trichlorof luoro- methane N O D ,

SOV dichlorodifluoro- methane N.D.

-. / 0

8SV tetrachloroethylene N . D .

23V chloroform 86v toluene N. D.

29V 1,l-dichloroethylene N. D. 0 7 & trichloroethylene N.D.

30V 1, 2-trans-dichloro- O8v vinyl chloride N. D .

c t h y l e n e N.D.

CLW 0 0 0 0 0 0 5 1 6 3

JTC E N V I R O N M E N T A L CONSULTWTS, I N C . P R I O R I T Y POLLUTMT ANALYSIS DATA SHEET

VOLATILE FRACTION

-

JTC SAMPLE # ! A - O 8 7 / A PROJECT NO. NF-12 . - NAVY SAMPLE # 7 x 5 DATE RECEIVED T I / - ) I g 1 METHOD NO. 624 DETECTION LIMIT 10 ug/lit

- - - - .-- -

P~RAMETER RESULT PARAMETER RESULT ug/lit . ~gi/lilt:

2V acrolein N . D . 32V 1,2-dichloropropane N.D.

4 V . benzene N . D .

6 V carbon tetrachloride N i D .

1 10V Ir 2-dichloroethane N.D.

IlV 1,l. l d d c h l o k - 9. .a ?C ethane m.

13V 1,l-dichloroethzne N O D .

14V 1,1,2-trichloro- ethane N . D .

1SV 1,1,2,2-tetra- chloroethane N.D.

1 6 V chloroethane N. D .

19V 2-chloroethylvinyl ether N.D.

Z 3 V chloroform 5; 8 m.

pylene N . D .

38V ethylbenzene N.D. L

44V methylene chloride N.D.

4SV methyl chloride N O D ,

4 6V met hvl bromide N-D-

48V dichlorobromo- / 5 methane

49V trichlorof luoro- methane N.D.

50V dichlorodifluoro- methane N . D -

8 S V tetrachloroethylene N.D.

8 6 V toluene N . D.

29V 1,l-dichloroethylene N . D . 07; trichloroethylent N.D.

30V 1, 2-trans-dichloro- 0 8 V vinyl chloride N.D. e t h y l e n e N.D.

N . D . N O T D6TECr60 N . A . =; NOT nr*r,r,rcntlr.tynNnr,uzur,

0 0 0 0 0 0 5 1 6 4

JTC E N V X R O N M E N T U CONSULTNJTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA SffEET

VOLATILE FRACTION

--

JTC SAMPLE # PROJECT NO. NF-12

NAVY SAMPLE # DATE RECEIVED

METCIOD NO. 624 DETECTION ~ Z M L T 10 u g / l i t

- - .=- -

PI)RAMETER RESULT PARAMETER RESULT ug/lit . ugY1i.k

2V acrolein N.D . 32V 1, 2-dichloropropane N.D.

3V acrylonitrile N.D .

4V. benzene N-D.

6V carbon tetrachloride Ni D.

10V I, 2-dichloroethane N.D.

1;V l,l,l-krichlo&- q,7 * ethane *-

1 3 V I, 1-dichloroethzme N . D .

l 4 V 1,1,2-trichxoro- ethane N . D .

1 5 V 1,1,2,2-tetra- chloroethane N . D .

1 6 V chloroethane N . D .

1 9 V 2-chloroethylvinyl e t h e r N . D .

33V 1,3-dichloropro- pylene N O D ,

38V ethylbenzene N.D. . 4 4 V r n e t h y l e n e chloride N O D ,

4SV m e k h v l chloride N-D-'

. 4 6 V methyl bromide N.D. t -

4 8 V d i c h l o r o b m m o - 3 m e t h a n e -&a.

4 9 V trichlorofluoro- m e t h a n e N . D -

50V dichlorodif luom- m e t h a n e N,D,

- 1 -

8 S V tetrachloroethylene N - D ,

2 3V c h l o r o f o r m \ I *. 8 6 v t o luene N . D.

