ce 2017 b5885 - url.t npo cgh-300… · din p(di-isononylphthalate ... dn op(di-n-octylphthalate)...

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This document is issued by the Company subject to its General Conditions of Service printed overleaf, available on request or accessible at http://www.sgs.com/en/Terms-and-Conditions.aspx and, for electronic format documents, subject to Terms and Conditions for Electronic Documents at http://www.sgs.com/en/Terms-and-Conditions/Termse-Document.aspx. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of client’s instruction, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. This document cannot be reproduced, except in full, without prior written approval of the Company. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested.

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= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = =

:

(1)

(2)

:

(1)Conclusion ： B as edon theperform ed tes ts on s u bm itted s am ple(s ),thetes t res u lts ofCadm iu m ,L ead,M ercu ry,Cr(V I),PB B s ,PB D E s ,D B P,B B P,D E H P,DIB P com ply with thelim its as s et byRoH S andam endingDirectiv e(E U )2015/863.

CERAM IC POW DER:N PO CG H -300N

Sam pleDes cription

Style/Item N o.

Pleas ereferto followingpages .

Test Requested

Sam pleReceiv ingDate

T es tingPeriod

Test Result(s)

Sam pleSu bm itted B y

As s pecifiedby client,with referenceto RoH S 2011/65/EU Annex IIandam endingDirectiv e(E U )2015/863todeterm ineCadm iu m ,L ead,M ercu ry,Cr(V I),PB B s ,PB D E s ,D B P,B B P,D E H P,DIB P contents in thes u bm itteds am ple(s ).

Pleas ereferto next pages fortheotheritem (s ).

JOH AN SON DIE L E C T RICS IN C .

M U L T IL AYE R CE RAM IC CAPACIT OR

Test Report N o.:CE/2017/B 5885 Date:2017/12/13

The following samples was/were submitted and identified by/on behalf of the applicant as :


15191B L E DSOE ST .,SYL M AR ,CAL IFOR N IA 91342

*CE/2017/B5885*

2017/11/30

2017/11/30T O 2017/12/13





Page:2of11Test Report N o.:CE/2017/B 5885 Date:2017/12/13



*CE/2017/B5885*

：

Result

No.1

2 n.d. 100

2 n.d. 1000

2 n.d. 1000

8 n.d. 1000

2 n.d. -

10 n.d. -

10 n.d. -

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. -

50 n.d. -

50 n.d. -

PAR T N AM E N o.1 W H IT E POW DE R

Test Result(s)

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

B erylliu m (B e)

B B P (B u tylB enzylphthalate)(CAS N o.:85-68-7)

DE H P (Di-(2-ethylhexyl)phthalate)(CAS N o.:117-81-7)

PFOA (CAS N o.:335-67-1)

Perflu orooctanes u lfonates(PFOS-Acid,M etalSalt,Am ide)

D B P (Dibu tylphthalate)(CASN o.:84-74-2)

DIB P (Di-is obu tylphthalate)(CASN o.:84-69-5)

DIDP (Di-is odecylphthalate)(CAS

N o.:26761-40-0;68515-49-1)

DIN P (Di-is ononylphthalate)(CAS

N o.:28553-12-0;68515-48-0)

D N OP (Di-n-octylphthalate)(CAS N o.:117-84-0)

M ercu ry (H g)

H exav alent Chrom iu m Cr(V I)(◆)

Cadm iu m (Cd)

L ead(Pb)

Test Item(s) Unit

m g/kg

m g/kg

W ith referenceto U S E PA 3550C (2007).Analys is was perform edby L C/M S.

W ith referenceto U S E PA 3052(1996).Analys is was perform edby ICP-AE S.

W ith referenceto IE C 62321-8(2017).Analys is was perform edby G C/M S.

m g/kg


m g/kg

Limit

W ith referenceto IE C 62321-7-2(2017)andperform edby U V -V IS.； W ith referencetoIE C 62321-5(2013)andperform edby ICP-AE S.

Method

W ith referenceto IE C 62321-5(2013)andperform edby ICP-AE S.

