beech grove rockpile phase 2 letter report draft

�� Beech Grove Redevelopment Commission 806 Main Street Beech Grove, Indiana 46107

PHASE II ENVIRONMENTAL INVESTIGATION REPORT

Beech Grove Rock Pile Site Bellefontaine Street and Garstang Street Beech Grove, Indiana Schneider Job No. 6892.002

March 28, 2008 Date:

Historic Fort Harrison 8901 Otis Avenue Indianapolis, IN 46216-1037

��

�� !��"��#��$�#%�&��'�()��*��(�)��)��+��(�)��)��

��

March 28, 2008 Mr. Terry Dilk Beech Grove Redevelopment Commission 806 Main Street Beech Grove, Indiana 46107 Re: Phase II Environmental Investigation Beech Grove Rock Pile Site Bellefontaine Street and Garstang Street

Beech Grove, Indiana Schneider Project No. 6892.002

Dear Mr. Dilk: In accordance with our proposal dated January 4, 2008, The Schneider

Corporation (Schneider) recently conducted Phase II environmental sampling

activities at the Rock Pile Site located southwest of the intersection of

Bellefontaine Street and Garstang Street in Beech Grove, Indiana (see

Attachment A for a site vicinity map). The scope of the Phase II sampling

activities was designed to investigate potential groundwater and soil impacts to

the subject site associated with recognized environmental conditions (RECs)

identified at the site during the completion of a Phase I Environmental Site

Assessment (ESA) for the property (ESA report dated February 11, 2008). The

purpose of this letter report is to present the findings of our recent Phase II site

sampling activities.

Background Site Information

The subject property, referred to as the Rock Pile Site, is approximately seven

(7) acres in size and is undeveloped with no building structures, though several

large piles of crushed rocks are currently present at the site. The following two

recognized environmental conditions (i.e., evidence of a past, existing, or a

material threat of a future release of hazardous substances or petroleum

products) were identified at the site during the performance of the Phase I

Environmental Site Assessment (ESA) for the site:

��

��

��

��

�� !��"��

#��$�#%�&��

,��'��)(�)��

�

��

-"��

.�.�/�01��2�3�(��

1"��.�

!��$�#%�&��(�

�

��

��/�%�2�4��1��

1"��(��

5��6��$�#%�&�(��

�

��

��5��"��7��

1"��-�'.��

4��$�#%�&�()�

�

��

�((�8��-�"��

1"��

8��9��3��$�#%�&)��

�

�

��

��

�.(��!��:��

1"��

!6��$�#!�.��

�

�

��

� ��

��!��2��-�"��

5��$�%5��)(�

�

�

�!��!""!!�

��

��&�;��6��*��7��

1"��(�

%��$�,%�()��

��

��

• Limited environmental investigation activities were conducted at the study site

in 1992 and 1993 on behalf of former prospective purchasers of the site.

Hydrocarbon contaminated fill material was identified in 1992 during the

completion of geotechnical soil borings at the site. Sampling of the fill material

identified the presence of several polynuclear aromatic hydrocarbons (referred

to as PAHs or by the synonym, PNAs). Subsequent site investigation work

conducted in 1993 reportedly confirmed the presence of PAHs in darkly stained

shallow fill material present at the site. Up to 1,000 cubic yards of PAH

contaminated fill material was estimated to be present at the study site.

• Three (3) Leaking Underground Storage Tank (LUST) sites that have reported

soil and groundwater impacts and are actively undergoing investigation and/or

remediation are located within 1/16th mile of the study site. Due to their close

proximity to the study site, it is possible that the groundwater quality of the

study site has been adversely impacted by these sites.

Scope of Phase II Investigation

The scope of the Phase II environmental sampling activities conducted at the study site

consisted of the following:

• Fourteen (14) soil borings were completed across the study site utilizing a

Geoprobe drilling rig. Each of the borings was completed to the depth of the

uppermost groundwater encountered. Ten (10) of the borings were located

around the perimeter of the study site, while the remaining four (4) borings

were located on the central/eastern portion of the study site (see Attachment B

for a sample location map). One (1) soil sample was collected from each of the

fourteen (14) soil boring locations at varying depth intervals. The depth interval

sampled from each soil boring was determined through the use of a photo

ionization detector (PID), in that the soil depth interval from each boring

resulting in the highest PID total hydrocarbon reading was sampled.

• Seven (7) samples of the uppermost groundwater at the site were collected

from seven (7) of the fourteen (14) soil borings that were completed as a part of

the soil sampling activities described above (at GP-2, GP-4, GP-6, GP-8, GP-

10, GP-11, and GP-12) (see Attachment B for sample locations). The

��

��

groundwater samples were collected unfiltered with small diameter bailers from

temporary 1 inch diameter PVC wells that were inserted into the seven (7) soil

boring locations.

• Borings from eleven (11) additional locations were completed across the site to

a depth of five (5) feet below the ground surface to visually inspect the site for

the presence of darkly stained shallow fill material that was described in

previous site environmental studies. No samples were collected for laboratory

analysis from locations where dark soils were not encountered; these locations

are also illustrated on the sample location figure provided in Attachment B.

• Each of the fourteen (14) soil samples and seven (7) groundwater samples

collected at the site were submitted under chain-of-custody documentation to

an analytical laboratory (Pace Analytical Services, Inc. of Indianapolis) for the

analysis of volatile organic compounds (VOCs), semi-volatile organic

compounds (SVOCs), polychlorinated biphenyls (PCBs), and RCRA 8 heavy

metals.

The sampling activities described above were conducted at the study site on January 24th,

25th, and 26th, 2008. Results of these sampling activities are discussed below.

Analytical Results

The analytical results from the Phase II sampling activities are summarized in Tables 1 and 2

that are provided in Attachment C. As shown in Table 1, heavy metal compounds were

detected in each of the fourteen (14) site soil samples collected. In four (4) of the site soil

sample locations, one (1) or more organic compounds (i.e., VOCs, SVOCs, and/or PCB

compounds) was also detected (from locations GP-9, GP-10, GP-13, and GP-23). These

four (4) soil samples were all collected from the eastern portion of the study site. It is noted,

however, that we suspect the lone VOC detection in soil sample GP-13 of acetone, a common

laboratory agent used for cleaning instruments, to be a laboratory artifact rather than

indicative of site conditions. The sample location figure in Attachment B graphically illustrates

the estimated extent of the area with organic impacts in site soils.

��

��

As shown in Table 2, heavy metal compounds were detected in each of the seven (7) site

groundwater samples. One (1) organic compound, PCB-1254, was also detected in one (1) of

the groundwater samples (GP-10). The complete analytical laboratory reports for the soil and

groundwater analyses are provided as Attachment D.

For comparative purposes, the tables in Attachment C also include Default Closure Levels

from the Indiana Department of Environmental Management (IDEM) Risk Integrated System

of Closure (RISC) Technical Guide for each of the compounds detected in the site samples. A

sample detection that exceeds one (1) or both of the associated RISC Default Closure Levels

is emphasized with a bold type box in the Attachment C tables. As shown in Table 1, five (5)

compounds detected in site soils exceeded an associated RISC level (arsenic, chromium,

lead, PCB-1254, and benzo(a)pyrene). Arsenic detections in site soils resulted in an

exceedance of the associated RISC Default Closure Levels for residential and/or industrial

site uses in thirteen (13) of the fourteen (14) soil sample locations. However, the levels of

arsenic detected in site soils, which range from 2.8 milligrams per kilogram (mg/kg) to 9

mg/kg, appear to be in line with typical background levels of arsenic in soil. Lead detections in

site soils resulted in an exceedance of the associated RISC Default Closure Levels in five (5)

of the fourteen (14) soil sample locations (GP-9, GP-10, GP-12, GP-13, and GP-23). These

five (5) soil sample locations are generally located on the eastern portion of the study site.

The chromium detections in site soils that exceeded an associated RISC Default Closure

Level occurred at GP-9 and GP-10; the PCB-1254 detection exceedance occurred at GP-9;

and the benzo(a)pyrene exceedances occurred at GP-9, GP-10, and GP-23.

As shown in Table 2, detections of heavy metal compounds in site groundwater resulted in an

exceedance of an associated RISC Default Closure Level in each of the seven (7) site

groundwater sample locations. The one detection of PCB-1254 at GP-10 also exceeded the

associated RISC Default Closure Levels.

Summary and Conclusions

Phase II environmental sampling activities were conducted at the Rock Pile Site located in

Beech Grove, Indiana on January 24th, 25th, and 26th, 2008 to investigate potential site

impacts to soil and groundwater associated with recognized environmental conditions

previously identified at the site during the completion of a Phase I ESA for the property.

��

��

Based on the results of the sampling activities, it appears that impacts to site soils are

generally limited to the eastern portion of the study site. These impacts appear likely to be

associated with fill materials present on this portion of the study site. Five (5) compounds

(arsenic, chromium, lead, PCB-1254, and benzo(a)pyrene) were detected in site soils at

concentrations above one or both of the associated IDEM RISC Default Closure Levels,

though the arsenic soil concentrations appear to be in line with typical soil background

concentrations.

Impacts to the uppermost site groundwater appear to be limited to heavy metal compounds

and one organic compound, PCB-1254. Concentrations of arsenic, barium, cadmium,

chromium, lead, selenium, and PCB-1254 from groundwater sampling locations across the

study site were found to exceed one or both of the associated RISC Default Closure Levels.

Due to the absence of any detectible levels of VOCs or SVOCs in site groundwater samples, it

appears that the study site groundwater has not been adversely impacted by the nearby

Leaking Underground Storage Tank (LUST) sites that were identified in the Phase I ESA

report.

It has been a pleasure to be of service to you and the Beech Grove Redevelopment

Commission on this project. Please feel free to call us at (317) 826-7292 or (317) 826-7285

respectively, if you have any questions or would like to further discuss the findings of our

Phase II investigation activities.

Sincerely, Douglas Petroff Environmental Project Manager W. Calvin Kelly Director – Environmental Services and Brownfields Redevelopment

��

��

Attachment A

Site Vicinity Map

�

��

�� !� �"""#�� #��$�� #�%&#%��

��

��'��(�)� �*��+�,��

-��.��,�/��$0�� !#��!�

��

��

��

Attachment B

Soil and Groundwater Sample Locations Map

The Schneider CorporationThe Schneider CorporationThe Schneider CorporationThe Schneider Corporation

Historic Fort Harrison 8901 Otis Avenue Indianapolis, IN 46216 www.schneidercorp.com 866.973.7100

Soil Boring Locations with Estimated Extent of Soil Impacts

Former Rock Pile Site Beech Grove, Indiana

Schneider Project Number 6892.002

GP-1

GP-2 GP-3

GP-4

GP-5

GP-6 GP-7 GP-8 GP-9

GP-10

GP-11

GP-12

GP-13

GP-23

Soil and groundwater sample location

GP-X

Soil sample location GP-Y

LEGEND

GP-24

GP-25 GP-14

GP-15

GP-16

GP-17

GP-20

GP-18

GP-19

GP-21

GP-22 Visual inspection only GP-Z

compound impacts in soil Estimated extent of organic

��

��

Attachment C

Sample Result Summary Tables

TABLE ISUMMARY OF SOIL DETECTIONS

Former Rock Pile SiteBellefontaine Street and Garstang StreetBeech Grove, Indiana

Constituent

Residential Industrial GP-1 GP-2 GP-3 GP-4 GP-5 GP-6 GP-7 GP-8 GP-9 GP-10 GP-11 GP-12 GP-13 GP-23(12-14) (6-8) (6-8) (2-4) (6-8) (2-4) (6-8) (12-14) (6-8) (2-4) (6-8) (2-4) (2-4) (5-7)

Arsenic 3.9 5.8 4.8 5.8 5.5 6.7 6.8 9 2.8 4 5.1 9 4.5 6.7 5.9 7.7Barium 1,600 10,000 33.6 54 50.2 52.3 50.6 78.9 59.6 20.6 315 382 49 78.7 53 52.6Chromium * 38 120 7.7 9.4 9.7 10.6 13.6 16.5 14.9 9.2 97.6 149 9 17.1 15.5 19.8Lead 81 230 5.8 8.3 7.6 37.5 10.7 11.2 8.2 6.2 1,160 1,480 7.5 96.7 81.8 101Selenium 5.2 53 ND ND ND 2.1 2.2 ND ND 2.5 ND 3.8 ND 2.4 ND 2.1

PCB-1254 * 1.8 5.3 ND ND ND ND ND ND ND ND 12.7 1.79 ND ND ND NDAcenaphthylene 18 180 ND ND ND ND ND ND ND ND 0.43 ND ND ND ND NDAnthracene 51 51 ND ND ND ND ND ND ND ND 0.954 ND ND ND ND 0.4Benzo(a)anthracene 5 15 ND ND ND ND ND ND ND ND 2.09 0.544 ND ND ND 1.02

Default RISC Level (mg/Kg) Soil (mg/Kg)

Benzo(a)anthracene 5 15 ND ND ND ND ND ND ND ND 2.09 0.544 ND ND ND 1.02Benzo(a)pyrene 0.5 1.5 ND ND ND ND ND ND ND ND 1.94 0.567 ND ND ND 0.777Benzo(b)fluoranthene 5 15 ND ND ND ND ND ND ND ND 2.52 0.843 ND ND ND 0.942Benzo(g,h,i)perylene -- -- ND ND ND ND ND ND ND ND 1.3 0.38 ND ND ND 0.44Benzo(k)fluoranthene 39 39 ND ND ND ND ND ND ND ND 1.29 ND ND ND ND 0.482Chrysene 25 25 ND ND ND ND ND ND ND ND 2.15 0.595 ND ND ND 1.05Fluoranthene 880 880 ND ND ND ND ND ND ND ND 4.4 1.09 ND ND ND 1.69Indeno(1,2,3-cd)pyrene 3.1 3.1 ND ND ND ND ND ND ND ND 1.17 ND ND ND ND 0.407Phenanthrene 13 170 ND ND ND ND ND ND ND ND 1.92 0.636 ND ND ND 0.976Pyrene 570 570 ND ND ND ND ND ND ND ND 3.63 0.942 ND ND ND 1.31Acetone 28 370 ND ND ND ND ND ND ND ND ND ND ND ND 0.115 NDNaphthalene 0.7 170 ND ND ND ND ND ND ND ND 0.209 ND ND ND ND ND

Notes:ND = Not DetectedBoxed value exceeds default residential RISC level Samples Collected January 24, 2008*PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VIDashes (--) indicates a Default RISC Level is not available for this constituent

TABLE 2SUMMARY OF GROUNDWATER DETECTIONS

Former Rock Pile SiteBellefontaine Street and Garstang StreetBeech Grove, Indiana

Constituent

Residential Industrial GP-2 GP-4 GP-6 GP-8 GP-10 GP-11 GP-12

Arsenic 0.01 0.01 0.16 0.078 0.0821 0.519 0.64 0.141 0.166Barium 2 20 1.24 0.86 0.976 3.26 8.46 1.08 2.11Cadmium 0.005 0.051 0.0132 0.005 0.0066 0.0295 0.0515 0.0073 0.0101Chromium * 0.1 0.31 0.371 0.249 0.258 0.802 1.79 0.269 0.343Lead 0.015 0.042 0.213 0.114 0.112 0.699 9.6 0.168 0.82Selenium 0.05 0.51 0.0497 0.0314 0.0312 0.161 0.215 0.06 0.0411

PCB-1254 * 0.0005 0.0014 ND ND ND ND 0.0035 ND ND

Default RISC Level (mg/L) Groundwater (mg/L)

PCB-1254 * 0.0005 0.0014 ND ND ND ND 0.0035 ND ND

Notes:ND = Not DetectedNA = Not AvailableBoxed value exceeds default residential RISC level Samples Collected January 25 and 26, 2008All samples were collected unfiltered*PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VI

��

��

Attachment D

Analytical Laboratory Data Reports

February 11, 2008

LIMS USE: FR - DOUG PETROFFLIMS OBJECT ID: 5011474

5011474Project:Pace Project No.:

RE:

Mr. Doug PetroffThe Schneider Corporation8901 Otis AveIndianapolis, IN 46216

Beech Grove 6892.002

Dear Mr. Petroff:Enclosed are the analytical results for sample(s) received by the laboratory on January 25, 2008.The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of thereport.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Donna Spyker

[email protected] Manager

Illinois/NELAC Certification Number: 100418Indiana Certification Number: C-49-06Kansas Certification Number: E-10247Kentucky Certification Number: 0042Ohio VAP: CL0065Pennsylvania: 68-00791West Virginia Certification Number: 330

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Page 1 of 90

Pace Analytical Services, Inc.7726 Moller Road

Indianapolis, IN 46268

(317)875-5894

SAMPLE SUMMARY

Pace Project No.:Project:

5011474Beech Grove 6892.002

Lab ID Sample ID Matrix Date Collected Date Received

5011474001 GP-1 (12-14) Solid 01/24/08 09:00 01/25/08 13:24

5011474002 GP-2(6-8) Solid 01/24/08 09:30 01/25/08 13:24

5011474003 GP-3(6-8) Solid 01/24/08 10:00 01/25/08 13:24

5011474004 GP-4(2-4) Solid 01/24/08 10:20 01/25/08 13:24

5011474005 GP-5(6-8) Solid 01/24/08 10:45 01/25/08 13:24

5011474006 GP-6(2-4) Solid 01/24/08 11:00 01/25/08 13:24

5011474007 GP-7(6-8) Solid 01/24/08 11:30 01/25/08 13:24

5011474008 GP-8(12-14) Solid 01/24/08 13:00 01/25/08 13:24

5011474009 GP-9(6-8) Solid 01/24/08 13:30 01/25/08 13:24

5011474010 GP-10(2-4) Solid 01/24/08 14:00 01/25/08 13:24

5011474011 GP-11(6-8) Solid 01/24/08 14:30 01/25/08 13:24

5011474012 GP-12(2-4) Solid 01/24/08 15:30 01/25/08 13:24

5011474013 GP-13(2-4) Solid 01/24/08 16:00 01/25/08 13:24

5011474014 GP-23(5-7) Solid 01/24/08 17:30 01/25/08 13:24



Page 2 of 90



(317)875-5894

SAMPLE ANALYTE COUNT


5011474Beech Grove 6892.002

Lab ID Sample ID MethodAnalytesReportedAnalysts

5011474001 GP-1 (12-14) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474002 GP-2(6-8) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474003 GP-3(6-8) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474004 GP-4(2-4) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474005 GP-5(6-8) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474006 GP-6(2-4) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474007 GP-7(6-8) ASTM D2974-87 1ILP



Page 3 of 90



(317)875-5894



5011474Beech Grove 6892.002


EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474008 GP-8(12-14) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474009 GP-9(6-8) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474010 GP-10(2-4) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474011 GP-11(6-8) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474012 GP-12(2-4) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474013 GP-13(2-4) ASTM D2974-87 1ILP

EPA 6010 7FRW



Page 4 of 90



(317)875-5894



5011474Beech Grove 6892.002


EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES

5011474014 GP-23(5-7) ASTM D2974-87 1ILP

EPA 6010 7FRW

EPA 7471 1LLB

EPA 8082 8SAQ

EPA 8260 73ALA

EPA 8270 66KES



Page 5 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002

Sample: GP-1 (12-14) Lab ID: 5011474001 Collected: 01/24/08 09:00 Received: 01/25/08 13:24 Matrix: SolidResults reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546

PCB-1016 (Aroclor 1016) ND ug/kg 39.7 1 02/01/08 13:49 12674-11-201/31/08 00:00PCB-1221 (Aroclor 1221) ND ug/kg 39.7 1 02/01/08 13:49 11104-28-201/31/08 00:00PCB-1232 (Aroclor 1232) ND ug/kg 39.7 1 02/01/08 13:49 11141-16-501/31/08 00:00PCB-1242 (Aroclor 1242) ND ug/kg 39.7 1 02/01/08 13:49 53469-21-901/31/08 00:00PCB-1248 (Aroclor 1248) ND ug/kg 39.7 1 02/01/08 13:49 12672-29-601/31/08 00:00PCB-1254 (Aroclor 1254) ND ug/kg 39.7 1 02/01/08 13:49 11097-69-101/31/08 00:00PCB-1260 (Aroclor 1260) ND ug/kg 39.7 1 02/01/08 13:49 11096-82-501/31/08 00:00Tetrachloro-m-xylene (S) 70 % 28-137 1 02/01/08 13:49 877-09-801/31/08 00:00

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050

Arsenic 4.8 mg/kg 2.1 1 02/01/08 08:52 7440-38-201/31/08 00:00Barium 33.6 mg/kg 2.1 1 02/01/08 08:52 7440-39-301/31/08 00:00Cadmium ND mg/kg 2.1 1 02/01/08 08:52 7440-43-901/31/08 00:00Chromium 7.7 mg/kg 2.1 1 02/01/08 08:52 7440-47-301/31/08 00:00Lead 5.8 mg/kg 2.1 1 02/01/08 08:52 7439-92-101/31/08 00:00Selenium ND mg/kg 2.1 1 02/01/08 08:52 7782-49-201/31/08 00:00Silver ND mg/kg 2.1 1 02/01/08 08:52 7440-22-401/31/08 00:00

7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471

Mercury ND mg/kg 0.38 1 01/29/08 16:47 7439-97-601/28/08 00:00

8270 MSSV SHORT LISTMICROWAVE

Analytical Method: EPA 8270 Preparation Method: EPA 3546

Acenaphthene ND ug/kg 375 1 01/31/08 02:35 83-32-901/30/08 00:00Acenaphthylene ND ug/kg 375 1 01/31/08 02:35 208-96-801/30/08 00:00Anthracene ND ug/kg 375 1 01/31/08 02:35 120-12-701/30/08 00:00Benzo(a)anthracene ND ug/kg 375 1 01/31/08 02:35 56-55-301/30/08 00:00Benzo(a)pyrene ND ug/kg 375 1 01/31/08 02:35 50-32-801/30/08 00:00Benzo(b)fluoranthene ND ug/kg 375 1 01/31/08 02:35 205-99-201/30/08 00:00Benzo(g,h,i)perylene ND ug/kg 375 1 01/31/08 02:35 191-24-201/30/08 00:00Benzo(k)fluoranthene ND ug/kg 375 1 01/31/08 02:35 207-08-901/30/08 00:00Benzyl alcohol ND ug/kg 749 1 01/31/08 02:35 100-51-601/30/08 00:004-Bromophenylphenyl ether ND ug/kg 375 1 01/31/08 02:35 101-55-301/30/08 00:00Butylbenzylphthalate ND ug/kg 375 1 01/31/08 02:35 85-68-701/30/08 00:004-Chloro-3-methylphenol ND ug/kg 749 1 01/31/08 02:35 59-50-701/30/08 00:004-Chloroaniline ND ug/kg 749 1 01/31/08 02:35 106-47-801/30/08 00:00bis(2-Chloroethoxy)methane ND ug/kg 375 1 01/31/08 02:35 111-91-101/30/08 00:00bis(2-Chloroethyl) ether ND ug/kg 375 1 01/31/08 02:35 111-44-401/30/08 00:00bis(2-Chloroisopropyl) ether ND ug/kg 375 1 01/31/08 02:35 108-60-101/30/08 00:002-Chloronaphthalene ND ug/kg 375 1 01/31/08 02:35 91-58-701/30/08 00:002-Chlorophenol ND ug/kg 375 1 01/31/08 02:35 95-57-801/30/08 00:004-Chlorophenylphenyl ether ND ug/kg 375 1 01/31/08 02:35 7005-72-301/30/08 00:00Chrysene ND ug/kg 375 1 01/31/08 02:35 218-01-901/30/08 00:00Dibenz(a,h)anthracene ND ug/kg 375 1 01/31/08 02:35 53-70-301/30/08 00:00Dibenzofuran ND ug/kg 375 1 01/31/08 02:35 132-64-901/30/08 00:003,3'-Dichlorobenzidine ND ug/kg 749 1 01/31/08 02:35 91-94-101/30/08 00:00



