characteristic testing - wadsworth center
TRANSCRIPT
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 1 of 132Solid and Hazardous Waste 180.3
Characteristic Testing
Analyte Technology Method Name ELAP Method Number
Ignitability 4001 99 EPA 1020B
3999 FLPT EPA 1010A
3998 FLPT EPA 1010B
1102 IGNT EPA 1030
Corrosivity (pH) 3802 GRAV EPA 1110A
1286 POT EPA 9040C
1287 POT EPA 9045D
E.P. Toxicity 4004 99 EPA 1310
TCLP 4005 99 EPA 1311
Synthetic Precipitation Leaching Proc. 4007 99 EPA 1312
Multiple Extraction Procedure 4033 99 EPA 1320
Free Liquids 1058 PA EPA 9095B
Metals I
Analyte Technology Method Name ELAP Method Number
Barium, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 2 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Barium, Total 4311 PREP EPA 3052
Cadmium, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Calcium, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Chromium, Total 7000 FAAS EPA 7000B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 3 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Chromium, Total 7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Copper, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 4 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Iron, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Lead, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4073 PREP ASTM E-1979-17
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 5 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Lead, Total 4311 PREP EPA 3052
Nickel, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Magnesium, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Manganese, Total 7000 FAAS EPA 7000B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 6 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Manganese, Total 7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Potassium, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Silver, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 7 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Silver, Total 4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Sodium, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Strontium, Total 7000 FAAS EPA 7000B
4035 FAAS EPA 7780A
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 8 of 132Solid and Hazardous Waste 180.3
Metals I
Analyte Technology Method Name ELAP Method Number
Strontium, Total 4087 PREP EPA 3051A
4311 PREP EPA 3052
Metals II
Analyte Technology Method Name ELAP Method Number
Aluminum, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Antimony, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4083 HGAAS EPA 7062
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 9 of 132Solid and Hazardous Waste 180.3
Metals II
Analyte Technology Method Name ELAP Method Number
Antimony, Total 4087 PREP EPA 3051A
4311 PREP EPA 3052
Arsenic, Total 4312 ASV EPA 7063
7010 GFAAS EPA 7010
4021 GFAAS EPA 7060A
4022 HGAAS EPA 7061A
4083 HGAAS EPA 7062
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Beryllium, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 10 of 132Solid and Hazardous Waste 180.3
Metals II
Analyte Technology Method Name ELAP Method Number
Beryllium, Total 4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Chromium VI 4068 COLOR EPA 7196A
4067 DPP EPA 7198
4028 FAAS EPA 7195
4029 FAAS EPA 7197
4313 IC EPA 7199
4318 PREP EPA 3060A
Lithium, Total 4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
Mercury, Total 4314 ASV EPA 7472
4040 CVAAS EPA 7471B
7473 CVAAS EPA 7473
7474 CVAFS EPA 7474
4087 PREP EPA 3051A
Selenium, Total 7010 GFAAS EPA 7010
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 11 of 132Solid and Hazardous Waste 180.3
Metals II
Analyte Technology Method Name ELAP Method Number
Selenium, Total 4034 HGAAS EPA 7741A
4085 HGAAS EPA 7742
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Vanadium, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4017 PREP EPA 3040A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 12 of 132Solid and Hazardous Waste 180.3
Metals II
Analyte Technology Method Name ELAP Method Number
Vanadium, Total 4311 PREP EPA 3052
Zinc, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4317 PREP EPA 3031
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Metals III
Analyte Technology Method Name ELAP Method Number
Cobalt, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4018 PREP EPA 3050B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 13 of 132Solid and Hazardous Waste 180.3
Metals III
Analyte Technology Method Name ELAP Method Number
Cobalt, Total 4087 PREP EPA 3051A
4311 PREP EPA 3052
Molybdenum, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Thallium, Total 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4317 PREP EPA 3031
4018 PREP EPA 3050B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 14 of 132Solid and Hazardous Waste 180.3
Metals III
Analyte Technology Method Name ELAP Method Number
Thallium, Total 4087 PREP EPA 3051A
4311 PREP EPA 3052
Tin, Total 7000 FAAS EPA 7000B
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
Titanium, Total 4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4066 PREP EPA 3020A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
Silica, Dissolved 4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 15 of 132Solid and Hazardous Waste 180.3
Acrylates
Analyte Technology Method Name ELAP Method Number
Acrolein (Propenal) 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4093 HPLC-UV EPA 8316
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Acrylonitrile 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4093 HPLC-UV EPA 8316
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Ethyl methacrylate 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Methyl acrylonitrile 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Methyl methacrylate 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Chlorinated Hydrocarbons
Analyte Technology Method Name ELAP Method Number
1-Chloronaphthalene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8275 GC-MS EPA 8275A
2-Chloronaphthalene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 16 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbons
Analyte Technology Method Name ELAP Method Number
2-Chloronaphthalene 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Hexachlorobenzene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Hexachlorobutadiene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Hexachlorocyclopentadiene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 17 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Hexachlorocyclopentadiene 4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Hexachloroethane 4097 GC-ECD EPA 8121
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Hexachlorophene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Hexachloropropene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Pentachlorobenzene 4097 GC-ECD EPA 8121
4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4086 PREP EPA 3545A
4077 PREP EPA 3546
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 18 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbons
Analyte Technology Method Name ELAP Method Number
1,2,3-Trichlorobenzene 4097 GC-ECD EPA 8121
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2,4-Trichlorobenzene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
1,3,5-Trichlorobenzene 4097 GC-ECD EPA 8121
1,2,4,5-Tetrachlorobenzene 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Haloethers
Analyte Technology Method Name ELAP Method Number
Bis(2-chloroethyl)ether 8111 GC-ECD EPA 8111
8410 GC-FTIR EPA 8410
8430 GC-FTIR EPA 8430
5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 19 of 132Solid and Hazardous Waste 180.3
Haloethers
Analyte Technology Method Name ELAP Method Number
Bis(2-chloroethyl)ether 5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Bis(2-chloroethoxy)methane 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,2'-Oxybis(1-chloropropane) 4097 GC-ECD EPA 8121
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
4-Bromophenylphenyl ether 8111 GC-ECD EPA 8111
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 20 of 132Solid and Hazardous Waste 180.3
Haloethers
Analyte Technology Method Name ELAP Method Number
4-Bromophenylphenyl ether 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8275 GC-MS EPA 8275A