MDL






m g/kg











*CE/2017/B5885*

Result

No.1

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

m g/kg

m g/kg

m g/kg

m g/kgH alogen-B rom ine(B r)(CAS N o.:10097-32-2)

H alogen-Iodine(I)(CAS N o.:14362-44-8)

H exabrom odiphenylether

H eptabrom odiphenylether

Dibrom obiphenyl

Decabrom obiphenyl

T etrabrom obiphenyl

m g/kg

H exabrom obiphenyl

T ribrom obiphenyl

Dibrom odiphenylether

Sum of PBDEs

M onobrom odiphenylether

Decabrom odiphenylether

T ribrom odiphenylether

T etrabrom odiphenylether

Pentabrom odiphenylether

Pentabrom obiphenyl

H eptabrom obiphenyl

N onabrom obiphenyl

Sum of PBBs

Octabrom obiphenyl

W ith referenceto B S E N 14582(2016).Analys is was perform edby IC.

m g/kg

Octabrom odiphenylether

N onabrom odiphenylether

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

M onobrom obiphenyl

Halogen

H alogen-Flu orine(F)(CAS N o.:14762-94-8)

H alogen-Chlorine(Cl)(CAS N o.:22537-15-1)

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg



m g/kg


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

Test Item(s) Unit Method MDL Limit

W ith referenceto IE C 62321-6 (2015)andperform edby G C/M S.








*CE/2017/B5885*

1.

2.

3.

4.

5.

Note：

"-"= N ot Regu lated

m g/kg= ppm ； 0.1wt% = 1000ppm

M D L = M ethodDetection L im it

n.d.= N ot Detected = les s than M D L

PFOS Reference Information : POPs - (EU) 757/2010

Ou tlawingPFOS as s u bs tances orpreparations in concentrations abov e0.001% (10ppm ),in s em i-finis hedprodu ctsorarticles orparts at a lev elabov e0.1%(1000ppm ),in textiles orothercoatedm aterials abov e1µ g/m ².

(◆)：T heres u lt ofCr(V I)is "n.d."as theres u lt ofChrom iu m (Cr)is les s than theM D L ofCr(V I),andconfirm ationtes t ofCr(V I)is not requ ired.IftheChrom iu m (Cr)content is not les s than theM D L ofCr(V I),confirm ation tes t ofCr(V I)is requ ired.








*CE/2017/B5885*

#FL OW

Analytical flow chart of Heavy Metal

T hes es am ples weredis s olv ed totally by pre-conditioningm ethodaccordingto below flow chart.（Cr6+ tes t m ethodexclu ded）

T echnician :JR W ang Su perv is or:T roy C hang

C u tting、Preparation

Sam pleM eas u rem ent

Aciddiges tion with m icrowav e/hotplate

Pb/Cd/Hg/Cr

Filtration

Solu tion Res idu e

1) Alkalifu s ion2) H Clto dis s olv e

ICP-AES

Cr6+

N on-m etal M etal

Dis s olv ingby

u ltras onication

Diges tingat

150~160℃

ABS / PC / PVC Others

B oilingwaterextraction

Cool,filterdiges tatethrou gh

filter

Adddiphenyl-

carbazideforcolor

dev elopm ent

M eas u rethe

abs orbanceat 540nm by U V -V IS

Separatingto get

aqu eou s phas e

Diges tingat 60℃

by u ltras onication

pH adju s tm ent

Adddiphenyl-carbazidefor

colordev elopm ent

M eas u retheabs orbanceat

540nm by U V -V IS





Page:6 of11Test Report N o.:CE/2017/B 5885 Date:2017/12/13



*CE/2017/B5885*

ICP-AE S

Acid diges tion by s u itableaciddependedon

different s am plem aterial(as below table)

Filtration

Solu tion Res idu e

1) AlkaliFu s ion2) H C lto dis s olv e


C u tting/Preparation

Steel,copper,alu m inu m ,s older Aqu aregia,H N O3,H C l,H F,H 2O2

G las s H N O3/H FG old,platinu m ,palladiu m ,ceram ic Aqu aregiaSilv er H N O3

Plas tic H 2SO4,H 2O2,H N O3,H C lOthers Addedappropriatereagent to totaldiges tion

T hes es am ples weredis s olv ed totally by pre-conditioningm ethodaccordingto below flow

chart.

