brackley property developments our ref: emw-bwb-zz-xx-rp ... · 1.1 bwb consulting ltd (bwb) was...

Brackley Property Developments

Fulcrum House

1 Oak Spinney Park

Ratby Lane

Leicester

LE3 3AW

Our Ref: EMW-BWB-ZZ-XX-RP-YE-0005_WA

Contact: Redmond Parker-Dunn/ Richard Robinson

Direct Dial: 0115 924 7347/ 0115 724 7344

Date: 28th September 2017

Dear James

WASTE ASSESSMENT: EDGAR MOBBS WAY, NORTHAMPTON

Introduction and Objectives

1.1 BWB Consulting Ltd (BWB) was instructed by Brackley Properties Ltd (the Client) to undertake

soil sampling at land located off Edger Mobbs Way, Northampton. The objective of the report

is to undertake a Waste Assessment of near surface materials currently present at the site, which

will be stripped and disposed of during development of the site.

Scope of Works

1.2 BWB obtained soil samples from the site on 6th September 2017 in general accordance with

techniques outlined in BS 5930:2015 and BS EN ISO 1997:2004 Part 1 and under the full -time

supervision of a suitably qualified Geo-Environmental Engineer from BWB. The ground

investigation comprised the following works:

Excavation of six hand pits to a maximum depth of 0.40 m below ground level (bgl);

and

Collection of soil samples for chemical analysis.

1.3 An exploratory hole location plan is presented as Drawing 1.

1.4 One soil sample was collected from each exploratory hole location and were sent to i2

Analytical (UKAS and MCERTS accredited) for chemical analysis. The following chemical

analytical testing was undertaken:

of 6

A soil suite (BWB Standard Suite) comprising arsenic, barium, beryllium, water soluble

boron, cadmium, chromium, hexavalent chromium, copper, lead, mercury, nickel,

selenium, vanadium, zinc, water soluble sulphate (2:1 extract), total phenols, total

cyanide, free cyanide, complex cyanide, fraction of organic carbon, pH, Polycyclic

Aromatic Hydrocarbons (PAHs) (United States Environment Protection Agency priority

16 compounds) and Total Petroleum Hydrocarbons (TPH) C6-C40;

TPH speciated to the UK Criteria Working Group (TPHCWG) aliphatic and aromatic

compounds;

asbestos screening; and

Full (Waste Acceptance Criteria) WAC Analysis.

1.5 The results of the soil chemical testing are presented as Appendix 1.

Ground Conditions Encountered

1.6 The ground conditions encountered within the six hand pits undertaken comprised the

following:

Hand Pit

Location

Description

HP01 Vegetation over brown slightly clayey gravelly SAND with abundant rootlets. Gravel

of fine to course angular to well-rounded quartz, mudstone and sandstone.


of fine to course angular to well-rounded quartz, sedimentary rock and occasional brick.

HP03 Vegetation over dark brown clayey gravelly SAND with abundant rootlets. Gravel of

fine to course angular to well-rounded quartz, sedimentary rock and brick.

HP04 Dark brown sandy organic CLAY with abundant rootlets.

HP05 Dark brown and yellow clayey SAND with abundant rootlets and occasional brick

cobbles.


of fine to course angular to well-rounded quartz and sedimentary rock.

1.7 No visual or olfactory evidence of contamination was noted during the exercise.

Waste Assessment

1.8 Soil samples have been characterised against hazardous waste criteria using Hazwasteonline.

The results of the waste classification are presented in Appendix 2. The assessment indicates

that the soils analysed are likely to be classified as non-hazardous. The waste classification

assessment only applies to those soils that have been tested. If other soils are to be disposed

of off-site then further analysis may be required.

1.9 No asbestos has been identified in the samples analysed. The presence of visible asbestos

containing materials in waste or at concentrations exceeding 0.1% by weight will classify the

waste as mixed and require disposal as hazardous waste irrespective of the chemical

properties of the waste.

of 6

1.10 WAC testing was completed on the samples the results indicated the wastes would be suitable

for disposal as stable non-reactive hazardous waste at a non-hazardous landfill.

Conclusions and Recommendations

1.11 The waste assessment deems the soil cover at the site to be classified as stable non-reactive

hazardous waste and suitable for off-site disposal at a non-hazardous landfill.

1.12 I trust the above meets your requirements, however, should you require any further information

please contact either Redmond Parker-Dunn or myself.

Yours sincerely,

Richard Robinson BSc (Hons) MCIWEM

Principal Environmental Consultant

0115 851 7344

[email protected]

Enc. Drawing 1 Exploratory Hole Location Plan

Appendix 1 Soil Chemical Laboratory Results

Appendix 2 HazWaste Online Assessment

mailto:[email protected]

of 6

DRAWING 1

EXPLORATORY HOLE LOCATION PLAN

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Stockpile removed

Issues & Revisions

Rev Date Details of issue / revision RevDrw

CONSULTANCY | ENVIRONMENTINFRASTRUCTURE | BUILDINGS

Birmingham | 0121 233 3322

Leeds | 0113 233 8000

Manchester | 0161 233 4260

London | 020 7407 3879

Nottingham | 0115 924 1100

www.bwbconsulting.com

BWB Ref: Date: Scale@A1:

Drawn: Reviewed:

Drawing Status

Project - Originator - Zone - Level - Type - Role - Number Status

Drawing Title

Project Title

Client

Rev

© Copyright BWB Consulting Ltd

P

EMW-BWB-XX-00-DR-YE-0001-WA

Final

R. Robinson R. Parker-Dunn

NTH2325

Hand Pit Locations

Edgar Mobbs Way,

Northampton

Brackley property

Developments

1:25028.09.2017

1

Notes

1. Do not scale this drawing. All dimensions must be checked/ verified

on site. If in doubt ask.

2. This drawing is to be read in conjunction with all relevant architects,

engineers and specialists drawings and specifications.

3. All dimensions in millimetres unless noted otherwise. All levels in

metres unless noted otherwise.

4. Any discrepancies noted on site are to be reported to the engineer

immediately.

Y:\NTH\NTH2325_Edgar Mobbs Way, Northampton\02. Project Delivery\01. WIP\Drawings\EMW-BWB-00-XX-DR-EN-0002_EHLP\EMW-BWB-00-XX-DR-EN-0002-Han Pit Locations.dwg

APPROX

Legend

P1 03.01.16 DRAFT RPDPT

P2 13.01.16 FINALLJW RPD

HP**

Hand Pit Location

of 6

APPENDIX 1

SOIL CHEMICAL LABORATORY RESULTS

Richard Robinson

t: 01923 225404f: 01923 237404

e: [email protected] e:

Project / Site name: Samples received on: 07/09/2017

Your job number: NTH2325 Samples instructed on: 07/09/2017

Your order number: POR013215 Analysis completed by: 15/09/2017

Report Issue Number: 1 Report issued on: 15/09/2017

Samples Analysed:

Signed:

Assistant Reporting ManagerFor & on behalf of i2 Analytical Ltd.

Standard Geotechnical, Asbestos and Chemical Testing Laboratory located at: ul. Pionierów 39, 41 -711 Ruda Śląska, Poland.

Accredited tests are defined within the report, opinions and interpretations expressed herein are outside the scope of accreditation.

Standard sample disposal times, unless otherwise agreed with the laboratory, are : soils - 4 weeks from reportingleachates - 2 weeks from reportingwaters - 2 weeks from reportingasbestos - 6 months from reporting

Excel copies of reports are only valid when accompanied by this PDF certificate.

[email protected]

Emma Winter

6 soil samples

Edgar Mobbs Way

BWB Consulting Limited5th FloorWaterfront HouseNottinghamNG2 3DQ

i2 Analytical Ltd.7 Woodshots Meadow,Croxley Green Business Park,Watford, Herts, WD18 8YS

Analytical Report Number : 17-59715

This certificate should not be reproduced, except in full, without the express permission of the laboratory.

The results included within the report are representative of the samples submitted for analysis.