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
4-Chlorophenylphenyl ether 8111 GC-ECD EPA 8111
8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Chloromethylmethyl ether 4095 GCELCD/PID EPA 8021B
Nitroaromatics and Isophorone
Analyte Technology Method Name ELAP Method Number
2-Amino-4,6-dinitrotoluene 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
4-Amino-2,6-dinitrotoluene 8331 HPLC-UV EPA 8330A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 21 of 132Solid and Hazardous Waste 180.3
Nitroaromatics and Isophorone
Analyte Technology Method Name ELAP Method Number
4-Amino-2,6-dinitrotoluene 8332 HPLC-UV EPA 8330B
3-Chloromethyl pyridine-HCl 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4-Dimethylaminoazobenzene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2,4-Dinitrotoluene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,6-Dinitrotoluene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 22 of 132Solid and Hazardous Waste 180.3
Nitroaromatics and Isophorone
Analyte Technology Method Name ELAP Method Number
2,6-Dinitrotoluene 3580 PREP EPA 3580A
3,5-Dinitroaniline 8332 HPLC-UV EPA 8330B
1,2-Dinitrobenzene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
1,3-Dinitrobenzene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
1,4-Dinitrobenzene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
Hexahydro-1,3,5-trinitro-1,3,5-triazine 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
Hydroquinone 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Isophorone 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Methyl-2,4,6-trinitrophenylnitramine 8331 HPLC-UV EPA 8330A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 23 of 132Solid and Hazardous Waste 180.3
Nitroaromatics and Isophorone
Analyte Technology Method Name ELAP Method Number
Methyl-2,4,6-trinitrophenylnitramine 8332 HPLC-UV EPA 8330B
1,4-Naphthoquinone 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
4-Nitroquinoline-1-oxide 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2-Nitrotoluene 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
3-Nitrotoluene 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
4-Nitrotoluene 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
Nitrobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
1061 PREP EPA 5035A-H
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 24 of 132Solid and Hazardous Waste 180.3
Nitroaromatics and Isophorone
Analyte Technology Method Name ELAP Method Number
Nitrobenzene 1060 PREP EPA 5035A-L
Nitroglycerine 8332 HPLC-UV EPA 8330B
Octahydro-tetranitro-tetrazocine 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
Pentaerythritol tetranitrate 8332 HPLC-UV EPA 8330B
Pyridine 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
1,3,5-Trinitrobenzene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
2,4,6-Trinitrotoluene 8331 HPLC-UV EPA 8330A
8332 HPLC-UV EPA 8330B
2,4,6-Trichloronitrobenzene 4047 GC-NPD EPA 8091
Phthalate Esters
Analyte Technology Method Name ELAP Method Number
Benzyl butyl phthalate 4096 GC-ECD EPA 8061A
4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 25 of 132Solid and Hazardous Waste 180.3
Phthalate Esters
Analyte Technology Method Name ELAP Method Number
Benzyl butyl phthalate 5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Bis(2-ethylhexyl) phthalate 4096 GC-ECD EPA 8061A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Diethyl phthalate 4096 GC-ECD EPA 8061A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Dimethyl phthalate 4096 GC-ECD EPA 8061A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 26 of 132Solid and Hazardous Waste 180.3
Phthalate Esters
Analyte Technology Method Name ELAP Method Number
Dimethyl phthalate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Di-n-butyl phthalate 4096 GC-ECD EPA 8061A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Di-n-octyl phthalate 4096 GC-ECD EPA 8061A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 27 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
Aroclor 1016 (PCB-1016) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1221 (PCB-1221) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1232 (PCB-1232) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 28 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
Aroclor 1232 (PCB-1232) 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1242 (PCB-1242) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1248 (PCB-1248) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1254 (PCB-1254) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 29 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
Aroclor 1254 (PCB-1254) 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1260 (PCB-1260) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3570 PREP EPA 3570
Aroclor 1262 (PCB-1262) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
Aroclor 1268 (PCB-1268) 2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
Aroclor 1016 (PCB-1016) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 30 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
Aroclor 1016 (PCB-1016) in Oil 3580 PREP EPA 3580A
Aroclor 1221 (PCB-1221) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
Aroclor 1232 (PCB-1232) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
Aroclor 1242 (PCB-1242) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
Aroclor 1248 (PCB-1248) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
Aroclor 1254 (PCB-1254) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 31 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
Aroclor 1260 (PCB-1260) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
3580 PREP EPA 3580A
Aroclor 1262 (PCB-1262) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
Aroclor 1268 (PCB-1268) in Oil 1209 GC-ECD ASTM D4059-91,00, e05
2167 GC-ECD ASTM D6160-98
4308 GC-ECD EPA 8082A
1035 GC-ECD EPA-600/4-81-045
PCB 1 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 2 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 3 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 4 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 32 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 4 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 5 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 6 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 7 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 8 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 9 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 10 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 33 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 10 1670 GC-HRMS EPA 1668C
PCB 11 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 12 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 13 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 14 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 15 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 16 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 17 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 34 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 17 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 18 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 19 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 20 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 21 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 22 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 23 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 35 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 23 1670 GC-HRMS EPA 1668C
PCB 24 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 25 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 26 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 27 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 28 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 29 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 30 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 36 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 30 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 31 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 32 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 33 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 34 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 35 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 36 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 37 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 36 1670 GC-HRMS EPA 1668C