T echnician:JR W ang

Su perv is or:T roy Chang

Flow Chart of digestion for the elements analysis performed by ICP-AES








*CE/2017/B5885*

#PIC

Analytical flow chart - PFOA/PFOS

T echnician:YalingT u Su perv is or:T roy C hang

Sam plepretreatm ent

Sam pleextraction by U ltras onicextraction

(Referencem ethod:U S E PA 3550C)

Concentrate/Dilu teExtracted s olu tion

Analys is w as perform edby L C/M S

Data








*CE/2017/B5885*

Analytical flow chart - Phthalate

T echnician:Andy H s u


【Test method: IEC 62321-8】

Sam plepretreatm ent/s eparation

Sam pledis s olv ed/extractedby T H F

Dilu teExtracted s olu tion

Analys is w as perform edby G C/M S








*CE/2017/B5885*

Analytical flow chart – PBB / PBDE

T echnician :YalingT u


Firs t tes tingproces s

Optionals creen proces s

C onfirm ation proces s

Sam ple

Screen analys is


Sam pleextraction /Soxhlet m ethod

C oncentrate/D ilu teExtracted s olu tion

G C/M S

Filter








*CE/2017/B5885*

Analytical flow chart - Halogen

T echnician:RitaC hen


Sam plepretreatm ent /Separation

W eightingandpu ttings am plein cell

Oxygen B om bCom bu s tion /Abs orption

Analys is was perform edby IC

Dilu tion to fixed v olu m e








*CE/2017/B5885*

** EndofReport **

* The tested sample / part is marked by an arrow if it's shown on the photo. *





Page:1of11

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= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = =

:

(1)

(2)

:

(1)Conclusion ： B as edon theperform ed tes ts on s u bm itted s am ple(s ),thetes t res u lts ofCadm iu m ,L ead,M ercu ry,Cr(V I),PB B s ,PB D E s ,D B P,B B P,D E H P,DIB P com ply with thelim its as s et byRoH S andam endingDirectiv e(E U )2015/863.


Test Requested


T es tingPeriod

Test Result(s)







Sam pleDes cription

Style/Item N o. IN N E R E L E C T RODE:N PO



*CE/2017/B5890*

2017/11/30

2017/11/30T O 2017/12/13









*CE/2017/B5890*

：

Result

No.1

2 n.d. 100

2 n.d. 1000

2 n.d. 1000

8 n.d. 1000

2 n.d. -

10 n.d. -

10 n.d. -

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. -

50 n.d. -

50 n.d. -

PAR T N AM E N o.1 G RAY PIE CE S

Test Result(s)

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg


B erylliu m (B e)



PFOA (CAS N o.:335-67-1)



N o.:26761-40-0;68515-49-1)


N o.:28553-12-0;68515-48-0)


M ercu ry (H g)


Cadm iu m (Cd)

L ead(Pb)

Test Item(s)



Unit

m g/kg

m g/kg


Limit


Method


MDL




m g/kg


m g/kg




m g/kg











*CE/2017/B5890*

Result

No.1

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

m g/kg

m g/kg

m g/kg








Dibrom obiphenyl

Decabrom obiphenyl


m g/kg W ith referenceto B S E N 14582(2016).Analys is was perform edby IC.

m g/kg

m g/kg

m g/kg

m g/kg

Halogen



m g/kg

m g/kg

Test Item(s) Method MDL Limit


H exabrom obiphenyl

T ribrom obiphenyl


Sum of PBDEs






Pentabrom obiphenyl


m g/kg

m g/kg

M onobrom obiphenyl

m g/kgN onabrom obiphenyl

Sum of PBBs

Octabrom obiphenyl

m g/kg

m g/kg

m g/kg


m g/kg


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

Unit








*CE/2017/B5890*

1.

2.

3.

4.

5.

Note：















*CE/2017/B5890*

#FL OW







Pb/Cd/Hg/Cr

Filtration

Solu tion Res idu e


ICP-AES

Cr6+

N on-m etal M etal

Dis s olv ingby

u ltras onication

Diges tingat

150~160℃




filter

Adddiphenyl-

carbazideforcolor

dev elopm ent

M eas u rethe


Separatingto get

aqu eou s phas e

Diges tingat 60℃


pH adju s tm ent


colordev elopm ent


540nm by U V -V IS








*CE/2017/B5890*

ICP-AE S



Filtration

Solu tion Res idu e








chart.