29V 1 , l -d i ch loroe thy l ene N . D . 07b t r i c h l o r o e t h y l o n k N . D .

30V 1,2-trans-dichloro- 08v vinyl c h l o r i d e N . D . ethylene N . D .

N -1). = NOT DETECI'ED N . A . :: NOT r\[*Pr, rcnu r.r.:/nNnr,Y x i-:o

D R I O R I T Y POLLUTNJT ANALYSIS DATA S ~ ~ E E T

VOLATILE FRACTION

JTC SAMPLE # 1 a-0871 A PROJECT NO. NF-12

N A ~ SAMPLE # Y 8 L HI DATE RECEIVED 51 j 3 185 '

METHOD NO. 624 DETECTION LIMIT 10 u g / l i t

- - . -- -

PJJRAMETER RESULT PARAMETER RESULT ug/l it . ugi/li-t

2 V acrolein N.D. 32V 1,2-dichloropropane N-D,

3V acrylonitrile N.D. 3 3 V 1,3-dichloropro- pylene N.D.

4V . benzene N.D. 3 8 V ethylbenzene N,D.

6V carbon tetrachloride N.D. 4 4 V m e t h y l e n e chloride N.D.

7 V chlorobenzqe N. D. 4SV m e t h y l chloride N.D.

1 0 V 1 , Z - d i c h l o r o e t h a n e N.D. I . 4 6V m e t h y l bxomide N.D.

1 1 V 1,l. 1-trichlok- 3 ,% % ethane M . 4 7 V bromoform

1 3 V 1,l-dichloroethane N.D.

1 4 V 1,1,2-trichloro- ethane N . D .

1 S V 1,1,2,2-tetra- chloroethane N . D .

16V c h l o r o e t h a n e N.D.

19V 2-chloroethylvinyl ether N . D .

2 3V c h l o r o f o r m (g ,a&

4 8V d i c h l o r o b r o m o - m e t h a n e

4 9V trichlorof luoro- m e t h a n e N.D.

50V d i c h l o r o d i f l u o ~ - m e t h a n e N-D,

51V c h l o r o d i b r o m o m e k h ~ e ~ ?Hre.

8 5 V t e t r a c h l o r o e t h y l e n e N . D .

8 6 V to luene N. D.

30V l,2-trans-dichloro- 88v vinyl chloride N . D . e t h y l e n e N.D.

CLW 0 0 0 0 0 0 5 1 6 6

YTC E N V I R O N M E N T A L CONSULTANTS, I N C . P R I O R I T Y POLLUTANT ANALYSIS DATA SI {EET

VOLATILE FRACTION

JTC SAMPLE # PROJECT NO. NF-12

NAVY SAMPLE # DATE RECEIVED 511 3 (f

METHOD NO. 624 DETECTION ~ ~ I M I T 10 ug / l i t

-5i3- - PARAMETER

- - - - - PaRAMETER RESULT RESULT

ug/lit ugY1i.t

2V acrolein N.D. 32V 1,2-dichloropropane N.D.

3V acrylonitrile N.D. 33V 1,3-dichloropro- pylene N . D ,

4 V . benzene N-D, - -- - - - 38V ethylbenzene N . D .

6V carbon tetrachloride N ; D. . 44V methylene chloride N. D,

7V chloxobenzqe N.D. 45V methyl chloride N.D.

1 0 V 1,2-dichloroethane -

N.D. I . 4 6V methyl bromide N.D.

I ~ V ~ , ~ , ~ - t r i c ~ . o k - . - /

14V 1,1,2-trichloro- ethane N . D .

1SV 1,1,2,2-tetra- chloroethane N.D.

16V chloroethane N . D .

1 9 V 2-chloroethylvinyl ether N . D .

23V chloroform I 3 e -

48V dichlorobromo- methane

49V trichlorof luoro- methane N . D -

50V dichlorodifluor0- methane N.D.

GY S1V chlorodibromoaethane

8 SV tetrachloxoethylene N.D.

86V toluene N.D.

30V 1, Z-trans-dichloro- 88v vinyl chloride N . D .

cttlylene N.D.