PCB 37 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 38 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 39 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 40 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 41 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 42 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 43 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 38 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 43 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 44 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 45 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 46 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 47 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 48 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 49 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 39 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 49 1670 GC-HRMS EPA 1668C
PCB 50 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 51 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 52 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 53 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 54 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 55 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 56 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 40 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 56 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 57 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 58 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 59 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 60 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 61 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 62 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 41 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 62 1670 GC-HRMS EPA 1668C
PCB 63 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 64 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 65 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 66 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 67 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 68 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 69 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 42 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 69 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 70 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 71 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 72 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 73 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 74 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 75 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 43 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 75 1670 GC-HRMS EPA 1668C
PCB 76 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 77 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 78 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 79 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 80 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 81 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 82 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 44 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 82 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 83 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 84 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 85 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 86 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 87 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 88 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 45 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 88 1670 GC-HRMS EPA 1668C
PCB 89 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 90 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 91 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 92 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 93 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 94 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 95 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 46 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 95 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 96 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 97 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 98 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 99 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 100 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 101 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 47 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 101 1670 GC-HRMS EPA 1668C
PCB 102 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 103 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 104 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 105 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 106 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 107 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 108 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 48 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 108 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 109 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 110 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 111 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 112 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 113 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 114 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 49 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 114 1670 GC-HRMS EPA 1668C
PCB 115 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 116 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 117 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 118 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 119 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 120 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 121 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 50 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 121 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 122 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 123 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 124 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 125 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 126 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 127 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 51 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 127 1670 GC-HRMS EPA 1668C
PCB 128 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 129 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 130 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 131 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 132 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 133 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 134 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 52 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 134 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 135 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 136 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 137 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 138 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 139 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 140 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 53 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 140 1670 GC-HRMS EPA 1668C
PCB 141 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 142 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 143 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 144 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 145 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 146 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 147 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 54 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 147 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 148 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 149 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 150 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 151 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 152 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 153 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 55 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 153 1670 GC-HRMS EPA 1668C