*CE/2017/B5890*

#PIC








Data








*CE/2017/B5890*
















*CE/2017/B5890*







Sam ple

Screen analys is




G C/M S

Filter








*CE/2017/B5890*
















*CE/2017/B5890*

** EndofReport **






Page:1of11

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= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = =

:

(1)

(2)

:

(1)








Sam pleDes cription

Style/Item N o. T E R M IN AT ION S:N PO



*CE/2017/B5894*

2017/11/30

2017/11/30T O 2017/12/13

Test Requested


T es tingPeriod

Test Result(s) Pleas ereferto followingpages .

Conclusion ： B as edon theperform ed tes ts on s u bm itted s am ple(s ),thetes t res u lts ofCadm iu m ,L ead,M ercu ry,Cr(V I),PB B s ,PB D E s ,D B P,B B P,D E H P,DIB P com ply with thelim its as s et byRoH S andam endingDirectiv e(E U )2015/863.








*CE/2017/B5894*

：

Result

No.1

2 n.d. 100

2 n.d. 1000

2 n.d. 1000

8 n.d. 1000

2 n.d. -

10 n.d. -

10 n.d. -

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. 1000

50 n.d. -

50 n.d. -

50 n.d. -



m g/kg


m g/kg




m g/kg




Unit

m g/kg

m g/kg



Method





LimitMDL


N o.:26761-40-0;68515-49-1)


N o.:28553-12-0;68515-48-0)


M ercu ry (H g)


Cadm iu m (Cd)

L ead(Pb)

Test Item(s)

B erylliu m (B e)



PFOA (CAS N o.:335-67-1)



PAR T N AM E N o.1 SIL V E R COL ORED PAST E

Test Result(s)

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg








*CE/2017/B5894*

Result

No.1

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

50 n.d. -

m g/kg


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

Unit

m g/kg

m g/kgN onabrom obiphenyl

Sum of PBBs

Octabrom obiphenyl

m g/kg

m g/kg

m g/kg

M onobrom obiphenyl

Test Item(s) Method MDL Limit


H exabrom obiphenyl

T ribrom obiphenyl


Sum of PBDEs






Pentabrom obiphenyl


m g/kg

m g/kg W ith referenceto B S E N 14582(2016).Analys is was perform edby IC.

m g/kg

Halogen









Dibrom obiphenyl

Decabrom obiphenyl


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg










*CE/2017/B5894*

1.

2.

3.

4.

5.




Note：












*CE/2017/B5894*

#FL OW







Pb/Cd/Hg/Cr

Filtration

Solu tion Res idu e


ICP-AES

Cr6+

N on-m etal M etal

Dis s olv ingby

u ltras onication

Diges tingat

150~160℃




filter

Adddiphenyl-

carbazideforcolor

dev elopm ent

M eas u rethe


Separatingto get

aqu eou s phas e

Diges tingat 60℃


pH adju s tm ent


colordev elopm ent


540nm by U V -V IS








*CE/2017/B5894*

ICP-AE S



Filtration

Solu tion Res idu e








chart.











*CE/2017/B5894*

#PIC








Data








*CE/2017/B5894*
















*CE/2017/B5894*







Sam ple

Screen analys is




G C/M S

Filter








*CE/2017/B5894*
















*CE/2017/B5894*

** EndofReport **






Page:1of11

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:

= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = =

:

(1)

(2)

:



*CE/2017/B5897*

2017/11/30

2017/11/30T O 2017/12/06


As s pecifiedby client,with referenceto RoH S 2011/65/EU Annex IIandam endingDirectiv e(E U )2015/863to determ ineCadm iu m ,L ead,M ercu ry,Cr(V I),PB B s ,PB D E s ,D B P,B B P,D E H P,DIB P contentsin thes u bm itted s am ple(s ).




TestRep ort N o.:CE/2017/B 5897 Date:2017/12/06

Thefollowingsam p les was/weresu bm ittedandidentifiedby/on behalfoftheap p licantas :

Sam pleDes cription

Style/Item N o.


TestReq u ested


T es tingPeriod

TestResu lt(s)

N IC K E L





Page:2of11



*CE/2017/B5897*


：

Resu lt

N o.1

2 n.d.

2 n.d.

2 n.d.