0 0 0 0 0 0 5 1 6 7 YTC E N V I R O N M E N T A L , CONSULTANTS, X N C .

PRIORITY POLLUTANT ANALYSIS DATA SfiEET

VOLATILE FRRCTION

JTC SAMPLE # _ PROJECT NO. NF-12 . I -

487 W NAVY SAMPLE # DATE RECEIVED 5 1 31 85 METHOD NO. 624 DETECTION $ 1 ~ 1 ~ 10 u g / l i t

--* - - -- - PaRAMETER RESULT PARAMETER RESULT

ug/ l i t ugi/lit

2 V acxolein N O D o 32V 1 , 2 - d i c h l o r o p r o p a n e N.D.

3~ acrylonitrile N . D .

4 V . benzene N.D.

6V carbon tetrachloride N i D .

IOV lr2-dichloroethane N.D.

v 1 , x i - 8 ,8 * ethane -N-;-D.

1 3 V 1,l-dichloroethme N . D .

1 4 V l,l, 2-trichloro- ethane N.D-

1 S V 1,1,2,2-tetra- chloroethane N . D .

1 6 V chloroethane N.D.

1 9 V 2-chloroethylvinyl e t h e r N-D.

44V m e t h y l e n e chloride N . D .

4SV m e t h y l chloride N.D.'

. 4 6V methyl bromide NODo

4 8 V d i c h l o r o b r o m o - - 3 2 m e t h a n e -HTD.

49V trichlorofluoro- m e t h a n e N . D ,

SOV dichlorodif luoro- m e t h a n e N.D.

S l V c h l o r o d i b r o m o m e t h a n e

8SV tetrachloroethylene N.D.

23V c h l o r o E o r m 10 TJ73-. 8 6 V to luene N . 0 .

30V 1 , 2 - t r a n s - d i c h l o r o - c t t l y l e n e N.D.

0 7~ t r i ch loroe thy len= N.D.

8 8 V v i n y l chloride N.D.

0 0 0 0 0 0 5 1 6 8 JTC E N V I R O N M E N T A L CONSULTWTS, XNC.

!?RXORXTY POLLUTANT ~ A L Y S ~ S DATA S I ~ E E T

VOLATILE FRACTION

J T C SAMPLE # PROJECT NO, NF-12

N A W SAMPLE # ~ t g -? U \ / D _ D A T E R E C E I V E D 5 1 ) - ) / 8 s T

METHOD NO. 624 DETECTION &EMIT 10 u g / l i t

PgRAMETER RESULT ug/ l i t

2 V acrolein N.D.

3V a c r y l o n i t r i l e N, D.

4 V . benzene N.D .

6V carbon t e t r a c h l o r i d e N;D-

1, Z, l,l-kxichlo&- 9, ethane (Y.U.

14V 1 , 1 , 2 - t r i c h l o r o - ethane N . D .

15V 1 ,1 ,2 ,2 - te tra - chloroethane N.D.

1 6 V chloroethane N.D.

19V 2 - c h l o r o e t h y l v i n y l e t h e r N.D.

23V chloroform

2 9 V 1 , l - d i c h l o r o e t h y l e n e N . D.

30V 1, Z-trans-dichloro- c t h y l e n e N . D .

-- - PARAMETER

- - . ? Z - RESULT

. ug;/li't

38V e thy lbenzene NID,

4 4 V methylene c h l o r i d e N O D .

4SV methyl chloride N.D.

46V methyl bromide N.D.

4 8V dichlorobromo- methane 3 La

49V t r i c h l o r o f l u o r o - methane N . D .

50V d i c h l o r o d i f luoro- methane N - D ,

-n

8SV tetrachloroethylene N . D .

8 6 V t o l u e n e N . D .

07V t r i c h l o r o e t h y l e n b N.D.

8 8 V v i n y l c h l o r i d e N . D .

N . D . = N01' DETECI'EO N . A . rz NOT AI'PT*LCAU~.I~~/ANAI,Y %I311