certificate of analysis...certificate of analysis order #: 31705 order name: king kalm cbd 600mg...
TRANSCRIPT
Reporting Limit 10 ppm *Total CBD = CBD + CBDA x 0.877 N/D - Not Detected, B/LOQ - Below Limit of Quantification
CERTIFICATE OF ANALYSISOrder #: 31705Order Name: King Kalm CBD600mgBatch#: 05282019Received: 05/28/2019Completed: 06/18/2019
King Kanine1856 N. Nob Hill Road #444Plantation FL, 33322(954) [email protected]
Sample
0.079% D9-THC
2.360% Total CBD
Cannabinoids TestGSL SOP 400 PREPARED: 06/10/2019 18:19:04 UPLOADED: 06/11/2019 14:39:19 cannabinoids weight(%) mg/gDELTA-9-TETRAHYDROCANNABINOL D9-THC 0.079% 0.793TETRAHYDROCANNABINOLIC ACID THCA N/D N/DCANNABIDIOL CBD 2.359% 23.592CANNABIDIOLIC ACID CBDA 0.001% 0.012CANNABIDIVARIN CBDV 0.015% 0.150CANNABICHROMENE CBC 0.132% 1.323CANNABINOL CBN N/D N/DCANNABIGEROL CBG 0.044% 0.438CANNABIGEROLIC ACID CBGA N/D N/DDELTA-8-TETRAHYDROCANNABINOL D8-THC N/D N/DTETRAHYDROCANNABIVARIN THCV N/D N/D
TOTAL D9-THC 0.079% 0.793TOTAL CBD* 2.360% 23.603TOTAL CANNABINOIDS 2.630% 26.308
NotesApproximately 718.2mg cannabinoids per 30mL
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 31705Order Name: King Kalm CBD600mgBatch#: 05282019Received: 05/28/2019Completed: 06/18/2019
King Kanine1856 N. Nob Hill Road #444Plantation FL, 33322(954) [email protected]
TERPENES: TOTAL (0.144%)Headspace GCMS - Shimadzu GCMS QP2020 with HS20
GSL SOP 404 Prepared: 06/10/2019 21:22:39 Uploaded: 06/11/2019 23:39:32
Terpene Results (%) LOQ (%) LOD (%)ALPHA-PINENE B/LOQ 0.0067% 0.0063%BETA-PINENE B/LOQ 0.0067% 0.0063%BORNEOL 0.017% 0.0067% 0.0063%CAMPHOR 0.007% 0.0067% 0.0063%CARYOPHYLLENE 0.015% 0.0067% 0.0063%CARYOPHYLLENE OXIDE 0.010% 0.0067% 0.0063%EUCALYPTOL 0.007% 0.0067% 0.0063%HUMULENE B/LOQ 0.0067% 0.0063%LIMONENE 0.009% 0.0067% 0.0063%
Terpene Results (%) LOQ (%) LOD (%)LINALOOL 0.069% 0.0067% 0.0063%
Terpenes Breakdown
Top Terpenes Results:
Tested for but not present:
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
PESTICIDE ANALYSIS:GSL SOP 401 PREPARED: 06/10/2019 22:08:01 UPLOADED: 06/11/2019 22:25:15
N/D = Not Detected, A/LOQ = Above LOQ Level, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level
CERTIFICATE OF ANALYSISOrder #: 31705Order Name: King Kalm CBD600mgBatch#: 05282019Received: 05/28/2019Completed: 06/18/2019
King Kanine1856 N. Nob Hill Road #444Plantation FL, 33322(954) [email protected]
LCMS-MS - Shimadzu LCMS-8060
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
ABAMECTIN B1A 0.100 N/D 0.003 0.001ACEPHATE 0.100 N/D 0.003 0.001ACEQUINOCYL 0.100 N/D 0.003 0.001ACETAMIPRID 0.100 N/D 0.003 0.001ALDICARB 0.100 N/D 0.003 0.001AZOXYSTROBIN 0.100 N/D 0.003 0.001BIFENAZATE 0.100 N/D 0.003 0.001BIFENTHRIN 3.000 N/D 0.003 0.001BOSCALID 0.100 N/D 0.003 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.003 0.001CHLORANTRANILIPROLE 10.000 N/D 0.003 0.001CHLORPYRIFOS 0.100 N/D 0.003 0.001CLOFENTEZINE 0.100 N/D 0.003 0.001DAMINOZIDE 0.100 N/D 0.003 0.001DIAZANON 0.100 N/D 0.003 0.001DICHLORVOS 0.100 N/D 0.003 0.001DIMETHOATE 0.100 N/D 0.003 0.001DIMETHOMORPH 2.000 N/D 0.003 0.001ETHOPROPHOS 0.100 N/D 0.003 0.001ETOFENPROX 0.100 N/D 0.003 0.001ETOXAZOLE 0.100 N/D 0.003 0.001FENHEXAMID 0.100 N/D 0.003 0.001FENOXYCARB 0.100 N/D 0.003 0.001FENPYROXIMATE 0.100 N/D 0.003 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 0.100 N/D 0.003 0.001FLUDIOXONIL 0.100 N/D 0.003 0.001HEXYTHIAZOX 0.100 N/D 0.003 0.001
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