Date: 02/11/2008 03:29 PM Page 6 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 375 1 01/31/08 02:35 120-83-201/30/08 00:00Diethylphthalate ND ug/kg 375 1 01/31/08 02:35 84-66-201/30/08 00:002,4-Dimethylphenol ND ug/kg 375 1 01/31/08 02:35 105-67-901/30/08 00:00Dimethylphthalate ND ug/kg 375 1 01/31/08 02:35 131-11-301/30/08 00:00Di-n-butylphthalate ND ug/kg 375 1 01/31/08 02:35 84-74-201/30/08 00:004,6-Dinitro-2-methylphenol ND ug/kg 1820 1 01/31/08 02:35 534-52-101/30/08 00:002,4-Dinitrophenol ND ug/kg 1820 1 01/31/08 02:35 51-28-501/30/08 00:002,4-Dinitrotoluene ND ug/kg 375 1 01/31/08 02:35 121-14-201/30/08 00:002,6-Dinitrotoluene ND ug/kg 375 1 01/31/08 02:35 606-20-201/30/08 00:00Di-n-octylphthalate ND ug/kg 375 1 01/31/08 02:35 117-84-001/30/08 00:00bis(2-Ethylhexyl)phthalate ND ug/kg 375 1 01/31/08 02:35 117-81-701/30/08 00:00Fluoranthene ND ug/kg 375 1 01/31/08 02:35 206-44-001/30/08 00:00Fluorene ND ug/kg 375 1 01/31/08 02:35 86-73-701/30/08 00:00Hexachloro-1,3-butadiene ND ug/kg 375 1 01/31/08 02:35 87-68-301/30/08 00:00Hexachlorobenzene ND ug/kg 375 1 01/31/08 02:35 118-74-101/30/08 00:00Hexachlorocyclopentadiene ND ug/kg 375 1 01/31/08 02:35 77-47-401/30/08 00:00Hexachloroethane ND ug/kg 375 1 01/31/08 02:35 67-72-101/30/08 00:00Indeno(1,2,3-cd)pyrene ND ug/kg 375 1 01/31/08 02:35 193-39-501/30/08 00:00Isophorone ND ug/kg 375 1 01/31/08 02:35 78-59-101/30/08 00:002-Methylnaphthalene ND ug/kg 375 1 01/31/08 02:35 91-57-601/30/08 00:002-Methylphenol(o-Cresol) ND ug/kg 375 1 01/31/08 02:35 95-48-701/30/08 00:003&4-Methylphenol(m&p Cresol) ND ug/kg 749 1 01/31/08 02:3501/30/08 00:00Naphthalene ND ug/kg 375 1 01/31/08 02:35 91-20-301/30/08 00:002-Nitroaniline ND ug/kg 1820 1 01/31/08 02:35 88-74-401/30/08 00:003-Nitroaniline ND ug/kg 1820 1 01/31/08 02:35 99-09-201/30/08 00:004-Nitroaniline ND ug/kg 1820 1 01/31/08 02:35 100-01-601/30/08 00:00Nitrobenzene ND ug/kg 375 1 01/31/08 02:35 98-95-301/30/08 00:002-Nitrophenol ND ug/kg 375 1 01/31/08 02:35 88-75-501/30/08 00:004-Nitrophenol ND ug/kg 1820 1 01/31/08 02:35 100-02-701/30/08 00:00N-Nitroso-di-n-propylamine ND ug/kg 375 1 01/31/08 02:35 621-64-701/30/08 00:00N-Nitrosodiphenylamine ND ug/kg 375 1 01/31/08 02:35 86-30-601/30/08 00:00Pentachlorophenol ND ug/kg 1820 1 01/31/08 02:35 87-86-501/30/08 00:00Phenanthrene ND ug/kg 341 1 01/31/08 02:35 85-01-801/30/08 00:00Phenol ND ug/kg 375 1 01/31/08 02:35 108-95-201/30/08 00:00Pyrene ND ug/kg 375 1 01/31/08 02:35 129-00-001/30/08 00:002,4,5-Trichlorophenol ND ug/kg 375 1 01/31/08 02:35 95-95-401/30/08 00:002,4,6-Trichlorophenol ND ug/kg 375 1 01/31/08 02:35 88-06-201/30/08 00:00Nitrobenzene-d5 (S) 79 % 50-117 1 01/31/08 02:35 4165-60-001/30/08 00:002-Fluorobiphenyl (S) 83 % 56-118 1 01/31/08 02:35 321-60-801/30/08 00:00Terphenyl-d14 (S) 87 % 55-118 1 01/31/08 02:35 1718-51-001/30/08 00:00Phenol-d6 (S) 77 % 41-124 1 01/31/08 02:35 13127-88-301/30/08 00:002-Fluorophenol (S) 79 % 35-117 1 01/31/08 02:35 367-12-401/30/08 00:002,4,6-Tribromophenol (S) 85 % 34-122 1 01/31/08 02:35 118-79-601/30/08 00:00



Date: 02/11/2008 03:29 PM Page 7 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002



8260 MSV 5035A VOA Analytical Method: EPA 8260

Acetone ND ug/kg 88.6 1 01/29/08 14:12 67-64-1Acrolein ND ug/kg 88.6 1 01/29/08 14:12 107-02-8Acrylonitrile ND ug/kg 88.6 1 01/29/08 14:12 107-13-1Benzene ND ug/kg 4.4 1 01/29/08 14:12 71-43-2Bromobenzene ND ug/kg 4.4 1 01/29/08 14:12 108-86-1Bromochloromethane ND ug/kg 4.4 1 01/29/08 14:12 74-97-5Bromodichloromethane ND ug/kg 4.4 1 01/29/08 14:12 75-27-4Bromoform ND ug/kg 4.4 1 01/29/08 14:12 75-25-2Bromomethane ND ug/kg 4.4 1 01/29/08 14:12 74-83-92-Butanone (MEK) ND ug/kg 22.1 1 01/29/08 14:12 78-93-3n-Butylbenzene ND ug/kg 4.4 1 01/29/08 14:12 104-51-8sec-Butylbenzene ND ug/kg 4.4 1 01/29/08 14:12 135-98-8tert-Butylbenzene ND ug/kg 4.4 1 01/29/08 14:12 98-06-6Carbon disulfide ND ug/kg 8.9 1 01/29/08 14:12 75-15-0Carbon tetrachloride ND ug/kg 4.4 1 01/29/08 14:12 56-23-5Chlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 108-90-7Chloroethane ND ug/kg 4.4 1 01/29/08 14:12 75-00-3Chloroform ND ug/kg 4.4 1 01/29/08 14:12 67-66-3Chloromethane ND ug/kg 4.4 1 01/29/08 14:12 74-87-32-Chlorotoluene ND ug/kg 4.4 1 01/29/08 14:12 95-49-84-Chlorotoluene ND ug/kg 4.4 1 01/29/08 14:12 106-43-4Dibromochloromethane ND ug/kg 4.4 1 01/29/08 14:12 124-48-11,2-Dibromoethane (EDB) ND ug/kg 4.4 1 01/29/08 14:12 106-93-4Dibromomethane ND ug/kg 4.4 1 01/29/08 14:12 74-95-31,2-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 95-50-11,3-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 541-73-11,4-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 106-46-7trans-1,4-Dichloro-2-butene ND ug/kg 88.6 1 01/29/08 14:12 110-57-6Dichlorodifluoromethane ND ug/kg 4.4 1 01/29/08 14:12 75-71-81,1-Dichloroethane ND ug/kg 4.4 1 01/29/08 14:12 75-34-31,2-Dichloroethane ND ug/kg 4.4 1 01/29/08 14:12 107-06-21,1-Dichloroethene ND ug/kg 4.4 1 01/29/08 14:12 75-35-4cis-1,2-Dichloroethene ND ug/kg 4.4 1 01/29/08 14:12 156-59-2trans-1,2-Dichloroethene ND ug/kg 4.4 1 01/29/08 14:12 156-60-51,2-Dichloropropane ND ug/kg 4.4 1 01/29/08 14:12 78-87-51,3-Dichloropropane ND ug/kg 4.4 1 01/29/08 14:12 142-28-92,2-Dichloropropane ND ug/kg 4.4 1 01/29/08 14:12 594-20-71,1-Dichloropropene ND ug/kg 4.4 1 01/29/08 14:12 563-58-6cis-1,3-Dichloropropene ND ug/kg 4.4 1 01/29/08 14:12 10061-01-5trans-1,3-Dichloropropene ND ug/kg 4.4 1 01/29/08 14:12 10061-02-6Ethylbenzene ND ug/kg 4.4 1 01/29/08 14:12 100-41-4Ethyl methacrylate ND ug/kg 8.9 1 01/29/08 14:12 97-63-2Hexachloro-1,3-butadiene ND ug/kg 4.4 1 01/29/08 14:12 87-68-3n-Hexane ND ug/kg 4.4 1 01/29/08 14:12 110-54-32-Hexanone ND ug/kg 88.6 1 01/29/08 14:12 591-78-6Iodomethane ND ug/kg 88.6 1 01/29/08 14:12 74-88-4



Date: 02/11/2008 03:29 PM Page 8 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




Isopropylbenzene (Cumene) ND ug/kg 4.4 1 01/29/08 14:12 98-82-8p-Isopropyltoluene ND ug/kg 4.4 1 01/29/08 14:12 99-87-6Methylene chloride ND ug/kg 17.7 1 01/29/08 14:12 75-09-24-Methyl-2-pentanone (MIBK) ND ug/kg 22.1 1 01/29/08 14:12 108-10-1Methyl-tert-butyl ether ND ug/kg 4.4 1 01/29/08 14:12 1634-04-4Naphthalene ND ug/kg 4.4 1 01/29/08 14:12 91-20-3n-Propylbenzene ND ug/kg 4.4 1 01/29/08 14:12 103-65-1Styrene ND ug/kg 4.4 1 01/29/08 14:12 100-42-51,1,1,2-Tetrachloroethane ND ug/kg 4.4 1 01/29/08 14:12 630-20-61,1,2,2-Tetrachloroethane ND ug/kg 4.4 1 01/29/08 14:12 79-34-5Tetrachloroethene ND ug/kg 4.4 1 01/29/08 14:12 127-18-4Toluene ND ug/kg 4.4 1 01/29/08 14:12 108-88-31,2,3-Trichlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 87-61-61,2,4-Trichlorobenzene ND ug/kg 4.4 1 01/29/08 14:12 120-82-11,1,1-Trichloroethane ND ug/kg 4.4 1 01/29/08 14:12 71-55-61,1,2-Trichloroethane ND ug/kg 4.4 1 01/29/08 14:12 79-00-5Trichloroethene ND ug/kg 4.4 1 01/29/08 14:12 79-01-6Trichlorofluoromethane ND ug/kg 4.4 1 01/29/08 14:12 75-69-41,2,3-Trichloropropane ND ug/kg 4.4 1 01/29/08 14:12 96-18-41,2,4-Trimethylbenzene ND ug/kg 4.4 1 01/29/08 14:12 95-63-61,3,5-Trimethylbenzene ND ug/kg 4.4 1 01/29/08 14:12 108-67-8Vinyl acetate ND ug/kg 88.6 1 01/29/08 14:12 108-05-4Vinyl chloride ND ug/kg 4.4 1 01/29/08 14:12 75-01-4Xylene (Total) ND ug/kg 8.9 1 01/29/08 14:12 1330-20-7Dibromofluoromethane (S) 98 % 82-130 1 01/29/08 14:12 1868-53-7Toluene-d8 (S) 98 % 81-120 1 01/29/08 14:12 2037-26-54-Bromofluorobenzene (S) 101 % 65-117 1 01/29/08 14:12 460-00-4

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 11.9 % 0.10 1 02/01/08 11:29



Date: 02/11/2008 03:29 PM Page 9 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002

Sample: GP-2(6-8) Lab ID: 5011474002 Collected: 01/24/08 09:30 Received: 01/25/08 13:24 Matrix: SolidResults reported on a "dry-weight" basis







Mercury ND mg/kg 0.39 1 01/29/08 16:51 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 10 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 11 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 12 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 13 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.37 1 01/29/08 16:53 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 14 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 15 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 16 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 17 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




PCB-1016 (Aroclor 1016) ND ug/kg 207 5 02/06/08 14:37 12674-11-2 1d02/05/08 00:00PCB-1221 (Aroclor 1221) ND ug/kg 207 5 02/06/08 14:37 11104-28-202/05/08 00:00PCB-1232 (Aroclor 1232) ND ug/kg 207 5 02/06/08 14:37 11141-16-502/05/08 00:00PCB-1242 (Aroclor 1242) ND ug/kg 207 5 02/06/08 14:37 53469-21-902/05/08 00:00PCB-1248 (Aroclor 1248) ND ug/kg 207 5 02/06/08 14:37 12672-29-602/05/08 00:00PCB-1254 (Aroclor 1254) ND ug/kg 207 5 02/06/08 14:37 11097-69-102/05/08 00:00PCB-1260 (Aroclor 1260) ND ug/kg 207 5 02/06/08 14:37 11096-82-502/05/08 00:00Tetrachloro-m-xylene (S) 22 % 28-137 5 02/06/08 14:37 877-09-8 S402/05/08 00:00


Arsenic 6.7 mg/kg 2.2 1 02/01/08 09:31 7440-38-201/31/08 00:00Barium 52.3 mg/kg 2.2 1 02/01/08 09:31 7440-39-301/31/08 00:00Cadmium ND mg/kg 2.2 1 02/01/08 09:31 7440-43-901/31/08 00:00Chromium 10.6 mg/kg 2.2 1 02/01/08 09:31 7440-47-301/31/08 00:00Lead 37.5 mg/kg 2.2 1 02/01/08 09:31 7439-92-101/31/08 00:00Selenium 2.1 mg/kg 2.2 1 02/01/08 09:31 7782-49-201/31/08 00:00Silver ND mg/kg 2.2 1 02/01/08 09:31 7440-22-401/31/08 00:00


Mercury ND mg/kg 0.39 1 01/29/08 16:54 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 18 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 3890 10 01/31/08 04:19 120-83-201/30/08 00:00Diethylphthalate ND ug/kg 3890 10 01/31/08 04:19 84-66-201/30/08 00:002,4-Dimethylphenol ND ug/kg 3890 10 01/31/08 04:19 105-67-901/30/08 00:00Dimethylphthalate ND ug/kg 3890 10 01/31/08 04:19 131-11-301/30/08 00:00Di-n-butylphthalate ND ug/kg 3890 10 01/31/08 04:19 84-74-201/30/08 00:004,6-Dinitro-2-methylphenol ND ug/kg 18800 10 01/31/08 04:19 534-52-101/30/08 00:002,4-Dinitrophenol ND ug/kg 18800 10 01/31/08 04:19 51-28-501/30/08 00:002,4-Dinitrotoluene ND ug/kg 3890 10 01/31/08 04:19 121-14-201/30/08 00:002,6-Dinitrotoluene ND ug/kg 3890 10 01/31/08 04:19 606-20-201/30/08 00:00Di-n-octylphthalate ND ug/kg 3890 10 01/31/08 04:19 117-84-001/30/08 00:00bis(2-Ethylhexyl)phthalate ND ug/kg 3890 10 01/31/08 04:19 117-81-701/30/08 00:00Fluoranthene ND ug/kg 3890 10 01/31/08 04:19 206-44-001/30/08 00:00Fluorene ND ug/kg 3890 10 01/31/08 04:19 86-73-701/30/08 00:00Hexachloro-1,3-butadiene ND ug/kg 3890 10 01/31/08 04:19 87-68-301/30/08 00:00Hexachlorobenzene ND ug/kg 3890 10 01/31/08 04:19 118-74-101/30/08 00:00Hexachlorocyclopentadiene ND ug/kg 3890 10 01/31/08 04:19 77-47-401/30/08 00:00Hexachloroethane ND ug/kg 3890 10 01/31/08 04:19 67-72-101/30/08 00:00Indeno(1,2,3-cd)pyrene ND ug/kg 3890 10 01/31/08 04:19 193-39-501/30/08 00:00Isophorone ND ug/kg 3890 10 01/31/08 04:19 78-59-101/30/08 00:002-Methylnaphthalene ND ug/kg 3890 10 01/31/08 04:19 91-57-601/30/08 00:002-Methylphenol(o-Cresol) ND ug/kg 3890 10 01/31/08 04:19 95-48-701/30/08 00:003&4-Methylphenol(m&p Cresol) ND ug/kg 7770 10 01/31/08 04:1901/30/08 00:00Naphthalene ND ug/kg 3890 10 01/31/08 04:19 91-20-301/30/08 00:002-Nitroaniline ND ug/kg 18800 10 01/31/08 04:19 88-74-401/30/08 00:003-Nitroaniline ND ug/kg 18800 10 01/31/08 04:19 99-09-201/30/08 00:004-Nitroaniline ND ug/kg 18800 10 01/31/08 04:19 100-01-601/30/08 00:00Nitrobenzene ND ug/kg 3890 10 01/31/08 04:19 98-95-301/30/08 00:002-Nitrophenol ND ug/kg 3890 10 01/31/08 04:19 88-75-501/30/08 00:004-Nitrophenol ND ug/kg 18800 10 01/31/08 04:19 100-02-701/30/08 00:00N-Nitroso-di-n-propylamine ND ug/kg 3890 10 01/31/08 04:19 621-64-701/30/08 00:00N-Nitrosodiphenylamine ND ug/kg 3890 10 01/31/08 04:19 86-30-601/30/08 00:00Pentachlorophenol ND ug/kg 18800 10 01/31/08 04:19 87-86-501/30/08 00:00Phenanthrene ND ug/kg 3530 10 01/31/08 04:19 85-01-801/30/08 00:00Phenol ND ug/kg 3890 10 01/31/08 04:19 108-95-2 2d01/30/08 00:00Pyrene ND ug/kg 3890 10 01/31/08 04:19 129-00-001/30/08 00:002,4,5-Trichlorophenol ND ug/kg 3890 10 01/31/08 04:19 95-95-401/30/08 00:002,4,6-Trichlorophenol ND ug/kg 3890 10 01/31/08 04:19 88-06-201/30/08 00:00Nitrobenzene-d5 (S) 48 % 50-117 10 01/31/08 04:19 4165-60-0 S401/30/08 00:002-Fluorobiphenyl (S) 44 % 56-118 10 01/31/08 04:19 321-60-8 S401/30/08 00:00Terphenyl-d14 (S) 46 % 55-118 10 01/31/08 04:19 1718-51-0 S401/30/08 00:00Phenol-d6 (S) 43 % 41-124 10 01/31/08 04:19 13127-88-301/30/08 00:002-Fluorophenol (S) 45 % 35-117 10 01/31/08 04:19 367-12-401/30/08 00:002,4,6-Tribromophenol (S) 41 % 34-122 10 01/31/08 04:19 118-79-601/30/08 00:00



Date: 02/11/2008 03:29 PM Page 19 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 20 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 21 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.40 1 01/29/08 16:55 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 22 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 23 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 24 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 25 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.39 1 01/29/08 16:57 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 26 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 27 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 28 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 29 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.43 1 01/29/08 16:58 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 30 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 31 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




Acetone ND ug/kg 103 1 01/29/08 18:07 67-64-1Acrolein ND ug/kg 103 1 01/29/08 18:07 107-02-8Acrylonitrile ND ug/kg 103 1 01/29/08 18:07 107-13-1Benzene ND ug/kg 5.2 1 01/29/08 18:07 71-43-2Bromobenzene ND ug/kg 5.2 1 01/29/08 18:07 108-86-1Bromochloromethane ND ug/kg 5.2 1 01/29/08 18:07 74-97-5Bromodichloromethane ND ug/kg 5.2 1 01/29/08 18:07 75-27-4Bromoform ND ug/kg 5.2 1 01/29/08 18:07 75-25-2Bromomethane ND ug/kg 5.2 1 01/29/08 18:07 74-83-92-Butanone (MEK) ND ug/kg 25.8 1 01/29/08 18:07 78-93-3n-Butylbenzene ND ug/kg 5.2 1 01/29/08 18:07 104-51-8sec-Butylbenzene ND ug/kg 5.2 1 01/29/08 18:07 135-98-8tert-Butylbenzene ND ug/kg 5.2 1 01/29/08 18:07 98-06-6Carbon disulfide ND ug/kg 10.3 1 01/29/08 18:07 75-15-0Carbon tetrachloride ND ug/kg 5.2 1 01/29/08 18:07 56-23-5Chlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 108-90-7Chloroethane ND ug/kg 5.2 1 01/29/08 18:07 75-00-3Chloroform ND ug/kg 5.2 1 01/29/08 18:07 67-66-3Chloromethane ND ug/kg 5.2 1 01/29/08 18:07 74-87-32-Chlorotoluene ND ug/kg 5.2 1 01/29/08 18:07 95-49-84-Chlorotoluene ND ug/kg 5.2 1 01/29/08 18:07 106-43-4Dibromochloromethane ND ug/kg 5.2 1 01/29/08 18:07 124-48-11,2-Dibromoethane (EDB) ND ug/kg 5.2 1 01/29/08 18:07 106-93-4Dibromomethane ND ug/kg 5.2 1 01/29/08 18:07 74-95-31,2-Dichlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 95-50-11,3-Dichlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 541-73-11,4-Dichlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 106-46-7trans-1,4-Dichloro-2-butene ND ug/kg 103 1 01/29/08 18:07 110-57-6Dichlorodifluoromethane ND ug/kg 5.2 1 01/29/08 18:07 75-71-81,1-Dichloroethane ND ug/kg 5.2 1 01/29/08 18:07 75-34-31,2-Dichloroethane ND ug/kg 5.2 1 01/29/08 18:07 107-06-21,1-Dichloroethene ND ug/kg 5.2 1 01/29/08 18:07 75-35-4cis-1,2-Dichloroethene ND ug/kg 5.2 1 01/29/08 18:07 156-59-2trans-1,2-Dichloroethene ND ug/kg 5.2 1 01/29/08 18:07 156-60-51,2-Dichloropropane ND ug/kg 5.2 1 01/29/08 18:07 78-87-51,3-Dichloropropane ND ug/kg 5.2 1 01/29/08 18:07 142-28-92,2-Dichloropropane ND ug/kg 5.2 1 01/29/08 18:07 594-20-71,1-Dichloropropene ND ug/kg 5.2 1 01/29/08 18:07 563-58-6cis-1,3-Dichloropropene ND ug/kg 5.2 1 01/29/08 18:07 10061-01-5trans-1,3-Dichloropropene ND ug/kg 5.2 1 01/29/08 18:07 10061-02-6Ethylbenzene ND ug/kg 5.2 1 01/29/08 18:07 100-41-4Ethyl methacrylate ND ug/kg 10.3 1 01/29/08 18:07 97-63-2Hexachloro-1,3-butadiene ND ug/kg 5.2 1 01/29/08 18:07 87-68-3n-Hexane ND ug/kg 5.2 1 01/29/08 18:07 110-54-32-Hexanone ND ug/kg 103 1 01/29/08 18:07 591-78-6Iodomethane ND ug/kg 103 1 01/29/08 18:07 74-88-4