0.10 n.d.

2 n.d.

10 n.d.

10 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

W ith referenceto IE C 62321-7-1(2015)andperform edby U V -V IS.

M ethod


M D L



W ith referenceto U S E PA 3050B (1996).Analys is was perform edby ICP-AE S.







m g/kg




N o.:26761-40-0;68515-49-1)



Unit

m g/kg

m g/kg


PFOA (CAS N o.:335-67-1)

B erylliu m (B e)

M ercu ry (H g)

H exav alent Chrom iu m Cr(V I)(#2)

Cadm iu m (Cd)

L ead(Pb)


TestItem (s)

m g/kg

m g/kg

m g/kgPerflu orooctanes u lfonates(PFOS-Acid,M etalSalt,Am ide)


N o.:28553-12-0;68515-48-0)



PAR T N AM E N o.1 SIL V E R COL ORED M E T A L

TestResu lt(s)

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

µ g/cm ²

m g/kg

m g/kg





Page:3of11



*CE/2017/B5897*


Resu lt

N o.1

- n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

- n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

TestItem (s) Unit M ethod M D L


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg




m g/kg


m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg

Su m ofPB B s


m g/kg

m g/kg

m g/kg


m g/kg

T ribrom obiphenyl

m g/kg

m g/kg


H alogen-B rom ine(B r)(CAS N o.:10097-32-2)

Octabrom obiphenyl

Pentabrom obiphenyl

M onobrom obiphenyl









H alogen

N onabrom obiphenyl


Dibrom obiphenyl

Decabrom obiphenyl




Su m ofPB DEs

H exabrom obiphenyl

m g/kg

m g/kg

m g/kg

m g/kg

m g/kg





Page:4of11



*CE/2017/B5897*


1.

2.

3.

4.

5.

PFO S Reference Inform ation:PO Ps -(EU ) 757/20 1 0

Ou tlawingPFOS as s u bs tances orpreparations in concentrations abov e0.001% (10ppm ),in s em i-finis hedprodu cts orarticles orparts at a lev elabov e0.1%(1000ppm ),in textiles orothercoatedm aterials abov e1µ g/m ².

(#2)=a.T hes am pleis pos itiv eforCr(V I)iftheCr(V I)concentration is greaterthan 0.13µ g/cm ².

T hes am plecoatingis cons idered to contain Cr(V I)b.T hes am pleis negativ eforCr(V I)ifCr(V I)is n.d.(concentration les s than 0.10µ g/cm ²).

T hecoatingis cons ideredanon-Cr(V I)bas edcoatingc.T heres u lt between 0.10µ g/cm ² and0.13µ g/cm ² is cons idered to beinconclu s iv e-u nav oidable

coatingv ariations m ay influ encethedeterm ination.

N ote：









Page:5of11



*CE/2017/B5897*


#FL OW

A nalyticalflow chartofH eavy M etal






Pb/Cd/H g/C r

Filtration

Solu tion Res idu e


ICP-AES

C r6+

N on-m etal M etal

Dis s olv ingby

u ltras onication

Diges tingat

150~160℃

A B S / PC / PVC O thers



filter

Adddiphenyl-

carbazideforcolor

dev elopm ent

M eas u rethe


Separatingto get

aqu eou s phas e

Diges tingat 60℃


pH adju s tm ent


colordev elopm ent


540nm by U V -V IS





Page:6 of11



*CE/2017/B5897*


ICP-AES

Aciddiges tion by s u itableaciddependedon


Filtration

Solu tion Res idu e

1) AlkaliFu s ion2) H Clto dis s olv e



Steel,copper,alu m inu m ,s older Aqu a regia,H N O3,H C l,H F,H 2O2

G las s H N O3/H FG old,platinu m ,palladiu m ,ceram ic Aqu a regiaSilv er H N O3

Plas tic H 2SO4,H 2O2,H N O3,H ClOthers Addedappropriatereagent to totaldiges tion


chart.


