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  • Laboratory Information Management System (LIMS)

    ATTACHMENT A2: Instrument Integration Mapping

    July, 2018

    1

  • C O N T E N T S

    Contents

    INTRODUCTION ............................................................................................................................... 3

    1.1 Purpose ............................................................................................................................................................. 3

    1.2 Terminology ...................................................................................................................................................... 3

    INSTRUMENT LIST ........................................................................................................................... 4

    INSTRUMENT INTEGRATION DETAILS ............................................................................................. 6

    1.3 Organics ............................................................................................................................................................ 6 GC/MS AGILENT VOA ............................................................................................................................... 6 1.3.1 GC/MS AGILENT VOA II ............................................................................................................................ 8 1.3.2 GC/MS THERMO ISQ .............................................................................................................................. 10 1.3.3 GC/MS THERMO ISQ 2 ........................................................................................................................... 11 1.3.4 GC/MS VARIAN 240 ............................................................................................................................... 14 1.3.1 GC/MS THERMO TSQ ............................................................................................................................. 15 1.3.2 GC TRACE ULTRA .................................................................................................................................... 18 1.3.3 GC TRACE 2000 ...................................................................................................................................... 19 1.3.4 GC ECD 1 & GC ECD 2 ............................................................................................................................. 21 1.3.5 IC TOC 1030............................................................................................................................................ 22 1.3.6 IC SYSTEM METROHM and IC COMPACT METROHM ............................................................................ 24 1.3.7

    1.4 Metals ............................................................................................................................................................. 25 HG ANALYZER TEKRAN ........................................................................................................................... 25 1.4.1 HG LEEMAN HYDRA II ............................................................................................................................ 27 1.4.1 ICP PE OPTIMA 5300DV ......................................................................................................................... 29 1.4.2 ICP-MS AGILENT 7900 ............................................................................................................................ 30 1.4.3 SPEC. FLRSC. VARIAN ............................................................................................................................. 32 1.4.4

    1.5 Inorganics ....................................................................................................................................................... 34 AUTOTITRATOR METROHM ................................................................................................................... 34 1.5.1 SPEC. UV/VIS AGILENT ........................................................................................................................... 35 1.5.2 SEGMENTED FLOW ................................................................................................................................ 38 1.5.3

    1.6 Biology ............................................................................................................................................................ 39 SKALAR ................................................................................................................................................... 39 1.6.1 MICROPLATE READER ............................................................................................................................ 41 1.6.2 GEL IMAGING SYSTEM ........................................................................................................................... 43 1.6.3

    1.7 Balances and Meters ...................................................................................................................................... 43 BALANCES .............................................................................................................................................. 43 1.7.1 Meters.................................................................................................................................................... 44 1.7.2

    2

  • I N T R O D U C T I O N

    1.1 Purpose

    This Instrument Integration Mapping report documents the instruments currently existing at the laboratory in each of the functional areas that are used each day to analyze incoming samples. The instruments listed in this document cover the following sections:

     Organics (Dept. 3)  Organics (Dept. 4)  Inorganics (Dept. 6)  Metals (Dept. 8)  Biology (Dept. 9)  Balances (Various Departments)  Meters (Various Departments)

    The primary purpose of the Instrument Integration Mapping report is to describe the current steps associated with the instrumentation and the movement of results into the LIMS and present the required mapping for future integration. As a part of this document, each instrument will be discussed and the output file(s) currently generated broken down so that vendors will have both an understanding of the current setup and process as well as to identify future needs to drive the automation process for instrument integration.

    1.2 Terminology

    Term Description

    EBMUD East Bay Municipal Utility District Laboratory

    COTS Commercial Off-the-Shelf, a system designed for wide distribution with few changes for a given installation

    LIMS Laboratory Information Management System

    RFP Request for Proposal

    DEM Data Entry Monster, the internal utility for uploading data via EXCEL spreadsheet

    3

  • I N S T R U M E N T L I S T The table below contains all of the instruments that are currently utilized by the laboratory. Some of the instruments on this list are not targeted for integration currently, but this will be decided after a vendor has been selected. Also included in this list are several balances that do not require integration but some may be connected to the selected LIMS with Wedge software. The laboratory does utilize Wedge software currently in the solids area however; they do not currently pass data directly into the existing LIMS. The weights are passed to a spreadsheet that is then consumed using a developed utility built in-house. The following table (Table 2.1) provides all instruments identified for this discussion.

    Table 2.1 – List of Instruments by Laboratory Group

    Laboratory Instrument Model Software Output Files Available

    Organics GC/MS AGILENT VOA Agilent 7890B/5977A MassHunter; Chemstation

    MassHunter_524THM.csv and MassHunter_524THM.pdf, Chemstation_8260.txt, Chemstation_gas.txt

    Organics GC/MS AGILENT VOA II Agilent 7890B/5977A MassHunter; Chemstation

    MassHunter_524THM.csv and MassHunter_524THM.pdf, Chemstation_8260.txt, Chemstation_gas.txt

    Organics GC/MS THERMO ISQ Trace 1300 GC/ISQ MS TraceFinder 3.5.2 TraceFinder_525.prn and TraceFinder_525.xlsx, TraceFinder_548.prn and TraceFinder_548.xlsx, TraceFinder_625.prn and TraceFinder_625.xlsx, TraceFinder_Diesel.prn and TraceFinder_Diesel.xlsx

    Organics GC/MS THERMO ISQ 2 Trace 1300 GC/ISQ MS TraceFinder 4.1 TraceFinder_8270.prn and TraceFinder_8270.xlsx

    Organics GC/MS VARIAN 240 Varian 240 Chemstation Organics GC/MS/MS THERMO

    TSQ Thermo TSQ EVO TraceFinder 4.1 TraceFinder_521.prn and

    TraceFinder_521.xlsx, TraceFinder_Geosmin.prn and TraceFinder_Geosmin.xlsx

    Organics GC TRACE ULTRA Thermo Trace GC Ultra TotalChrom 6.3.2 TotalChrom_552.TX0 and TotalChrom_608.TX0

    Organics GC TRACE 2000 Thermo Trace GC 2000 with ECD

    TotalChrom 6.3.2 TotalChrom_552.TX0 and TotalChrom_608.TX0

    Organics GC ECD 1 Thermo Trace 1300 with ECD

    Chromeleon 7.2.7 None available yet

    Organics GC ECD 2 Thermo Trace 1300 with ECD

    Chromeleon 7.2.7 None available yet

    Organics IC COMPACT METROHM

    Metrohm 930 Compact IC MagicNet 3.1 MagicNet_300anions.csv

    4

  • Laboratory Instrument Model Software Output Files Available

    Organics IC SYSTEM METROHM Metrohm 850 Professional IC

    MagicNet 3.1 MagicNet_300anions.csv

    Organics IC TOC 1030 OI Analytical 1030W TOC Analyzer

    ATOC ATOC.txt

    Inorganics AUTOTITRATOR METROHM

    METROHM 905 Met