Iss No 17-59715-1 Edgar Mobbs Way NTH2325

Page 1 of 8

Analytical Report Number: 17-59715

Project / Site name: Edgar Mobbs Way

Your Order No: POR013215

Lab Sample Number 812765 812766 812767 812768 812769Sample Reference HP01 HP02 HP03 HP04 HP05Sample Number 001 002 003 004 005Depth (m) 0.20-0.20 0.10-0.10 0.20-0.20 0.20-0.20 0.20-0.20Date Sampled 06/09/2017 06/09/2017 06/09/2017 06/09/2017 06/09/2017Time Taken None Supplied None Supplied None Supplied None Supplied None Supplied

Analytical Parameter

(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Stone Content % 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Moisture Content % N/A NONE 8.7 11 13 18 21Total mass of sample received kg 0.001 NONE 1.5 1.1 1.4 1.4 1.3

Asbestos in Soil Type N/A ISO 17025 Not-detected Not-detected Not-detected Not-detected Not-detected

General Inorganics

pH - Automated pH Units N/A MCERTS 7.9 7.5 8.1 8.1 8.0Total Cyanide mg/kg 1 MCERTS < 1 < 1 < 1 < 1 < 1Complex Cyanide mg/kg 1 MCERTS < 1 < 1 < 1 < 1 < 1Free Cyanide mg/kg 1 MCERTS < 1 < 1 < 1 < 1 < 1Water Soluble SO4 16hr extraction (2:1 Leachate Equivalent) g/l 0.00125 MCERTS 0.059 0.016 0.021 0.097 0.021Total Sulphur mg/kg 50 MCERTS 490 670 850 770 880Fraction Organic Carbon (FOC) N/A 0.001 NONE 0.016 0.042 0.040 0.020 0.016

Total Phenols

Total Phenols (monohydric) mg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0

Speciated PAHs

Naphthalene mg/kg 0.05 MCERTS < 0.05 < 0.05 < 0.05 < 0.05 < 0.05Acenaphthylene mg/kg 0.05 MCERTS < 0.05 < 0.05 < 0.05 < 0.05 < 0.05Acenaphthene mg/kg 0.05 MCERTS < 0.05 < 0.05 < 0.05 < 0.05 < 0.05Fluorene mg/kg 0.05 MCERTS < 0.05 < 0.05 < 0.05 < 0.05 < 0.05Phenanthrene mg/kg 0.05 MCERTS 0.60 0.20 0.34 0.33 0.28Anthracene mg/kg 0.05 MCERTS 0.17 < 0.05 0.13 0.10 < 0.05Fluoranthene mg/kg 0.05 MCERTS 1.3 0.49 1.0 1.0 0.66Pyrene mg/kg 0.05 MCERTS 1.2 0.47 0.96 0.96 0.61Benzo(a)anthracene mg/kg 0.05 MCERTS 0.92 0.36 0.72 0.68 0.49Chrysene mg/kg 0.05 MCERTS 0.73 0.30 0.62 0.60 0.32Benzo(b)fluoranthene mg/kg 0.05 MCERTS 1.5 0.65 1.2 1.2 0.67Benzo(k)fluoranthene mg/kg 0.05 MCERTS 0.48 0.17 0.43 0.30 0.27Benzo(a)pyrene mg/kg 0.05 MCERTS 1.0 0.46 0.87 0.74 0.50Indeno(1,2,3-cd)pyrene mg/kg 0.05 MCERTS 0.65 0.27 0.51 0.45 0.30Dibenz(a,h)anthracene mg/kg 0.05 MCERTS 0.18 < 0.05 0.15 0.12 0.10Benzo(ghi)perylene mg/kg 0.05 MCERTS 0.59 0.23 0.47 0.39 0.28

Total PAH

Speciated Total EPA-16 PAHs mg/kg 0.8 MCERTS 9.39 3.60 7.45 6.94 4.48

Heavy Metals / Metalloids

Arsenic (aqua regia extractable) mg/kg 1 MCERTS 21 20 29 21 19Barium (aqua regia extractable) mg/kg 1 MCERTS 92 76 190 110 150Beryllium (aqua regia extractable) mg/kg 0.06 MCERTS 1.5 1.2 2.1 1.5 1.8Boron (water soluble) mg/kg 0.2 MCERTS 1.8 1.5 2.7 1.9 2.0Cadmium (aqua regia extractable) mg/kg 0.2 MCERTS < 0.2 < 0.2 < 0.2 < 0.2 < 0.2Chromium (hexavalent) mg/kg 4 MCERTS < 4.0 < 4.0 < 4.0 < 4.0 < 4.0Chromium (aqua regia extractable) mg/kg 1 MCERTS 55 43 43 39 47Copper (aqua regia extractable) mg/kg 1 MCERTS 31 29 95 42 46Lead (aqua regia extractable) mg/kg 1 MCERTS 82 47 200 110 93Mercury (aqua regia extractable) mg/kg 0.3 MCERTS < 0.3 < 0.3 < 0.3 < 0.3 < 0.3Nickel (aqua regia extractable) mg/kg 1 MCERTS 33 26 34 31 31Selenium (aqua regia extractable) mg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0Vanadium (aqua regia extractable) mg/kg 1 MCERTS 80 62 61 64 66Zinc (aqua regia extractable) mg/kg 1 MCERTS 140 94 240 150 180




Page 2 of 8




Lab Sample Number 812765 812766 812767 812768 812769Sample Reference HP01 HP02 HP03 HP04 HP05Sample Number 001 002 003 004 005Depth (m) 0.20-0.20 0.10-0.10 0.20-0.20 0.20-0.20 0.20-0.20Date Sampled 06/09/2017 06/09/2017 06/09/2017 06/09/2017 06/09/2017Time Taken None Supplied None Supplied None Supplied None Supplied None Supplied


(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Monoaromatics

Benzene ug/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0Toluene µg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0Ethylbenzene µg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0p & m-xylene µg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0o-xylene µg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0MTBE (Methyl Tertiary Butyl Ether) µg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0

Petroleum Hydrocarbons

TPH C10 - C40 mg/kg 10 MCERTS 97 46 94 21 21

TPH2 (C6 - C10) mg/kg 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

TPH-CWG - Aliphatic >EC5 - EC6 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aliphatic >EC6 - EC8 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aliphatic >EC8 - EC10 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aliphatic >EC10 - EC12 mg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0TPH-CWG - Aliphatic >EC12 - EC16 mg/kg 2 MCERTS < 2.0 < 2.0 < 2.0 < 2.0 < 2.0TPH-CWG - Aliphatic >EC16 - EC21 mg/kg 8 MCERTS < 8.0 < 8.0 < 8.0 < 8.0 < 8.0TPH-CWG - Aliphatic >EC21 - EC35 mg/kg 8 MCERTS 20 < 8.0 < 8.0 < 8.0 < 8.0TPH-CWG - Aliphatic (EC5 - EC35) mg/kg 10 MCERTS 22 < 10 11 < 10 < 10

TPH-CWG - Aromatic >EC5 - EC7 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aromatic >EC7 - EC8 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aromatic >EC8 - EC10 mg/kg 0.001 MCERTS < 0.001 < 0.001 < 0.001 < 0.001 < 0.001TPH-CWG - Aromatic >EC10 - EC12 mg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0TPH-CWG - Aromatic >EC12 - EC16 mg/kg 2 MCERTS < 2.0 < 2.0 3.2 < 2.0 < 2.0TPH-CWG - Aromatic >EC16 - EC21 mg/kg 10 MCERTS < 10 < 10 12 < 10 < 10TPH-CWG - Aromatic >EC21 - EC35 mg/kg 10 MCERTS 55 31 60 11 12TPH-CWG - Aromatic (EC5 - EC35) mg/kg 10 MCERTS 65 36 75 14 16




Page 3 of 8




Lab Sample Number

Sample Reference

Sample Number

Depth (m)

Date Sampled

Time Taken


(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Stone Content % 0.1 NONE

Moisture Content % N/A NONE

Total mass of sample received kg 0.001 NONE

Asbestos in Soil Type N/A ISO 17025

General Inorganics

pH - Automated pH Units N/A MCERTS

Total Cyanide mg/kg 1 MCERTS

Complex Cyanide mg/kg 1 MCERTS

Free Cyanide mg/kg 1 MCERTSWater Soluble SO4 16hr extraction (2:1 Leachate Equivalent) g/l 0.00125 MCERTS