IMAZALIL 0.100 N/D 0.003 0.001IMIDACLOPRID 5.000 N/D 0.003 0.001KRESOXIM-METHYL 0.100 N/D 0.003 0.001MALATHION 0.500 N/D 0.003 0.001METALAXYL 2.000 N/D 0.003 0.001METHIOCARB 0.100 N/D 0.003 0.001METHOMYL 1.000 N/D 0.003 0.001MEVINPHOS 0.100 N/D 0.003 0.001MYCLOBUTANIL 0.100 N/D 0.003 0.001NALED 0.100 N/D 0.003 0.001OXAMYL 0.500 N/D 0.003 0.001PACLOBUTRAZOL 0.100 N/D 0.003 0.001PERMETHRINS 0.500 N/D 0.003 0.001PHOSMET 0.100 N/D 0.003 0.001PIPERONYLBUTOXIDE
3.000 N/D 0.003 0.001
PRALLETHRIN 0.100 N/D 0.003 0.001PROPICONAZOLE 0.100 N/D 0.003 0.001PROPOXUR 0.100 N/D 0.003 0.001PYRETHRINS(PYRETHRIN I)
0.500 N/D 0.003 0.001
PYRIDABEN 0.100 N/D 0.003 0.001SPINETORAM 0.100 N/D 0.003 0.001SPINOSAD 0.100 N/D 0.003 0.001SPIROMESIFEN 0.100 N/D 0.003 0.001SPIROTETRAMAT 0.100 N/D 0.003 0.001SPIROXAMINE 0.100 N/D 0.003 0.001TEBUCONAZOLE 0.100 N/D 0.003 0.001THIACLOPRID 0.100 N/D 0.003 0.001THIAMETHOXAM 5.000 N/D 0.003 0.001TRIFLOXYSTROBIN 0.100 N/D 0.003 0.001
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 31705Order Name: King Kalm CBD600mgBatch#: 05282019Received: 05/28/2019Completed: 06/18/2019
King Kanine1856 N. Nob Hill Road #444Plantation FL, 33322(954) [email protected]
RESIDUAL SOLVENTS:Headspace GCMS - Shimadzu GCMS QP2020 with HS20
GSL SOP 405Prepared: 06/10/2019 21:23:46 Uploaded: 06/11/2019 23:59:01
Residual Solvent Action Level (ppm) Results (ppm) LOQ (ppm) LOD (ppm)ACETONE 5,000 N/D 140 20ACETONITRILE 410 N/D 25 1BENZENE 1 N/D 1 0.5BUTANE 5,000 N/D 50 10CHLOROFORM 1 N/D 1 0.5DICHLOROETHANE 1 N/D 1 0.5DICHLOROMETHANE 1 N/D 1 0.5ETHANOL 5,000 N/D 140 20ETHYL ACETATE 5,000 N/D 140 20ETHYL ETHER 5,000 N/D 140 20ISOPROPYL ALCOHOL 5,000 N/D 140 20METHANOL 3,000 N/D 100 20N-HEPTANE 5,000 N/D 140 20N-HEXANE 290 N/D 18 10PENTANE 5,000 N/D 140 20PROPANE 5,000 N/D 20 1TOLUENE 890 N/D 53 1TRICHLOROETHENE 0 N/D 0 0XYLENES 2,170 N/D 130 20
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 31705Order Name: King Kalm CBD600mgBatch#: 05282019Received: 05/28/2019Completed: 06/18/2019
King Kanine1856 N. Nob Hill Road #444Plantation FL, 33322(954) [email protected]
Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060GSL SOP 401 Uploaded: 06/11/2019 22:25:53
Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20 N/DAFLATOXIN B2 20 N/DAFLATOXIN G1 20 N/DAFLATOXIN G2 20 N/DOCHRATOXIN A 20 N/D
LOQ is 4ppb, LOD is 1ppb
Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030GSL SOP 403 Uploaded: 06/18/2019 03:28:43
Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200 B/LOQCADMIUM (CD) 200 B/LOQMERCURY (HG) 100 B/LOQLEAD (PB) 500 B/LOQ
Lower Limit of Quantitation (LOQ) is 75 ppb
Microbial Analysis:PCR - Agilent AriaMX
Microbial Analysis GSL SOP 406 Uploaded: 06/12/2019 17:02:38
Test Test MethodUsed Device Used LOD Allowable Amount Actual
Result Pass/Fail
STEC E. COLI* USP 61/62† ARIAMX PCR 2 COPIES OF DNA PRESENCE / ABSENTBELOW
LODPASS
SALMONELLA* USP 61/62† ARIAMX PCR 5 COPIES OF DNA PRESENCE / ABSENTBELOW
LODPASS
ASPERGILLUS USP 61/62† ARIAMX PCR ASP_LOD*** PRESENCE / ABSENTBELOW
LODPASS
† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex *** Flavus = 2 Copies of DNA / Fumigatis = 2 Copies of DNA Niger = 20 Copies of DNA / Terrus = 10 copies of DNA
Water Activity:HD-3A Water Activity Meter - GSL SOP 407 Uploaded: 06/10/2019 23:13:27
Water0.53
Filth and Foreign Materials Analysis:Microscope - Amscope Simul-Focal Trinocular Stereo Zoom Microscope - GSL SOP 409 Uploaded: 05/30/2019 19:09:30
No foreign materials detected.
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.