PCB 154 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 155 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 156 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 157 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 158 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 159 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 160 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 56 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 160 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 161 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 162 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 163 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 164 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 165 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 166 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 57 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 166 1670 GC-HRMS EPA 1668C
PCB 167 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 168 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 169 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 170 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 171 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 172 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 173 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 58 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 173 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 174 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 175 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 176 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 177 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 178 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 179 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 59 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 179 1670 GC-HRMS EPA 1668C
PCB 180 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 181 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 182 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 183 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 184 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 185 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 186 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 60 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 186 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 187 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 188 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 189 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 190 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 191 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 192 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 61 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 192 1670 GC-HRMS EPA 1668C
PCB 193 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 194 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 195 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 196 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 197 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 198 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 199 4308 GC-ECD EPA 8082A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 62 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 199 1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 200 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 201 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 202 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 203 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 204 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 205 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 63 of 132Solid and Hazardous Waste 180.3
Polychlorinated Biphenyls
Analyte Technology Method Name ELAP Method Number
PCB 205 1670 GC-HRMS EPA 1668C
PCB 206 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 207 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 208 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB 209 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
PCB Congeners, Total 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
2-Acetylaminofluorene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Acenaphthene 1019 GC-FID EPA 8100
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 64 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Acenaphthene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Anthracene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Acenaphthylene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 65 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Acenaphthylene 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Benzo(a)anthracene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Benzo(a)pyrene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 66 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Benzo(a)pyrene 3570 PREP EPA 3570
3580 PREP EPA 3580A
Benzo(b)fluoranthene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Benzo(g,h,i)perylene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Benzo(k)fluoranthene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 67 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Benzo(k)fluoranthene 5064 GC-MS EPA 8270E
8275 GC-MS EPA 8275A
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Chrysene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Dibenzo(a,j)acridine 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Dibenzo(a,h)acridine 1019 GC-FID EPA 8100
Dibenzo(a,h)anthracene 1019 GC-FID EPA 8100
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 68 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Dibenzo(a,h)anthracene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Dibenzo(a,e)pyrene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
7,12-Dimethylbenzyl (a) anthracene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Fluoranthene 4049 GC-ECD EPA 8081B
1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 69 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Fluoranthene 3580 PREP EPA 3580A
Fluorene 4049 GC-ECD EPA 8081B
1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Indeno(1,2,3-cd)pyrene 4049 GC-ECD EPA 8081B
1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
3-Methylcholanthrene 1019 GC-FID EPA 8100
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 70 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
3-Methylcholanthrene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Naphthalene 4049 GC-ECD EPA 8081B
1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
4303 PREP EPA 3585
Phenanthrene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 71 of 132Solid and Hazardous Waste 180.3
Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Pyrene 1019 GC-FID EPA 8100
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4300 PREP EPA 3561
3570 PREP EPA 3570
3580 PREP EPA 3580A
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Acenaphthylene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Acenaphthene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 72 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Acenaphthene Low Level 5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Anthracene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Benzo(a)anthracene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 73 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Benzo(a)anthracene Low Level 4300 PREP EPA 3561