Total Sulphur mg/kg 50 MCERTS

Fraction Organic Carbon (FOC) N/A 0.001 NONE

Total Phenols

Total Phenols (monohydric) mg/kg 1 MCERTS

Speciated PAHs

Naphthalene mg/kg 0.05 MCERTS

Acenaphthylene mg/kg 0.05 MCERTS

Acenaphthene mg/kg 0.05 MCERTS

Fluorene mg/kg 0.05 MCERTS

Phenanthrene mg/kg 0.05 MCERTS

Anthracene mg/kg 0.05 MCERTS

Fluoranthene mg/kg 0.05 MCERTS

Pyrene mg/kg 0.05 MCERTS

Benzo(a)anthracene mg/kg 0.05 MCERTS

Chrysene mg/kg 0.05 MCERTS

Benzo(b)fluoranthene mg/kg 0.05 MCERTS

Benzo(k)fluoranthene mg/kg 0.05 MCERTS

Benzo(a)pyrene mg/kg 0.05 MCERTS

Indeno(1,2,3-cd)pyrene mg/kg 0.05 MCERTS

Dibenz(a,h)anthracene mg/kg 0.05 MCERTS

Benzo(ghi)perylene mg/kg 0.05 MCERTS

Total PAH

Speciated Total EPA-16 PAHs mg/kg 0.8 MCERTS

Heavy Metals / Metalloids

Arsenic (aqua regia extractable) mg/kg 1 MCERTS

Barium (aqua regia extractable) mg/kg 1 MCERTS

Beryllium (aqua regia extractable) mg/kg 0.06 MCERTS

Boron (water soluble) mg/kg 0.2 MCERTS

Cadmium (aqua regia extractable) mg/kg 0.2 MCERTS

Chromium (hexavalent) mg/kg 4 MCERTS

Chromium (aqua regia extractable) mg/kg 1 MCERTS

Copper (aqua regia extractable) mg/kg 1 MCERTS

Lead (aqua regia extractable) mg/kg 1 MCERTS

Mercury (aqua regia extractable) mg/kg 0.3 MCERTS

Nickel (aqua regia extractable) mg/kg 1 MCERTS

Selenium (aqua regia extractable) mg/kg 1 MCERTS

Vanadium (aqua regia extractable) mg/kg 1 MCERTS

Zinc (aqua regia extractable) mg/kg 1 MCERTS

812770

HP06006

0.10-0.1006/09/2017

None Supplied

< 0.1101.1

Not-detected

7.5< 1< 1< 1

0.013510

0.021

< 1.0

< 0.05< 0.05< 0.05< 0.050.420.141.11.00.740.621.30.360.880.500.130.43

7.53

25761.11.3

< 0.2< 4.0

382058

< 0.323

< 1.04793




Page 4 of 8




Lab Sample Number

Sample Reference

Sample Number

Depth (m)

Date Sampled

Time Taken


(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Monoaromatics

Benzene ug/kg 1 MCERTS

Toluene µg/kg 1 MCERTS

Ethylbenzene µg/kg 1 MCERTS

p & m-xylene µg/kg 1 MCERTS

o-xylene µg/kg 1 MCERTS

MTBE (Methyl Tertiary Butyl Ether) µg/kg 1 MCERTS

Petroleum Hydrocarbons

TPH C10 - C40 mg/kg 10 MCERTS

TPH2 (C6 - C10) mg/kg 0.1 MCERTS

TPH-CWG - Aliphatic >EC5 - EC6 mg/kg 0.001 MCERTS



TPH-CWG - Aliphatic >EC10 - EC12 mg/kg 1 MCERTS



TPH-CWG - Aliphatic >EC21 - EC35 mg/kg 8 MCERTSTPH-CWG - Aliphatic (EC5 - EC35) mg/kg 10 MCERTS

TPH-CWG - Aromatic >EC5 - EC7 mg/kg 0.001 MCERTS



TPH-CWG - Aromatic >EC10 - EC12 mg/kg 1 MCERTS



TPH-CWG - Aromatic >EC21 - EC35 mg/kg 10 MCERTSTPH-CWG - Aromatic (EC5 - EC35) mg/kg 10 MCERTS

812770

HP06006

0.10-0.1006/09/2017

None Supplied

< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0

30

< 0.1

< 0.001< 0.001< 0.001< 1.0< 2.0< 8.0< 8.0< 10

< 0.001< 0.001< 0.001< 1.0< 2.0< 101620




Page 5 of 8



Lab Sample

Number

Sample

Reference

Sample

NumberDepth (m) Sample Description *

812765 HP01 001 0.20-0.20 Light brown loam and clay with gravel and vegetation.812766 HP02 002 0.10-0.10 Brown loam and clay with vegetation and gravel812767 HP03 003 0.20-0.20 Brown loam and clay with gravel and vegetation.812768 HP04 004 0.20-0.20 Brown clay and loam with vegetation and brick.812769 HP05 005 0.20-0.20 Brown clay and loam with vegetation.812770 HP06 006 0.10-0.10 Brown sandy loam with vegetation and gravel

* These descriptions are only intended to act as a cross check if sample identities are questioned. The major constituent of the sample is intended to act with respect to MCERTS validation. The laboratory is accredited for sand, clay and loam (MCERTS) soil types. Data for unaccredited types of solid should be interpreted with care.

Stone content of a sample is calculated as the % weight of the stones not passing a 10 mm sieve. Results are not corrected for stone content.




Page 6 of 8



Water matrix abbreviations: Surface Water (SW) Potable Water (PW) Ground Water (GW) Process Water (PrW)

Analytical Test Name Analytical Method Description Analytical Method ReferenceMethod

number

Wet / Dry

Analysis

Accreditation

Status

Asbestos identification in soil Asbestos Identification with the use of polarised light microscopy in conjunction with disperion staining techniques.

In house method based on HSG 248 A001-PL D ISO 17025

Boron, water soluble, in soil Determination of water soluble boron in soil by hot water extract followed by ICP-OES.

In-house method based on Second Site Properties version 3

L038-PL D MCERTS

BTEX and MTBE in soil (Monoaromatics)

Determination of BTEX in soil by headspace GC-MS.

In-house method based on USEPA8260 L073B-PL W MCERTS

Complex Cyanide in soil Determination of complex cyanide by calculation. In-house method based on Examination of Water and Wastewater 20th Edition: Clesceri, Greenberg & Eaton (Skalar)

L080-PL W MCERTS

D.O. for Gravimetric Quant if Screen/ID positive

Dependent option for Gravimetric Quant if Screen/ID positive scheduled.

In house asbestos methods A001 & A006. A006-PL D NONE

Fraction of Organic Carbon in soil Determination of fraction of organic carbon in soil by oxidising with potassium dichromate followed by titration with iron (II) sulphate.

In-house method based on BS1377 Part 3, 1990, Chemical and Electrochemical Tests

L023-PL D NONE

Free cyanide in soil Determination of free cyanide by distillation followed by colorimetry.

In-house method based on Examination of Water and Wastewater 20th Edition: Clesceri, Greenberg & Eaton (Skalar)

L080-PL W MCERTS

Hexavalent chromium in soil Determination of hexavalent chromium in soil by extraction in water then by acidification, addition of 1,5 diphenylcarbazide followed by colorimetry.

In-house method L080-PL W MCERTS

Metals in soil by ICP-OES Determination of metals in soil by aqua-regia digestion followed by ICP-OES.

In-house method based on MEWAM 2006 Methods for the Determination of Metals in Soil.

L038-PL D MCERTS

Moisture Content Moisture content, determined gravimetrically. In-house method based on BS1377 Part 2, 1990, Chemical and Electrochemical Tests

L019-UK/PL W NONE

Monohydric phenols in soil Determination of phenols in soil by extraction with sodium hydroxide followed by distillation followed by colorimetry.

In-house method based on Examination of Water and Wastewater 20th Edition: Clesceri, Greenberg & Eaton (skalar)

L080-PL W MCERTS

pH in soil (automated) Determination of pH in soil by addition of water followed by automated electrometric measurement.

In-house method based on BS1377 Part 3, 1990, Chemical and Electrochemical Tests

L099-PL D MCERTS

Speciated EPA-16 PAHs in soil Determination of PAH compounds in soil by extraction in dichloromethane and hexane followed by GC-MS with the use of surrogate and internal standards.

In-house method based on USEPA 8270 L064-PL D MCERTS

Stones content of soil Standard preparation for all samples unless otherwise detailed. Gravimetric determination of stone > 10 mm as % dry weight.

In-house method based on British Standard Methods and MCERTS requirements.

L019-UK/PL D NONE

Sulphate, water soluble, in soil (16hr extraction)

Determination of water soluble sulphate by ICP-OES. Results reported directly (leachate equivalent) and corrected for extraction ratio (soil equivalent).