Su perv is or:T roy C hang

Flow Chartofdigestion for theelem ents analysis p erform edby IC P-A ES





Page:7of11



*CE/2017/B5897*


A nalyticalflow chart-PFO A /PFO S





Concentrate/Dilu teE xtracted s olu tion

Analys is was perform edby L C/M S

Data





Page:8of11



*CE/2017/B5897*


A nalyticalflow chart-Phthalate


Su perv is or:T roy C hang

【Testm ethod:IEC 62321 -8】



Dilu teE xtracted s olu tion

Analys is was perform edby G C/M S





Page:9of11



*CE/2017/B5897*


A nalyticalflow chart–PB B / PB DE






Sam ple

Screen analys is



C oncentrate/Dilu teExtracted s olu tion

G C/M S

Filter





Page:10of11



*CE/2017/B5897*


A nalyticalflow chart-H alogen

T echnician:R ita C hen




Oxygen B om bC om bu s tion /Abs orption


D ilu tion to fixed v olu m e





Page:11of11



*CE/2017/B5897*


#PIC

** EndofReport **

*Thetestedsam p le / p artis m arkedby an arrow ifit's shown on the p hoto.*





Page : 1 of 11

:

:

:

:

:

============================================================================================

:

(1)

(2)

:Test Result(s)

Test Report No. : CE/2017/B5898A Date : 2017/12/14


Sample Description

Style/Item No.

Please refer to following pages.

Test Requested

Sample Receiving Date

Testing Period 2017/11/30 TO 2017/12/06

Sample Submitted By

As specified by client, with reference to RoHS 2011/65/EU Annex II and amending Directive (EU)2015/863 to determine Cadmium, Lead, Mercury, Cr(VI), PBBs, PBDEs, DBP, BBP, DEHP, DIBP contentsin the submitted sample(s).

Please refer to next pages for the other item(s).

JOHANSON DIELECTRICS INC.

MULTILAYER CERAMIC CAPACITOR

TIN BALL


15191 BLEDSOE ST., SYLMAR, CALIFORNIA 91342

*CE/2017/B5898A*

2017/11/30





Page : 2 of 11Test Report No. : CE/2017/B5898A Date : 2017/12/14



*CE/2017/B5898A*

：

Result

No.1

2 n.d.

2 43.6

2 n.d.

0.10 n.d.

2 n.d.

10 n.d.

10 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

PART NAME No.1 SILVER COLORED METAL

Test Result(s)

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

DINP (Di-isononyl phthalate)(CAS No.: 28553-12-0; 68515-48-0)DNOP (Di-n-octyl phthalate)(CAS No.: 117-84-0)

mg/kgPFOA (CAS No.: 335-67-1)

DBP (Dibutyl phthalate) (CAS No.:

84-74-2)

Unit

mg/kg

mg/kg

With reference to IEC 62321-8 (2017).Analysis was performed by GC/MS.

Perfluorooctane sulfonates(PFOS-Acid, Metal Salt, Amide)

Beryllium (Be)

Mercury (Hg)

Hexavalent Chromium Cr(VI)(#2)

Cadmium (Cd)

Lead (Pb)

BBP (Butyl Benzyl phthalate)(CAS No.: 85-68-7)

Test Item(s)

mg/kg

mg/kg

With reference to US EPA 3550C (2007).Analysis was performed by LC/MS.

With reference to US EPA 3550C (2007).Analysis was performed by LC/MS.





mg/kg



mg/kg

With reference to IEC 62321-5 (2013) andperformed by ICP-AES.


With reference to US EPA 3050B (1996).Analysis was performed by ICP-AES.

µg/cm²

mg/kg

With reference to IEC 62321-7-1 (2015) andperformed by UV-VIS.

Method


MDL

DEHP (Di- (2-ethylhexyl) phthalate)

(CAS No.: 117-81-7)

DIBP (Di-isobutyl phthalate) (CASNo.: 84-69-5)

DIDP (Di-isodecyl phthalate)(CAS No.: 26761-40-0; 68515-49-1)








*CE/2017/B5898A*

Result

No.1

- n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

- n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

5 n.d.

50 n.d.

50 n.d.

50 n.d.