Benzo(b)fluoranthene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Benzo(k)fluoranthene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Benzo(g,h,i)perylene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 74 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Benzo(g,h,i)perylene Low Level 4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Benzo(a)pyrene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Chrysene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Dibenzo(a,h)anthracene Low Level 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 75 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Dibenzo(a,h)anthracene Low Level 5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Fluoranthene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Fluorene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 76 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Fluorene Low Level 4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Indeno(1,2,3-cd)pyrene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Naphthalene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Phenanthrene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 77 of 132Solid and Hazardous Waste 180.3
Low Level Polynuclear Aromatic Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Phenanthrene Low Level 5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Pyrene Low Level 5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
4060 HPLC-FLUOR EPA 8310
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4300 PREP EPA 3561
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
4-Chloro-3-methylphenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 78 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
4-Chloro-3-methylphenol 4051 PREP EPA 3550C
3580 PREP EPA 3580A
2-Chlorophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,4-Dichlorophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,6-Dichlorophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2,4-Dimethylphenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 79 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
2,4-Dimethylphenol 4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,4-Dinitrophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2-Methylphenol 4045 GC-FID EPA 8041A
8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
3-Methylphenol 4045 GC-FID EPA 8041A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 80 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
3-Methylphenol 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4-Methylphenol 4045 GC-FID EPA 8041A
8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2-Methyl-4,6-dinitrophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2-Nitrophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 81 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
2-Nitrophenol 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
4-Nitrophenol 4100 GC-ECD EPA 8151A
4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Pentachlorophenol 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Phenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 82 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
Phenol 4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,3,4,6 Tetrachlorophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2,4,6-Trichlorophenol 4045 GC-FID EPA 8041A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
2,4,5-Trichlorophenol 4100 GC-ECD EPA 8151A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 83 of 132Solid and Hazardous Waste 180.3
Priority Pollutant Phenols
Analyte Technology Method Name ELAP Method Number
Thiophenol 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
1,2,4-Trichlorobenzene, Volatile 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3580 PREP EPA 3580A
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Benzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
n-Butylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
sec-Butylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 84 of 132Solid and Hazardous Waste 180.3
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
sec-Butylbenzene 4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
tert-Butylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Bromobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Chlorobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
2-Chlorotoluene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 85 of 132Solid and Hazardous Waste 180.3
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
4-Chlorotoluene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1,2-Dichlorobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3580 PREP EPA 3580A
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,3-Dichlorobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3580 PREP EPA 3580A
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,4-Dichlorobenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3580 PREP EPA 3580A
4303 PREP EPA 3585
4301 PREP EPA 5021A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 86 of 132Solid and Hazardous Waste 180.3
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
1,4-Dichlorobenzene 1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Ethyl benzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Isopropylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
p-Isopropyltoluene (P-Cymene) 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Naphthalene, Volatile 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 87 of 132Solid and Hazardous Waste 180.3
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
Naphthalene, Volatile 1060 PREP EPA 5035A-L
n-Propylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Toluene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Total Xylenes 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
m/p-Xylenes 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 88 of 132Solid and Hazardous Waste 180.3
Volatile Aromatics
Analyte Technology Method Name ELAP Method Number
m/p-Xylenes 1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
o-Xylene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2,4-Trimethylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1,3,5-Trimethylbenzene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
Styrene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3570 PREP EPA 3570
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 89 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
Bromoacetone 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
Bromochloromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Bromodichloromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Bromoform 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Bromomethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 90 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
Bromomethane 4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Carbon tetrachloride 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Chloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
2-Chloro-1,3-butadiene (Chloroprene) 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
2-Chloroethylvinyl ether 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 91 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
2-Chloroethylvinyl ether 4095 GCELCD/PID EPA 8021B
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Chloroform 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Chloromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
cis-1,4-Dichloro-2-butene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
trans-1,4-Dichloro-2-butene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2-Dibromo-3-chloropropane 4089 GC-MS EPA 8260C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 92 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
1,2-Dibromo-3-chloropropane 4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3580 PREP EPA 3580A
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2-Dibromoethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,3-Dichloro-2-propanol 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
3-Chloropropene (Allyl chloride) 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
cis-1,3-Dichloropropene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 93 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
trans-1,3-Dichloropropene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Dibromochloromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Dibromomethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Dichlorodifluoromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 94 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
Dichlorodifluoromethane 1060 PREP EPA 5035A-L