Date: 02/11/2008 03:29 PM Page 32 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




Isopropylbenzene (Cumene) ND ug/kg 5.2 1 01/29/08 18:07 98-82-8p-Isopropyltoluene ND ug/kg 5.2 1 01/29/08 18:07 99-87-6Methylene chloride ND ug/kg 20.7 1 01/29/08 18:07 75-09-24-Methyl-2-pentanone (MIBK) ND ug/kg 25.8 1 01/29/08 18:07 108-10-1Methyl-tert-butyl ether ND ug/kg 5.2 1 01/29/08 18:07 1634-04-4Naphthalene ND ug/kg 5.2 1 01/29/08 18:07 91-20-3n-Propylbenzene ND ug/kg 5.2 1 01/29/08 18:07 103-65-1Styrene ND ug/kg 5.2 1 01/29/08 18:07 100-42-51,1,1,2-Tetrachloroethane ND ug/kg 5.2 1 01/29/08 18:07 630-20-61,1,2,2-Tetrachloroethane ND ug/kg 5.2 1 01/29/08 18:07 79-34-5Tetrachloroethene ND ug/kg 5.2 1 01/29/08 18:07 127-18-4Toluene ND ug/kg 5.2 1 01/29/08 18:07 108-88-31,2,3-Trichlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 87-61-61,2,4-Trichlorobenzene ND ug/kg 5.2 1 01/29/08 18:07 120-82-11,1,1-Trichloroethane ND ug/kg 5.2 1 01/29/08 18:07 71-55-61,1,2-Trichloroethane ND ug/kg 5.2 1 01/29/08 18:07 79-00-5Trichloroethene ND ug/kg 5.2 1 01/29/08 18:07 79-01-6Trichlorofluoromethane ND ug/kg 5.2 1 01/29/08 18:07 75-69-41,2,3-Trichloropropane ND ug/kg 5.2 1 01/29/08 18:07 96-18-41,2,4-Trimethylbenzene ND ug/kg 5.2 1 01/29/08 18:07 95-63-61,3,5-Trimethylbenzene ND ug/kg 5.2 1 01/29/08 18:07 108-67-8Vinyl acetate ND ug/kg 103 1 01/29/08 18:07 108-05-4Vinyl chloride ND ug/kg 5.2 1 01/29/08 18:07 75-01-4Xylene (Total) ND ug/kg 10.3 1 01/29/08 18:07 1330-20-7Dibromofluoromethane (S) 101 % 82-130 1 01/29/08 18:07 1868-53-7Toluene-d8 (S) 96 % 81-120 1 01/29/08 18:07 2037-26-54-Bromofluorobenzene (S) 99 % 65-117 1 01/29/08 18:07 460-00-4





Date: 02/11/2008 03:29 PM Page 33 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.35 1 01/29/08 17:00 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 34 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 35 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 36 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 37 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




PCB-1016 (Aroclor 1016) ND ug/kg 3900 100 02/06/08 16:44 12674-11-202/05/08 00:00PCB-1221 (Aroclor 1221) ND ug/kg 3900 100 02/06/08 16:44 11104-28-202/05/08 00:00PCB-1232 (Aroclor 1232) ND ug/kg 3900 100 02/06/08 16:44 11141-16-502/05/08 00:00PCB-1242 (Aroclor 1242) ND ug/kg 3900 100 02/06/08 16:44 53469-21-902/05/08 00:00PCB-1248 (Aroclor 1248) ND ug/kg 3900 100 02/06/08 16:44 12672-29-602/05/08 00:00PCB-1254 (Aroclor 1254) 12700 ug/kg 3900 100 02/06/08 16:44 11097-69-102/05/08 00:00PCB-1260 (Aroclor 1260) ND ug/kg 3900 100 02/06/08 16:44 11096-82-502/05/08 00:00Tetrachloro-m-xylene (S) 0 % 28-137 100 02/06/08 16:44 877-09-8 S402/05/08 00:00


Arsenic 5.1 mg/kg 2.1 1 02/01/08 10:11 7440-38-201/31/08 00:00Barium 315 mg/kg 2.1 1 02/01/08 10:11 7440-39-301/31/08 00:00Cadmium ND mg/kg 2.1 1 02/01/08 10:11 7440-43-901/31/08 00:00Chromium 97.6 mg/kg 2.1 1 02/01/08 10:11 7440-47-301/31/08 00:00Lead 1160 mg/kg 2.1 1 02/01/08 10:11 7439-92-101/31/08 00:00Selenium ND mg/kg 2.1 1 02/01/08 10:11 7782-49-201/31/08 00:00Silver ND mg/kg 2.1 1 02/01/08 10:11 7440-22-401/31/08 00:00


Mercury ND mg/kg 0.38 1 01/29/08 17:01 7439-97-601/28/08 00:00



Acenaphthene ND ug/kg 367 1 01/31/08 00:29 83-32-901/29/08 00:00Acenaphthylene 430 ug/kg 367 1 01/31/08 00:29 208-96-801/29/08 00:00Anthracene 954 ug/kg 367 1 01/31/08 00:29 120-12-701/29/08 00:00Benzo(a)anthracene 2090 ug/kg 367 1 01/31/08 00:29 56-55-301/29/08 00:00Benzo(a)pyrene 1940 ug/kg 367 1 01/31/08 00:29 50-32-801/29/08 00:00Benzo(b)fluoranthene 2520 ug/kg 367 1 01/31/08 00:29 205-99-201/29/08 00:00Benzo(g,h,i)perylene 1300 ug/kg 367 1 01/31/08 00:29 191-24-201/29/08 00:00Benzo(k)fluoranthene 1290 ug/kg 367 1 01/31/08 00:29 207-08-901/29/08 00:00Benzyl alcohol ND ug/kg 735 1 01/31/08 00:29 100-51-601/29/08 00:004-Bromophenylphenyl ether ND ug/kg 367 1 01/31/08 00:29 101-55-301/29/08 00:00Butylbenzylphthalate ND ug/kg 367 1 01/31/08 00:29 85-68-701/29/08 00:004-Chloro-3-methylphenol ND ug/kg 735 1 01/31/08 00:29 59-50-701/29/08 00:004-Chloroaniline ND ug/kg 735 1 01/31/08 00:29 106-47-801/29/08 00:00bis(2-Chloroethoxy)methane ND ug/kg 367 1 01/31/08 00:29 111-91-101/29/08 00:00bis(2-Chloroethyl) ether ND ug/kg 367 1 01/31/08 00:29 111-44-401/29/08 00:00bis(2-Chloroisopropyl) ether ND ug/kg 367 1 01/31/08 00:29 108-60-101/29/08 00:002-Chloronaphthalene ND ug/kg 367 1 01/31/08 00:29 91-58-701/29/08 00:002-Chlorophenol ND ug/kg 367 1 01/31/08 00:29 95-57-801/29/08 00:004-Chlorophenylphenyl ether ND ug/kg 367 1 01/31/08 00:29 7005-72-301/29/08 00:00Chrysene 2150 ug/kg 367 1 01/31/08 00:29 218-01-901/29/08 00:00Dibenz(a,h)anthracene ND ug/kg 367 1 01/31/08 00:29 53-70-301/29/08 00:00Dibenzofuran ND ug/kg 367 1 01/31/08 00:29 132-64-901/29/08 00:003,3'-Dichlorobenzidine ND ug/kg 735 1 01/31/08 00:29 91-94-101/29/08 00:00



Date: 02/11/2008 03:29 PM Page 38 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 367 1 01/31/08 00:29 120-83-201/29/08 00:00Diethylphthalate ND ug/kg 367 1 01/31/08 00:29 84-66-201/29/08 00:002,4-Dimethylphenol ND ug/kg 367 1 01/31/08 00:29 105-67-901/29/08 00:00Dimethylphthalate ND ug/kg 367 1 01/31/08 00:29 131-11-301/29/08 00:00Di-n-butylphthalate ND ug/kg 367 1 01/31/08 00:29 84-74-201/29/08 00:004,6-Dinitro-2-methylphenol ND ug/kg 1780 1 01/31/08 00:29 534-52-101/29/08 00:002,4-Dinitrophenol ND ug/kg 1780 1 01/31/08 00:29 51-28-501/29/08 00:002,4-Dinitrotoluene ND ug/kg 367 1 01/31/08 00:29 121-14-201/29/08 00:002,6-Dinitrotoluene ND ug/kg 367 1 01/31/08 00:29 606-20-201/29/08 00:00Di-n-octylphthalate ND ug/kg 367 1 01/31/08 00:29 117-84-001/29/08 00:00bis(2-Ethylhexyl)phthalate ND ug/kg 367 1 01/31/08 00:29 117-81-701/29/08 00:00Fluoranthene 4400 ug/kg 367 1 01/31/08 00:29 206-44-001/29/08 00:00Fluorene ND ug/kg 367 1 01/31/08 00:29 86-73-701/29/08 00:00Hexachloro-1,3-butadiene ND ug/kg 367 1 01/31/08 00:29 87-68-301/29/08 00:00Hexachlorobenzene ND ug/kg 367 1 01/31/08 00:29 118-74-101/29/08 00:00Hexachlorocyclopentadiene ND ug/kg 367 1 01/31/08 00:29 77-47-401/29/08 00:00Hexachloroethane ND ug/kg 367 1 01/31/08 00:29 67-72-101/29/08 00:00Indeno(1,2,3-cd)pyrene 1170 ug/kg 367 1 01/31/08 00:29 193-39-501/29/08 00:00Isophorone ND ug/kg 367 1 01/31/08 00:29 78-59-101/29/08 00:002-Methylnaphthalene ND ug/kg 367 1 01/31/08 00:29 91-57-601/29/08 00:002-Methylphenol(o-Cresol) ND ug/kg 367 1 01/31/08 00:29 95-48-701/29/08 00:003&4-Methylphenol(m&p Cresol) ND ug/kg 735 1 01/31/08 00:2901/29/08 00:00Naphthalene ND ug/kg 367 1 01/31/08 00:29 91-20-301/29/08 00:002-Nitroaniline ND ug/kg 1780 1 01/31/08 00:29 88-74-401/29/08 00:003-Nitroaniline ND ug/kg 1780 1 01/31/08 00:29 99-09-201/29/08 00:004-Nitroaniline ND ug/kg 1780 1 01/31/08 00:29 100-01-601/29/08 00:00Nitrobenzene ND ug/kg 367 1 01/31/08 00:29 98-95-301/29/08 00:002-Nitrophenol ND ug/kg 367 1 01/31/08 00:29 88-75-501/29/08 00:004-Nitrophenol ND ug/kg 1780 1 01/31/08 00:29 100-02-701/29/08 00:00N-Nitroso-di-n-propylamine ND ug/kg 367 1 01/31/08 00:29 621-64-701/29/08 00:00N-Nitrosodiphenylamine ND ug/kg 367 1 01/31/08 00:29 86-30-601/29/08 00:00Pentachlorophenol ND ug/kg 1780 1 01/31/08 00:29 87-86-501/29/08 00:00Phenanthrene 1920 ug/kg 334 1 01/31/08 00:29 85-01-801/29/08 00:00Phenol ND ug/kg 367 1 01/31/08 00:29 108-95-201/29/08 00:00Pyrene 3630 ug/kg 367 1 01/31/08 00:29 129-00-001/29/08 00:002,4,5-Trichlorophenol ND ug/kg 367 1 01/31/08 00:29 95-95-401/29/08 00:002,4,6-Trichlorophenol ND ug/kg 367 1 01/31/08 00:29 88-06-201/29/08 00:00Nitrobenzene-d5 (S) 71 % 50-117 1 01/31/08 00:29 4165-60-001/29/08 00:002-Fluorobiphenyl (S) 72 % 56-118 1 01/31/08 00:29 321-60-801/29/08 00:00Terphenyl-d14 (S) 75 % 55-118 1 01/31/08 00:29 1718-51-001/29/08 00:00Phenol-d6 (S) 71 % 41-124 1 01/31/08 00:29 13127-88-301/29/08 00:002-Fluorophenol (S) 72 % 35-117 1 01/31/08 00:29 367-12-401/29/08 00:002,4,6-Tribromophenol (S) 80 % 34-122 1 01/31/08 00:29 118-79-601/29/08 00:00



Date: 02/11/2008 03:29 PM Page 39 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 40 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




Isopropylbenzene (Cumene) ND ug/kg 4.2 1 01/29/08 19:25 98-82-8p-Isopropyltoluene ND ug/kg 4.2 1 01/29/08 19:25 99-87-6Methylene chloride ND ug/kg 16.9 1 01/29/08 19:25 75-09-24-Methyl-2-pentanone (MIBK) ND ug/kg 21.2 1 01/29/08 19:25 108-10-1Methyl-tert-butyl ether ND ug/kg 4.2 1 01/29/08 19:25 1634-04-4Naphthalene 209 ug/kg 4.2 1 01/29/08 19:25 91-20-3n-Propylbenzene ND ug/kg 4.2 1 01/29/08 19:25 103-65-1Styrene ND ug/kg 4.2 1 01/29/08 19:25 100-42-51,1,1,2-Tetrachloroethane ND ug/kg 4.2 1 01/29/08 19:25 630-20-61,1,2,2-Tetrachloroethane ND ug/kg 4.2 1 01/29/08 19:25 79-34-5Tetrachloroethene ND ug/kg 4.2 1 01/29/08 19:25 127-18-4Toluene ND ug/kg 4.2 1 01/29/08 19:25 108-88-31,2,3-Trichlorobenzene ND ug/kg 4.2 1 01/29/08 19:25 87-61-61,2,4-Trichlorobenzene ND ug/kg 4.2 1 01/29/08 19:25 120-82-11,1,1-Trichloroethane ND ug/kg 4.2 1 01/29/08 19:25 71-55-61,1,2-Trichloroethane ND ug/kg 4.2 1 01/29/08 19:25 79-00-5Trichloroethene ND ug/kg 4.2 1 01/29/08 19:25 79-01-6Trichlorofluoromethane ND ug/kg 4.2 1 01/29/08 19:25 75-69-41,2,3-Trichloropropane ND ug/kg 4.2 1 01/29/08 19:25 96-18-41,2,4-Trimethylbenzene ND ug/kg 4.2 1 01/29/08 19:25 95-63-61,3,5-Trimethylbenzene ND ug/kg 4.2 1 01/29/08 19:25 108-67-8Vinyl acetate ND ug/kg 84.7 1 01/29/08 19:25 108-05-4Vinyl chloride ND ug/kg 4.2 1 01/29/08 19:25 75-01-4Xylene (Total) ND ug/kg 8.5 1 01/29/08 19:25 1330-20-7Dibromofluoromethane (S) 97 % 82-130 1 01/29/08 19:25 1868-53-7Toluene-d8 (S) 100 % 81-120 1 01/29/08 19:25 2037-26-54-Bromofluorobenzene (S) 95 % 65-117 1 01/29/08 19:25 460-00-4





Date: 02/11/2008 03:29 PM Page 41 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




PCB-1016 (Aroclor 1016) ND ug/kg 803 20 02/08/08 15:30 12674-11-202/05/08 00:00PCB-1221 (Aroclor 1221) ND ug/kg 803 20 02/08/08 15:30 11104-28-202/05/08 00:00PCB-1232 (Aroclor 1232) ND ug/kg 803 20 02/08/08 15:30 11141-16-502/05/08 00:00PCB-1242 (Aroclor 1242) ND ug/kg 803 20 02/08/08 15:30 53469-21-902/05/08 00:00PCB-1248 (Aroclor 1248) ND ug/kg 803 20 02/08/08 15:30 12672-29-602/05/08 00:00PCB-1254 (Aroclor 1254) 1790 ug/kg 803 20 02/08/08 15:30 11097-69-102/05/08 00:00PCB-1260 (Aroclor 1260) ND ug/kg 803 20 02/08/08 15:30 11096-82-502/05/08 00:00Tetrachloro-m-xylene (S) 0 % 20-130 20 02/08/08 15:30 877-09-8 S402/05/08 00:00


Arsenic 9.0 mg/kg 2.2 1 02/01/08 10:17 7440-38-201/31/08 00:00Barium 382 mg/kg 2.2 1 02/01/08 10:17 7440-39-301/31/08 00:00Cadmium ND mg/kg 2.2 1 02/01/08 10:17 7440-43-901/31/08 00:00Chromium 149 mg/kg 2.2 1 02/01/08 10:17 7440-47-301/31/08 00:00Lead 1480 mg/kg 2.2 1 02/01/08 10:17 7439-92-101/31/08 00:00Selenium 3.8 mg/kg 2.2 1 02/01/08 10:17 7782-49-201/31/08 00:00Silver ND mg/kg 2.2 1 02/01/08 10:17 7440-22-401/31/08 00:00


Mercury ND mg/kg 0.38 1 01/29/08 17:02 7439-97-601/28/08 00:00



Acenaphthene ND ug/kg 379 1 01/31/08 00:09 83-32-901/29/08 00:00Acenaphthylene ND ug/kg 379 1 01/31/08 00:09 208-96-801/29/08 00:00Anthracene ND ug/kg 379 1 01/31/08 00:09 120-12-701/29/08 00:00Benzo(a)anthracene 544 ug/kg 379 1 01/31/08 00:09 56-55-301/29/08 00:00Benzo(a)pyrene 567 ug/kg 379 1 01/31/08 00:09 50-32-801/29/08 00:00Benzo(b)fluoranthene 843 ug/kg 379 1 01/31/08 00:09 205-99-201/29/08 00:00Benzo(g,h,i)perylene 380 ug/kg 379 1 01/31/08 00:09 191-24-201/29/08 00:00Benzo(k)fluoranthene ND ug/kg 379 1 01/31/08 00:09 207-08-901/29/08 00:00Benzyl alcohol ND ug/kg 757 1 01/31/08 00:09 100-51-601/29/08 00:004-Bromophenylphenyl ether ND ug/kg 379 1 01/31/08 00:09 101-55-301/29/08 00:00Butylbenzylphthalate ND ug/kg 379 1 01/31/08 00:09 85-68-701/29/08 00:004-Chloro-3-methylphenol ND ug/kg 757 1 01/31/08 00:09 59-50-701/29/08 00:004-Chloroaniline ND ug/kg 757 1 01/31/08 00:09 106-47-801/29/08 00:00bis(2-Chloroethoxy)methane ND ug/kg 379 1 01/31/08 00:09 111-91-101/29/08 00:00bis(2-Chloroethyl) ether ND ug/kg 379 1 01/31/08 00:09 111-44-401/29/08 00:00bis(2-Chloroisopropyl) ether ND ug/kg 379 1 01/31/08 00:09 108-60-101/29/08 00:002-Chloronaphthalene ND ug/kg 379 1 01/31/08 00:09 91-58-701/29/08 00:002-Chlorophenol ND ug/kg 379 1 01/31/08 00:09 95-57-801/29/08 00:004-Chlorophenylphenyl ether ND ug/kg 379 1 01/31/08 00:09 7005-72-301/29/08 00:00Chrysene 595 ug/kg 379 1 01/31/08 00:09 218-01-901/29/08 00:00Dibenz(a,h)anthracene ND ug/kg 379 1 01/31/08 00:09 53-70-301/29/08 00:00Dibenzofuran ND ug/kg 379 1 01/31/08 00:09 132-64-901/29/08 00:003,3'-Dichlorobenzidine ND ug/kg 757 1 01/31/08 00:09 91-94-101/29/08 00:00



Date: 02/11/2008 03:29 PM Page 42 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 379 1 01/31/08 00:09 120-83-201/29/08 00:00Diethylphthalate ND ug/kg 379 1 01/31/08 00:09 84-66-201/29/08 00:002,4-Dimethylphenol ND ug/kg 379 1 01/31/08 00:09 105-67-901/29/08 00:00Dimethylphthalate ND ug/kg 379 1 01/31/08 00:09 131-11-301/29/08 00:00Di-n-butylphthalate ND ug/kg 379 1 01/31/08 00:09 84-74-201/29/08 00:004,6-Dinitro-2-methylphenol ND ug/kg 1840 1 01/31/08 00:09 534-52-101/29/08 00:002,4-Dinitrophenol ND ug/kg 1840 1 01/31/08 00:09 51-28-501/29/08 00:002,4-Dinitrotoluene ND ug/kg 379 1 01/31/08 00:09 121-14-201/29/08 00:002,6-Dinitrotoluene ND ug/kg 379 1 01/31/08 00:09 606-20-201/29/08 00:00Di-n-octylphthalate ND ug/kg 379 1 01/31/08 00:09 117-84-001/29/08 00:00bis(2-Ethylhexyl)phthalate ND ug/kg 379 1 01/31/08 00:09 117-81-701/29/08 00:00Fluoranthene 1090 ug/kg 379 1 01/31/08 00:09 206-44-001/29/08 00:00Fluorene ND ug/kg 379 1 01/31/08 00:09 86-73-701/29/08 00:00Hexachloro-1,3-butadiene ND ug/kg 379 1 01/31/08 00:09 87-68-301/29/08 00:00Hexachlorobenzene ND ug/kg 379 1 01/31/08 00:09 118-74-101/29/08 00:00Hexachlorocyclopentadiene ND ug/kg 379 1 01/31/08 00:09 77-47-401/29/08 00:00Hexachloroethane ND ug/kg 379 1 01/31/08 00:09 67-72-101/29/08 00:00Indeno(1,2,3-cd)pyrene ND ug/kg 379 1 01/31/08 00:09 193-39-501/29/08 00:00Isophorone ND ug/kg 379 1 01/31/08 00:09 78-59-101/29/08 00:002-Methylnaphthalene ND ug/kg 379 1 01/31/08 00:09 91-57-601/29/08 00:002-Methylphenol(o-Cresol) ND ug/kg 379 1 01/31/08 00:09 95-48-701/29/08 00:003&4-Methylphenol(m&p Cresol) ND ug/kg 757 1 01/31/08 00:0901/29/08 00:00Naphthalene ND ug/kg 379 1 01/31/08 00:09 91-20-301/29/08 00:002-Nitroaniline ND ug/kg 1840 1 01/31/08 00:09 88-74-401/29/08 00:003-Nitroaniline ND ug/kg 1840 1 01/31/08 00:09 99-09-201/29/08 00:004-Nitroaniline ND ug/kg 1840 1 01/31/08 00:09 100-01-601/29/08 00:00Nitrobenzene ND ug/kg 379 1 01/31/08 00:09 98-95-301/29/08 00:002-Nitrophenol ND ug/kg 379 1 01/31/08 00:09 88-75-501/29/08 00:004-Nitrophenol ND ug/kg 1840 1 01/31/08 00:09 100-02-701/29/08 00:00N-Nitroso-di-n-propylamine ND ug/kg 379 1 01/31/08 00:09 621-64-701/29/08 00:00N-Nitrosodiphenylamine ND ug/kg 379 1 01/31/08 00:09 86-30-601/29/08 00:00Pentachlorophenol ND ug/kg 1840 1 01/31/08 00:09 87-86-501/29/08 00:00Phenanthrene 636 ug/kg 344 1 01/31/08 00:09 85-01-801/29/08 00:00Phenol ND ug/kg 379 1 01/31/08 00:09 108-95-201/29/08 00:00Pyrene 942 ug/kg 379 1 01/31/08 00:09 129-00-001/29/08 00:002,4,5-Trichlorophenol ND ug/kg 379 1 01/31/08 00:09 95-95-401/29/08 00:002,4,6-Trichlorophenol ND ug/kg 379 1 01/31/08 00:09 88-06-201/29/08 00:00Nitrobenzene-d5 (S) 71 % 50-117 1 01/31/08 00:09 4165-60-001/29/08 00:002-Fluorobiphenyl (S) 75 % 56-118 1 01/31/08 00:09 321-60-801/29/08 00:00Terphenyl-d14 (S) 77 % 55-118 1 01/31/08 00:09 1718-51-001/29/08 00:00Phenol-d6 (S) 69 % 41-124 1 01/31/08 00:09 13127-88-301/29/08 00:002-Fluorophenol (S) 67 % 35-117 1 01/31/08 00:09 367-12-401/29/08 00:002,4,6-Tribromophenol (S) 72 % 34-122 1 01/31/08 00:09 118-79-601/29/08 00:00



