article title: facile synthesis of 4 …10.1007...article title: facile synthesis of...
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Article Title: Facile Synthesis of 4-Hydroxycinnamaldehydes
Journal Name: BioEnergy Research
Authors: Yimin Zhu*,†,‡ , Allison Mohammadi†, and John Ralph†,‡
Affiliations: †Department of Biochemistry and ‡DOE Great Lakes Bioenergy Research Center,
University of Wisconsin-Madison, 1710 University Ave, Madison, WI 53726
E-mail: [email protected].
Supplementary Material: Spectra of compounds 1a-d and 2a-d.
[ppm] 8 6 4 2
8.82
72
7.57
347.
5526
7.54
917.
5416
7.53
566.
9908
6.95
946.
8876
6.88
396.
8703
3.77
99
3.20
71
[ppm] 200 150 100 50
167.
7515
160.
0857
143.
3217
130.
6689
127.
7832
116.
5725
114.
0697
62.1
679
32.5
305
[ppm] 8 6 4
8.21
95
7.59
507.
5636
7.28
657.
2825
7.17
927.
1753
7.16
287.
1588
7.01
896.
9875
6.88
266.
8663
3.88
883.
7685
3.22
22
[ppm] 200 150 100 50 0
167.
7449
149.
5370
148.
5745
143.
8635
128.
1067
123.
0955
116.
0957
114.
1228
111.
7510
62.1
508
56.2
559
32.5
583
[ppm] 200 150 100 50
167.
6862
148.
8402
144.
2054
138.
9722
126.
8476
114.
3640
106.
6502
62.1
493
56.6
297
32.5
598
[ppm] 7 6 5 4
7.52
237.
4908
7.06
397.
0598
6.98
036.
9762
6.96
396.
9598
6.89
476.
8633
6.79
006.
7737
3.78
61
3.28
57
[ppm] 150 100 50
169.
2440
149.
2918
146.
7798
145.
4928
128.
2445
122.
6802
116.
4804
115.
1731
112.
9392
62.3
837
32.7
762
[ppm] 8 6 4
9.64
259.
6271
9.09
18
7.62
537.
6077
7.57
37
6.94
416.
9268
6.63
606.
6205
6.60
436.
5888
[ppm] 8 6 4
9.64
289.
6273
8.40
18
7.58
797.
5562
7.38
837.
3843
7.22
057.
2166
7.20
417.
2002
6.92
006.
9037
6.68
376.
6682
6.65
216.
6366
3.92
51
[ppm] 200 150 100 50
193.
9062
154.
0873
150.
8280
148.
8433
127.
4010
127.
0012
124.
7886
116.
1978
111.
4477
56.3
118
[ppm] 8 6 4 2
9.62
719.
6116
8.49
96
7.54
207.
5104
7.21
587.
2116
7.12
847.
1243
7.11
217.
1079
6.91
846.
9021
6.56
186.
5463
6.53
026.
5147