1,1-Dichloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2-Dichloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,1-Dichloroethene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
cis-1,2-Dichloroethene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 95 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
cis-1,2-Dichloroethene 4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
trans-1,2-Dichloroethene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,1-Dichloropropene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2-Dichloropropane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,3-Dichloropropane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 96 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
1,3-Dichloropropane 4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
2,2-Dichloropropane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Hexachlorobutadiene, Volatile 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Methylene chloride 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Methyl iodide 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
1,1,1,2-Tetrachloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 97 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
1,1,1,2-Tetrachloroethane 4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,1,2,2-Tetrachloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Tetrachloroethene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,1,1-Trichloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 98 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
1,1,2-Trichloroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Trichloroethene 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Trichlorofluoromethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,2,3-Trichloropropane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 99 of 132Solid and Hazardous Waste 180.3
Volatile Halocarbons
Analyte Technology Method Name ELAP Method Number
1,2,3-Trichloropropane 1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
1,1,2-Trichloro-1,2,2-Trifluoroethane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Vinyl chloride 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Aldrin 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Atrazine 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
alpha-BHC 4049 GC-ECD EPA 8081B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 100 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
alpha-BHC 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
beta-BHC 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
delta-BHC 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 101 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Lindane 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
alpha-Chlordane 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
gamma-Chlordane 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
Chlordane Total 4049 GC-ECD EPA 8081B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 102 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Chlordane Total 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Chlorobenzilate 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2,4'-DDD (Mitotane) 4049 GC-ECD EPA 8081B
4,4'-DDD 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
4,4'-DDE 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 103 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
4,4'-DDE 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
4,4'-DDT 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Diallate 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Dieldrin 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Endosulfan I 4049 GC-ECD EPA 8081B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 104 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Endosulfan I 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Endosulfan II 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Endosulfan sulfate 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 105 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Endrin 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Endrin aldehyde 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Endrin Ketone 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 106 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Endrin Ketone 3580 PREP EPA 3580A
Heptachlor 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Heptachlor epoxide 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Isodrin 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Mirex 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Methoxychlor 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 107 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Methoxychlor 5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Toxaphene 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Kepone 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Pentachloronitrobenzene 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4047 GC-NPD EPA 8091
Trifluralin 4049 GC-ECD EPA 8081B
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 108 of 132Solid and Hazardous Waste 180.3
Chlorinated Hydrocarbon Pesticides
Analyte Technology Method Name ELAP Method Number
Trifluralin 4047 GC-NPD EPA 8091
Simazine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Chlorophenoxy Acid Pesticides
Analyte Technology Method Name ELAP Method Number
2,4-DB 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
2,4-D 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
2,4,5-T 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
2,4,5-TP (Silvex) 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
Dicamba 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 109 of 132Solid and Hazardous Waste 180.3
Chlorophenoxy Acid Pesticides
Analyte Technology Method Name ELAP Method Number
Dichloroprop 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
Dinoseb 4100 GC-ECD EPA 8151A
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8322 HPLC-TSMS EPA 8321B
4086 PREP EPA 3545A
4077 PREP EPA 3546
3580 PREP EPA 3580A
Dalapon 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
MCPA 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
MCPP 4100 GC-ECD EPA 8151A
8322 HPLC-TSMS EPA 8321B
Pentachlorophenol 4100 GC-ECD EPA 8151A
4077 PREP EPA 3546
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
Azinphos ethyl 4098 GC-NPD EPA 8141B
Azinphos methyl 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Bolstar 4098 GC-NPD EPA 8141B
Carbophenothion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 110 of 132Solid and Hazardous Waste 180.3
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
Carbophenothion 4098 GC-NPD EPA 8141B
Coumaphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Chlorpyriphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Chlorpyriphos methyl 4098 GC-NPD EPA 8141B
Chlorphenvinphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Crotoxyphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Cyanizine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Demeton-O 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Demeton-S 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Diazinon 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Dichlorfenthion 4098 GC-NPD EPA 8141B
Dichlorvos 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 111 of 132Solid and Hazardous Waste 180.3
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
Dichlorvos 5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Dicrotophos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Dimethoate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Dioxathion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Disulfoton 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
Ethion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Ethoprop 4098 GC-NPD EPA 8141B
EPN 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Famphur 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 112 of 132Solid and Hazardous Waste 180.3
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
Famphur 5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Fenitrothion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Fensulfothion 4098 GC-NPD EPA 8141B
Fenthion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Fonophos 4098 GC-NPD EPA 8141B
Isophenphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Malathion 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Mevinphos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Monocrotophos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
NALED 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Parathion ethyl 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 113 of 132Solid and Hazardous Waste 180.3
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
Parathion ethyl 5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Parathion methyl 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Pendimethalin 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Phorate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Phosphamidon 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Prometon 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Prometryn 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Ronnel 4098 GC-NPD EPA 8141B
Sulfotepp 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
TEPP 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 114 of 132Solid and Hazardous Waste 180.3
Organophosphate Pesticides
Analyte Technology Method Name ELAP Method Number
TEPP 4098 GC-NPD EPA 8141B
Terbufos 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Thionazin 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Tokuthion 4098 GC-NPD EPA 8141B
Trichlorfon 4098 GC-NPD EPA 8141B
Trichloronate 4098 GC-NPD EPA 8141B
Volatile Chlorinated Organics
Analyte Technology Method Name ELAP Method Number
Benzyl chloride 4308 GC-ECD EPA 8082A
4097 GC-ECD EPA 8121
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Epichlorohydrin 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
Miscellaneous
Analyte Technology Method Name ELAP Method Number
Asbestos in Friable Material 4008 PLM EPA 600/M4/82/020
1981 PLM Item 198.1 of Manual
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 115 of 132Solid and Hazardous Waste 180.3
Miscellaneous
Analyte Technology Method Name ELAP Method Number
Asbestos in Non-Friable Material-TEM 4070 TEM Item 198.4 of Manual
Asbestos in Non-Friable Material-PLM 1986 PLM Item 198.6 of Manual (NOB by PLM)
Asbestos-Vermiculite-Containing Materials 4601 PLM Item 198.8 of Manual
Boron, Total 4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
4016 PREP EPA 3005A
4015 PREP EPA 3010A
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Cyanide, Total 9380 AUTO EPA 9012B
4014 COLOR EPA 9014
9379 PREP EPA 9010C
Cyanide, Free 9377 COLOR EPA 9016
Formaldehyde 8316 HPLC-UV EPA 8315A
Lead in Paint 9500 FAAS ASTM D3335-85A
7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
2583 ICP-AES SM 21-23 3120B (-99)
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
1059 PREP AOAC 974.02
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 116 of 132Solid and Hazardous Waste 180.3
Miscellaneous
Analyte Technology Method Name ELAP Method Number
Lead in Paint 9502 PREP ASTM D3335-85A
4073 PREP ASTM E-1979-17
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Lead in Dust Wipes 7000 FAAS EPA 7000B
7010 GFAAS EPA 7010
4078 ICP-AES EPA 6010C
4080 ICP-AES EPA 6010D
9508 ICP-AES NIOSH 9100
4081 ICP-MS EPA 6020A
4088 ICP-MS EPA 6020B
9910 PREP ASTM E-1644-17
4073 PREP ASTM E-1979-17
4018 PREP EPA 3050B
4087 PREP EPA 3051A
4311 PREP EPA 3052
Organic Carbon, Total 9961 IR EPA 9060A
1210 IR Lloyd Kahn Method
Perchlorate 1183 HPLC-ESMS EPA 6850
6860 IC-ESI-MS EPA 6860
Phenols 9965 COLOR EPA 9065
9966 COLOR EPA 9066
9967 COLOR EPA 9067
Specific Conductance 9378 COND EPA 9050A
Sulfide (as S) 4010 PREP EPA 9030B
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 117 of 132Solid and Hazardous Waste 180.3
Miscellaneous
Analyte Technology Method Name ELAP Method Number
Sulfide (as S) 4011 TITR EPA 9031
4316 TITR EPA 9034
Extractable Organic Halides 9923 COUL EPA 9023
Total Organic Halides 9025 COUL EPA 9020B
9026 NAA EPA 9022
Critical Agents
Analyte Technology Method Name ELAP Method Number
B. Anthracis, Swabs and Swipes 9900 99 NYSDOH Approved Method
B. Anthracis, Powders, Fluids, Bulk Mat. 9900 99 NYSDOH Approved Method
Botulinum Neurotoxin 9900 99 NYSDOH Approved Method
Brucella 9900 99 NYSDOH Approved Method
Burkholderia mallei 9900 99 NYSDOH Approved Method
Burkholderia pseudomallei 9900 99 NYSDOH Approved Method
F. tularensis 9900 99 NYSDOH Approved Method
Orthopox 9900 99 NYSDOH Approved Method
Ricin Toxin 9900 99 NYSDOH Approved Method
Y. pestis 9900 99 NYSDOH Approved Method
Benzidines
Analyte Technology Method Name ELAP Method Number
Benzidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8325 HPLC-PBMS EPA 8325
3,3'-Dichlorobenzidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8325 HPLC-PBMS EPA 8325
3,3'-Dimethylbenzidine 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 118 of 132Solid and Hazardous Waste 180.3
Benzidines
Analyte Technology Method Name ELAP Method Number
3,3'-Dimethylbenzidine 5064 GC-MS EPA 8270E
8325 HPLC-PBMS EPA 8325
Volatile Organics
Analyte Technology Method Name ELAP Method Number
Acetone 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
8316 HPLC-UV EPA 8315A
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Acetonitrile 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
8033 GC-NPD EPA 8033
Carbon Disulfide 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Cyclohexane 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Di-ethyl ether 4089 GC-MS EPA 8260C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 119 of 132Solid and Hazardous Waste 180.3
Volatile Organics
Analyte Technology Method Name ELAP Method Number
Di-ethyl ether 4074 GC-MS EPA 8260D
1,4-Dioxane 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4101 GC-MS EPA 8260C SIM
4074 GC-MS EPA 8260D
4102 GC-MS EPA 8260D SIM
5058 GC-MS EPA 8270D
5059 GC-MS EPA 8270D SIM
5064 GC-MS EPA 8270E
5065 GC-MS EPA 8270E SIM
Ethyl Acetate 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Ethylene Glycol 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Isobutyl alcohol 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Isopropanol 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
2-Hexanone 4089 GC-MS EPA 8260C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 120 of 132Solid and Hazardous Waste 180.3
Volatile Organics
Analyte Technology Method Name ELAP Method Number
2-Hexanone 4074 GC-MS EPA 8260D
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
2-Butanone (Methylethyl ketone) 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Methyl acetate 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Methyl cyclohexane 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Methyl tert-butyl ether 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4095 GCELCD/PID EPA 8021B
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 121 of 132Solid and Hazardous Waste 180.3
Volatile Organics
Analyte Technology Method Name ELAP Method Number
Methyl tert-butyl ether 1060 PREP EPA 5035A-L
4-Methyl-2-Pentanone 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
4303 PREP EPA 3585
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
n-Butanol 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
2-Nitropropane 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Propionitrile 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
o-Toluidine 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
tert-butyl alcohol 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
Tetrahydrofuran 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 122 of 132Solid and Hazardous Waste 180.3
Volatile Organics
Analyte Technology Method Name ELAP Method Number
Vinyl acetate 4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Semi-Volatile Organics
Analyte Technology Method Name ELAP Method Number
Acetophenone 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4-Amino biphenyl 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Aramite 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Benzoic Acid 4308 GC-ECD EPA 8082A
8410 GC-FTIR EPA 8410
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Benzyl alcohol 4308 GC-ECD EPA 8082A
1668 GC-HRMS EPA 1668A
1669 GC-HRMS EPA 1668B
1670 GC-HRMS EPA 1668C
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Benzaldehyde 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 123 of 132Solid and Hazardous Waste 180.3
Semi-Volatile Organics