Date: 02/11/2008 03:29 PM Page 43 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 44 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 45 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.40 1 01/29/08 17:04 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 46 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 47 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 48 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 49 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




PCB-1016 (Aroclor 1016) ND ug/kg 199 5 02/06/08 15:45 12674-11-2 3d02/05/08 00:00PCB-1221 (Aroclor 1221) ND ug/kg 199 5 02/06/08 15:45 11104-28-202/05/08 00:00PCB-1232 (Aroclor 1232) ND ug/kg 199 5 02/06/08 15:45 11141-16-502/05/08 00:00PCB-1242 (Aroclor 1242) ND ug/kg 199 5 02/06/08 15:45 53469-21-902/05/08 00:00PCB-1248 (Aroclor 1248) ND ug/kg 199 5 02/06/08 15:45 12672-29-602/05/08 00:00PCB-1254 (Aroclor 1254) ND ug/kg 199 5 02/06/08 15:45 11097-69-102/05/08 00:00PCB-1260 (Aroclor 1260) ND ug/kg 199 5 02/06/08 15:45 11096-82-502/05/08 00:00Tetrachloro-m-xylene (S) 0 % 28-137 5 02/06/08 15:45 877-09-8 S402/05/08 00:00




Mercury ND mg/kg 0.37 1 01/29/08 17:08 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 50 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 3750 10 01/31/08 01:53 120-83-201/29/08 00:00Diethylphthalate ND ug/kg 3750 10 01/31/08 01:53 84-66-201/29/08 00:002,4-Dimethylphenol ND ug/kg 3750 10 01/31/08 01:53 105-67-901/29/08 00:00Dimethylphthalate ND ug/kg 3750 10 01/31/08 01:53 131-11-301/29/08 00:00Di-n-butylphthalate ND ug/kg 3750 10 01/31/08 01:53 84-74-201/29/08 00:004,6-Dinitro-2-methylphenol ND ug/kg 18200 10 01/31/08 01:53 534-52-101/29/08 00:002,4-Dinitrophenol ND ug/kg 18200 10 01/31/08 01:53 51-28-501/29/08 00:002,4-Dinitrotoluene ND ug/kg 3750 10 01/31/08 01:53 121-14-201/29/08 00:002,6-Dinitrotoluene ND ug/kg 3750 10 01/31/08 01:53 606-20-201/29/08 00:00Di-n-octylphthalate ND ug/kg 3750 10 01/31/08 01:53 117-84-001/29/08 00:00bis(2-Ethylhexyl)phthalate ND ug/kg 3750 10 01/31/08 01:53 117-81-701/29/08 00:00Fluoranthene ND ug/kg 3750 10 01/31/08 01:53 206-44-001/29/08 00:00Fluorene ND ug/kg 3750 10 01/31/08 01:53 86-73-701/29/08 00:00Hexachloro-1,3-butadiene ND ug/kg 3750 10 01/31/08 01:53 87-68-301/29/08 00:00Hexachlorobenzene ND ug/kg 3750 10 01/31/08 01:53 118-74-101/29/08 00:00Hexachlorocyclopentadiene ND ug/kg 3750 10 01/31/08 01:53 77-47-401/29/08 00:00Hexachloroethane ND ug/kg 3750 10 01/31/08 01:53 67-72-101/29/08 00:00Indeno(1,2,3-cd)pyrene ND ug/kg 3750 10 01/31/08 01:53 193-39-501/29/08 00:00Isophorone ND ug/kg 3750 10 01/31/08 01:53 78-59-101/29/08 00:002-Methylnaphthalene ND ug/kg 3750 10 01/31/08 01:53 91-57-601/29/08 00:002-Methylphenol(o-Cresol) ND ug/kg 3750 10 01/31/08 01:53 95-48-701/29/08 00:003&4-Methylphenol(m&p Cresol) ND ug/kg 7500 10 01/31/08 01:5301/29/08 00:00Naphthalene ND ug/kg 3750 10 01/31/08 01:53 91-20-301/29/08 00:002-Nitroaniline ND ug/kg 18200 10 01/31/08 01:53 88-74-401/29/08 00:003-Nitroaniline ND ug/kg 18200 10 01/31/08 01:53 99-09-201/29/08 00:004-Nitroaniline ND ug/kg 18200 10 01/31/08 01:53 100-01-601/29/08 00:00Nitrobenzene ND ug/kg 3750 10 01/31/08 01:53 98-95-301/29/08 00:002-Nitrophenol ND ug/kg 3750 10 01/31/08 01:53 88-75-501/29/08 00:004-Nitrophenol ND ug/kg 18200 10 01/31/08 01:53 100-02-701/29/08 00:00N-Nitroso-di-n-propylamine ND ug/kg 3750 10 01/31/08 01:53 621-64-701/29/08 00:00N-Nitrosodiphenylamine ND ug/kg 3750 10 01/31/08 01:53 86-30-601/29/08 00:00Pentachlorophenol ND ug/kg 18200 10 01/31/08 01:53 87-86-501/29/08 00:00Phenanthrene ND ug/kg 3410 10 01/31/08 01:53 85-01-801/29/08 00:00Phenol ND ug/kg 3750 10 01/31/08 01:53 108-95-2 4d01/29/08 00:00Pyrene ND ug/kg 3750 10 01/31/08 01:53 129-00-001/29/08 00:002,4,5-Trichlorophenol ND ug/kg 3750 10 01/31/08 01:53 95-95-401/29/08 00:002,4,6-Trichlorophenol ND ug/kg 3750 10 01/31/08 01:53 88-06-201/29/08 00:00Nitrobenzene-d5 (S) 76 % 50-117 10 01/31/08 01:53 4165-60-001/29/08 00:002-Fluorobiphenyl (S) 83 % 56-118 10 01/31/08 01:53 321-60-801/29/08 00:00Terphenyl-d14 (S) 83 % 55-118 10 01/31/08 01:53 1718-51-001/29/08 00:00Phenol-d6 (S) 79 % 41-124 10 01/31/08 01:53 13127-88-301/29/08 00:002-Fluorophenol (S) 77 % 35-117 10 01/31/08 01:53 367-12-401/29/08 00:002,4,6-Tribromophenol (S) 77 % 34-122 10 01/31/08 01:53 118-79-601/29/08 00:00



Date: 02/11/2008 03:29 PM Page 51 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 52 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 53 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Mercury ND mg/kg 0.40 1 01/29/08 16:23 7439-97-601/28/08 00:00






Date: 02/11/2008 03:29 PM Page 54 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002








Date: 02/11/2008 03:29 PM Page 55 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002




Acetone 115 ug/kg 87.7 1 01/29/08 21:41 67-64-1Acrolein ND ug/kg 87.7 1 01/29/08 21:41 107-02-8Acrylonitrile ND ug/kg 87.7 1 01/29/08 21:41 107-13-1Benzene ND ug/kg 4.4 1 01/29/08 21:41 71-43-2Bromobenzene ND ug/kg 4.4 1 01/29/08 21:41 108-86-1Bromochloromethane ND ug/kg 4.4 1 01/29/08 21:41 74-97-5Bromodichloromethane ND ug/kg 4.4 1 01/29/08 21:41 75-27-4Bromoform ND ug/kg 4.4 1 01/29/08 21:41 75-25-2Bromomethane ND ug/kg 4.4 1 01/29/08 21:41 74-83-92-Butanone (MEK) ND ug/kg 21.9 1 01/29/08 21:41 78-93-3n-Butylbenzene ND ug/kg 4.4 1 01/29/08 21:41 104-51-8sec-Butylbenzene ND ug/kg 4.4 1 01/29/08 21:41 135-98-8tert-Butylbenzene ND ug/kg 4.4 1 01/29/08 21:41 98-06-6Carbon disulfide ND ug/kg 8.8 1 01/29/08 21:41 75-15-0Carbon tetrachloride ND ug/kg 4.4 1 01/29/08 21:41 56-23-5Chlorobenzene ND ug/kg 4.4 1 01/29/08 21:41 108-90-7Chloroethane ND ug/kg 4.4 1 01/29/08 21:41 75-00-3Chloroform ND ug/kg 4.4 1 01/29/08 21:41 67-66-3Chloromethane ND ug/kg 4.4 1 01/29/08 21:41 74-87-32-Chlorotoluene ND ug/kg 4.4 1 01/29/08 21:41 95-49-84-Chlorotoluene ND ug/kg 4.4 1 01/29/08 21:41 106-43-4Dibromochloromethane ND ug/kg 4.4 1 01/29/08 21:41 124-48-11,2-Dibromoethane (EDB) ND ug/kg 4.4 1 01/29/08 21:41 106-93-4Dibromomethane ND ug/kg 4.4 1 01/29/08 21:41 74-95-31,2-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 21:41 95-50-11,3-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 21:41 541-73-11,4-Dichlorobenzene ND ug/kg 4.4 1 01/29/08 21:41 106-46-7trans-1,4-Dichloro-2-butene ND ug/kg 87.7 1 01/29/08 21:41 110-57-6Dichlorodifluoromethane ND ug/kg 4.4 1 01/29/08 21:41 75-71-81,1-Dichloroethane ND ug/kg 4.4 1 01/29/08 21:41 75-34-31,2-Dichloroethane ND ug/kg 4.4 1 01/29/08 21:41 107-06-21,1-Dichloroethene ND ug/kg 4.4 1 01/29/08 21:41 75-35-4cis-1,2-Dichloroethene ND ug/kg 4.4 1 01/29/08 21:41 156-59-2trans-1,2-Dichloroethene ND ug/kg 4.4 1 01/29/08 21:41 156-60-51,2-Dichloropropane ND ug/kg 4.4 1 01/29/08 21:41 78-87-51,3-Dichloropropane ND ug/kg 4.4 1 01/29/08 21:41 142-28-92,2-Dichloropropane ND ug/kg 4.4 1 01/29/08 21:41 594-20-71,1-Dichloropropene ND ug/kg 4.4 1 01/29/08 21:41 563-58-6cis-1,3-Dichloropropene ND ug/kg 4.4 1 01/29/08 21:41 10061-01-5trans-1,3-Dichloropropene ND ug/kg 4.4 1 01/29/08 21:41 10061-02-6Ethylbenzene ND ug/kg 4.4 1 01/29/08 21:41 100-41-4Ethyl methacrylate ND ug/kg 8.8 1 01/29/08 21:41 97-63-2Hexachloro-1,3-butadiene ND ug/kg 4.4 1 01/29/08 21:41 87-68-3n-Hexane ND ug/kg 4.4 1 01/29/08 21:41 110-54-32-Hexanone ND ug/kg 87.7 1 01/29/08 21:41 591-78-6Iodomethane ND ug/kg 87.7 1 01/29/08 21:41 74-88-4



Date: 02/11/2008 03:29 PM Page 56 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 57 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002






Arsenic 7.7 mg/kg 2.2 1 02/01/08 10:40 7440-38-201/31/08 00:00Barium 52.6 mg/kg 2.2 1 02/01/08 10:40 7440-39-301/31/08 00:00Cadmium ND mg/kg 2.2 1 02/01/08 10:40 7440-43-901/31/08 00:00Chromium 19.8 mg/kg 2.2 1 02/01/08 10:40 7440-47-301/31/08 00:00Lead 101 mg/kg 2.2 1 02/01/08 10:40 7439-92-101/31/08 00:00Selenium 2.1 mg/kg 2.2 1 02/01/08 10:40 7782-49-201/31/08 00:00Silver ND mg/kg 2.2 1 02/01/08 10:40 7440-22-401/31/08 00:00


Mercury ND mg/kg 0.36 1 01/29/08 16:25 7439-97-601/28/08 00:00



Acenaphthene ND ug/kg 371 1 02/04/08 14:24 83-32-902/01/08 20:55Acenaphthylene ND ug/kg 371 1 02/04/08 14:24 208-96-802/01/08 20:55Anthracene 400 ug/kg 371 1 02/04/08 14:24 120-12-702/01/08 20:55Benzo(a)anthracene 1020 ug/kg 371 1 02/04/08 14:24 56-55-302/01/08 20:55Benzo(a)pyrene 777 ug/kg 371 1 02/04/08 14:24 50-32-802/01/08 20:55Benzo(b)fluoranthene 942 ug/kg 371 1 02/04/08 14:24 205-99-202/01/08 20:55Benzo(g,h,i)perylene 440 ug/kg 371 1 02/04/08 14:24 191-24-202/01/08 20:55Benzo(k)fluoranthene 482 ug/kg 371 1 02/04/08 14:24 207-08-902/01/08 20:55Benzyl alcohol ND ug/kg 742 1 02/04/08 14:24 100-51-602/01/08 20:554-Bromophenylphenyl ether ND ug/kg 371 1 02/04/08 14:24 101-55-302/01/08 20:55Butylbenzylphthalate ND ug/kg 371 1 02/04/08 14:24 85-68-702/01/08 20:554-Chloro-3-methylphenol ND ug/kg 742 1 02/04/08 14:24 59-50-702/01/08 20:554-Chloroaniline ND ug/kg 742 1 02/04/08 14:24 106-47-802/01/08 20:55bis(2-Chloroethoxy)methane ND ug/kg 371 1 02/04/08 14:24 111-91-102/01/08 20:55bis(2-Chloroethyl) ether ND ug/kg 371 1 02/04/08 14:24 111-44-402/01/08 20:55bis(2-Chloroisopropyl) ether ND ug/kg 371 1 02/04/08 14:24 108-60-102/01/08 20:552-Chloronaphthalene ND ug/kg 371 1 02/04/08 14:24 91-58-702/01/08 20:552-Chlorophenol ND ug/kg 371 1 02/04/08 14:24 95-57-802/01/08 20:554-Chlorophenylphenyl ether ND ug/kg 371 1 02/04/08 14:24 7005-72-302/01/08 20:55Chrysene 1050 ug/kg 371 1 02/04/08 14:24 218-01-902/01/08 20:55Dibenz(a,h)anthracene ND ug/kg 371 1 02/04/08 14:24 53-70-302/01/08 20:55Dibenzofuran ND ug/kg 371 1 02/04/08 14:24 132-64-902/01/08 20:553,3'-Dichlorobenzidine ND ug/kg 742 1 02/04/08 14:24 91-94-102/01/08 20:55



Date: 02/11/2008 03:29 PM Page 58 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002





2,4-Dichlorophenol ND ug/kg 371 1 02/04/08 14:24 120-83-202/01/08 20:55Diethylphthalate ND ug/kg 371 1 02/04/08 14:24 84-66-202/01/08 20:552,4-Dimethylphenol ND ug/kg 371 1 02/04/08 14:24 105-67-902/01/08 20:55Dimethylphthalate ND ug/kg 371 1 02/04/08 14:24 131-11-302/01/08 20:55Di-n-butylphthalate ND ug/kg 371 1 02/04/08 14:24 84-74-202/01/08 20:554,6-Dinitro-2-methylphenol ND ug/kg 1800 1 02/04/08 14:24 534-52-102/01/08 20:552,4-Dinitrophenol ND ug/kg 1800 1 02/04/08 14:24 51-28-502/01/08 20:552,4-Dinitrotoluene ND ug/kg 371 1 02/04/08 14:24 121-14-202/01/08 20:552,6-Dinitrotoluene ND ug/kg 371 1 02/04/08 14:24 606-20-202/01/08 20:55Di-n-octylphthalate ND ug/kg 371 1 02/04/08 14:24 117-84-002/01/08 20:55bis(2-Ethylhexyl)phthalate ND ug/kg 371 1 02/04/08 14:24 117-81-702/01/08 20:55Fluoranthene 1690 ug/kg 371 1 02/04/08 14:24 206-44-002/01/08 20:55Fluorene ND ug/kg 371 1 02/04/08 14:24 86-73-702/01/08 20:55Hexachloro-1,3-butadiene ND ug/kg 371 1 02/04/08 14:24 87-68-302/01/08 20:55Hexachlorobenzene ND ug/kg 371 1 02/04/08 14:24 118-74-102/01/08 20:55Hexachlorocyclopentadiene ND ug/kg 371 1 02/04/08 14:24 77-47-402/01/08 20:55Hexachloroethane ND ug/kg 371 1 02/04/08 14:24 67-72-102/01/08 20:55Indeno(1,2,3-cd)pyrene 407 ug/kg 371 1 02/04/08 14:24 193-39-502/01/08 20:55Isophorone ND ug/kg 371 1 02/04/08 14:24 78-59-102/01/08 20:552-Methylnaphthalene ND ug/kg 371 1 02/04/08 14:24 91-57-602/01/08 20:552-Methylphenol(o-Cresol) ND ug/kg 371 1 02/04/08 14:24 95-48-702/01/08 20:553&4-Methylphenol(m&p Cresol) ND ug/kg 742 1 02/04/08 14:2402/01/08 20:55Naphthalene ND ug/kg 371 1 02/04/08 14:24 91-20-302/01/08 20:552-Nitroaniline ND ug/kg 1800 1 02/04/08 14:24 88-74-402/01/08 20:553-Nitroaniline ND ug/kg 1800 1 02/04/08 14:24 99-09-202/01/08 20:554-Nitroaniline ND ug/kg 1800 1 02/04/08 14:24 100-01-602/01/08 20:55Nitrobenzene ND ug/kg 371 1 02/04/08 14:24 98-95-302/01/08 20:552-Nitrophenol ND ug/kg 371 1 02/04/08 14:24 88-75-502/01/08 20:554-Nitrophenol ND ug/kg 1800 1 02/04/08 14:24 100-02-702/01/08 20:55N-Nitroso-di-n-propylamine ND ug/kg 371 1 02/04/08 14:24 621-64-702/01/08 20:55N-Nitrosodiphenylamine ND ug/kg 371 1 02/04/08 14:24 86-30-602/01/08 20:55Pentachlorophenol ND ug/kg 1800 1 02/04/08 14:24 87-86-502/01/08 20:55Phenanthrene 976 ug/kg 337 1 02/04/08 14:24 85-01-802/01/08 20:55Phenol ND ug/kg 371 1 02/04/08 14:24 108-95-202/01/08 20:55Pyrene 1310 ug/kg 371 1 02/04/08 14:24 129-00-002/01/08 20:552,4,5-Trichlorophenol ND ug/kg 371 1 02/04/08 14:24 95-95-402/01/08 20:552,4,6-Trichlorophenol ND ug/kg 371 1 02/04/08 14:24 88-06-202/01/08 20:55Nitrobenzene-d5 (S) 66 % 50-117 1 02/04/08 14:24 4165-60-002/01/08 20:552-Fluorobiphenyl (S) 82 % 56-118 1 02/04/08 14:24 321-60-802/01/08 20:55Terphenyl-d14 (S) 77 % 55-118 1 02/04/08 14:24 1718-51-002/01/08 20:55Phenol-d6 (S) 70 % 41-124 1 02/04/08 14:24 13127-88-302/01/08 20:552-Fluorophenol (S) 77 % 35-117 1 02/04/08 14:24 367-12-402/01/08 20:552,4,6-Tribromophenol (S) 77 % 34-122 1 02/04/08 14:24 118-79-602/01/08 20:55



Date: 02/11/2008 03:29 PM Page 59 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002







Date: 02/11/2008 03:29 PM Page 60 of 90



(317)875-5894

ANALYTICAL RESULTS


5011474Beech Grove 6892.002









Date: 02/11/2008 03:29 PM Page 61 of 90



(317)875-5894

QUALITY CONTROL DATA


5011474Beech Grove 6892.002

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

MERP/1508EPA 7471

EPA 74717471 Mercury

Associated Lab Samples: 5011474013, 5011474014

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 126575


Mercury mg/kg ND 0.33

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

126576LABORATORY CONTROL SAMPLE:LCSSpike

Mercury mg/kg 0.51.5 101 80-120

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

126577MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

5011473001

126578

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .62 110 75-125101 8 20.62ND 0.72 0.66



Date: 02/11/2008 03:29 PM Page 62 of 90



(317)875-5894



5011474Beech Grove 6892.002



MERP/1509EPA 7471


Associated Lab Samples: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,5011474009, 5011474010, 5011474011, 5011474012





Mercury mg/kg ND 0.33

Parameter UnitsLCS



Mercury mg/kg 0.50.5 101 80-120

Parameter UnitsMS



MSSpikeResult

5011471001

126582

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .53 101 75-125100 1 20.53ND 0.53 0.53



Date: 02/11/2008 03:29 PM Page 63 of 90



(317)875-5894



5011474Beech Grove 6892.002



OEXT/5896EPA 3546

EPA 82708270 Solid MSSV Microwave Short Spike

Associated Lab Samples: 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013





2,4,5-Trichlorophenol ug/kg ND 3302,4,6-Trichlorophenol ug/kg ND 3302,4-Dichlorophenol ug/kg ND 3302,4-Dimethylphenol ug/kg ND 3302,4-Dinitrophenol ug/kg ND 16002,4-Dinitrotoluene ug/kg ND 3302,6-Dinitrotoluene ug/kg ND 3302-Chloronaphthalene ug/kg ND 3302-Chlorophenol ug/kg ND 3302-Methylnaphthalene ug/kg ND 3302-Methylphenol(o-Cresol) ug/kg ND 3302-Nitroaniline ug/kg ND 16002-Nitrophenol ug/kg ND 3303&4-Methylphenol(m&p Cresol) ug/kg ND 6603,3'-Dichlorobenzidine ug/kg ND 6603-Nitroaniline ug/kg ND 16004,6-Dinitro-2-methylphenol ug/kg ND 16004-Bromophenylphenyl ether ug/kg ND 3304-Chloro-3-methylphenol ug/kg ND 6604-Chloroaniline ug/kg ND 6604-Chlorophenylphenyl ether ug/kg ND 3304-Nitroaniline ug/kg ND 16004-Nitrophenol ug/kg ND 1600Acenaphthene ug/kg ND 330Acenaphthylene ug/kg ND 330Anthracene ug/kg ND 330Benzo(a)anthracene ug/kg ND 330Benzo(a)pyrene ug/kg ND 330Benzo(b)fluoranthene ug/kg ND 330Benzo(g,h,i)perylene ug/kg ND 330Benzo(k)fluoranthene ug/kg ND 330Benzyl alcohol ug/kg ND 660bis(2-Chloroethoxy)methane ug/kg ND 330bis(2-Chloroethyl) ether ug/kg ND 330bis(2-Chloroisopropyl) ether ug/kg ND 330bis(2-Ethylhexyl)phthalate ug/kg ND 330Butylbenzylphthalate ug/kg ND 330Chrysene ug/kg ND 330Di-n-butylphthalate ug/kg ND 330 JDi-n-octylphthalate ug/kg ND 330Dibenz(a,h)anthracene ug/kg ND 330Dibenzofuran ug/kg ND 330Diethylphthalate ug/kg ND 330



