certificate of analysis...111920.r02 vav-09-1020 lot# 947.077 121220.r01 6970145500298 190624060...
TRANSCRIPT
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
12/21/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, US
Kaycha Labspinnacle pre roll
N/AMatrix: Flower
Certificateof Analysis
Sample:GA01211003-003Harvest/Lot ID: 1578
Seed to Sale #N/ABatch Date :N/A
Batch#: 12Sample Size Received: 10 gram
Retail Product Size: 1Ordered : 12/04/20Sampled : 12/04/20
Completed: 12/21/20 Expires: 12/21/21Sampling Method: SOP Client Method
Dec 21, 2020 | Pinnacle Hemp2900 Davis BlvdJoplin, MO, 64804, US
TESTEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsTESTED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolvents
NOT TESTED
FilthPASSED
Water ActivityPASSED
MoisturePASSED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
0.144%Total CBD
13.351%Total Cannabinoids
24.151%
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
ND10.613% 0.213% 0.078% 4.042% ND ND ND 8.677% 0.361% 0.164%
ND106.130mg/g
2.130mg/g
0.780mg/g
40.420mg/g ND ND ND
86.770mg/g
3.610mg/g
1.640mg/g
LOD 0.001 0.001 0.001 0.001 0.0001 0.001 0.001 0.0001 0.001 0.001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :508 0.2033g 12/14/20 11:12:14 1791Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 12/15/20 12:46:26 Batch Date : 12/11/20 17:47:25
Analytical Batch -GA019849POTInstrument Used : GA-HPLC-001 2030C Plus(Carl) Running On : 12/14/20 14:52:14
Reagent Dilution Consums. ID
110320.57 40 280630187111920.R02 VAV-09-1020 Lot# 947.077121220.R01 6970145500298
19062406016466-042
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By2206 9.0g 12/14/20 1791Analyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 12/11/20 15:44:23Analytical Batch -GA019846FIL Reviewed On - 12/11/20 16:36:30Instrument Used : GA-Filth/Foreign Material MicroscopeRunning On :
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 2259 3.5199g 12/11/20 0.1 aw 0.65aw 0.374 aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 12/11/20 15:54:25Analytical Batch -GA019848WAT Reviewed On - 12/11/20 17:02:12Instrument Used : GA-085 Rotronic HygroPalmRunning On : 12/11/20 16:30:17
Moisture PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultMOISTURE CONTENT 2206 0.545g 12/11/20 1 % 15% 7.340 %
Analysis Method -MoistureAnalysis SOP.T.40.011 Batch Date : 12/11/20 15:51:26Analytical Batch -GA019847MOI Reviewed On - 12/14/20 07:46:41Instrument Used : GA-084 Moisture AnalyzerRunning On :
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
12/21/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, US
Kaycha Labspinnacle pre roll
N/AMatrix : Flower
Certificate of Analysis TESTEDPinnacle Hemp
2900 Davis BlvdJoplin, MO, 64804, USTelephone: 8334367283Email: [email protected]
Sample : GA01211003-003Harvest/LOT ID: 1578Batch# : 12Sampled : 12/04/20Ordered : 12/04/20
Sample Size Received : 10 gramCompleted : 12/21/20Expires: 12/21/21Sample Method : SOP Client Method
Page 2 of 4
Terpenes TESTEDTerpenes LOD Units Result (%)
ALPHA-HUMULENE 0.007 % 0.068ALPHA-CEDRENE 0.007 % NDSABINENE 0.007 % NDSABINENEHYDRATE
0.007 % ND
TERPINEOL 0.007 % 0.052TERPINOLENE 0.007 % NDBETA-CARYOPHYLLENE
0.007 % 0.178
TRANS-NEROLIDOL 0.007 % NDVALENCENE 0.007 % NDALPHA-BISABOLOL 0.007 % 0.092CARYOPHYLLENEOXIDE
0.007 % 0.024
CAMPHOR 0.013 % NDCAMPHENE 0.007 % NDBORNEOL 0.013 % NDBETA-PINENE 0.007 % NDBETA-MYRCENE 0.007 % 0.046ALPHA-TERPINENE 0.007 % NDALPHA-PINENE 0.007 % NDCEDROL 0.007 % NDPULEGONE 0.007 % NDALPHA-PHELLANDRENE
0.007 % ND
OCIMENE 0.007 % NDNEROL 0.007 % NDLINALOOL 0.007 % NDLIMONENE 0.007 % 0.147GUAIOL 0.007 % 0.119GERANYL ACETATE 0.007 % NDGERANIOL 0.007 % NDGAMMA-TERPINENE
0.007 % ND
FENCHONE 0.007 % NDFARNESENE 0.007 % ND