Analyte Technology Method Name ELAP Method Number
Benzaldehyde 5064 GC-MS EPA 8270E
8316 HPLC-UV EPA 8315A
1,1'-Biphenyl 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Caprolactam 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
1,2-Dichlorobenzene, Semi-volatile 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
1,3-Dichlorobenzene, Semi-volatile 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
1,4-Dichlorobenzene, Semi-volatile 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
4319 PREP EPA 3541
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 124 of 132Solid and Hazardous Waste 180.3
Semi-Volatile Organics
Analyte Technology Method Name ELAP Method Number
1,4-Dichlorobenzene, Semi-volatile 4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Dibenzofuran 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8275 GC-MS EPA 8275A
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Diethyl sulfate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Dihydrosafrole 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Ethyl methanesulfonate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Isosafrole 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2-Methylnaphthalene 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4056 PREP EPA 3540C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 125 of 132Solid and Hazardous Waste 180.3
Semi-Volatile Organics
Analyte Technology Method Name ELAP Method Number
2-Methylnaphthalene 4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
Methyl methanesulfonate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Phenacetin 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2-Picoline 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Piperonyl sulfoxide 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Resorcinol 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Safrole 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4098 GC-NPD EPA 8141B
Toluene Diisocyanate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
O,O,O-Triethyl phosphorothioate 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Amines
Analyte Technology Method Name ELAP Method Number
Aniline 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 126 of 132Solid and Hazardous Waste 180.3
Amines
Analyte Technology Method Name ELAP Method Number
Aniline 8131 GC-NPD EPA 8131
o-Anisidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Carbazole 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2-Chloroaniline 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8131 GC-NPD EPA 8131
4-Chloroaniline 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8131 GC-NPD EPA 8131
4-Chloro-1,2-phenylenediamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4-Chloro-1,3-phenylenediamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
5-Chloro-2-methylaniline 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
a,a-Dimethylphenethylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Diphenylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
1-Naphthylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
2-Naphthylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 127 of 132Solid and Hazardous Waste 180.3
Amines
Analyte Technology Method Name ELAP Method Number
2-Nitroaniline 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8131 GC-NPD EPA 8131
3-Nitroaniline 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8131 GC-NPD EPA 8131
4-Nitroaniline 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8131 GC-NPD EPA 8131
5-Nitro-o-toluidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Methapyrilene 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4,4'-Methylenebis(2-chloroaniline) 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
4,4'-Oxydianiline 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
1,4-Phenylenediamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
1,2-Diphenylhydrazine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Pronamide 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 128 of 132Solid and Hazardous Waste 180.3
Carbamate Pesticides
Analyte Technology Method Name ELAP Method Number
Aldicarb Sulfoxide 8322 HPLC-TSMS EPA 8321B
Aldicarb 8318 HPLC-FLUOR EPA 8318A
8322 HPLC-TSMS EPA 8321B
Aldicarb Sulfone 8318 HPLC-FLUOR EPA 8318A
8322 HPLC-TSMS EPA 8321B
Carbofuran 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8318 HPLC-FLUOR EPA 8318A
8322 HPLC-TSMS EPA 8321B
Nitrosoamines
Analyte Technology Method Name ELAP Method Number
N-Nitrosodiphenylamine 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8070 GC-NPD EPA 8070A
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
N-Nitrosodimethylamine 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8070 GC-NPD EPA 8070A
4056 PREP EPA 3540C
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 129 of 132Solid and Hazardous Waste 180.3
Nitrosoamines
Analyte Technology Method Name ELAP Method Number
N-Nitrosodimethylamine 4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
N-Nitrosodiethylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
N-nitrosomethylethylamine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
N-Nitrosodi-n-butylamine 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4089 GC-MS EPA 8260C
4074 GC-MS EPA 8260D
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
N-Nitrosodi-n-propylamine 8410 GC-FTIR EPA 8410
5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
8070 GC-NPD EPA 8070A
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
3580 PREP EPA 3580A
N-nitrosomorpholine 5058 GC-MS EPA 8270D
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 130 of 132Solid and Hazardous Waste 180.3
Nitrosoamines
Analyte Technology Method Name ELAP Method Number
N-nitrosomorpholine 5064 GC-MS EPA 8270E
N-nitrosopiperidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
N-Nitrosopyrrolidine 5058 GC-MS EPA 8270D
5064 GC-MS EPA 8270E
Minerals
Analyte Technology Method Name ELAP Method Number
Bromide 9956 IC-COND EPA 9056A
9211 POT EPA 9211
Chloride 9250 COLOR EPA 9250
9251 COLOR EPA 9251
9956 IC-COND EPA 9056A
9957 IC-COND EPA 9057
9212 POT EPA 9212
9252 TITR EPA 9253
Fluoride, Total 9956 IC-COND EPA 9056A
9214 POT EPA 9214
Sulfate (as SO4) 9935 COLOR EPA 9035
9936 COLOR EPA 9036
9938 COLOR EPA 9038
9956 IC-COND EPA 9056A
Nutrients
Analyte Technology Method Name ELAP Method Number
Nitrate (as N) 9956 IC-COND EPA 9056A
9215 POT EPA 9210A
Nitrite (as N) 9956 IC-COND EPA 9056A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 131 of 132Solid and Hazardous Waste 180.3
Nutrients
Analyte Technology Method Name ELAP Method Number
Orthophosphate (as P) 9956 IC-COND EPA 9056A
Petroleum Hydrocarbons
Analyte Technology Method Name ELAP Method Number
Diesel Range Organics 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4056 PREP EPA 3540C
4319 PREP EPA 3541
4086 PREP EPA 3545A
4077 PREP EPA 3546
4051 PREP EPA 3550C
4301 PREP EPA 5021A
Gasoline Range Organics 9996 GC-FID EPA 8015C
9992 GC-FID EPA 8015D
4301 PREP EPA 5021A
1061 PREP EPA 5035A-H
1060 PREP EPA 5035A-L
Oil and Grease Total Recoverable (HEM) 9972 GRAV EPA 9071B (Solvent:Hexane)
Dioxins and Furans
Analyte Technology Method Name ELAP Method Number
2,3,7,8-Tetrachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
2,3,4,7,8-Pentachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,7,8-Pentachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,7,8-Hexachlorodibenzofuran 5084 GC-HRMS EPA 8290A
SUBJECT DATE PAGE Item No.
Approved Methods: 02/10/2021 132 of 132Solid and Hazardous Waste 180.3
Dioxins and Furans
Analyte Technology Method Name ELAP Method Number
1,2,3,4,7,8-Hexachlorodibenzofuran 5085 GC-LRMS EPA 8280B
1,2,3,6,7,8-Hexachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,7,8,9-Hexachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
2,3,4,6,7,8-Hexachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,6,7,8-Heptachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,7,8,9-Heptachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,6,7,8,9-Octachlorodibenzofuran 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
2,3,7,8-Tetrachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,7,8-Pentachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B
1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 5084 GC-HRMS EPA 8290A
5085 GC-LRMS EPA 8280B