Date: 02/11/2008 03:29 PM Page 64 of 90



(317)875-5894



5011474Beech Grove 6892.002





Dimethylphthalate ug/kg ND 330Fluoranthene ug/kg ND 330Fluorene ug/kg ND 330Hexachloro-1,3-butadiene ug/kg ND 330Hexachlorobenzene ug/kg ND 330Hexachlorocyclopentadiene ug/kg ND 330Hexachloroethane ug/kg ND 330Indeno(1,2,3-cd)pyrene ug/kg ND 330Isophorone ug/kg ND 330N-Nitroso-di-n-propylamine ug/kg ND 330N-Nitrosodiphenylamine ug/kg ND 330Naphthalene ug/kg ND 330Nitrobenzene ug/kg ND 330Pentachlorophenol ug/kg ND 1600Phenanthrene ug/kg ND 300Phenol ug/kg ND 330Pyrene ug/kg ND 3302,4,6-Tribromophenol (S) % 73 34-1222-Fluorobiphenyl (S) % 79 56-1182-Fluorophenol (S) % 77 35-117Nitrobenzene-d5 (S) % 73 50-117Phenol-d6 (S) % 72 41-124Terphenyl-d14 (S) % 77 55-118

Parameter UnitsLCS



2,4-Dinitrotoluene ug/kg 27503330 82 54-1242-Chlorophenol ug/kg 27303330 82 56-1114-Chloro-3-methylphenol ug/kg 26403330 79 61-1154-Nitrophenol ug/kg 28803330 86 42-122Acenaphthene ug/kg 28703330 86 57-113N-Nitroso-di-n-propylamine ug/kg 26403330 79 52-128Pentachlorophenol ug/kg 23103330 69 24-132Phenol ug/kg 28303330 85 54-117Pyrene ug/kg 28503330 85 51-1192,4,6-Tribromophenol (S) % 79 34-1222-Fluorobiphenyl (S) % 82 56-1182-Fluorophenol (S) % 81 35-117Nitrobenzene-d5 (S) % 78 50-117Phenol-d6 (S) % 81 41-124Terphenyl-d14 (S) % 82 55-118



Date: 02/11/2008 03:29 PM Page 65 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsMS



MSSpikeResult

5011538002

126810

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2,4-Dinitrotoluene ug/kg R14370 113 57-12171 45 204370ND 4940 31202-Chlorophenol ug/kg R14370 122 35-12567 58 204370ND 5320 29304-Chloro-3-methylphenol ug/kg R14370 106 55-12060 55 204370ND 4620 26304-Nitrophenol ug/kg R14370 121 27-13073 49 204370ND 5280 3200Acenaphthene ug/kg M0,R14370 135 55-11480 51 204370ND 5890 3480N-Nitroso-di-n-propylamine ug/kg R14370 130 40-13377 51 204370ND 5680 3380Pentachlorophenol ug/kg 4370 79 10-13546 204370ND 3470 2000JPhenol ug/kg R14370 118 36-13067 55 204370ND 5160 2930Pyrene ug/kg 4370 105 51-121110 4 204370563 5170 53602,4,6-Tribromophenol (S) % R153 34-12268 202-Fluorobiphenyl (S) % 67 56-11875 202-Fluorophenol (S) % 62 35-11768 20Nitrobenzene-d5 (S) % 62 50-11767 20Phenol-d6 (S) % R155 41-12470 20Terphenyl-d14 (S) % R1,S051 55-11868 20



Date: 02/11/2008 03:29 PM Page 66 of 90



(317)875-5894



5011474Beech Grove 6892.002



OEXT/5909EPA 3546


Associated Lab Samples: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005





2,4,5-Trichlorophenol ug/kg ND 3302,4,6-Trichlorophenol ug/kg ND 3302,4-Dichlorophenol ug/kg ND 3302,4-Dimethylphenol ug/kg ND 3302,4-Dinitrophenol ug/kg ND 16002,4-Dinitrotoluene ug/kg ND 3302,6-Dinitrotoluene ug/kg ND 3302-Chloronaphthalene ug/kg ND 3302-Chlorophenol ug/kg ND 3302-Methylnaphthalene ug/kg ND 3302-Methylphenol(o-Cresol) ug/kg ND 3302-Nitroaniline ug/kg ND 16002-Nitrophenol ug/kg ND 3303&4-Methylphenol(m&p Cresol) ug/kg ND 6603,3'-Dichlorobenzidine ug/kg ND 6603-Nitroaniline ug/kg ND 16004,6-Dinitro-2-methylphenol ug/kg ND 16004-Bromophenylphenyl ether ug/kg ND 3304-Chloro-3-methylphenol ug/kg ND 6604-Chloroaniline ug/kg ND 6604-Chlorophenylphenyl ether ug/kg ND 3304-Nitroaniline ug/kg ND 16004-Nitrophenol ug/kg ND 1600Acenaphthene ug/kg ND 330Acenaphthylene ug/kg ND 330Anthracene ug/kg ND 330Benzo(a)anthracene ug/kg ND 330Benzo(a)pyrene ug/kg ND 330Benzo(b)fluoranthene ug/kg ND 330Benzo(g,h,i)perylene ug/kg ND 330Benzo(k)fluoranthene ug/kg ND 330Benzyl alcohol ug/kg ND 660bis(2-Chloroethoxy)methane ug/kg ND 330bis(2-Chloroethyl) ether ug/kg ND 330bis(2-Chloroisopropyl) ether ug/kg ND 330bis(2-Ethylhexyl)phthalate ug/kg ND 330Butylbenzylphthalate ug/kg ND 330Chrysene ug/kg ND 330Di-n-butylphthalate ug/kg ND 330 JDi-n-octylphthalate ug/kg ND 330Dibenz(a,h)anthracene ug/kg ND 330Dibenzofuran ug/kg ND 330Diethylphthalate ug/kg ND 330



Date: 02/11/2008 03:29 PM Page 67 of 90



(317)875-5894



5011474Beech Grove 6892.002






Parameter UnitsLCS






Date: 02/11/2008 03:29 PM Page 68 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsMS



MSSpikeResult

5011565001

127150

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2,4-Dinitrotoluene ug/kg 3960 63 57-12158 9 203960ND 2500 22902-Chlorophenol ug/kg 3960 62 35-12562 1 203960ND 2440 24604-Chloro-3-methylphenol ug/kg 3960 58 55-12056 3 203960ND 2320 22404-Nitrophenol ug/kg 3960 67 27-13061 9 203960ND 2650 2430Acenaphthene ug/kg 3960 62 55-11463 2 203960ND 2470 2520N-Nitroso-di-n-propylamine ug/kg 3960 64 40-13368 6 203960ND 2530 2700Pentachlorophenol ug/kg 3960 56 10-13554 3 203960ND 2200 2130Phenol ug/kg 3960 62 36-13065 4 203960ND 2470 2580Pyrene ug/kg 3960 63 51-12160 5 203960ND 2510 23802,4,6-Tribromophenol (S) % 64 34-12260 202-Fluorobiphenyl (S) % 66 56-11863 202-Fluorophenol (S) % 68 35-11768 20Nitrobenzene-d5 (S) % 62 50-11764 20Phenol-d6 (S) % 64 41-12462 20Terphenyl-d14 (S) % 68 55-11860 20



Date: 02/11/2008 03:29 PM Page 69 of 90



(317)875-5894



5011474Beech Grove 6892.002



MSV/7190EPA 8260

EPA 82608260 MSV 5035A Volatile Organics






1,1,1,2-Tetrachloroethane ug/kg ND 5.01,1,1-Trichloroethane ug/kg ND 5.01,1,2,2-Tetrachloroethane ug/kg ND 5.01,1,2-Trichloroethane ug/kg ND 5.01,1-Dichloroethane ug/kg ND 5.01,1-Dichloroethene ug/kg ND 5.01,1-Dichloropropene ug/kg ND 5.01,2,3-Trichlorobenzene ug/kg ND 5.01,2,3-Trichloropropane ug/kg ND 5.01,2,4-Trichlorobenzene ug/kg ND 5.01,2,4-Trimethylbenzene ug/kg ND 5.01,2-Dibromoethane (EDB) ug/kg ND 5.01,2-Dichlorobenzene ug/kg ND 5.01,2-Dichloroethane ug/kg ND 5.01,2-Dichloropropane ug/kg ND 5.01,3,5-Trimethylbenzene ug/kg ND 5.01,3-Dichlorobenzene ug/kg ND 5.01,3-Dichloropropane ug/kg ND 5.01,4-Dichlorobenzene ug/kg ND 5.02,2-Dichloropropane ug/kg ND 5.02-Butanone (MEK) ug/kg ND 25.02-Chlorotoluene ug/kg ND 5.02-Hexanone ug/kg ND 1004-Chlorotoluene ug/kg ND 5.04-Methyl-2-pentanone (MIBK) ug/kg ND 25.0Acetone ug/kg ND 100Acrolein ug/kg ND 100Acrylonitrile ug/kg ND 100Benzene ug/kg ND 5.0Bromobenzene ug/kg ND 5.0Bromochloromethane ug/kg ND 5.0Bromodichloromethane ug/kg ND 5.0Bromoform ug/kg ND 5.0Bromomethane ug/kg ND 5.0Carbon disulfide ug/kg ND 10.0Carbon tetrachloride ug/kg ND 5.0Chlorobenzene ug/kg ND 5.0Chloroethane ug/kg ND 5.0Chloroform ug/kg ND 5.0Chloromethane ug/kg ND 5.0cis-1,2-Dichloroethene ug/kg ND 5.0



Date: 02/11/2008 03:29 PM Page 70 of 90



(317)875-5894



5011474Beech Grove 6892.002





cis-1,3-Dichloropropene ug/kg ND 5.0Dibromochloromethane ug/kg ND 5.0Dibromomethane ug/kg ND 5.0Dichlorodifluoromethane ug/kg ND 5.0Ethyl methacrylate ug/kg ND 10.0Ethylbenzene ug/kg ND 5.0Hexachloro-1,3-butadiene ug/kg ND 5.0Iodomethane ug/kg ND 100Isopropylbenzene (Cumene) ug/kg ND 5.0Methyl-tert-butyl ether ug/kg ND 5.0Methylene chloride ug/kg ND 20.0n-Butylbenzene ug/kg ND 5.0n-Hexane ug/kg ND 5.0n-Propylbenzene ug/kg ND 5.0Naphthalene ug/kg ND 5.0p-Isopropyltoluene ug/kg ND 5.0sec-Butylbenzene ug/kg ND 5.0Styrene ug/kg ND 5.0tert-Butylbenzene ug/kg ND 5.0Tetrachloroethene ug/kg ND 5.0Toluene ug/kg ND 5.0trans-1,2-Dichloroethene ug/kg ND 5.0trans-1,3-Dichloropropene ug/kg ND 5.0trans-1,4-Dichloro-2-butene ug/kg ND 100Trichloroethene ug/kg ND 5.0Trichlorofluoromethane ug/kg ND 5.0Vinyl acetate ug/kg ND 100Vinyl chloride ug/kg ND 5.0Xylene (Total) ug/kg ND 10.04-Bromofluorobenzene (S) % 98 65-117Dibromofluoromethane (S) % 100 82-130Toluene-d8 (S) % 99 81-120

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/kg 43.850 88 69-1241,1,1-Trichloroethane ug/kg 48.650 97 67-1291,1,2,2-Tetrachloroethane ug/kg 55.950 112 68-1301,1,2-Trichloroethane ug/kg 55.250 110 72-1291,1-Dichloroethane ug/kg 48.750 97 68-1281,1-Dichloroethene ug/kg 51.950 104 65-1381,1-Dichloropropene ug/kg 48.750 97 71-1261,2,3-Trichlorobenzene ug/kg 47.150 94 63-130



Date: 02/11/2008 03:29 PM Page 71 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



1,2,3-Trichloropropane ug/kg 51.650 103 52-1311,2,4-Trichlorobenzene ug/kg 40.850 82 59-1321,2,4-Trimethylbenzene ug/kg 45.350 91 72-1291,2-Dibromoethane (EDB) ug/kg 50.550 101 71-1261,2-Dichlorobenzene ug/kg 44.950 90 72-1281,2-Dichloroethane ug/kg 52.050 104 63-1301,2-Dichloropropane ug/kg 51.750 103 73-1241,3,5-Trimethylbenzene ug/kg 45.150 90 72-1321,3-Dichlorobenzene ug/kg 44.450 89 73-1301,3-Dichloropropane ug/kg 53.250 106 71-1271,4-Dichlorobenzene ug/kg 47.250 94 71-1252,2-Dichloropropane ug/kg 41.550 83 61-1342-Butanone (MEK) ug/kg 286250 114 59-1502-Chlorotoluene ug/kg 46.450 93 73-1352-Hexanone ug/kg 297250 119 46-1504-Chlorotoluene ug/kg 43.550 87 72-1304-Methyl-2-pentanone (MIBK) ug/kg 275250 110 54-146Acetone ug/kg 280250 112 41-150Acrolein ug/kg 3600 L01000 360 50-150Acrylonitrile ug/kg 11201000 112 50-150Benzene ug/kg 49.250 98 72-129Bromobenzene ug/kg 48.150 96 72-127Bromochloromethane ug/kg 57.150 114 63-144Bromodichloromethane ug/kg 45.850 92 71-128Bromoform ug/kg 38.050 76 62-124Bromomethane ug/kg 56.950 114 45-144Carbon disulfide ug/kg 97.1100 97 63-171Carbon tetrachloride ug/kg 41.650 83 59-130Chlorobenzene ug/kg 45.650 91 73-125Chloroethane ug/kg 58.350 117 60-140Chloroform ug/kg 48.450 97 67-127Chloromethane ug/kg 47.650 95 38-141cis-1,2-Dichloroethene ug/kg 51.450 103 76-132cis-1,3-Dichloropropene ug/kg 41.450 83 61-114Dibromochloromethane ug/kg 41.550 83 70-131Dibromomethane ug/kg 52.850 106 75-132Dichlorodifluoromethane ug/kg 41.750 83 50-179Ethyl methacrylate ug/kg 56.050 112 50-150Ethylbenzene ug/kg 46.850 94 77-131Hexachloro-1,3-butadiene ug/kg 44.350 89 70-133Iodomethane ug/kg 96.8J100 97 70-130Isopropylbenzene (Cumene) ug/kg 43.250 86 72-128Methyl-tert-butyl ether ug/kg 111100 111 66-139Methylene chloride ug/kg 52.550 105 48-121n-Butylbenzene ug/kg 42.950 86 68-132n-Hexane ug/kg 54.050 108 70-130n-Propylbenzene ug/kg 46.750 93 74-136Naphthalene ug/kg 52.250 104 60-131



Date: 02/11/2008 03:29 PM Page 72 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



p-Isopropyltoluene ug/kg 37.050 74 69-134sec-Butylbenzene ug/kg 46.750 93 74-135Styrene ug/kg 44.950 90 75-125tert-Butylbenzene ug/kg 37.050 74 69-124Tetrachloroethene ug/kg 43.750 87 55-123Toluene ug/kg 49.750 99 75-127trans-1,2-Dichloroethene ug/kg 50.150 100 71-131trans-1,3-Dichloropropene ug/kg 41.250 82 62-114trans-1,4-Dichloro-2-butene ug/kg 39.9J50 80 50-150Trichloroethene ug/kg 50.750 101 72-123Trichlorofluoromethane ug/kg 44.250 88 62-150Vinyl acetate ug/kg 181200 91 50-150Vinyl chloride ug/kg 41.750 83 54-136Xylene (Total) ug/kg 134150 89 70-1304-Bromofluorobenzene (S) % 101 65-117Dibromofluoromethane (S) % 101 82-130Toluene-d8 (S) % 100 81-120



Date: 02/11/2008 03:29 PM Page 73 of 90



(317)875-5894



5011474Beech Grove 6892.002



MSV/7193EPA 8260


Associated Lab Samples: 5011474013





1,1,1,2-Tetrachloroethane ug/kg ND 5.01,1,1-Trichloroethane ug/kg ND 5.01,1,2,2-Tetrachloroethane ug/kg ND 5.01,1,2-Trichloroethane ug/kg ND 5.01,1-Dichloroethane ug/kg ND 5.01,1-Dichloroethene ug/kg ND 5.01,1-Dichloropropene ug/kg ND 5.01,2,3-Trichlorobenzene ug/kg ND 5.01,2,3-Trichloropropane ug/kg ND 5.01,2,4-Trichlorobenzene ug/kg ND 5.01,2,4-Trimethylbenzene ug/kg ND 5.01,2-Dibromoethane (EDB) ug/kg ND 5.01,2-Dichlorobenzene ug/kg ND 5.01,2-Dichloroethane ug/kg ND 5.01,2-Dichloropropane ug/kg ND 5.01,3,5-Trimethylbenzene ug/kg ND 5.01,3-Dichlorobenzene ug/kg ND 5.01,3-Dichloropropane ug/kg ND 5.01,4-Dichlorobenzene ug/kg ND 5.02,2-Dichloropropane ug/kg ND 5.02-Butanone (MEK) ug/kg ND 25.02-Chlorotoluene ug/kg ND 5.02-Hexanone ug/kg ND 1004-Chlorotoluene ug/kg ND 5.04-Methyl-2-pentanone (MIBK) ug/kg ND 25.0Acetone ug/kg ND 100Acrolein ug/kg ND 100Acrylonitrile ug/kg ND 100Benzene ug/kg ND 5.0Bromobenzene ug/kg ND 5.0Bromochloromethane ug/kg ND 5.0Bromodichloromethane ug/kg ND 5.0Bromoform ug/kg ND 5.0Bromomethane ug/kg ND 5.0Carbon disulfide ug/kg ND 10.0Carbon tetrachloride ug/kg ND 5.0Chlorobenzene ug/kg ND 5.0Chloroethane ug/kg ND 5.0Chloroform ug/kg ND 5.0Chloromethane ug/kg ND 5.0cis-1,2-Dichloroethene ug/kg ND 5.0cis-1,3-Dichloropropene ug/kg ND 5.0Dibromochloromethane ug/kg ND 5.0



Date: 02/11/2008 03:29 PM Page 74 of 90



(317)875-5894



5011474Beech Grove 6892.002





Dibromomethane ug/kg ND 5.0Dichlorodifluoromethane ug/kg ND 5.0Ethyl methacrylate ug/kg ND 10.0Ethylbenzene ug/kg ND 5.0Hexachloro-1,3-butadiene ug/kg ND 5.0Iodomethane ug/kg ND 100Isopropylbenzene (Cumene) ug/kg ND 5.0Methyl-tert-butyl ether ug/kg ND 5.0Methylene chloride ug/kg ND 20.0n-Butylbenzene ug/kg ND 5.0n-Hexane ug/kg ND 5.0n-Propylbenzene ug/kg ND 5.0Naphthalene ug/kg ND 5.0p-Isopropyltoluene ug/kg ND 5.0sec-Butylbenzene ug/kg ND 5.0Styrene ug/kg ND 5.0tert-Butylbenzene ug/kg ND 5.0Tetrachloroethene ug/kg ND 5.0Toluene ug/kg ND 5.0trans-1,2-Dichloroethene ug/kg ND 5.0trans-1,3-Dichloropropene ug/kg ND 5.0trans-1,4-Dichloro-2-butene ug/kg ND 100Trichloroethene ug/kg ND 5.0Trichlorofluoromethane ug/kg ND 5.0Vinyl acetate ug/kg ND 100Vinyl chloride ug/kg ND 5.0Xylene (Total) ug/kg ND 10.04-Bromofluorobenzene (S) % 98 65-117Dibromofluoromethane (S) % 99 82-130Toluene-d8 (S) % 99 81-120

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/kg 41.350 83 69-1241,1,1-Trichloroethane ug/kg 47.350 95 67-1291,1,2,2-Tetrachloroethane ug/kg 50.950 102 68-1301,1,2-Trichloroethane ug/kg 55.050 110 72-1291,1-Dichloroethane ug/kg 50.650 101 68-1281,1-Dichloroethene ug/kg 53.150 106 65-1381,1-Dichloropropene ug/kg 51.050 102 71-1261,2,3-Trichlorobenzene ug/kg 48.250 96 63-1301,2,3-Trichloropropane ug/kg 48.550 97 52-1311,2,4-Trichlorobenzene ug/kg 44.450 89 59-1321,2,4-Trimethylbenzene ug/kg 43.850 88 72-129



Date: 02/11/2008 03:29 PM Page 75 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



1,2-Dibromoethane (EDB) ug/kg 51.150 102 71-1261,2-Dichlorobenzene ug/kg 46.650 93 72-1281,2-Dichloroethane ug/kg 52.750 105 63-1301,2-Dichloropropane ug/kg 53.350 107 73-1241,3,5-Trimethylbenzene ug/kg 44.150 88 72-1321,3-Dichlorobenzene ug/kg 44.450 89 73-1301,3-Dichloropropane ug/kg 52.850 106 71-1271,4-Dichlorobenzene ug/kg 45.450 91 71-1252,2-Dichloropropane ug/kg 42.150 84 61-1342-Butanone (MEK) ug/kg 292250 117 59-1502-Chlorotoluene ug/kg 46.150 92 73-1352-Hexanone ug/kg 283250 113 46-1504-Chlorotoluene ug/kg 43.650 87 72-1304-Methyl-2-pentanone (MIBK) ug/kg 265250 106 54-146Acetone ug/kg 286250 114 41-150Acrolein ug/kg 3700 L01000 370 50-150Acrylonitrile ug/kg 11501000 115 50-150Benzene ug/kg 50.150 100 72-129Bromobenzene ug/kg 49.050 98 72-127Bromochloromethane ug/kg 53.850 108 63-144Bromodichloromethane ug/kg 44.650 89 71-128Bromoform ug/kg 37.350 75 62-124Bromomethane ug/kg 49.450 99 45-144Carbon disulfide ug/kg 101100 101 63-171Carbon tetrachloride ug/kg 41.050 82 59-130Chlorobenzene ug/kg 46.550 93 73-125Chloroethane ug/kg 38.250 76 60-140Chloroform ug/kg 49.550 99 67-127Chloromethane ug/kg 42.550 85 38-141cis-1,2-Dichloroethene ug/kg 52.250 104 76-132cis-1,3-Dichloropropene ug/kg 39.250 78 61-114Dibromochloromethane ug/kg 39.550 79 70-131Dibromomethane ug/kg 54.850 110 75-132Dichlorodifluoromethane ug/kg 41.650 83 50-179Ethyl methacrylate ug/kg 50.950 102 50-150Ethylbenzene ug/kg 47.350 95 77-131Hexachloro-1,3-butadiene ug/kg 43.150 86 70-133Iodomethane ug/kg 93.1J100 93 70-130Isopropylbenzene (Cumene) ug/kg 45.250 90 72-128Methyl-tert-butyl ether ug/kg 114100 114 66-139Methylene chloride ug/kg 50.450 101 48-121n-Butylbenzene ug/kg 42.250 84 68-132n-Hexane ug/kg 52.750 105 70-130n-Propylbenzene ug/kg 46.250 92 74-136Naphthalene ug/kg 51.650 103 60-131p-Isopropyltoluene ug/kg 42.150 84 69-134sec-Butylbenzene ug/kg 45.650 91 74-135Styrene ug/kg 44.150 88 75-125