Terpenes LOD Units Result(%)
EUCALYPTOL 0.007 % ND NDISOBORNEOL 0.007 % ND NDHEXAHYDROTHYMOL
0.007 % ND ND
FENCHYLALCOHOL
0.007 % 0.025 0.025
3-CARENE 0.007 % ND NDCIS-NEROLIDOL
0.007 % ND ND
ISOPULEGOL 0.007 % ND ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By2155 1.0318g 12/14/20 12:12:38 650
Analysis Method -SOP.T.40.090Analytical Batch -GA019861TER Reviewed On - 12/17/20 16:37:57Instrument Used : GA-GCMS-002 QP2010SRunning On : 12/15/20 13:21:26Batch Date : 12/12/20 12:31:10
Reagent Dilution Consums. ID
060920.22 10 280630187VAV-09-1020 Lot# 947.0776970145500298P734631 / P741189516466-042
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total 0.756
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
12/21/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, US
Kaycha Labspinnacle pre roll
N/AMatrix : Flower
Certificate of Analysis TESTEDPinnacle Hemp
2900 Davis BlvdJoplin, MO, 64804, USTelephone: 8334367283Email: [email protected]
Sample : GA01211003-003Harvest/LOT ID: 1578Batch# : 12Sampled : 12/04/20Ordered : 12/04/20
Sample Size Received : 10 gramCompleted : 12/21/20Expires: 12/21/21Sample Method : SOP Client Method
Page 3 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultACEPHATE 0.01 ppm 3 NDABAMECTIN B1A 0.01 ppm 0.3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.1 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 ND
Pesticides LOD Units Action Level ResultPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.01 PPM 20 ND
TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 NDPENTACHLORONITROBENZENE(PCNB) *
0.01 PPM 0.2 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 3 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 1 NDCYPERMETHRIN * 0.01 PPM 1 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By1850 , 1541 0.9936g 12/21/20 09:12:34 1850 , 1541Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.30.065, SOP.T40.070Analytical Batch - GA020091PES ,GA020095VOL
Reviewed On- 12/11/20 16:36:30
Instrument Used : GA-LCMS-001 Pes , GA-GCMS-003 Triple Quad PestRunning On : 12/19/20 14:06:20 , 12/19/2008:44:13Batch Date : 12/17/20 17:03:59
Reagent Dilution Consums. ID120920.R09 10 282066106121120.R10 VAV-09-1020 Lot# 947.077121120.R01 6970145500298
VAV-09-1020 (947.077) / ALK-09-1412 (9291.179)P734631 / P7411895
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations forregulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparation forPesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). * VolatilePesticide screening is performed using GC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
12/21/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, US
Kaycha Labspinnacle pre roll
N/AMatrix : Flower
Certificate of Analysis TESTEDPinnacle Hemp
2900 Davis BlvdJoplin, MO, 64804, USTelephone: 8334367283Email: [email protected]
Sample : GA01211003-003Harvest/LOT ID: 1578Batch# : 12Sampled : 12/04/20Ordered : 12/04/20
Sample Size Received : 10 gramCompleted : 12/21/20Expires: 12/21/21Sample Method : SOP Client Method
Page 4 of 4
Microbials PASSED
Analyte LOD ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043 / SOP.T.40.044Analytical Batch -GA020153MIC Batch Date : 12/18/20Instrument Used : GA-093 PathogenDx Scanner (MIC)Running On :
Analyzed by Weight Extraction date Extracted By1790 0.9450g 12/18/20 2119
Reagent Dilution Consums. ID080120.R01120820.R23
10 001001001001002005
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -GA020092MYC | Reviewed On - 12/21/20 12:59:07Instrument Used : GA-LCMS-001 MYCRunning On : 12/19/20 14:06:29Batch Date : 12/17/20 17:07:33
Analyzed by Weight Extraction date Extracted By1850 0.9936g 12/21/20 09:12:32 1850
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be