In-house method based on BS1377 Part 3, 1990, Chemical and Electrochemical Tests, 2:1 water:soil extraction, analysis by ICP-OES.

L038-PL D MCERTS

Total cyanide in soil Determination of total cyanide by distillation followed by colorimetry.

In-house method based on Examination of Water and Wastewater 20th Edition: Clesceri, Greenberg & Eaton (Skalar)

L080-PL W MCERTS

Total Sulphur in soil Determination of total sulphur in soil by extraction with aqua-regia, potassium bromide/bromate followed by ICP-OES.

In-house method based on BS1377 Part 3, 1990, and MEWAM 2006 Methods for the Determination of Metals in Soil

L038-PL D MCERTS




Page 7 of 8





number

Wet / Dry

Analysis

Accreditation

Status

TPH Banding in Soil by FID Determination of hexane extractable hydrocarbons in soil by GC-FID.

In-house method, TPH with carbon banding.

L076-PL W MCERTS

TPH2 (Soil) Determination of hydrocarbons C6-C10 by headspace GC-MS.

In-house method based on USEPA8260 L088-PL W MCERTS

TPHCWG (Soil) Determination of hexane extractable hydrocarbons in soil by GC-MS/GC-FID.

In-house method L088/76-PL W MCERTS

For method numbers ending in 'UK' analysis have been carried out in our laboratory in the United Kingdom.

For method numbers ending in 'PL' analysis have been carried out in our laboratory in Poland.

Soil analytical results are expressed on a dry weight basis. Where analysis is carried out on as-received the results obtained are multiplied by a moisture

correction factor that is determined gravimetrically using the moisture content which is carried out at a maximum of 30oC.




Page 8 of 8




Page 1 of 10

i2 Analytical Telephone: 01923 225404

7 Woodshots Meadow Fax: 01923 237404Croxley Green Business Park email:[email protected]

Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)

Solid Waste Analysis

TOC (%)** 1.5 3% 5% 6%

Loss on Ignition (%) ** 7.0 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** 0.042 1 -- --

Mineral Oil (mg/kg) 23 500 -- --

Total PAH (WAC-17) (mg/kg) 9.7 100 -- --

pH (units)** 7.8 -- >6 --

Acid Neutralisation Capacity (mol / kg) 11 -- To be evaluated To be evaluated

Arsenic * 0.0025 0.0210 0.5 2 25

Barium * 0.0128 0.107 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0019 0.016 0.5 10 70

Copper * 0.0067 0.056 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0026 0.0215 0.5 10 30

Nickel * < 0.0003 < 0.0030 0.4 10 40

Lead * 0.0020 0.016 0.5 10 50

Antimony * 0.0031 0.026 0.06 0.7 5

Selenium * 0.0042 < 0.040 0.1 0.5 7

Zinc * 0.0055 0.046 4 50 200

Chloride * 1.2 10 800 4000 25000

Fluoride 0.91 7.6 10 150 500

Sulphate * 11 89 1000 20000 50000

TDS 73 610 4000 60000 100000

Phenol Index (Monhydric Phenols) * < 0.010 < 0.10 1 - -

Leach Test Information

Stone Content (%) < 0.1

Sample Mass (kg) 1.5

Dry Matter (%) 91

Moisture (%) 8.7

Waste Acceptance Criteria Analytical Results17-59716

BWBCONSULT

Edgar Mobbs Way

Lab Reference (Sample Number) 812771 / 812772

Landfill Waste Acceptance Criteria

Limits

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

Hazardous

Waste Landfill

HP01 001

0.20-0.20

800 1000

Eluate Analysis

(BS EN 12457 - 2 preparation utilising end over end leaching

procedure)

10:1 10:01Limit values for compliance leaching test

using BS EN 12457-2 at L/S 10 l/kg (mg/kg)

mg/l mg/kg

DOC 6.06 50.6 500

Results are expressed on a dry weight basis, after correction for moisture content where applicable. *= UKAS accredited (liquid eluate analysis only)

Stated limits are for guidance only and i2 cannot be held responsible for any discrepencies with current legislation ** = MCERTS accrediited

Landfill WAC analysis (specifically leaching test results) must not be used for hazardous waste classification purposes as defined by the Waste (England and Wales) Regulations 2011 (as

amended) and EA Guidance WM3.

This analysis is only applicable for landfill acceptance criteria (The Environmental Permitting (England and Wales) Regulations) and does not give any indication as to whether a waste may be

hazardous or non-hazardous.




Page 2 of 10



Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)


TOC (%)** 4.2 3% 5% 6%

Loss on Ignition (%) ** 12.9 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** < 0.007 1 -- --

Mineral Oil (mg/kg) < 10 500 -- --


pH (units)** 7.6 -- >6 --

Acid Neutralisation Capacity (mol / kg) 8.3 -- To be evaluated To be evaluated

Arsenic * < 0.0011 < 0.0110 0.5 2 25

Barium * 0.0197 0.163 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0045 0.037 0.5 10 70

Copper * 0.012 0.10 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0015 0.0128 0.5 10 30

Nickel * 0.0012 0.010 0.4 10 40

Lead * 0.0060 0.050 0.5 10 50

Antimony * < 0.0017 < 0.017 0.06 0.7 5

Selenium * < 0.0040 < 0.040 0.1 0.5 7

Zinc * 0.0095 0.078 4 50 200

Chloride * 2.8 23 800 4000 25000

Fluoride 0.42 3.5 10 150 500

Sulphate * 3.6 30 1000 20000 50000

TDS 94 770 4000 60000 100000





Dry Matter (%) 82

Moisture (%) 18


BWBCONSULT

Edgar Mobbs Way



Limits

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

Hazardous

Waste Landfill

HP02 002

0.10-0.10

800 1000

Eluate Analysis


procedure)



mg/l mg/kg

DOC 8.49 70.2 500










Page 3 of 10



Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)


TOC (%)** 4.0 3% 5% 6%

Loss on Ignition (%) ** 19.5 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** < 0.007 1 -- --

Mineral Oil (mg/kg) 12 500 -- --


pH (units)** 7.5 -- >6 --


Arsenic * < 0.0011 < 0.0110 0.5 2 25

Barium * 0.0392 0.341 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0047 0.041 0.5 10 70

Copper * 0.020 0.17 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0027 0.0239 0.5 10 30

Nickel * 0.0017 0.015 0.4 10 40

Lead * 0.0066 0.058 0.5 10 50

Antimony * < 0.0017 < 0.017 0.06 0.7 5

Selenium * < 0.0040 < 0.040 0.1 0.5 7

Zinc * 0.011 0.094 4 50 200

Chloride * 2.5 22 800 4000 25000

Fluoride 0.40 3.5 10 150 500

Sulphate * 4.9 42 1000 20000 50000

TDS 94 820 4000 60000 100000





Dry Matter (%) 84

Moisture (%) 16


BWBCONSULT

Edgar Mobbs Way



Limits

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

Hazardous

Waste Landfill

HP03 003

0.20-0.20

800 1000

Eluate Analysis


procedure)



mg/l mg/kg

DOC 9.83 85.7 500










Page 4 of 10



Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)


TOC (%)** 2.0 3% 5% 6%

Loss on Ignition (%) ** 10.8 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** < 0.007 1 -- --



pH (units)** 8.0 -- >6 --


Arsenic * 0.0011 < 0.0110 0.5 2 25

Barium * 0.0287 0.247 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0053 0.046 0.5 10 70

Copper * 0.012 0.11 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0020 0.0169 0.5 10 30

Nickel * 0.0019 0.017 0.4 10 40

Lead * 0.0064 0.055 0.5 10 50

Antimony * 0.0020 0.018 0.06 0.7 5

Selenium * < 0.0040 < 0.040 0.1 0.5 7

Zinc * 0.015 0.13 4 50 200

Chloride * 2.1 18 800 4000 25000

Fluoride 0.59 5.1 10 150 500

Sulphate * 5.2 45 1000 20000 50000

TDS 82 710 4000 60000 100000





Dry Matter (%) 82

Moisture (%) 18


BWBCONSULT

Edgar Mobbs Way



Limits

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

Hazardous

Waste Landfill

HP04 004

0.20-0.20

800 1000

Eluate Analysis


procedure)



mg/l mg/kg

DOC 7.02 60.5 500










Page 5 of 10



Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)