Date: 02/11/2008 03:29 PM Page 76 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



tert-Butylbenzene ug/kg 38.750 77 69-124Tetrachloroethene ug/kg 42.750 85 55-123Toluene ug/kg 47.950 96 75-127trans-1,2-Dichloroethene ug/kg 51.050 102 71-131trans-1,3-Dichloropropene ug/kg 38.850 78 62-114trans-1,4-Dichloro-2-butene ug/kg 41.7J50 83 50-150Trichloroethene ug/kg 50.950 102 72-123Trichlorofluoromethane ug/kg 42.850 86 62-150Vinyl acetate ug/kg 173200 87 50-150Vinyl chloride ug/kg 42.450 85 54-136Xylene (Total) ug/kg 136150 90 70-1304-Bromofluorobenzene (S) % 103 65-117Dibromofluoromethane (S) % 101 82-130Toluene-d8 (S) % 99 81-120



Date: 02/11/2008 03:29 PM Page 77 of 90



(317)875-5894



5011474Beech Grove 6892.002



MSV/7194EPA 8260







1,1,1,2-Tetrachloroethane ug/kg ND 5.01,1,1-Trichloroethane ug/kg ND 5.01,1,2,2-Tetrachloroethane ug/kg ND 5.01,1,2-Trichloroethane ug/kg ND 5.01,1-Dichloroethane ug/kg ND 5.01,1-Dichloroethene ug/kg ND 5.01,1-Dichloropropene ug/kg ND 5.01,2,3-Trichlorobenzene ug/kg ND 5.01,2,3-Trichloropropane ug/kg ND 5.01,2,4-Trichlorobenzene ug/kg ND 5.01,2,4-Trimethylbenzene ug/kg ND 5.01,2-Dibromoethane (EDB) ug/kg ND 5.01,2-Dichlorobenzene ug/kg ND 5.01,2-Dichloroethane ug/kg ND 5.01,2-Dichloropropane ug/kg ND 5.01,3,5-Trimethylbenzene ug/kg ND 5.01,3-Dichlorobenzene ug/kg ND 5.01,3-Dichloropropane ug/kg ND 5.01,4-Dichlorobenzene ug/kg ND 5.02,2-Dichloropropane ug/kg ND 5.02-Butanone (MEK) ug/kg ND 25.02-Chlorotoluene ug/kg ND 5.02-Hexanone ug/kg ND 1004-Chlorotoluene ug/kg ND 5.04-Methyl-2-pentanone (MIBK) ug/kg ND 25.0Acetone ug/kg ND 100Acrolein ug/kg ND 100Acrylonitrile ug/kg ND 100Benzene ug/kg ND 5.0Bromobenzene ug/kg ND 5.0Bromochloromethane ug/kg ND 5.0Bromodichloromethane ug/kg ND 5.0Bromoform ug/kg ND 5.0Bromomethane ug/kg ND 5.0Carbon disulfide ug/kg ND 10.0Carbon tetrachloride ug/kg ND 5.0Chlorobenzene ug/kg ND 5.0Chloroethane ug/kg ND 5.0Chloroform ug/kg ND 5.0Chloromethane ug/kg ND 5.0cis-1,2-Dichloroethene ug/kg ND 5.0cis-1,3-Dichloropropene ug/kg ND 5.0Dibromochloromethane ug/kg ND 5.0



Date: 02/11/2008 03:29 PM Page 78 of 90



(317)875-5894



5011474Beech Grove 6892.002





Dibromomethane ug/kg ND 5.0Dichlorodifluoromethane ug/kg ND 5.0Ethyl methacrylate ug/kg ND 10.0Ethylbenzene ug/kg ND 5.0Hexachloro-1,3-butadiene ug/kg ND 5.0Iodomethane ug/kg ND 100Isopropylbenzene (Cumene) ug/kg ND 5.0Methyl-tert-butyl ether ug/kg ND 5.0Methylene chloride ug/kg ND 20.0n-Butylbenzene ug/kg ND 5.0n-Hexane ug/kg ND 5.0n-Propylbenzene ug/kg ND 5.0Naphthalene ug/kg ND 5.0p-Isopropyltoluene ug/kg ND 5.0sec-Butylbenzene ug/kg ND 5.0Styrene ug/kg ND 5.0tert-Butylbenzene ug/kg ND 5.0Tetrachloroethene ug/kg ND 5.0Toluene ug/kg ND 5.0trans-1,2-Dichloroethene ug/kg ND 5.0trans-1,3-Dichloropropene ug/kg ND 5.0trans-1,4-Dichloro-2-butene ug/kg ND 100Trichloroethene ug/kg ND 5.0Trichlorofluoromethane ug/kg ND 5.0Vinyl acetate ug/kg ND 100Vinyl chloride ug/kg ND 5.0Xylene (Total) ug/kg ND 10.04-Bromofluorobenzene (S) % 99 65-117Dibromofluoromethane (S) % 97 82-130Toluene-d8 (S) % 99 81-120

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/kg 35.350 71 69-1241,1,1-Trichloroethane ug/kg 41.850 84 67-1291,1,2,2-Tetrachloroethane ug/kg 50.850 102 68-1301,1,2-Trichloroethane ug/kg 49.950 100 72-1291,1-Dichloroethane ug/kg 48.150 96 68-1281,1-Dichloroethene ug/kg 50.250 100 65-1381,1-Dichloropropene ug/kg 49.250 98 71-1261,2,3-Trichlorobenzene ug/kg 48.050 96 63-1301,2,3-Trichloropropane ug/kg 49.050 98 52-1311,2,4-Trichlorobenzene ug/kg 45.150 90 59-1321,2,4-Trimethylbenzene ug/kg 44.750 89 72-129



Date: 02/11/2008 03:29 PM Page 79 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



1,2-Dibromoethane (EDB) ug/kg 45.450 91 71-1261,2-Dichlorobenzene ug/kg 46.450 93 72-1281,2-Dichloroethane ug/kg 48.950 98 63-1301,2-Dichloropropane ug/kg 52.250 104 73-1241,3,5-Trimethylbenzene ug/kg 44.650 89 72-1321,3-Dichlorobenzene ug/kg 45.850 92 73-1301,3-Dichloropropane ug/kg 49.650 99 71-1271,4-Dichlorobenzene ug/kg 46.050 92 71-1252,2-Dichloropropane ug/kg 41.850 84 61-1342-Butanone (MEK) ug/kg 287250 115 59-1502-Chlorotoluene ug/kg 47.050 94 73-1352-Hexanone ug/kg 268250 107 46-1504-Chlorotoluene ug/kg 44.250 88 72-1304-Methyl-2-pentanone (MIBK) ug/kg 250250 100 54-146Acetone ug/kg 282250 113 41-150Acrolein ug/kg 3440 L01000 344 50-150Acrylonitrile ug/kg 10801000 108 50-150Benzene ug/kg 48.050 96 72-129Bromobenzene ug/kg 47.250 94 72-127Bromochloromethane ug/kg 51.650 103 63-144Bromodichloromethane ug/kg 40.450 81 71-128Bromoform ug/kg 31.250 62 62-124Bromomethane ug/kg 52.450 105 45-144Carbon disulfide ug/kg 99.6100 100 63-171Carbon tetrachloride ug/kg 34.650 69 59-130Chlorobenzene ug/kg 45.150 90 73-125Chloroethane ug/kg 42.750 85 60-140Chloroform ug/kg 46.650 93 67-127Chloromethane ug/kg 48.750 97 38-141cis-1,2-Dichloroethene ug/kg 50.250 100 76-132cis-1,3-Dichloropropene ug/kg 38.350 77 61-114Dibromochloromethane ug/kg 33.8 L050 68 70-131Dibromomethane ug/kg 51.650 103 75-132Dichlorodifluoromethane ug/kg 41.350 83 50-179Ethyl methacrylate ug/kg 44.750 89 50-150Ethylbenzene ug/kg 46.250 92 77-131Hexachloro-1,3-butadiene ug/kg 43.250 86 70-133Iodomethane ug/kg 90.7J100 91 70-130Isopropylbenzene (Cumene) ug/kg 44.850 90 72-128Methyl-tert-butyl ether ug/kg 103100 103 66-139Methylene chloride ug/kg 45.550 91 48-121n-Butylbenzene ug/kg 43.250 86 68-132n-Hexane ug/kg 50.450 101 70-130n-Propylbenzene ug/kg 48.050 96 74-136Naphthalene ug/kg 48.450 97 60-131p-Isopropyltoluene ug/kg 43.150 86 69-134sec-Butylbenzene ug/kg 45.950 92 74-135Styrene ug/kg 43.550 87 75-125



Date: 02/11/2008 03:29 PM Page 80 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsLCS



tert-Butylbenzene ug/kg 41.550 83 69-124Tetrachloroethene ug/kg 41.750 83 55-123Toluene ug/kg 46.150 92 75-127trans-1,2-Dichloroethene ug/kg 49.050 98 71-131trans-1,3-Dichloropropene ug/kg 37.950 76 62-114trans-1,4-Dichloro-2-butene ug/kg 44.8J50 90 50-150Trichloroethene ug/kg 48.050 96 72-123Trichlorofluoromethane ug/kg 42.350 85 62-150Vinyl acetate ug/kg 179200 90 50-150Vinyl chloride ug/kg 48.650 97 54-136Xylene (Total) ug/kg 134150 89 70-1304-Bromofluorobenzene (S) % 104 65-117Dibromofluoromethane (S) % 97 82-130Toluene-d8 (S) % 98 81-120



Date: 02/11/2008 03:29 PM Page 81 of 90



(317)875-5894



5011474Beech Grove 6892.002



MPRP/2495EPA 3050

EPA 60106010 MET

Associated Lab Samples: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014




Associated Lab Samples: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014

Arsenic mg/kg ND 2.0Barium mg/kg ND 2.0Cadmium mg/kg ND 2.0Chromium mg/kg ND 2.0Lead mg/kg ND 2.0Selenium mg/kg ND 2.0Silver mg/kg ND 2.0

Parameter UnitsLCS



Arsenic mg/kg 52.950 106 80-120Barium mg/kg 50.150 100 80-120Cadmium mg/kg 49.750 99 80-120Chromium mg/kg 49.450 99 80-120Lead mg/kg 49.850 100 80-120Selenium mg/kg 50.550 101 80-120Silver mg/kg 25.325 101 80-120

Parameter UnitsMS



MSSpikeResult

5011474001

127481

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg 55.1 90 75-12588 8 2051.74.8 54.7 50.2Barium mg/kg 55.1 108 75-125102 7 2051.733.6 93.0 86.4Cadmium mg/kg 55.1 82 75-12581 8 2051.7ND 45.6 42.1Chromium mg/kg 55.1 92 75-12589 8 2051.77.7 58.4 53.7Lead mg/kg 55.1 86 75-12584 8 2051.75.8 53.5 49.2Selenium mg/kg 55.1 85 75-12583 9 2051.7ND 48.3 44.3Silver mg/kg 27.6 96 75-12595 7 2025.8ND 26.5 24.6



Date: 02/11/2008 03:29 PM Page 82 of 90



(317)875-5894



5011474Beech Grove 6892.002



OEXT/5929EPA 3546

EPA 80828082 GCS PCB

Associated Lab Samples: 5011474001, 5011474002, 5011474003




Associated Lab Samples: 5011474001, 5011474002, 5011474003

PCB-1016 (Aroclor 1016) ug/kg ND 35.0PCB-1221 (Aroclor 1221) ug/kg ND 35.0PCB-1232 (Aroclor 1232) ug/kg ND 35.0PCB-1242 (Aroclor 1242) ug/kg ND 35.0PCB-1248 (Aroclor 1248) ug/kg ND 35.0PCB-1254 (Aroclor 1254) ug/kg ND 35.0PCB-1260 (Aroclor 1260) ug/kg ND 35.0Tetrachloro-m-xylene (S) % 100 28-137

Parameter UnitsLCS



PCB-1016 (Aroclor 1016) ug/kg 173167 104 50-150PCB-1260 (Aroclor 1260) ug/kg 172167 103 50-150Tetrachloro-m-xylene (S) % 99 28-137

Parameter UnitsMS



MSSpikeResult

5011585002

127506

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

PCB-1016 (Aroclor 1016) ug/kg 189 80 50-15069 14 20189ND 151 131PCB-1260 (Aroclor 1260) ug/kg 189 73 50-15065 11 20189ND 137 122Tetrachloro-m-xylene (S) % 74 28-13765 20



Date: 02/11/2008 03:29 PM Page 83 of 90



(317)875-5894



5011474Beech Grove 6892.002



PMST/2211ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture


Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

5011626001127969SAMPLE DUPLICATE:

Percent Moisture % 2.9 4 52.8

Parameter UnitsDup



Percent Moisture % 14.3 2 514.0



Date: 02/11/2008 03:29 PM Page 84 of 90



(317)875-5894



5011474Beech Grove 6892.002



PMST/2212ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture


Parameter UnitsDup



Percent Moisture % 11.9 R214 513.7



Date: 02/11/2008 03:29 PM Page 85 of 90



(317)875-5894



5011474Beech Grove 6892.002



OEXT/5984EPA 3546







2,4,5-Trichlorophenol ug/kg ND 3302,4,6-Trichlorophenol ug/kg ND 3302,4-Dichlorophenol ug/kg ND 3302,4-Dimethylphenol ug/kg ND 3302,4-Dinitrophenol ug/kg ND 16002,4-Dinitrotoluene ug/kg ND 3302,6-Dinitrotoluene ug/kg ND 3302-Chloronaphthalene ug/kg ND 3302-Chlorophenol ug/kg ND 3302-Methylnaphthalene ug/kg ND 3302-Methylphenol(o-Cresol) ug/kg ND 3302-Nitroaniline ug/kg ND 16002-Nitrophenol ug/kg ND 3303&4-Methylphenol(m&p Cresol) ug/kg ND 6603,3'-Dichlorobenzidine ug/kg ND 6603-Nitroaniline ug/kg ND 16004,6-Dinitro-2-methylphenol ug/kg ND 16004-Bromophenylphenyl ether ug/kg ND 3304-Chloro-3-methylphenol ug/kg ND 6604-Chloroaniline ug/kg ND 6604-Chlorophenylphenyl ether ug/kg ND 3304-Nitroaniline ug/kg ND 16004-Nitrophenol ug/kg ND 1600Acenaphthene ug/kg ND 330Acenaphthylene ug/kg ND 330Anthracene ug/kg ND 330Benzo(a)anthracene ug/kg ND 330Benzo(a)pyrene ug/kg ND 330Benzo(b)fluoranthene ug/kg ND 330Benzo(g,h,i)perylene ug/kg ND 330Benzo(k)fluoranthene ug/kg ND 330Benzyl alcohol ug/kg ND 660bis(2-Chloroethoxy)methane ug/kg ND 330bis(2-Chloroethyl) ether ug/kg ND 330bis(2-Chloroisopropyl) ether ug/kg ND 330bis(2-Ethylhexyl)phthalate ug/kg ND 330Butylbenzylphthalate ug/kg ND 330Chrysene ug/kg ND 330Di-n-butylphthalate ug/kg ND 330Di-n-octylphthalate ug/kg ND 330Dibenz(a,h)anthracene ug/kg ND 330Dibenzofuran ug/kg ND 330Diethylphthalate ug/kg ND 330



Date: 02/11/2008 03:29 PM Page 86 of 90



(317)875-5894



5011474Beech Grove 6892.002






Parameter UnitsLCS






Date: 02/11/2008 03:29 PM Page 87 of 90



(317)875-5894



5011474Beech Grove 6892.002

Parameter UnitsMS



MSSpikeResult

5011626001

128276

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2,4-Dinitrotoluene ug/kg 3420 64 57-12164 1 203420ND 2180 22002-Chlorophenol ug/kg M03420 6 35-1255 203420ND 196J 175J4-Chloro-3-methylphenol ug/kg M03420 24 55-12022 8 203420ND 823 7604-Nitrophenol ug/kg M03420 0 27-1300 203420ND ND NDAcenaphthene ug/kg 3420 64 55-11468 6 203420ND 2190 2340N-Nitroso-di-n-propylamine ug/kg 3420 57 40-13367 16 203420ND 1970 2300Pentachlorophenol ug/kg M03420 0 10-1350 203420ND ND NDPhenol ug/kg M03420 36 36-13032 9 203420ND 1530 1400Pyrene ug/kg 3420 66 51-12173 10 203420ND 2330 25602,4,6-Tribromophenol (S) % S00 34-1220 202-Fluorobiphenyl (S) % 75 56-11879 202-Fluorophenol (S) % S07 35-1175 20Nitrobenzene-d5 (S) % 67 50-11771 20Phenol-d6 (S) % S040 41-12438 20Terphenyl-d14 (S) % 87 55-11892 20



Date: 02/11/2008 03:29 PM Page 88 of 90



(317)875-5894



5011474Beech Grove 6892.002



OEXT/6013EPA 3546

EPA 80828082 GCS PCB

Associated Lab Samples: 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011,5011474012, 5011474013, 5011474014




Associated Lab Samples: 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011,5011474012, 5011474013, 5011474014

PCB-1016 (Aroclor 1016) ug/kg ND 35.0PCB-1221 (Aroclor 1221) ug/kg ND 35.0PCB-1232 (Aroclor 1232) ug/kg ND 35.0PCB-1242 (Aroclor 1242) ug/kg ND 35.0PCB-1248 (Aroclor 1248) ug/kg ND 35.0PCB-1254 (Aroclor 1254) ug/kg ND 35.0PCB-1260 (Aroclor 1260) ug/kg ND 35.0Tetrachloro-m-xylene (S) % 83 28-137

Parameter UnitsLCS



PCB-1016 (Aroclor 1016) ug/kg 148167 89 50-150PCB-1260 (Aroclor 1260) ug/kg 137167 82 50-150Tetrachloro-m-xylene (S) % 84 28-137

Parameter UnitsMS



MSSpikeResult

5011662001

128789

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

PCB-1016 (Aroclor 1016) ug/kg 175 56 50-15050 11 20175ND 98.0 88.1PCB-1260 (Aroclor 1260) ug/kg 175 56 50-15063 12 20175ND 98.0 110Tetrachloro-m-xylene (S) % 48 28-13743 20



Date: 02/11/2008 03:29 PM Page 89 of 90



(317)875-5894

QUALIFIERS


5011474Beech Grove 6892.002

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

ANALYTE QUALIFIERS

The Sample was analyzed at dilution due to its physical characteristics. SAQ 02.08.081dDue to the viscosity of the extract, it was run at 10x. KES 1-31-072dThe Sample was analyzed at dilution due to its physical charachteristics. SAQ 02.08.083dDue to the viscosity of the extract, it was run at 10x. KES 1-31-084dAnalyte detected below reporting limit, therefore result is an estimate.JAnalyte recovery in the laboratory control sample (LCS) was outside QC limits.L0Matrix spike recovery was outside laboratory control limits.M0RPD value was outside control limits.R1RPD value was outside control limits due to matrix interferenceR2Surrogate recovery outside laboratory control limits.S0Surrogate recovery not evaluated against control limits due to sample dilution.S4



Date: 02/11/2008 03:29 PM Page 90 of 90



(317)875-5894

February 12, 2008

LIMS USE: FR - DOUG PETROFFLIMS OBJECT ID: 5011526

5011526Project:Pace Project No.:

RE:

Mr. Doug PetroffThe Schneider Corporation8901 Otis AveIndianapolis, IN 46216

Beech Grove Site 6892.002

Dear Mr. Petroff:Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2008.The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of thereport.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Donna Spyker

[email protected] Manager

Illinois/NELAC Certification Number: 100418Indiana Certification Number: C-49-06Kansas Certification Number: E-10247Kentucky Certification Number: 0042Ohio VAP: CL0065Pennsylvania: 68-00791West Virginia Certification Number: 330

Enclosures



Page 1 of 42



(317)875-5894

SAMPLE SUMMARY


5011526Beech Grove Site 6892.002

Lab ID Sample ID Matrix Date Collected Date Received

5011526001 GP-11 Water 01/25/08 10:30 01/28/08 11:48

5011526002 GP-10 Water 01/25/08 11:30 01/28/08 11:48

5011526003 GP-8 Water 01/25/08 13:30 01/28/08 11:48

5011526004 GP-12 Water 01/25/08 15:30 01/28/08 11:48

5011526005 GP-2 Water 01/25/08 17:00 01/28/08 11:48

5011526006 GP-4 Water 01/26/08 12:30 01/28/08 11:48

5011526007 GP-6 Water 01/26/08 14:00 01/28/08 11:48



Page 2 of 42



(317)875-5894





5011526001 GP-11 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526002 GP-10 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526003 GP-8 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526004 GP-12 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526005 GP-2 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526006 GP-4 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES

5011526007 GP-6 EPA 6010 7FRW

EPA 7470 1LLB

EPA 8082 8SAQ

EPA 8260 72SLB

EPA 8270 66KES



Page 3 of 42



(317)875-5894

ANALYTICAL RESULTS



Sample: GP-11 Lab ID: 5011526001 Collected: 01/25/08 10:30 Received: 01/28/08 11:48 Matrix: Water



PCB-1016 (Aroclor 1016) ND ug/L 0.68 1 01/31/08 15:23 12674-11-201/30/08 00:00PCB-1221 (Aroclor 1221) ND ug/L 0.68 1 01/31/08 15:23 11104-28-201/30/08 00:00PCB-1232 (Aroclor 1232) ND ug/L 0.68 1 01/31/08 15:23 11141-16-501/30/08 00:00PCB-1242 (Aroclor 1242) ND ug/L 0.68 1 01/31/08 15:23 53469-21-901/30/08 00:00PCB-1248 (Aroclor 1248) ND ug/L 0.68 1 01/31/08 15:23 12672-29-601/30/08 00:00PCB-1254 (Aroclor 1254) ND ug/L 0.68 1 01/31/08 15:23 11097-69-101/30/08 00:00PCB-1260 (Aroclor 1260) ND ug/L 0.68 1 01/31/08 15:23 11096-82-501/30/08 00:00Tetrachloro-m-xylene (S) 94 % 10-143 1 01/31/08 15:23 877-09-801/30/08 00:00


