certificate of analysis - xpirient · 2020. 8. 10. · 500 batch#: 002160-xfn513 received:...
TRANSCRIPT
Reporting Limit 10 ppm *Total CBD = CBD + CBDA x 0.877 N/D - Not Detected, B/LOQ - Below Limit of Quantification
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
Sample
N/D D9-THC
5.539% Total CBD
525.3 mg Cannabinoids per
unit
523.5 mg CBD per
unit
1 unit = 10 ml per unit x density (0.945) xCannabinoid concentration
Cannabinoids TestSHIMADZU INTEGRATED UPLC-PDAGSL SOP 400 PREPARED: 08/04/2020 17:47:57 UPLOADED: 08/04/2020 12:30:35 Cannabinoids LOQ weight(%) mg/g mg/unitD9-THC 10 PPM N/D N/D N/DTHCA 10 PPM N/D N/D N/DCBD 10 PPM 5.539% 55.393 523.5CBDA 20 PPM N/D N/D N/DCBDV 20 PPM 0.020% 0.195 1.8CBC 10 PPM N/D N/D N/DCBN 10 PPM N/D N/D N/DCBG 10 PPM N/D N/D N/DCBGA 20 PPM N/D N/D N/DD8-THC 10 PPM N/D N/D N/DTHCV 10 PPM N/D N/D N/D
TOTAL D9-THC N/D N/D N/DTOTAL CBD* 5.539% 55.393 523.5TOTAL CANNABINOIDS 5.559% 55.588 525.3
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
TERPENES: TOTAL (0.032%)Headspace GCMS - Shimadzu GCMS QP2020 with HS20
GSL SOP 404 Prepared: 08/03/2020 18:45:50 Uploaded: 08/05/2020 13:09:23
Terpene Results (%) LOQ (%) LOD (%)ALPHA-PINENE B/LOQ 0.0067% 0.0063%BETA-PINENE B/LOQ 0.0067% 0.0063%CARYOPHYLLENE 0.008% 0.0067% 0.0063%EUCALYPTOL 0.013% 0.0067% 0.0063%LIMONENE B/LOQ 0.0067% 0.0063%
Terpenes Breakdown
Top Terpenes Results:
Tested for but not present:
CAMPHENE, BETA-MYRCENE, 3-CARENE, ALPHA-TERPINENE, TRANS-BETA-OCIMENE, P-CYMENE, CIS-BETA-OCIMENE, GAMMA.-TERPINENE, TERPINOLENE, LINALOOL, ISOPULEGOL, GERANIOL,HUMULENE, CIS-NEROLIDOL, TRANS-NEROLIDOL, GUAIOL, CARYOPHYLLENE OXIDE, ALPHA-BISABOLOL
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
PESTICIDE ANALYSIS:GSL SOP 401 PREPARED: 08/03/2020 19:22:31 UPLOADED: 08/05/2020 10:49:44
N/D = Not Detected, A/LOQ = Above LOQ Level, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
GCMS-MS - Shimadzu GCMS-TQ8040
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
CAPTAN 3.000 N/D 0.003 0.001CHLORDANE 0.100 N/D 0.003 0.001CHLORFENAPYR 0.100 N/D 0.003 0.001COUMAPHOS 0.100 N/D 0.003 0.001
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
CYFLUTHRIN 1.000 N/D 0.003 0.001CYPERMETHRIN 1.000 N/D 0.003 0.001PENTACHLORONITROBENZENE 0.200 N/D 0.003 0.001
LCMS-MS - Shimadzu LCMS-8060
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
ABAMECTIN B1A 0.300 N/D 0.005 0.001ACEPHATE 3.000 N/D 0.001 0.001ACEQUINOCYL 2.000 N/D 0.001 0.001ACETAMIPRID 3.000 N/D 0.005 0.001ALDICARB 0.100 N/D 0.005 0.001AZOXYSTROBIN 3.000 N/D 0.001 0.001BIFENAZATE 3.000 N/D 0.005 0.001BIFENTHRIN 0.500 N/D 0.005 0.001BOSCALID 3.000 N/D 0.005 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.001 0.001CHLORANTRANILIPROLE 3.000 N/D 0.005 0.005CHLORMEQUATCHLORIDE
3.000 N/D 0.025 0.025
CHLORPYRIFOS 0.100 N/D 0.001 0.001CLOFENTEZINE 0.500 N/D 0.001 0.001DAMINOZIDE 0.100 N/D 0.005 0.001DIAZINON 0.200 N/D 0.001 0.001DICHLORVOS 0.100 N/D 0.005 0.001DIMETHOATE 0.100 N/D 0.001 0.001DIMETHOMORPH 3.000 N/D 0.005 0.001ETHOPROPHOS 0.100 N/D 0.001 0.001ETOFENPROX 0.100 N/D 0.001 0.001ETOXAZOLE 1.500 N/D 0.010 0.005FENHEXAMID 3.000 N/D 0.005 0.001FENOXYCARB 0.100 N/D 0.005 0.001FENPYROXIMATE 2.000 N/D 0.001 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 2.000 N/D 0.025 0.010FLUDIOXONIL 3.000 N/D 0.003 0.001HEXYTHIAZOX 2.000 N/D 0.005 0.001
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