TOC (%)** 1.6 3% 5% 6%

Loss on Ignition (%) ** 12.9 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** < 0.007 1 -- --



pH (units)** 8.0 -- >6 --


Arsenic * < 0.0011 < 0.0110 0.5 2 25

Barium * 0.0171 0.146 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0018 0.016 0.5 10 70

Copper * 0.0068 0.058 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0035 0.0302 0.5 10 30

Nickel * 0.0008 0.0069 0.4 10 40

Lead * 0.0040 0.034 0.5 10 50

Antimony * < 0.0017 < 0.017 0.06 0.7 5

Selenium * < 0.0040 < 0.040 0.1 0.5 7

Zinc * 0.0078 0.067 4 50 200

Chloride * 1.3 11 800 4000 25000

Fluoride 0.73 6.2 10 150 500

Sulphate * 3.9 33 1000 20000 50000

TDS 71 610 4000 60000 100000





Dry Matter (%) 79

Moisture (%) 21


BWBCONSULT

Edgar Mobbs Way



Limits

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

Hazardous

Waste Landfill

HP05 005

0.20-0.20

800 1000

Eluate Analysis


procedure)



mg/l mg/kg

DOC 5.25 44.8 500










Page 6 of 10



Watford, WD18 8YS

Report No:

Client:

Location

Sampling Date

Sample ID

Depth (m)


TOC (%)** 2.1 3% 5% 6%

Loss on Ignition (%) ** 7.9 -- -- 10%

BTEX (µg/kg) ** < 10 6000 -- --

Sum of PCBs (mg/kg) ** < 0.007 1 -- --



pH (units)** 7.4 -- >6 --


Arsenic * < 0.0011 < 0.0110 0.5 2 25

Barium * 0.0142 0.117 20 100 300

Cadmium * < 0.0001 < 0.0008 0.04 1 5

Chromium * 0.0028 0.023 0.5 10 70

Copper * 0.0084 0.069 2 50 100

Mercury * < 0.0005 < 0.0050 0.01 0.2 2

Molybdenum * 0.0011 0.0095 0.5 10 30

Nickel * < 0.0003 < 0.0030 0.4 10 40

Lead * 0.0037 0.031 0.5 10 50

Antimony * < 0.0017 < 0.017 0.06 0.7 5

Selenium * < 0.0040 < 0.040 0.1 0.5 7

Zinc * 0.0067 0.056 4 50 200

Chloride * 1.9 15 800 4000 25000

Fluoride 0.48 4.0 10 150 500

Sulphate * 3.1 26 1000 20000 50000

TDS 59 480 4000 60000 100000





Dry Matter (%) 90

Moisture (%) 10



Limits


Hazardous

Waste Landfill

HP06 006

0.10-0.10

BWBCONSULT

Edgar Mobbs Way

mg/l

06/09/2017

Inert Waste

Landfill

Stable Non-

reactive

HAZARDOUS

waste in non-

hazardous

Landfill

500 800 1000

Eluate Analysis


procedure)



mg/kg

DOC 6.16 51.0










Page 7 of 10



Lab Sample

Number

Sample

Reference

Sample

NumberDepth (m) Sample Description *

812771 HP01 001 0.20-0.20 Light brown loam and clay with gravel and vegetation.

812773 HP02 002 0.10-0.10 Brown loam and clay with vegetation.

812775 HP03 003 0.20-0.20 Brown loam and clay with vegetation and gravel

812777 HP04 004 0.20-0.20 Brown clay and loam with vegetation and brick.

812779 HP05 005 0.20-0.20 Brown clay and loam with vegetation.

812781 HP06 006 0.10-0.10 Brown sandy loam with vegetation and gravel

* These descriptions are only intended to act as a cross check if sample identities are questioned. The major constituent of the sample is intended to act with respect to MCERTS validation. The

laboratory is accredited for sand, clay and loam (MCERTS) soil types. Data for unaccredited types of solid should be interpreted with care.

Stone content of a sample is calculated as the % weight of the stones not passing a 10 mm sieve. Results are not corrected for stone content.




Page 8 of 10





number

Wet / Dry

Analysis

Accreditation

Status

Acid neutralisation capacity of soil Determination of acid neutralisation capacity by

addition of acid or alkali followed by electronic

probe.

In-house method based on Guidance an

Sampling and Testing of Wastes to Meet

Landfill Waste Acceptance""

L046-UK W NONE

BS EN 12457-2 (10:1) Leachate Prep 10:1 (as recieved, moisture adjusted) end over end

extraction with water for 24 hours. Eluate filtered

prior to analysis.

In-house method based on BSEN12457-2. L043-PL W NONE

BTEX in soil (Monoaromatics) Determination of BTEX in soil by headspace GC-MS. In-house method based on USEPA8260 L073B-PL W MCERTS

Chloride 10:1 WAC Determination of Chloride colorimetrically by

discrete analyser.

In house based on MEWAM Method ISBN

0117516260.

L082-PL W ISO 17025

Dissolved organic carbon 10:1 WAC Determination of dissolved inorganic carbon in

leachate by TOC/DOC NDIR Analyser.

In-house method based on Examination of

Water and Wastewater 20th Edition:

Clesceri, Greenberg & Eaton

L037-PL W NONE

Fluoride 10:1 WAC Determination of fluoride in leachate by 1:1ratio

with a buffer solution followed by Ion Selective

Electrode.

In-house method based on Use of Total

Ionic Strength Adjustment Buffer for

Electrode Determination"

L033B-PL W ISO 17025

Loss on ignition of soil @ 450oC Determination of loss on ignition in soil by

gravimetrically with the sample being ignited in a

muffle furnace.

In-house method based on BS1377 Part 3,

1990, Chemical and Electrochemical Tests

L047-PL D MCERTS

Metals in leachate by ICP-OES Determination of metals in leachate by acidification

followed by ICP-OES.

In-house method based on MEWAM 2006

Methods for the Determination of Metals in

Soil""

L039-PL W ISO 17025

Mineral Oil (Soil) C10 - C40 Determination of mineral oil fraction extractable

hydrocarbons in soil by GC-MS/GC-FID.

in-house method L076-PL D NONE

Moisture Content Moisture content, determined gravimetrically. In-house method based on BS1377 Part 2,


L019-UK/PL W NONE

Monohydric phenols 10:1 WAC Determination of phenols in leachate by distillation

followed by colorimetry.




L080-PL W ISO 17025




Page 9 of 10





number

Wet / Dry

Analysis

Accreditation

Status

PCB's By GC-MS in soil Determination of PCB by extraction with acetone

and hexane followed by GC-MS.

In-house method based on USEPA 8082 L027-PL D MCERTS

pH in soil Determination of pH in soil by addition of water

followed by electrometric measurement.



L005-PL W MCERTS

Speciated WAC-17 PAHs in soil Determination of PAH compounds in soil by

extraction in dichloromethane and hexane followed

by GC-MS with the use of surrogate and internal

standards.

In-house method based on USEPA 8270 L064-PL D NONE

Stones content of soil Standard preparation for all samples unless

otherwise detailed. Gravimetric determination of

stone > 10 mm as % dry weight.

In-house method based on British Standard

Methods and MCERTS requirements.

L019-UK/PL D NONE

Sulphate 10:1 WAC Determination of sulphate in leachate by ICP-OES In-house method based on MEWAM 1986

Methods for the Determination of Metals in

Soil""

L039-PL W ISO 17025

Total dissolved solids 10:1 WAC Determination of total dissolved solids in water by

electrometric measurement.




L004-PL W NONE

Total organic carbon (Automated) in

soil

Determination of organic matter in soil by oxidising

with potassium dichromate followed by titration with

iron (II) sulphate.


1990, Chemical and Electrochemical Tests""

L009-PL D MCERTS

For method numbers ending in 'UK' analysis have been carried out in our laboratory in the United Kingdom.

For method numbers ending in 'PL' analysis have been carried out in our laboratory in Poland.

Soil analytical results are expressed on a dry weight basis. Where analysis is carried out on as-received the results obtained are multiplied by a moisture

correction factor that is determined gravimetrically using the moisture content which is carried out at a maximum of 30oC.