Arsenic 141 ug/L 10.0 1 01/31/08 03:20 7440-38-201/29/08 00:00Barium 1080 ug/L 100 1 01/31/08 03:20 7440-39-301/29/08 00:00Cadmium 7.3 ug/L 5.0 1 01/31/08 03:20 7440-43-901/29/08 00:00Chromium 269 ug/L 10.0 1 01/31/08 03:20 7440-47-301/29/08 00:00Lead 168 ug/L 10.0 1 01/31/08 03:20 7439-92-101/29/08 00:00Selenium 60.0 ug/L 10.0 1 01/31/08 03:20 7782-49-201/29/08 00:00Silver ND ug/L 50.0 1 01/31/08 03:20 7440-22-401/29/08 00:00


Mercury ND ug/L 6.0 1 01/30/08 15:45 7439-97-601/29/08 00:00

8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510

Acenaphthene ND ug/L 12.2 1 01/30/08 18:51 83-32-901/29/08 00:00Acenaphthylene ND ug/L 12.2 1 01/30/08 18:51 208-96-801/29/08 00:00Anthracene ND ug/L 12.2 1 01/30/08 18:51 120-12-701/29/08 00:00Benzo(a)anthracene ND ug/L 12.2 1 01/30/08 18:51 56-55-301/29/08 00:00Benzo(a)pyrene ND ug/L 12.2 1 01/30/08 18:51 50-32-801/29/08 00:00Benzo(b)fluoranthene ND ug/L 12.2 1 01/30/08 18:51 205-99-201/29/08 00:00Benzo(g,h,i)perylene ND ug/L 12.2 1 01/30/08 18:51 191-24-201/29/08 00:00Benzo(k)fluoranthene ND ug/L 12.2 1 01/30/08 18:51 207-08-901/29/08 00:00Benzyl alcohol ND ug/L 24.4 1 01/30/08 18:51 100-51-601/29/08 00:004-Bromophenylphenyl ether ND ug/L 12.2 1 01/30/08 18:51 101-55-301/29/08 00:00Butylbenzylphthalate ND ug/L 12.2 1 01/30/08 18:51 85-68-701/29/08 00:004-Chloro-3-methylphenol ND ug/L 24.4 1 01/30/08 18:51 59-50-701/29/08 00:004-Chloroaniline ND ug/L 24.4 1 01/30/08 18:51 106-47-801/29/08 00:00bis(2-Chloroethoxy)methane ND ug/L 12.2 1 01/30/08 18:51 111-91-101/29/08 00:00bis(2-Chloroethyl) ether ND ug/L 12.2 1 01/30/08 18:51 111-44-401/29/08 00:00bis(2-Chloroisopropyl) ether ND ug/L 6.1 1 01/30/08 18:51 108-60-101/29/08 00:002-Chloronaphthalene ND ug/L 12.2 1 01/30/08 18:51 91-58-701/29/08 00:002-Chlorophenol ND ug/L 12.2 1 01/30/08 18:51 95-57-801/29/08 00:004-Chlorophenylphenyl ether ND ug/L 12.2 1 01/30/08 18:51 7005-72-301/29/08 00:00Chrysene ND ug/L 12.2 1 01/30/08 18:51 218-01-901/29/08 00:00Dibenz(a,h)anthracene ND ug/L 12.2 1 01/30/08 18:51 53-70-301/29/08 00:00Dibenzofuran ND ug/L 12.2 1 01/30/08 18:51 132-64-901/29/08 00:003,3'-Dichlorobenzidine ND ug/L 24.4 1 01/30/08 18:51 91-94-101/29/08 00:002,4-Dichlorophenol ND ug/L 12.2 1 01/30/08 18:51 120-83-201/29/08 00:00



Date: 02/12/2008 03:16 PM Page 4 of 42



(317)875-5894

ANALYTICAL RESULTS






Diethylphthalate ND ug/L 12.2 1 01/30/08 18:51 84-66-201/29/08 00:002,4-Dimethylphenol ND ug/L 12.2 1 01/30/08 18:51 105-67-901/29/08 00:00Dimethylphthalate ND ug/L 12.2 1 01/30/08 18:51 131-11-301/29/08 00:00Di-n-butylphthalate ND ug/L 12.2 1 01/30/08 18:51 84-74-201/29/08 00:004,6-Dinitro-2-methylphenol ND ug/L 61.0 1 01/30/08 18:51 534-52-101/29/08 00:002,4-Dinitrophenol ND ug/L 61.0 1 01/30/08 18:51 51-28-501/29/08 00:002,4-Dinitrotoluene ND ug/L 12.2 1 01/30/08 18:51 121-14-201/29/08 00:002,6-Dinitrotoluene ND ug/L 12.2 1 01/30/08 18:51 606-20-201/29/08 00:00Di-n-octylphthalate ND ug/L 12.2 1 01/30/08 18:51 117-84-001/29/08 00:00bis(2-Ethylhexyl)phthalate ND ug/L 6.1 1 01/30/08 18:51 117-81-701/29/08 00:00Fluoranthene ND ug/L 12.2 1 01/30/08 18:51 206-44-001/29/08 00:00Fluorene ND ug/L 12.2 1 01/30/08 18:51 86-73-701/29/08 00:00Hexachloro-1,3-butadiene ND ug/L 6.1 1 01/30/08 18:51 87-68-301/29/08 00:00Hexachlorobenzene ND ug/L 12.2 1 01/30/08 18:51 118-74-101/29/08 00:00Hexachlorocyclopentadiene ND ug/L 24.4 1 01/30/08 18:51 77-47-401/29/08 00:00Hexachloroethane ND ug/L 12.2 1 01/30/08 18:51 67-72-101/29/08 00:00Indeno(1,2,3-cd)pyrene ND ug/L 12.2 1 01/30/08 18:51 193-39-501/29/08 00:00Isophorone ND ug/L 12.2 1 01/30/08 18:51 78-59-101/29/08 00:002-Methylnaphthalene ND ug/L 12.2 1 01/30/08 18:51 91-57-601/29/08 00:002-Methylphenol(o-Cresol) ND ug/L 12.2 1 01/30/08 18:51 95-48-701/29/08 00:003&4-Methylphenol(m&p Cresol) ND ug/L 24.4 1 01/30/08 18:5101/29/08 00:00Naphthalene ND ug/L 6.1 1 01/30/08 18:51 91-20-301/29/08 00:002-Nitroaniline ND ug/L 61.0 1 01/30/08 18:51 88-74-401/29/08 00:003-Nitroaniline ND ug/L 61.0 1 01/30/08 18:51 99-09-201/29/08 00:004-Nitroaniline ND ug/L 61.0 1 01/30/08 18:51 100-01-601/29/08 00:00Nitrobenzene ND ug/L 12.2 1 01/30/08 18:51 98-95-301/29/08 00:002-Nitrophenol ND ug/L 12.2 1 01/30/08 18:51 88-75-501/29/08 00:004-Nitrophenol ND ug/L 61.0 1 01/30/08 18:51 100-02-701/29/08 00:00N-Nitroso-di-n-propylamine ND ug/L 12.2 1 01/30/08 18:51 621-64-701/29/08 00:00N-Nitrosodiphenylamine ND ug/L 12.2 1 01/30/08 18:51 86-30-601/29/08 00:00Pentachlorophenol ND ug/L 61.0 1 01/30/08 18:51 87-86-501/29/08 00:00Phenanthrene ND ug/L 12.2 1 01/30/08 18:51 85-01-801/29/08 00:00Phenol ND ug/L 12.2 1 01/30/08 18:51 108-95-201/29/08 00:00Pyrene ND ug/L 12.2 1 01/30/08 18:51 129-00-001/29/08 00:002,4,5-Trichlorophenol ND ug/L 12.2 1 01/30/08 18:51 95-95-401/29/08 00:002,4,6-Trichlorophenol ND ug/L 12.2 1 01/30/08 18:51 88-06-201/29/08 00:00Nitrobenzene-d5 (S) 76 % 40-112 1 01/30/08 18:51 4165-60-001/29/08 00:002-Fluorobiphenyl (S) 72 % 31-114 1 01/30/08 18:51 321-60-801/29/08 00:00Terphenyl-d14 (S) 71 % 10-116 1 01/30/08 18:51 1718-51-001/29/08 00:00Phenol-d6 (S) 38 % 10-100 1 01/30/08 18:51 13127-88-301/29/08 00:002-Fluorophenol (S) 59 % 13-100 1 01/30/08 18:51 367-12-401/29/08 00:002,4,6-Tribromophenol (S) 73 % 26-125 1 01/30/08 18:51 118-79-601/29/08 00:00

8260 MSV Analytical Method: EPA 8260

Acetone ND ug/L 100 1 01/31/08 10:54 67-64-1Acrolein ND ug/L 100 1 01/31/08 10:54 107-02-8Acrylonitrile ND ug/L 100 1 01/31/08 10:54 107-13-1



Date: 02/12/2008 03:16 PM Page 5 of 42



(317)875-5894

ANALYTICAL RESULTS






Benzene ND ug/L 5.0 1 01/31/08 10:54 71-43-2Bromobenzene ND ug/L 5.0 1 01/31/08 10:54 108-86-1Bromochloromethane ND ug/L 5.0 1 01/31/08 10:54 74-97-5Bromodichloromethane ND ug/L 5.0 1 01/31/08 10:54 75-27-4Bromoform ND ug/L 5.0 1 01/31/08 10:54 75-25-2Bromomethane ND ug/L 5.0 1 01/31/08 10:54 74-83-92-Butanone (MEK) ND ug/L 25.0 1 01/31/08 10:54 78-93-3n-Butylbenzene ND ug/L 5.0 1 01/31/08 10:54 104-51-8sec-Butylbenzene ND ug/L 5.0 1 01/31/08 10:54 135-98-8tert-Butylbenzene ND ug/L 5.0 1 01/31/08 10:54 98-06-6Carbon disulfide ND ug/L 10.0 1 01/31/08 10:54 75-15-0Carbon tetrachloride ND ug/L 5.0 1 01/31/08 10:54 56-23-5Chlorobenzene ND ug/L 5.0 1 01/31/08 10:54 108-90-7Chloroethane ND ug/L 5.0 1 01/31/08 10:54 75-00-3Chloroform ND ug/L 5.0 1 01/31/08 10:54 67-66-3Chloromethane ND ug/L 5.0 1 01/31/08 10:54 74-87-32-Chlorotoluene ND ug/L 5.0 1 01/31/08 10:54 95-49-84-Chlorotoluene ND ug/L 5.0 1 01/31/08 10:54 106-43-4Dibromochloromethane ND ug/L 5.0 1 01/31/08 10:54 124-48-11,2-Dibromoethane (EDB) ND ug/L 5.0 1 01/31/08 10:54 106-93-4Dibromomethane ND ug/L 5.0 1 01/31/08 10:54 74-95-31,2-Dichlorobenzene ND ug/L 5.0 1 01/31/08 10:54 95-50-11,3-Dichlorobenzene ND ug/L 5.0 1 01/31/08 10:54 541-73-11,4-Dichlorobenzene ND ug/L 5.0 1 01/31/08 10:54 106-46-7trans-1,4-Dichloro-2-butene ND ug/L 100 1 01/31/08 10:54 110-57-6Dichlorodifluoromethane ND ug/L 5.0 1 01/31/08 10:54 75-71-81,1-Dichloroethane ND ug/L 5.0 1 01/31/08 10:54 75-34-31,2-Dichloroethane ND ug/L 5.0 1 01/31/08 10:54 107-06-21,1-Dichloroethene ND ug/L 5.0 1 01/31/08 10:54 75-35-4cis-1,2-Dichloroethene ND ug/L 5.0 1 01/31/08 10:54 156-59-2trans-1,2-Dichloroethene ND ug/L 5.0 1 01/31/08 10:54 156-60-51,2-Dichloropropane ND ug/L 5.0 1 01/31/08 10:54 78-87-51,3-Dichloropropane ND ug/L 5.0 1 01/31/08 10:54 142-28-92,2-Dichloropropane ND ug/L 5.0 1 01/31/08 10:54 594-20-71,1-Dichloropropene ND ug/L 5.0 1 01/31/08 10:54 563-58-6cis-1,3-Dichloropropene ND ug/L 5.0 1 01/31/08 10:54 10061-01-5trans-1,3-Dichloropropene ND ug/L 5.0 1 01/31/08 10:54 10061-02-6Ethylbenzene ND ug/L 5.0 1 01/31/08 10:54 100-41-4Ethyl methacrylate ND ug/L 100 1 01/31/08 10:54 97-63-2Hexachloro-1,3-butadiene ND ug/L 5.0 1 01/31/08 10:54 87-68-32-Hexanone ND ug/L 25.0 1 01/31/08 10:54 591-78-6Iodomethane ND ug/L 10.0 1 01/31/08 10:54 74-88-4Isopropylbenzene (Cumene) ND ug/L 5.0 1 01/31/08 10:54 98-82-8p-Isopropyltoluene ND ug/L 5.0 1 01/31/08 10:54 99-87-6Methylene chloride ND ug/L 5.0 1 01/31/08 10:54 75-09-24-Methyl-2-pentanone (MIBK) ND ug/L 25.0 1 01/31/08 10:54 108-10-1Methyl-tert-butyl ether ND ug/L 4.0 1 01/31/08 10:54 1634-04-4



Date: 02/12/2008 03:16 PM Page 6 of 42



(317)875-5894

ANALYTICAL RESULTS






Naphthalene ND ug/L 5.0 1 01/31/08 10:54 91-20-3n-Propylbenzene ND ug/L 5.0 1 01/31/08 10:54 103-65-1Styrene ND ug/L 5.0 1 01/31/08 10:54 100-42-51,1,1,2-Tetrachloroethane ND ug/L 5.0 1 01/31/08 10:54 630-20-61,1,2,2-Tetrachloroethane ND ug/L 5.0 1 01/31/08 10:54 79-34-5Tetrachloroethene ND ug/L 5.0 1 01/31/08 10:54 127-18-4Toluene ND ug/L 5.0 1 01/31/08 10:54 108-88-31,2,3-Trichlorobenzene ND ug/L 5.0 1 01/31/08 10:54 87-61-61,2,4-Trichlorobenzene ND ug/L 5.0 1 01/31/08 10:54 120-82-11,1,1-Trichloroethane ND ug/L 5.0 1 01/31/08 10:54 71-55-61,1,2-Trichloroethane ND ug/L 5.0 1 01/31/08 10:54 79-00-5Trichloroethene ND ug/L 5.0 1 01/31/08 10:54 79-01-6Trichlorofluoromethane ND ug/L 5.0 1 01/31/08 10:54 75-69-41,2,3-Trichloropropane ND ug/L 5.0 1 01/31/08 10:54 96-18-41,2,4-Trimethylbenzene ND ug/L 5.0 1 01/31/08 10:54 95-63-61,3,5-Trimethylbenzene ND ug/L 5.0 1 01/31/08 10:54 108-67-8Vinyl acetate ND ug/L 10.0 1 01/31/08 10:54 108-05-4Vinyl chloride ND ug/L 2.0 1 01/31/08 10:54 75-01-4Xylene (Total) ND ug/L 10.0 1 01/31/08 10:54 1330-20-7Dibromofluoromethane (S) 106 % 82-122 1 01/31/08 10:54 1868-53-74-Bromofluorobenzene (S) 101 % 73-120 1 01/31/08 10:54 460-00-4Toluene-d8 (S) 98 % 80-120 1 01/31/08 10:54 2037-26-5



Date: 02/12/2008 03:16 PM Page 7 of 42



(317)875-5894

ANALYTICAL RESULTS






PCB-1016 (Aroclor 1016) ND ug/L 1.1 1 02/07/08 16:41 12674-11-201/30/08 00:00PCB-1221 (Aroclor 1221) ND ug/L 1.1 1 02/07/08 16:41 11104-28-201/30/08 00:00PCB-1232 (Aroclor 1232) ND ug/L 1.1 1 02/07/08 16:41 11141-16-501/30/08 00:00PCB-1242 (Aroclor 1242) ND ug/L 1.1 1 02/07/08 16:41 53469-21-901/30/08 00:00PCB-1248 (Aroclor 1248) ND ug/L 1.1 1 02/07/08 16:41 12672-29-601/30/08 00:00PCB-1254 (Aroclor 1254) 3.5 ug/L 1.1 1 02/07/08 16:41 11097-69-101/30/08 00:00PCB-1260 (Aroclor 1260) ND ug/L 1.1 1 02/07/08 16:41 11096-82-501/30/08 00:00Tetrachloro-m-xylene (S) 66 % 10-143 1 02/07/08 16:41 877-09-801/30/08 00:00


Arsenic 640 ug/L 50.0 1 01/31/08 03:26 7440-38-201/29/08 00:00Barium 8460 ug/L 500 1 01/31/08 03:26 7440-39-301/29/08 00:00Cadmium 51.5 ug/L 25.0 1 01/31/08 03:26 7440-43-901/29/08 00:00Chromium 1790 ug/L 50.0 1 01/31/08 03:26 7440-47-301/29/08 00:00Lead 9600 ug/L 50.0 1 01/31/08 03:26 7439-92-101/29/08 00:00Selenium 215 ug/L 50.0 1 01/31/08 03:26 7782-49-201/29/08 00:00Silver ND ug/L 250 1 01/31/08 03:26 7440-22-401/29/08 00:00


Mercury ND ug/L 20.0 1 01/30/08 15:47 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 8 of 42



(317)875-5894

ANALYTICAL RESULTS











Date: 02/12/2008 03:16 PM Page 9 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 10 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 11 of 42



(317)875-5894

ANALYTICAL RESULTS








Arsenic 519 ug/L 50.0 1 01/31/08 03:31 7440-38-201/29/08 00:00Barium 3260 ug/L 500 1 01/31/08 03:31 7440-39-301/29/08 00:00Cadmium 29.5 ug/L 25.0 1 01/31/08 03:31 7440-43-901/29/08 00:00Chromium 802 ug/L 50.0 1 01/31/08 03:31 7440-47-301/29/08 00:00Lead 699 ug/L 50.0 1 01/31/08 03:31 7439-92-101/29/08 00:00Selenium 161 ug/L 50.0 1 01/31/08 03:31 7782-49-201/29/08 00:00Silver ND ug/L 250 1 01/31/08 03:31 7440-22-401/29/08 00:00


Mercury ND ug/L 20.0 1 01/30/08 15:48 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 12 of 42



(317)875-5894

ANALYTICAL RESULTS











Date: 02/12/2008 03:16 PM Page 13 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 14 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 15 of 42



(317)875-5894

ANALYTICAL RESULTS










Mercury ND ug/L 20.0 1 01/30/08 16:44 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 16 of 42



(317)875-5894

ANALYTICAL RESULTS











Date: 02/12/2008 03:16 PM Page 17 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 18 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 19 of 42



(317)875-5894

ANALYTICAL RESULTS










Mercury ND ug/L 20.0 1 01/30/08 16:45 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 20 of 42



(317)875-5894

ANALYTICAL RESULTS











Date: 02/12/2008 03:16 PM Page 21 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 22 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 23 of 42



(317)875-5894

ANALYTICAL RESULTS








Arsenic 78.0 ug/L 10.0 1 01/31/08 03:48 7440-38-201/29/08 00:00Barium 860 ug/L 100 1 01/31/08 03:48 7440-39-301/29/08 00:00Cadmium 5.0 ug/L 5.0 1 01/31/08 03:48 7440-43-901/29/08 00:00Chromium 249 ug/L 10.0 1 01/31/08 03:48 7440-47-301/29/08 00:00Lead 114 ug/L 10.0 1 01/31/08 03:48 7439-92-101/29/08 00:00Selenium 31.4 ug/L 10.0 1 01/31/08 03:48 7782-49-201/29/08 00:00Silver ND ug/L 50.0 1 01/31/08 03:48 7440-22-401/29/08 00:00


Mercury ND ug/L 6.0 1 01/30/08 16:47 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 24 of 42



(317)875-5894

ANALYTICAL RESULTS











Date: 02/12/2008 03:16 PM Page 25 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 26 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 27 of 42



(317)875-5894

ANALYTICAL RESULTS








Arsenic 82.1 ug/L 10.0 1 01/31/08 03:54 7440-38-201/29/08 00:00Barium 976 ug/L 100 1 01/31/08 03:54 7440-39-301/29/08 00:00Cadmium 6.6 ug/L 5.0 1 01/31/08 03:54 7440-43-901/29/08 00:00Chromium 258 ug/L 10.0 1 01/31/08 03:54 7440-47-301/29/08 00:00Lead 112 ug/L 10.0 1 01/31/08 03:54 7439-92-101/29/08 00:00Selenium 31.2 ug/L 10.0 1 01/31/08 03:54 7782-49-201/29/08 00:00Silver ND ug/L 50.0 1 01/31/08 03:54 7440-22-401/29/08 00:00