IMAZALIL 0.100 N/D 0.005 0.001IMIDACLOPRID 3.000 N/D 0.005 0.001KRESOXIM-METHYL 1.000 N/D 0.010 0.005MALATHION 2.000 N/D 0.005 0.001METALAXYL 3.000 N/D 0.001 0.001METHIOCARB 0.100 N/D 0.005 0.001METHOMYL 0.100 N/D 0.001 0.001MEVINPHOS 0.100 N/D 0.001 0.001MYCLOBUTANIL 3.000 N/D 0.005 0.001NALED 0.500 N/D 0.005 0.001OXAMYL 0.500 N/D 0.001 0.001PACLOBUTRAZOL 0.100 N/D 0.005 0.001PERMETHRINS 1.000 N/D 0.005 0.001PHOSMET 0.200 N/D 0.005 0.001PIPERONYLBUTOXIDE
3.000 N/D 0.001 0.001
PRALLETHRIN 0.400 N/D 0.005 0.005PROPICONAZOLE 1.000 N/D 0.010 0.005PROPOXUR 0.100 N/D 0.001 0.001PYRETHRINS(PYRETHRIN I)
1.000 N/D 0.005 0.005
PYRIDABEN 3.000 N/D 0.005 0.001SPINETORAM 3.000 N/D 0.001 0.001SPINOSAD 3.000 N/D 0.001 0.001SPIROMESIFEN 3.000 N/D 0.005 0.001SPIROTETRAMAT 3.000 N/D 0.001 0.001SPIROXAMINE 0.100 N/D 0.001 0.001TEBUCONAZOLE 1.000 N/D 0.005 0.001THIACLOPRID 0.100 N/D 0.001 0.001THIAMETHOXAM 1.000 N/D 0.001 0.001TRIFLOXYSTROBIN 3.000 N/D 0.001 0.001
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
RESIDUAL SOLVENTS:Headspace GCMS - Shimadzu GCMS QP2020 with HS20
GSL SOP 405Prepared: 08/05/2020 15:59:39 Uploaded: 08/07/2020 14:29:51
Residual Solvent Action Level (ppm) Results (ppm) LOQ (ppm) LOD (ppm)1,1-DICHLOROETHENE 8 N/D 0.63 0.631,2- DICHLOROETHANE 2 N/D 0.12 0.02ACETONE 5,000 N/D 140 20ACETONITRILE 410 N/D 25 1BENZENE 1 N/D 1 0.5BUTANE 5,000 N/D 50 10CHLOROFORM 1 N/D 1 0.5CIS 1,2-DICHLOROETHENE 5 N/D 0.73 0.18ETHANOL 5,000 N/D 140 20ETHYL ACETATE 5,000 N/D 140 20ETHYL ETHER 5,000 N/D 140 20ETHYLENE OXIDE 1 N/D 0 0ISOPROPYL ALCOHOL 5,000 N/D 140 20METHANOL 3,000 N/D 100 20METHYLENE CHLORIDE 125 N/D 0.15 0.15N-HEPTANE 5,000 N/D 140 20N-HEXANE 290 N/D 18 10PENTANE 5,000 N/D 140 20PROPANE 5,000 N/D 20 1TOLUENE 890 N/D 53 1TRANS 1,2-DICHLOROETHENE 5 N/D 0.73 0.18TRICHLOROETHENE 1 N/D 1 0.5XYLENES 150 N/D 130 20
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex ** CFU/g Calculation based on MIP/Extract matrix *** Flavus = 2 Copies of DNA / Fumigatis = 2 Copies of DNA Niger = 20 Copies of DNA / Terrus = 10 copies of DNA
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
Microbial Analysis:PCR - Agilent AriaMX
Microbial Analysis GSL SOP 406 Uploaded: 08/06/2020 09:38:38
MICROBIAL ANALYSIS:
Test SOP Test Method Device Used LOD AllowableCriteria Actual Result Pass/Fail
TOTAL YEAST AND MOLD 406.01 USP 61/62† ARIAMX PCRCFU/G BYSAMPLETYPE**
10,000 CFU/G NOT DETECTED PASS
STEC E. COLI* 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
PATHOGENIC E. COLI 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
SALMONELLA* 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
PCR - Agilent AriaMX
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 58830Order Name: X Factor Relief500Batch#: 002160-XFN513Received: 07/30/2020Completed: 08/08/2020
Florida Nutrition INC11818 Race Track RoadTampa FL, 33626(813) [email protected]
Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060GSL SOP 401 Uploaded: 08/04/2020 18:26:44
Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20 N/DAFLATOXIN B2 20 N/DAFLATOXIN G1 20 N/DAFLATOXIN G2 20 N/DOCHRATOXIN A 20 N/D
LOQ is 1ppb, LOD is 1ppb
Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030GSL SOP 403 Uploaded: 08/05/2020 15:24:58
Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200 B/LOQCADMIUM (CD) 200 B/LOQMERCURY (HG) 100 B/LOQLEAD (PB) 500 B/LOQ
Lower Limit of Quantitation (LOQ) is 75 ppb
Moisture Analysis:Shimadzu MOC63U Moisture Balance - GSL SOP 411 Uploaded: 08/07/2020 07:16:41
Moisture %3.4%
Water Activity:HD-3A Water Activity Meter - GSL SOP 407 Uploaded: 08/08/2020 11:09:05
Water0.61
Filth and Foreign Materials Analysis:Microscope - Amscope Simul-Focal Trinocular Stereo Zoom Microscope - GSL SOP 409 Uploaded: 08/08/2020 11:21:52
Pass: No Foreign Materials Detected
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.