Page 10 of 10

of 6

APPENDIX 2

HAZWASTE ONLINE ASSESSMENT

www.hazwasteonline.com 5U925-EUQT3-SSN68 Page 1 of 23

Waste Classification Report

5U925-EUQT3-SSN68

Job name

NTH2325 Edgar Mobbs

Description/Comments

Topsoil strip waste assessment

Project

NTH2325

Site

Edgar Mobbs Way

Waste Stream Template

BWB Contaminated Land Suite WM3

Classified by

Name:Richard RobinsonDate:28/09/2017 09:42:46 UTCTelephone:0115 924 1100

Company:BWB Consulting Ltd5th FloorWaterfront House, Station StreetNottinghamNG2 3DQ

Report

Created by: Richard RobinsonCreated date: 28/09/2017 09:42 UTC

Job summary# Sample Name Depth [m] Classification Result Hazard properties Page1 HP01 0.20-0.20 Non Hazardous 2

2 HP02 0.10-0.10 Non Hazardous 5





Appendices PageAppendix A: Classifier defined and non CLP determinands 20Appendix B: Rationale for selection of metal species 22Appendix C: Version 22

Report created by Richard Robinson on 28/09/2017

Page 2 of 23 5U925-EUQT3-SSN68 www.hazwasteonline.com

Classification of sample: HP01

Non Hazardous WasteClassified as 17 05 04

in the List of Waste

Sample details

Sample Name:HP01Sample Depth:0.20-0.20 mMoisture content:8.7%(no correction)

LoW Code:Chapter: 17: Construction and Demolition Wastes (including excavated soil

from contaminated sites)Entry: 17 05 04 (Soil and stones other than those mentioned in 17 05

03)

Hazard properties

None identified

Determinands

Moisture content: 8.7% No Moisture Correction applied (MC)

#Determinand

CLP

Not

e

User entered dataConv.Factor

Compound conc.Classification

value

MC

App

lied

Conc. NotUsed

CLP index number EC Number CAS Number

1confirm TPH has NOT arisen from diesel or petrol

2arsenic { arsenic trioxide }

21 mg/kg 1.32 27.727 mg/kg 0.00277 %033-003-00-0 215-481-4 1327-53-3

3beryllium { beryllium oxide }

1.5 mg/kg 2.775 4.163 mg/kg 0.000416 %004-003-00-8 215-133-1 1304-56-9

4

boron { boron tribromide/trichloride/trifluoride(combined) }

1.8 mg/kg 13.43 24.174 mg/kg 0.00242 % 10294-33-4,10294-34-5,7637-07-2

5cadmium { cadmium sulfide }

1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6

6 chromium { chromium(III) oxide } 55 mg/kg 1.462 80.386 mg/kg 0.00804 % 215-160-9 1308-38-9

7 copper { dicopper oxide; copper (I) oxide } 31 mg/kg 1.126 34.903 mg/kg 0.00349 %029-002-00-X 215-270-7 1317-39-1

8lead { lead chromate }

1 82 mg/kg 1.56 127.905 mg/kg 0.0082 %082-004-00-2 231-846-0 7758-97-6

9mercury { mercury dichloride }

<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7

10nickel { nickel dihydroxide }

33 mg/kg 1.579 52.123 mg/kg 0.00521 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11

selenium { selenium compounds with the exception ofcadmium sulphoselenide and those specified elsewherein this Annex } <1 mg/kg 2.554 <2.554 mg/kg <0.000255 % <LOD

034-002-00-8

12zinc { zinc chromate }

140 mg/kg 2.774 388.381 mg/kg 0.0388 %024-007-00-3

13pH

7.9 pH 7.9 pH 7.9 pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14

cyanides { salts of hydrogen cyanide with theexception of complex cyanides such as ferrocyanides,ferricyanides and mercuric oxycyanide and thosespecified elsewhere in this Annex }

<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5

15TPH (C6 to C40) petroleum group

97 mg/kg 97 mg/kg 0.0097 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

0.17 mg/kg 0.17 mg/kg 0.000017 % 204-371-1 120-12-7

23benzo[a]anthracene

0.92 mg/kg 0.92 mg/kg 0.000092 %601-033-00-9 200-280-6 56-55-3

24benzo[a]pyrene; benzo[def]chrysene

1 mg/kg 1 mg/kg 0.0001 %601-032-00-3 200-028-5 50-32-8

25benzo[b]fluoranthene

1.5 mg/kg 1.5 mg/kg 0.00015 %601-034-00-4 205-911-9 205-99-2

26benzo[ghi]perylene

0.59 mg/kg 0.59 mg/kg 0.000059 % 205-883-8 191-24-2

27benzo[k]fluoranthene

0.48 mg/kg 0.48 mg/kg 0.000048 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.73 mg/kg 0.73 mg/kg 0.000073 %601-048-00-0 205-923-4 218-01-9

29dibenz[a,h]anthracene

0.18 mg/kg 0.18 mg/kg 0.000018 %601-041-00-2 200-181-8 53-70-3

30fluoranthene

1.3 mg/kg 1.3 mg/kg 0.00013 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7

32indeno[123-cd]pyrene

0.65 mg/kg 0.65 mg/kg 0.000065 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.6 mg/kg 0.6 mg/kg 0.00006 % 201-581-5 85-01-8

35pyrene

1.2 mg/kg 1.2 mg/kg 0.00012 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.081 %



KeyUser supplied data

Determinand values ignored for classification, see column 'Conc. Not Used' for reason

Determinand defined or amended by HazWasteOnline (see Appendix A)

Speciated Deteminand - Unless the Determinand is Note 1, the Conversion Factor is used to calculate the compoundconcentration

<LOD Below limit of detectionCLP: Note 1 Only the metal concentration has been used for classification

Supplementary Hazardous Property Information

HP 3(i) on Flam. Liq. 1; H224, Flam. Liq. 2; H225, Flam. Liq. 3; H226: Force this Hazardous property to non hazardous becauseNo sources of volatile contamination identified.






Sample details

Sample Name:HP02Sample Depth:0.10-0.10 mMoisture content:11%(no correction)



03)

Hazard properties

None identified

Determinands

Moisture content: 11% No Moisture Correction applied (MC)

#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed




20 mg/kg 1.32 26.407 mg/kg 0.00264 %033-003-00-0 215-481-4 1327-53-3


1.2 mg/kg 2.775 3.33 mg/kg 0.000333 %004-003-00-8 215-133-1 1304-56-9

4


1.5 mg/kg 13.43 20.145 mg/kg 0.00201 % 10294-33-4,10294-34-5,7637-07-2


1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6




1 47 mg/kg 1.56 73.311 mg/kg 0.0047 %082-004-00-2 231-846-0 7758-97-6


<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7


26 mg/kg 1.579 41.067 mg/kg 0.00411 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11


034-002-00-8


94 mg/kg 2.774 260.77 mg/kg 0.0261 %024-007-00-3

13pH

7.5 pH 7.5 pH 7.5 pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


46 mg/kg 46 mg/kg 0.0046 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 204-371-1 120-12-7


0.36 mg/kg 0.36 mg/kg 0.000036 %601-033-00-9 200-280-6 56-55-3


0.46 mg/kg 0.46 mg/kg 0.000046 %601-032-00-3 200-028-5 50-32-8


0.65 mg/kg 0.65 mg/kg 0.000065 %601-034-00-4 205-911-9 205-99-2


0.23 mg/kg 0.23 mg/kg 0.000023 % 205-883-8 191-24-2


0.17 mg/kg 0.17 mg/kg 0.000017 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.3 mg/kg 0.3 mg/kg 0.00003 %601-048-00-0 205-923-4 218-01-9


<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-041-00-2 200-181-8 53-70-3

30fluoranthene

0.49 mg/kg 0.49 mg/kg 0.000049 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7


0.27 mg/kg 0.27 mg/kg 0.000027 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.2 mg/kg 0.2 mg/kg 0.00002 % 201-581-5 85-01-8

35pyrene

0.47 mg/kg 0.47 mg/kg 0.000047 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.0554 %






Sample details




03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed




29 mg/kg 1.32 38.289 mg/kg 0.00383 %033-003-00-0 215-481-4 1327-53-3


2.1 mg/kg 2.775 5.828 mg/kg 0.000583 %004-003-00-8 215-133-1 1304-56-9

4


2.7 mg/kg 13.43 36.261 mg/kg 0.00363 % 10294-33-4,10294-34-5,7637-07-2


1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6




1 200 mg/kg 1.56 311.963 mg/kg 0.02 %082-004-00-2 231-846-0 7758-97-6


<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7


34 mg/kg 1.579 53.703 mg/kg 0.00537 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11