Mercury ND ug/L 2.0 1 01/30/08 16:48 7439-97-601/29/08 00:00





Date: 02/12/2008 03:16 PM Page 28 of 42



(317)875-5894

ANALYTICAL RESULTS






Diethylphthalate ND ug/L 14.7 1 01/30/08 19:22 84-66-201/29/08 00:002,4-Dimethylphenol ND ug/L 14.7 1 01/30/08 19:22 105-67-901/29/08 00:00Dimethylphthalate ND ug/L 14.7 1 01/30/08 19:22 131-11-301/29/08 00:00Di-n-butylphthalate ND ug/L 14.7 1 01/30/08 19:22 84-74-201/29/08 00:004,6-Dinitro-2-methylphenol ND ug/L 73.5 1 01/30/08 19:22 534-52-101/29/08 00:002,4-Dinitrophenol ND ug/L 73.5 1 01/30/08 19:22 51-28-501/29/08 00:002,4-Dinitrotoluene ND ug/L 14.7 1 01/30/08 19:22 121-14-201/29/08 00:002,6-Dinitrotoluene ND ug/L 14.7 1 01/30/08 19:22 606-20-201/29/08 00:00Di-n-octylphthalate ND ug/L 14.7 1 01/30/08 19:22 117-84-001/29/08 00:00bis(2-Ethylhexyl)phthalate ND ug/L 7.4 1 01/30/08 19:22 117-81-701/29/08 00:00Fluoranthene ND ug/L 14.7 1 01/30/08 19:22 206-44-001/29/08 00:00Fluorene ND ug/L 14.7 1 01/30/08 19:22 86-73-701/29/08 00:00Hexachloro-1,3-butadiene ND ug/L 7.4 1 01/30/08 19:22 87-68-301/29/08 00:00Hexachlorobenzene ND ug/L 14.7 1 01/30/08 19:22 118-74-101/29/08 00:00Hexachlorocyclopentadiene ND ug/L 29.4 1 01/30/08 19:22 77-47-401/29/08 00:00Hexachloroethane ND ug/L 14.7 1 01/30/08 19:22 67-72-101/29/08 00:00Indeno(1,2,3-cd)pyrene ND ug/L 14.7 1 01/30/08 19:22 193-39-501/29/08 00:00Isophorone ND ug/L 14.7 1 01/30/08 19:22 78-59-101/29/08 00:002-Methylnaphthalene ND ug/L 14.7 1 01/30/08 19:22 91-57-601/29/08 00:002-Methylphenol(o-Cresol) ND ug/L 14.7 1 01/30/08 19:22 95-48-701/29/08 00:003&4-Methylphenol(m&p Cresol) ND ug/L 29.4 1 01/30/08 19:2201/29/08 00:00Naphthalene ND ug/L 7.4 1 01/30/08 19:22 91-20-301/29/08 00:002-Nitroaniline ND ug/L 73.5 1 01/30/08 19:22 88-74-401/29/08 00:003-Nitroaniline ND ug/L 73.5 1 01/30/08 19:22 99-09-201/29/08 00:004-Nitroaniline ND ug/L 73.5 1 01/30/08 19:22 100-01-601/29/08 00:00Nitrobenzene ND ug/L 14.7 1 01/30/08 19:22 98-95-301/29/08 00:002-Nitrophenol ND ug/L 14.7 1 01/30/08 19:22 88-75-501/29/08 00:004-Nitrophenol ND ug/L 73.5 1 01/30/08 19:22 100-02-701/29/08 00:00N-Nitroso-di-n-propylamine ND ug/L 14.7 1 01/30/08 19:22 621-64-701/29/08 00:00N-Nitrosodiphenylamine ND ug/L 14.7 1 01/30/08 19:22 86-30-601/29/08 00:00Pentachlorophenol ND ug/L 73.5 1 01/30/08 19:22 87-86-501/29/08 00:00Phenanthrene ND ug/L 14.7 1 01/30/08 19:22 85-01-801/29/08 00:00Phenol ND ug/L 14.7 1 01/30/08 19:22 108-95-201/29/08 00:00Pyrene ND ug/L 14.7 1 01/30/08 19:22 129-00-001/29/08 00:002,4,5-Trichlorophenol ND ug/L 14.7 1 01/30/08 19:22 95-95-401/29/08 00:002,4,6-Trichlorophenol ND ug/L 14.7 1 01/30/08 19:22 88-06-201/29/08 00:00Nitrobenzene-d5 (S) 158 % 40-112 1 01/30/08 19:22 4165-60-0 S301/29/08 00:002-Fluorobiphenyl (S) 147 % 31-114 1 01/30/08 19:22 321-60-8 S301/29/08 00:00Terphenyl-d14 (S) 146 % 10-116 1 01/30/08 19:22 1718-51-0 S301/29/08 00:00Phenol-d6 (S) 91 % 10-100 1 01/30/08 19:22 13127-88-301/29/08 00:002-Fluorophenol (S) 134 % 13-100 1 01/30/08 19:22 367-12-4 S301/29/08 00:002,4,6-Tribromophenol (S) 151 % 26-125 1 01/30/08 19:22 118-79-6 S301/29/08 00:00





Date: 02/12/2008 03:16 PM Page 29 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 30 of 42



(317)875-5894

ANALYTICAL RESULTS









Date: 02/12/2008 03:16 PM Page 31 of 42



(317)875-5894






OEXT/5892EPA 3510

EPA 82708270 Water MSSV

Associated Lab Samples: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007





2,4,5-Trichlorophenol ug/L ND 10.02,4,6-Trichlorophenol ug/L ND 10.02,4-Dichlorophenol ug/L ND 10.02,4-Dimethylphenol ug/L ND 10.02,4-Dinitrophenol ug/L ND 50.02,4-Dinitrotoluene ug/L ND 10.02,6-Dinitrotoluene ug/L ND 10.02-Chloronaphthalene ug/L ND 10.02-Chlorophenol ug/L ND 10.02-Methylnaphthalene ug/L ND 10.02-Methylphenol(o-Cresol) ug/L ND 10.02-Nitroaniline ug/L ND 50.02-Nitrophenol ug/L ND 10.03&4-Methylphenol(m&p Cresol) ug/L ND 20.03,3'-Dichlorobenzidine ug/L ND 20.03-Nitroaniline ug/L ND 50.04,6-Dinitro-2-methylphenol ug/L ND 50.04-Bromophenylphenyl ether ug/L ND 10.04-Chloro-3-methylphenol ug/L ND 20.04-Chloroaniline ug/L ND 20.04-Chlorophenylphenyl ether ug/L ND 10.04-Nitroaniline ug/L ND 50.04-Nitrophenol ug/L ND 50.0Acenaphthene ug/L ND 10.0Acenaphthylene ug/L ND 10.0Anthracene ug/L ND 10.0Benzo(a)anthracene ug/L ND 10.0Benzo(a)pyrene ug/L ND 10.0Benzo(b)fluoranthene ug/L ND 10.0Benzo(g,h,i)perylene ug/L ND 10.0Benzo(k)fluoranthene ug/L ND 10.0Benzyl alcohol ug/L ND 20.0bis(2-Chloroethoxy)methane ug/L ND 10.0bis(2-Chloroethyl) ether ug/L ND 10.0bis(2-Chloroisopropyl) ether ug/L ND 5.0bis(2-Ethylhexyl)phthalate ug/L ND 5.0Butylbenzylphthalate ug/L ND 10.0Chrysene ug/L ND 10.0Di-n-butylphthalate ug/L ND 10.0Di-n-octylphthalate ug/L ND 10.0Dibenz(a,h)anthracene ug/L ND 10.0Dibenzofuran ug/L ND 10.0Diethylphthalate ug/L ND 10.0



Date: 02/12/2008 03:16 PM Page 32 of 42



(317)875-5894








Dimethylphthalate ug/L ND 10.0Fluoranthene ug/L ND 10.0Fluorene ug/L ND 10.0Hexachloro-1,3-butadiene ug/L ND 5.0Hexachlorobenzene ug/L ND 10.0Hexachlorocyclopentadiene ug/L ND 20.0Hexachloroethane ug/L ND 10.0Indeno(1,2,3-cd)pyrene ug/L ND 10.0Isophorone ug/L ND 10.0N-Nitroso-di-n-propylamine ug/L ND 10.0N-Nitrosodiphenylamine ug/L ND 10.0Naphthalene ug/L ND 5.0Nitrobenzene ug/L ND 10.0Pentachlorophenol ug/L ND 50.0Phenanthrene ug/L ND 10.0Phenol ug/L ND 10.0Pyrene ug/L ND 10.02,4,6-Tribromophenol (S) % 82 26-1252-Fluorobiphenyl (S) % 75 31-1142-Fluorophenol (S) % 52 13-100Nitrobenzene-d5 (S) % 81 40-112Phenol-d6 (S) % 34 10-100Terphenyl-d14 (S) % 89 10-116

Parameter UnitsLCS



2,4-Dinitrotoluene ug/L 93.1100 93 39-1292-Chlorophenol ug/L 80.5100 81 39-1054-Chloro-3-methylphenol ug/L 82.6100 83 44-1154-Nitrophenol ug/L 44.8J100 45 10-80Acenaphthene ug/L 86.9100 87 40-116N-Nitroso-di-n-propylamine ug/L 89.8100 90 35-129Pentachlorophenol ug/L 81.8100 82 16-133Phenol ug/L 36.6100 37 12-120Pyrene ug/L 93.1100 93 44-1262,4,6-Tribromophenol (S) % 89 26-1252-Fluorobiphenyl (S) % 79 31-1142-Fluorophenol (S) % 57 13-100Nitrobenzene-d5 (S) % 85 40-112Phenol-d6 (S) % 36 10-100Terphenyl-d14 (S) % 95 10-116



Date: 02/12/2008 03:16 PM Page 33 of 42



(317)875-5894






MPRP/2490EPA 3010

EPA 60106010 MET






Arsenic ug/L ND 10.0Barium ug/L ND 100Cadmium ug/L ND 5.0Chromium ug/L ND 10.0Lead ug/L ND 10.0Selenium ug/L ND 10.0Silver ug/L ND 50.0

Parameter UnitsLCS



Arsenic ug/L 9931000 99 80-120Barium ug/L 9441000 94 80-120Cadmium ug/L 9621000 96 80-120Chromium ug/L 9371000 94 80-120Lead ug/L 9581000 96 80-120Selenium ug/L 9641000 96 80-120Silver ug/L 501500 100 80-120

Parameter UnitsMS



MSSpikeResult

5011471008

126788

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic ug/L 1000 80 75-12577 1 2010001730 2540 2500Barium ug/L P61000 78 75-12535 4 2010009700 10500 10000Cadmium ug/L 1000 79 75-12580 1 20100014.2 802 812Chromium ug/L 1000 82 75-12581 1 201000268 1090 1080Lead ug/L 1000 79 75-12579 0 201000791 1580 1580Selenium ug/L 1000 78 75-12577 1 201000114 892 882Silver ug/L 500 92 75-12590 2 20500ND 462 455



Date: 02/12/2008 03:16 PM Page 34 of 42



(317)875-5894






MERP/1511EPA 7470







Mercury ug/L ND 2.0

Parameter UnitsLCS



Mercury ug/L 4.25 83 80-120

Parameter UnitsMS



MSSpikeResult

5011471008

126814

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 50 83 75-12578 6 2050ND 41.8 39.4



Date: 02/12/2008 03:16 PM Page 35 of 42



(317)875-5894






OEXT/5911EPA 3510

EPA 80828082 GCS PCB Mod






PCB-1016 (Aroclor 1016) ug/L ND 0.50PCB-1221 (Aroclor 1221) ug/L ND 0.50PCB-1232 (Aroclor 1232) ug/L ND 0.50PCB-1242 (Aroclor 1242) ug/L ND 0.50PCB-1248 (Aroclor 1248) ug/L ND 0.50PCB-1254 (Aroclor 1254) ug/L ND 0.50PCB-1260 (Aroclor 1260) ug/L ND 0.50Tetrachloro-m-xylene (S) % 84 10-143

Parameter UnitsLCS



PCB-1016 (Aroclor 1016) ug/L 5.05 101 40-160PCB-1260 (Aroclor 1260) ug/L 4.85 96 40-160Tetrachloro-m-xylene (S) % 85 10-143



Date: 02/12/2008 03:16 PM Page 36 of 42



(317)875-5894






MSV/7225EPA 8260

EPA 82608260 MSV






1,1,1,2-Tetrachloroethane ug/L ND 5.01,1,1-Trichloroethane ug/L ND 5.01,1,2,2-Tetrachloroethane ug/L ND 5.01,1,2-Trichloroethane ug/L ND 5.01,1-Dichloroethane ug/L ND 5.01,1-Dichloroethene ug/L ND 5.01,1-Dichloropropene ug/L ND 5.01,2,3-Trichlorobenzene ug/L ND 5.01,2,3-Trichloropropane ug/L ND 5.01,2,4-Trichlorobenzene ug/L ND 5.01,2,4-Trimethylbenzene ug/L ND 5.01,2-Dibromoethane (EDB) ug/L ND 5.01,2-Dichlorobenzene ug/L ND 5.01,2-Dichloroethane ug/L ND 5.01,2-Dichloropropane ug/L ND 5.01,3,5-Trimethylbenzene ug/L ND 5.01,3-Dichlorobenzene ug/L ND 5.01,3-Dichloropropane ug/L ND 5.01,4-Dichlorobenzene ug/L ND 5.02,2-Dichloropropane ug/L ND 5.02-Butanone (MEK) ug/L ND 25.02-Chlorotoluene ug/L ND 5.02-Hexanone ug/L ND 25.04-Chlorotoluene ug/L ND 5.04-Methyl-2-pentanone (MIBK) ug/L ND 25.0Acetone ug/L ND 100Acrolein ug/L ND 100Acrylonitrile ug/L ND 100Benzene ug/L ND 5.0Bromobenzene ug/L ND 5.0Bromochloromethane ug/L ND 5.0Bromodichloromethane ug/L ND 5.0Bromoform ug/L ND 5.0Bromomethane ug/L ND 5.0Carbon disulfide ug/L ND 10.0Carbon tetrachloride ug/L ND 5.0Chlorobenzene ug/L ND 5.0Chloroethane ug/L ND 5.0Chloroform ug/L ND 5.0Chloromethane ug/L ND 5.0cis-1,2-Dichloroethene ug/L ND 5.0cis-1,3-Dichloropropene ug/L ND 5.0Dibromochloromethane ug/L ND 5.0



Date: 02/12/2008 03:16 PM Page 37 of 42



(317)875-5894








Dibromomethane ug/L ND 5.0Dichlorodifluoromethane ug/L ND 5.0Ethyl methacrylate ug/L ND 100Ethylbenzene ug/L ND 5.0Hexachloro-1,3-butadiene ug/L ND 5.0Iodomethane ug/L ND 10.0Isopropylbenzene (Cumene) ug/L ND 5.0Methyl-tert-butyl ether ug/L ND 4.0Methylene chloride ug/L ND 5.0n-Butylbenzene ug/L ND 5.0n-Propylbenzene ug/L ND 5.0Naphthalene ug/L ND 5.0p-Isopropyltoluene ug/L ND 5.0sec-Butylbenzene ug/L ND 5.0Styrene ug/L ND 5.0tert-Butylbenzene ug/L ND 5.0Tetrachloroethene ug/L ND 5.0Toluene ug/L ND 5.0trans-1,2-Dichloroethene ug/L ND 5.0trans-1,3-Dichloropropene ug/L ND 5.0trans-1,4-Dichloro-2-butene ug/L ND 100Trichloroethene ug/L ND 5.0Trichlorofluoromethane ug/L ND 5.0Vinyl acetate ug/L ND 10.0Vinyl chloride ug/L ND 2.0Xylene (Total) ug/L ND 10.04-Bromofluorobenzene (S) % 99 73-120Dibromofluoromethane (S) % 106 82-122Toluene-d8 (S) % 98 80-120

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/L 53.950 108 70-1261,1,1-Trichloroethane ug/L 54.250 108 70-1281,1,2,2-Tetrachloroethane ug/L 47.050 94 66-1341,1,2-Trichloroethane ug/L 49.950 100 71-1311,1-Dichloroethane ug/L 50.150 100 72-1251,1-Dichloroethene ug/L 53.650 107 66-1401,1-Dichloropropene ug/L 52.650 105 72-1251,2,3-Trichlorobenzene ug/L 50.250 100 63-1301,2,3-Trichloropropane ug/L 48.050 96 50-1391,2,4-Trichlorobenzene ug/L 49.450 99 61-1291,2,4-Trimethylbenzene ug/L 46.950 94 72-1281,2-Dibromoethane (EDB) ug/L 48.350 97 70-130



Date: 02/12/2008 03:16 PM Page 38 of 42



(317)875-5894




Parameter UnitsLCS



1,2-Dichlorobenzene ug/L 47.850 96 72-1291,2-Dichloroethane ug/L 53.250 106 66-1311,2-Dichloropropane ug/L 50.750 101 72-1251,3,5-Trimethylbenzene ug/L 46.150 92 72-1301,3-Dichlorobenzene ug/L 47.450 95 74-1281,3-Dichloropropane ug/L 48.750 97 70-1301,4-Dichlorobenzene ug/L 47.550 95 72-1242,2-Dichloropropane ug/L 57.350 115 62-1342-Butanone (MEK) ug/L 237250 95 44-1502-Chlorotoluene ug/L 44.750 89 74-1332-Hexanone ug/L 263250 105 38-1504-Chlorotoluene ug/L 45.250 90 73-1294-Methyl-2-pentanone (MIBK) ug/L 241250 96 55-142Acetone ug/L 307250 123 29-150Acrolein ug/L 219 L01000 22 50-150Acrylonitrile ug/L 9481000 95 50-150Benzene ug/L 46.850 94 75-126Bromobenzene ug/L 47.150 94 72-129Bromochloromethane ug/L 48.650 97 67-139Bromodichloromethane ug/L 55.050 110 70-130Bromoform ug/L 45.150 90 63-127Bromomethane ug/L 39.650 79 43-146Carbon disulfide ug/L 107100 107 52-172Carbon tetrachloride ug/L 59.550 119 65-125Chlorobenzene ug/L 45.050 90 74-123Chloroethane ug/L 63.350 127 61-141Chloroform ug/L 49.850 100 68-127Chloromethane ug/L 39.450 79 42-138cis-1,2-Dichloroethene ug/L 49.650 99 77-132cis-1,3-Dichloropropene ug/L 45.750 91 60-119Dibromochloromethane ug/L 53.850 108 72-133Dibromomethane ug/L 51.850 104 76-133Dichlorodifluoromethane ug/L 40.850 82 50-179Ethyl methacrylate ug/L 48.8J50 98 70-130Ethylbenzene ug/L 47.050 94 70-129Hexachloro-1,3-butadiene ug/L 53.150 106 71-132Iodomethane ug/L 86.1100 86 70-130Isopropylbenzene (Cumene) ug/L 48.850 98 74-126Methyl-tert-butyl ether ug/L 106100 106 68-139Methylene chloride ug/L 49.750 99 50-119n-Butylbenzene ug/L 51.950 104 70-130n-Propylbenzene ug/L 48.650 97 74-135Naphthalene ug/L 50.950 102 56-134p-Isopropyltoluene ug/L 48.250 96 70-133sec-Butylbenzene ug/L 48.450 97 75-133Styrene ug/L 47.050 94 75-125tert-Butylbenzene ug/L 40.250 80 69-121Tetrachloroethene ug/L 40.950 82 55-121



Date: 02/12/2008 03:16 PM Page 39 of 42



(317)875-5894




Parameter UnitsLCS



Toluene ug/L 46.150 92 72-126trans-1,2-Dichloroethene ug/L 55.750 111 73-131trans-1,3-Dichloropropene ug/L 47.450 95 59-119trans-1,4-Dichloro-2-butene ug/L 51.5J50 103 50-150Trichloroethene ug/L 49.650 99 73-123Trichlorofluoromethane ug/L 48.650 97 65-145Vinyl acetate ug/L 199200 100 50-150Vinyl chloride ug/L 39.250 78 54-139Xylene (Total) ug/L 143150 95 72-1274-Bromofluorobenzene (S) % 104 73-120Dibromofluoromethane (S) % 105 82-122Toluene-d8 (S) % 97 80-120

Parameter UnitsMS


127886MATRIX SPIKE SAMPLE:MSSpike

Result5011524001

1,1,1,2-Tetrachloroethane ug/L 50.650 101 54-134ND1,1,1-Trichloroethane ug/L 55.650 111 63-130ND1,1,2,2-Tetrachloroethane ug/L 45.650 91 59-139ND1,1,2-Trichloroethane ug/L 48.350 97 64-136ND1,1-Dichloroethane ug/L 50.150 100 67-129ND1,1-Dichloroethene ug/L 57.550 115 59-150ND1,1-Dichloropropene ug/L 54.250 108 68-127ND1,2,3-Trichlorobenzene ug/L 46.250 92 39-136ND1,2,3-Trichloropropane ug/L 45.750 91 41-137ND1,2,4-Trichlorobenzene ug/L 45.350 91 34-137ND1,2,4-Trimethylbenzene ug/L 45.650 91 36-143ND1,2-Dibromoethane (EDB) ug/L 45.750 91 64-132ND1,2-Dichlorobenzene ug/L 46.650 93 52-136ND1,2-Dichloroethane ug/L 52.150 104 62-134ND1,2-Dichloropropane ug/L 49.850 100 67-128ND1,3,5-Trimethylbenzene ug/L 45.850 92 33-145ND1,3-Dichlorobenzene ug/L 45.350 91 47-139ND1,3-Dichloropropane ug/L 47.550 95 63-134ND1,4-Dichlorobenzene ug/L 45.550 91 46-135ND2,2-Dichloropropane ug/L 57.950 116 51-136ND2-Butanone (MEK) ug/L 231250 92 54-148ND2-Chlorotoluene ug/L 45.350 91 43-147ND2-Hexanone ug/L 251250 100 60-140ND4-Chlorotoluene ug/L 44.850 90 46-139ND4-Methyl-2-pentanone (MIBK) ug/L 233250 93 56-147NDAcetone ug/L 256250 103 27-163NDAcrolein ug/L 2040 M01000 204 50-150NDAcrylonitrile ug/L 9241000 92 50-150NDBenzene ug/L 47.550 95 66-135NDBromobenzene ug/L 46.150 92 57-135NDBromochloromethane ug/L 47.650 95 61-142ND



Date: 02/12/2008 03:16 PM Page 40 of 42



(317)875-5894




Parameter UnitsMS


127886MATRIX SPIKE SAMPLE:MSSpike

Result5011524001

Bromodichloromethane ug/L 51.950 104 60-135NDBromoform ug/L 43.350 87 50-127NDBromomethane ug/L 41.450 83 32-148NDCarbon disulfide ug/L 111100 111 46-173NDCarbon tetrachloride ug/L 59.750 119 51-130NDChlorobenzene ug/L 43.950 88 59-135NDChloroethane ug/L 64.850 130 58-153NDChloroform ug/L 49.650 99 61-133NDChloromethane ug/L 40.850 82 44-135NDcis-1,2-Dichloroethene ug/L 49.550 99 75-133NDcis-1,3-Dichloropropene ug/L 44.150 88 51-121NDDibromochloromethane ug/L 50.250 100 56-139NDDibromomethane ug/L 50.550 101 70-136NDDichlorodifluoromethane ug/L 46.550 93 25-175NDEthyl methacrylate ug/L 47.2J50 94 50-150NDEthylbenzene ug/L 46.550 93 59-143NDHexachloro-1,3-butadiene ug/L 50.750 101 50-155NDIodomethane ug/L 84.1100 84 70-130NDIsopropylbenzene (Cumene) ug/L 49.250 98 48-139NDMethyl-tert-butyl ether ug/L 104100 104 62-147NDMethylene chloride ug/L 50.050 100 46-119NDn-Butylbenzene ug/L 50.450 101 50-156NDn-Propylbenzene ug/L 48.250 96 33-153NDNaphthalene ug/L 47.250 94 40-136NDp-Isopropyltoluene ug/L 47.750 95 38-143NDsec-Butylbenzene ug/L 48.650 97 35-151NDStyrene ug/L 46.550 93 53-133NDtert-Butylbenzene ug/L 38.750 77 37-136NDTetrachloroethene ug/L 41.850 84 40-127NDToluene ug/L 45.750 91 63-137NDtrans-1,2-Dichloroethene ug/L 57.050 114 70-134NDtrans-1,3-Dichloropropene ug/L 44.550 89 49-121NDtrans-1,4-Dichloro-2-butene ug/L 46.8J50 94 50-150NDTrichloroethene ug/L 50.350 101 61-131NDTrichlorofluoromethane ug/L 53.350 107 64-146NDVinyl acetate ug/L 180200 90 50-150NDVinyl chloride ug/L 43.550 87 54-140NDXylene (Total) ug/L 144150 96 54-140ND4-Bromofluorobenzene (S) % 103 73-120Dibromofluoromethane (S) % 104 82-122Toluene-d8 (S) % 97 80-120



Date: 02/12/2008 03:16 PM Page 41 of 42



(317)875-5894

QUALIFIERS



DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

BATCH QUALIFIERS

Batch: MSSV/2236A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[1]

Batch: GCSV/2315A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[1]

ANALYTE QUALIFIERS

Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0Matrix spike recovery was outside laboratory control limits.M0Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than thespike level.

P6

Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.Results unaffected by high bias.

S3



Date: 02/12/2008 03:16 PM Page 42 of 42



(317)875-5894

beech grove rockpile phase 2 letter report draft

Documents