50 n.d.

mg/kg

mg/kg

Halogen-Iodine (I)(CAS No.: 14362-44-8)

Dibromobiphenyl

Decabromobiphenyl

Octabromodiphenyl ether

Nonabromodiphenyl ether

Tetrabromobiphenyl

Sum of PBDEs

Hexabromobiphenyl

Monobromodiphenyl ether

mg/kg

Tribromobiphenyl

mg/kg

mg/kg

Halogen-Chlorine (Cl)(CAS No.: 22537-15-1)

Halogen-Bromine (Br)(CAS No.: 10097-32-2)

Octabromobiphenyl

Pentabromobiphenyl

Monobromobiphenyl

Tetrabromodiphenyl ether

Dibromodiphenyl ether

Tribromodiphenyl ether

Pentabromodiphenyl ether

Hexabromodiphenyl ether

Heptabromodiphenyl ether

Heptabromobiphenyl

Halogen-Fluorine (F)(CAS No.: 14762-94-8)

Halogen

Nonabromobiphenyl

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Sum of PBBs

Decabromodiphenyl ether

mg/kg

mg/kg

mg/kg

With reference to BS EN 14582 (2016).Analysis was performed by IC.



mg/kg


mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Test Item(s) Unit Method MDL

With reference to IEC 62321-6 (2015) andperformed by GC/MS.








*CE/2017/B5898A*

1.

2.

3.

4.

5. (#2) =a. The sample is positive for Cr(VI) if the Cr(VI) concentration is greater than 0.13 µg/cm².

The sample coating is considered to contain Cr(VI)b. The sample is negative for Cr(VI) if Cr(VI) is n.d. (concentration less than 0.10 µg/cm²).

The coating is considered a non-Cr(VI) based coatingc. The result between 0.10 µg/cm² and 0.13 µg/cm² is considered to be inconclusive - unavoidable

coating variations may influence the determination.

Note：

" - " = Not Regulated

mg/kg = ppm； 0.1wt% = 1000ppm

MDL = Method Detection Limit

n.d. = Not Detected = less than MDL


Outlawing PFOS as substances or preparations in concentrations above 0.001% (10ppm), in semi-finishedproducts or articles or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1µg/m².








*CE/2017/B5898A*

#FLOW


These samples were dissolved totally by pre-conditioning method according to below flow chart.（Cr6+ test method excluded）

Technician : JR Wang Supervisor: Troy Chang

Cutting、Preparation

Sample Measurement

Acid digestion with microwave / hotplate

Pb/Cd/Hg/Cr

Filtration

Solution Residue

1) Alkali fusion2) HCl to dissolve

ICP-AES

Cr6+

Non-metal Metal

Dissolving by

ultrasonication

Digesting at

150~160℃


Boiling waterextraction

Cool, filterdigestate through

filter

Add diphenyl-

carbazide for color

development

Measure the

absorbance at 540nm by UV-VIS

Separating to get

aqueous phase

Digesting at 60℃

by ultrasonication

pH adjustment

Add diphenyl-carbazide for

color development

Measure the absorbance at

540 nm by UV-VIS








*CE/2017/B5898A*

ICP-AES

Acid digestion by suitable acid depended on

different sample material (as below table)

Filtration

Solution Residue

1) Alkali Fusion2) HCl to dissolve

Sample Measurement

Cutting / Preparation

Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2

Glass HNO3/HFGold, platinum, palladium, ceramic Aqua regiaSilver HNO3

Plastic H2SO4, H2O2, HNO3, HClOthers Added appropriate reagent to total digestion

These samples were dissolved totally by pre-conditioning method according to below flow

chart.

Technician: JR Wang

Supervisor: Troy Chang









*CE/2017/B5898A*


Technician: Yaling Tu Supervisor: Troy Chang

Sample pretreatment

Sample extraction by Ultrasonic extraction

(Reference method: US EPA 3550C)

Concentrate/Dilute Extracted solution

Analysis was performed by LC/MS

Data








*CE/2017/B5898A*


Technician: Andy Hsu



Sample pretreatment/separation

Sample dissolved/extracted by THF

Dilute Extracted solution

Analysis was performed by GC/MS








*CE/2017/B5898A*


Technician : Yaling Tu


First testing process

Optional screen process

Confirmation process

Sample

Screen analysis

Sample pretreatment

Sample extraction /Soxhlet method

Concentrate/DiluteExtracted solution

GC/MS

Filter








*CE/2017/B5898A*


Technician: Rita Chen


Sample pretreatment / Separation

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorption

Analysis was performed by IC

Dilution to fixed volume








*CE/2017/B5898A*

#PIC

** End of Report **