034-002-00-8


240 mg/kg 2.774 665.795 mg/kg 0.0666 %024-007-00-3

13pH

8.1 pH 8.1 pH 8.1 pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


94 mg/kg 94 mg/kg 0.0094 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

0.13 mg/kg 0.13 mg/kg 0.000013 % 204-371-1 120-12-7


0.72 mg/kg 0.72 mg/kg 0.000072 %601-033-00-9 200-280-6 56-55-3


0.87 mg/kg 0.87 mg/kg 0.000087 %601-032-00-3 200-028-5 50-32-8


1.2 mg/kg 1.2 mg/kg 0.00012 %601-034-00-4 205-911-9 205-99-2


0.47 mg/kg 0.47 mg/kg 0.000047 % 205-883-8 191-24-2


0.43 mg/kg 0.43 mg/kg 0.000043 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.62 mg/kg 0.62 mg/kg 0.000062 %601-048-00-0 205-923-4 218-01-9


0.15 mg/kg 0.15 mg/kg 0.000015 %601-041-00-2 200-181-8 53-70-3

30fluoranthene

1 mg/kg 1 mg/kg 0.0001 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7


0.51 mg/kg 0.51 mg/kg 0.000051 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.34 mg/kg 0.34 mg/kg 0.000034 % 201-581-5 85-01-8

35pyrene

0.96 mg/kg 0.96 mg/kg 0.000096 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.128 %






Sample details




03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed




21 mg/kg 1.32 27.727 mg/kg 0.00277 %033-003-00-0 215-481-4 1327-53-3


1.5 mg/kg 2.775 4.163 mg/kg 0.000416 %004-003-00-8 215-133-1 1304-56-9

4


1.9 mg/kg 13.43 25.517 mg/kg 0.00255 % 10294-33-4,10294-34-5,7637-07-2


1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6




1 110 mg/kg 1.56 171.58 mg/kg 0.011 %082-004-00-2 231-846-0 7758-97-6


<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7


31 mg/kg 1.579 48.964 mg/kg 0.0049 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11


034-002-00-8


150 mg/kg 2.774 416.122 mg/kg 0.0416 %024-007-00-3

13pH

8.1 pH 8.1 pH 8.1 pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


21 mg/kg 21 mg/kg 0.0021 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

0.1 mg/kg 0.1 mg/kg 0.00001 % 204-371-1 120-12-7


0.68 mg/kg 0.68 mg/kg 0.000068 %601-033-00-9 200-280-6 56-55-3


0.74 mg/kg 0.74 mg/kg 0.000074 %601-032-00-3 200-028-5 50-32-8


1.2 mg/kg 1.2 mg/kg 0.00012 %601-034-00-4 205-911-9 205-99-2


0.39 mg/kg 0.39 mg/kg 0.000039 % 205-883-8 191-24-2


0.3 mg/kg 0.3 mg/kg 0.00003 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.6 mg/kg 0.6 mg/kg 0.00006 %601-048-00-0 205-923-4 218-01-9


0.12 mg/kg 0.12 mg/kg 0.000012 %601-041-00-2 200-181-8 53-70-3

30fluoranthene

1 mg/kg 1 mg/kg 0.0001 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7


0.45 mg/kg 0.45 mg/kg 0.000045 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.33 mg/kg 0.33 mg/kg 0.000033 % 201-581-5 85-01-8

35pyrene

0.96 mg/kg 0.96 mg/kg 0.000096 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.0775 %






Sample details




03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed




19 mg/kg 1.32 25.086 mg/kg 0.00251 %033-003-00-0 215-481-4 1327-53-3


1.8 mg/kg 2.775 4.996 mg/kg 0.0005 %004-003-00-8 215-133-1 1304-56-9

4


2 mg/kg 13.43 26.86 mg/kg 0.00269 % 10294-33-4,10294-34-5,7637-07-2


1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6




1 93 mg/kg 1.56 145.063 mg/kg 0.0093 %082-004-00-2 231-846-0 7758-97-6


<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7


31 mg/kg 1.579 48.964 mg/kg 0.0049 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11


034-002-00-8


180 mg/kg 2.774 499.346 mg/kg 0.0499 %024-007-00-3

13pH

8 pH 8 pH 8pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


21 mg/kg 21 mg/kg 0.0021 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 204-371-1 120-12-7


0.49 mg/kg 0.49 mg/kg 0.000049 %601-033-00-9 200-280-6 56-55-3


0.5 mg/kg 0.5 mg/kg 0.00005 %601-032-00-3 200-028-5 50-32-8


0.67 mg/kg 0.67 mg/kg 0.000067 %601-034-00-4 205-911-9 205-99-2


0.28 mg/kg 0.28 mg/kg 0.000028 % 205-883-8 191-24-2


0.27 mg/kg 0.27 mg/kg 0.000027 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.32 mg/kg 0.32 mg/kg 0.000032 %601-048-00-0 205-923-4 218-01-9


0.1 mg/kg 0.1 mg/kg 0.00001 %601-041-00-2 200-181-8 53-70-3

30fluoranthene

0.66 mg/kg 0.66 mg/kg 0.000066 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7


0.3 mg/kg 0.3 mg/kg 0.00003 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.28 mg/kg 0.28 mg/kg 0.000028 % 201-581-5 85-01-8

35pyrene

0.61 mg/kg 0.61 mg/kg 0.000061 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.0855 %






Sample details




03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed




25 mg/kg 1.32 33.008 mg/kg 0.0033 %033-003-00-0 215-481-4 1327-53-3


1.1 mg/kg 2.775 3.053 mg/kg 0.000305 %004-003-00-8 215-133-1 1304-56-9

4


1.3 mg/kg 13.43 17.459 mg/kg 0.00175 % 10294-33-4,10294-34-5,7637-07-2


1 <0.2 mg/kg 1.285 <0.257 mg/kg <0.00002 % <LOD048-010-00-4 215-147-8 1306-23-6




1 58 mg/kg 1.56 90.469 mg/kg 0.0058 %082-004-00-2 231-846-0 7758-97-6


<0.3 mg/kg 1.353 <0.406 mg/kg <0.0000406 % <LOD080-010-00-X 231-299-8 7487-94-7


23 mg/kg 1.579 36.328 mg/kg 0.00363 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

11


034-002-00-8


93 mg/kg 2.774 257.996 mg/kg 0.0258 %024-007-00-3

13pH

7.5 pH 7.5 pH 7.5 pH PH



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


14


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


30 mg/kg 30 mg/kg 0.003 % TPH

16benzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-020-00-8 200-753-7 71-43-2

17ethylbenzene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-023-00-4 202-849-4 100-41-4

18toluene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-021-00-3 203-625-9 108-88-3

19

xylene

<1 mg/kg <1 mg/kg <0.0001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

20acenaphthene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-469-6 83-32-9

21acenaphthylene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 205-917-1 208-96-8

22anthracene

0.14 mg/kg 0.14 mg/kg 0.000014 % 204-371-1 120-12-7


0.74 mg/kg 0.74 mg/kg 0.000074 %601-033-00-9 200-280-6 56-55-3


0.88 mg/kg 0.88 mg/kg 0.000088 %601-032-00-3 200-028-5 50-32-8


1.3 mg/kg 1.3 mg/kg 0.00013 %601-034-00-4 205-911-9 205-99-2


0.43 mg/kg 0.43 mg/kg 0.000043 % 205-883-8 191-24-2


0.36 mg/kg 0.36 mg/kg 0.000036 %601-036-00-5 205-916-6 207-08-9

28chrysene

0.62 mg/kg 0.62 mg/kg 0.000062 %601-048-00-0 205-923-4 218-01-9


0.13 mg/kg 0.13 mg/kg 0.000013 %601-041-00-2 200-181-8 53-70-3

30fluoranthene

1.1 mg/kg 1.1 mg/kg 0.00011 % 205-912-4 206-44-0

31fluorene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD 201-695-5 86-73-7


0.5 mg/kg 0.5 mg/kg 0.00005 % 205-893-2 193-39-5

33naphthalene

<0.05 mg/kg <0.05 mg/kg <0.000005 % <LOD601-052-00-2 202-049-5 91-20-3

34phenanthrene

0.42 mg/kg 0.42 mg/kg 0.000042 % 201-581-5 85-01-8

35pyrene

1 mg/kg 1 mg/kg 0.0001 % 204-927-3 129-00-0

36phenol

<1 mg/kg <1 mg/kg <0.0001 % <LOD604-001-00-2 203-632-7 108-95-2

Total: 0.0532 %



Appendix A: Classifier defined and non CLP determinands

confirm TPH has NOT arisen from diesel or petrol

Description/Comments: Chapter 3, section 4b requires a positive confirmation for benzo[a]pyrene to be used as a marker in evaluatingCarc. 1B; H350 (HP 7) and Muta. 1B; H340 (HP 11)Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: None.Hazard Statements: None.

boron tribromide/trichloride/trifluoride (combined) (CAS Number: 10294-33-4, 10294-34-5, 7637-07-2)

Conversion factor: 13.43Description/Comments: Combines the hazard statements and the average of the conversion factors for boron tribromide, borontrichloride and boron trifluorideData source: N/AData source date: 06/08/2015Risk Phrases: R14 , T+ R26/28 , C R34 , C R35Hazard Statements: EUH014 , Acute Tox. 2 H330 , Acute Tox. 2 H300 , Skin Corr. 1A H314 , Skin Corr. 1B H314

chromium(III) oxide (EC Number: 215-160-9, CAS Number: 1308-38-9)

Conversion factor: 1.462Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R20 , R22 , R36 , R37 , R38 , R42 , R43 , R50/53 , R60 , R61Hazard Statements: Acute Tox. 4 H332 , Acute Tox. 4 H302 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Resp. Sens. 1H334 , Skin Sens. 1 H317 , Repr. 1B H360FD , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

dicopper oxide; copper (I) oxide (EC Number: 215-270-7, CAS Number: 1317-39-1)

CLP index number: 029-002-00-XData source: Regulation (EU) 2016/1179 of 19 July 2016 (ATP9)Additional Risk Phrases: N R50/53 , N R50/53 >= 0.25 %Additional Hazard Statement(s): None.Reason for additional Hazards Statement(s)/Risk Phrase(s):10/10/2016 - N R50/53 risk phrase sourced from: WM3 v1 still uses ecotoxic risk phrases10/10/2016 - N R50/53 >= 0.25 % risk phrase sourced from: WM3 v1 still uses ecotoxic risk phrases

pH (CAS Number: PH)

Description/Comments: Appendix C4Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: None.Hazard Statements: None.

salts of hydrogen cyanide with the exception of complex cyanides such as ferrocyanides, ferricyanides and mercuricoxycyanide and those specified elsewhere in this Annex

CLP index number: 006-007-00-5Data source: Commission Regulation (EC) No 790/2009 - 1st Adaptation to Technical Progress for Regulation (EC) No 1272/2008.(ATP1)Additional Risk Phrases: None.Additional Hazard Statement(s): EUH032 >= 0.2 %Reason for additional Hazards Statement(s)/Risk Phrase(s):14/12/2015 - EUH032 >= 0.2 % hazard statement sourced from: WM3, Table C12.2

TPH (C6 to C40) petroleum group (CAS Number: TPH)

Description/Comments: Hazard statements taken from WM3 1st Edition 2015; Risk phrases: WM2 3rd Edition 2013Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: R10 , R45 , R46 , R51/53 , R63 , R65Hazard Statements: Flam. Liq. 3 H226 , Asp. Tox. 1 H304 , STOT RE 2 H373 , Muta. 1B H340 , Carc. 1B H350 , Repr. 2 H361d ,Aquatic Chronic 2 H411



ethylbenzene (EC Number: 202-849-4, CAS Number: 100-41-4)

CLP index number: 601-023-00-4Data source: Commission Regulation (EU) No 605/2014 – 6th Adaptation to Technical Progress for Regulation (EC) No 1272/2008.(ATP6)Additional Risk Phrases: None.Additional Hazard Statement(s): Carc. 2 H351Reason for additional Hazards Statement(s)/Risk Phrase(s):03/06/2015 - Carc. 2 H351 hazard statement sourced from: IARC Group 2B (77) 2000

acenaphthene (EC Number: 201-469-6, CAS Number: 83-32-9)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R36 , R37 , R38 , N R50/53 , N R51/53Hazard Statements: Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410 , AquaticChronic 2 H411

acenaphthylene (EC Number: 205-917-1, CAS Number: 208-96-8)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R22 , R26 , R27 , R36 , R37 , R38Hazard Statements: Acute Tox. 4 H302 , Acute Tox. 1 H330 , Acute Tox. 1 H310 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315

anthracene (EC Number: 204-371-1, CAS Number: 120-12-7)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R36 , R37 , R38 , R43 , N R50/53Hazard Statements: Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Skin Sens. 1 H317 , Aquatic Acute 1 H400 , AquaticChronic 1 H410

benzo[ghi]perylene (EC Number: 205-883-8, CAS Number: 191-24-2)

Description/Comments: Data from C&L Inventory Database; SDS Sigma Aldrich 28/02/2015Data source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 23/07/2015Risk Phrases: N R50/53Hazard Statements: Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

fluoranthene (EC Number: 205-912-4, CAS Number: 206-44-0)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 21/08/2015Risk Phrases: Xn R22 , N R50/53Hazard Statements: Acute Tox. 4 H302 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

fluorene (EC Number: 201-695-5, CAS Number: 86-73-7)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: N R50/53Hazard Statements: Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

indeno[123-cd]pyrene (EC Number: 205-893-2, CAS Number: 193-39-5)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: R40Hazard Statements: Carc. 2 H351

phenanthrene (EC Number: 201-581-5, CAS Number: 85-01-8)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: R22 , R36 , R37 , R38 , R40 , R43 , N R50/53Hazard Statements: Acute Tox. 4 H302 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Carc. 2 H351 , Skin Sens. 1 H317 , Aquatic Acute 1 H400, Aquatic Chronic 1 H410 , Skin Irrit. 2 H315



pyrene (EC Number: 204-927-3, CAS Number: 129-00-0)

Description/Comments: Data from C&L Inventory Database; SDS Sigma Aldrich 2014Data source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 21/08/2015Risk Phrases: Xi R36/37/38 , N R50/53Hazard Statements: Skin Irrit. 2 H315 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

Appendix B: Rationale for selection of metal species

arsenic {arsenic trioxide}

Worst case species based on risk phrases

beryllium {beryllium oxide}


boron {boron tribromide/trichloride/trifluoride (combined)}


cadmium {cadmium sulfide}


chromium {chromium(III) oxide}

No Chromium VI in test results.

copper {dicopper oxide; copper (I) oxide}

Most likely common species

lead {lead chromate}


mercury {mercury dichloride}


nickel {nickel dihydroxide}


selenium {selenium compounds with the exception of cadmium sulphoselenide and those specified elsewhere in this Annex}


zinc {zinc chromate}


cyanides {salts of hydrogen cyanide with the exception of complex cyanides such as ferrocyanides, ferricyanides andmercuric oxycyanide and those specified elsewhere in this Annex}

Worst case species

Appendix C: Version

HazWasteOnline Classification Engine: WM3 1st Edition, May 2015HazWasteOnline Classification Engine Version: 2017.269.3405.6897 (26 Sep 2017)HazWasteOnline Database: 2017.269.3405.6897 (26 Sep 2017)



This classification utilises the following guidance and legislation:WM3 - Waste Classification - May 2015CLP Regulation - Regulation 1272/2008/EC of 16 December 20081st ATP - Regulation 790/2009/EC of 10 August 20092nd ATP - Regulation 286/2011/EC of 10 March 20113rd ATP - Regulation 618/2012/EU of 10 July 20124th ATP - Regulation 487/2013/EU of 8 May 2013Correction to 1st ATP - Regulation 758/2013/EU of 7 August 20135th ATP - Regulation 944/2013/EU of 2 October 20136th ATP - Regulation 605/2014/EU of 5 June 2014WFD Annex III replacement - Regulation 1357/2014/EU of 18 December 2014Revised List of Wastes 2014 - Decision 2014/955/EU of 18 December 20147th ATP - Regulation 2015/1221/EU of 24 July 20158th ATP - Regulation (EU) 2016/918 of 19 May 20169th ATP - Regulation (EU) 2016/1179 of 19 July 201610th ATP - Regulation (EU) 2017/776 of 4 May 2017POPs Regulation 2004 - Regulation 850/2004/EC of 29 April 20041st ATP to POPs Regulation - Regulation 756/2010/EU of 24 August 20102nd ATP to POPs Regulation - Regulation 757/2010/EU of 24 August 2010

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