appendix g report entitled new orleans municipal yacht harbor … · 2017-10-02 · sampling and...

Appendix G

Report entitled New Orleans Municipal Yacht Harbor Sediment

Sampling and Analysis Investigation Report, dated February 2017

NEW ORLEANS MUNICIPAL YACHT HARBOR SEDIMENT SAMPLING AND ANALYSIS

INVESTIGATION REPORT

NEW ORLEANS, LOUISIANA

Prepared for:

MOFFATT & NICHOL

BATON ROUGE, LOUISIANA

FEBRUARY 2017

17170 Perkins Road Baton Rouge, Louisiana 70810

{225) 755-1000

CK Project No. 14436

TABLE OF CONTENTS

New Orleans Municipal Yacht Harbor

Sediment San1pling and Analysis

Section Page

1.0 INTRODUCTION ............................................................................................................ 1 2.0 SAMPLE COLLECTION .................................................................................................... 1

3.0 INVESTIGATION RESULTS .............................................................................................. 2

3.1 Site Geology and Hydrology ............................................................................... 2 3.2 Analytical Results and Evaluation ...................................................................... 2

4.0 SUMMARY AND CONCLUSIONS .................................................................................... 3

Figure

1 Site Location Map 2 Sample Location Map

Table 1 Sediment Analytical Summary 2 SPLP Summary

Appendix A Laboratory Reports

LIST OF FIGURES

LIST OF TABLES

LIST OF APPENDICES

CK Associates

1.0 INTRODUCTION

New Orleans Municipal Yacht Harbor Sediment Sampling and Analysis

Moffatt & Nichol is managing repairs to infrastructure damaged by Hurricane Katrina at the

New Orleans Municipal Yacht Harbor (Figure 1). CK Associates (CK) was retained to conduct sampling and analysis of the sediment prior to initiation of dredging activities. Moffatt & Nichol

may place the dredged material on an adjacent upland permitted area within the West End

proper. Sampling and analysis of the sediment surface was requested to determine concentrations of potential constituents of concern (COCs) within the material to be dredged.

The dredge activities planned include the removal of one foot of sediment on the west side of

the dredge area and two feet of sediment removal on the east side.

Sampling and analysis of sediments within the Municipal Yacht Harbor was previously

conducted in 2009. The current sampling and analysis was conducted within a portion of the

area that was sampled in 2009 (Figure 2). Sediment samples were analyzed for the original list

of COCs analyzed in 2009.

2.0 SAMPLE COLLECTION

Ten samples were collected within the area to be dredged (Figure 2) on January 11 and 13,

2017. The sample locations were evenly spaced within the dredging area in order to capture sediment samples representative of the sediment material to be removed. Samples were

collected manually with a Ponar dredge deployed from a work boat platform.

A sufficient volume of sediment material was collected from each location to conduct the requested analyses and associated quality assurance and quality control samples (QA/QC).

Each sample was collected with a Ponar dredge and emptied into a stainless steel pan on the

boat deck. Samples were collected directly into laboratory-provided containers appropriate for the requested analyses. Samples collected for volatile constituents were collected first into

pre-weighed Terracore sampling kits. One duplicate, matrix spike, and matrix spike duplicate

sample were collected and analyzed. One sample of rinsate water was collected on each sampling day. All samples were labeled with unique sample identification, recorded on a chain

of-custody form, and placed into iced coolers for transport to the analytical laboratory.

CK personnel donned new, clean sampling gloves prior to handling samples or sampling

equipment. All non-disposable sampling equipment was decontaminated prior to arriving on

site and between sample locations. All unused sediment and rinsate water was returned to the

harbor.

The analyses that were completed in the 2009 evaluation were requested for all samples.

These include the Louisiana Department of Environmental Quality's (LDEQ) Risk Evaluation

Corrective Action Program (RECAP) regulated metals, volatile organic compounds (VOCs),

semivolatile organic compounds (SVOCs), Total Petroleum Hydrocarbon (TPH) Volatile Phase

Hydrocarbons (VPH) and Extractable Phase Hydrocarbons (EPH), hexavalent chromium, pesticides, cyanide, and nitrate. Moisture content was conducted on each sample, and all

1 CK Associates


analytical results were reported on a dry weight basis. All analyses were completed by a LDEQaccredited laboratory, TestAmerica, in Pensacola, Florida. Analyses were conducted using the following methodologies:

• VOCs by EPA Method 8260

• SVOCs by EPA Method 8270 • VPH/EPH by MADEP

• Metals by EPA Methods 6010 & 7470 • Hexavalent chromium by EPA Method 7196 • Pesticides by EPA Methods 8011 & 8081 • Cyanide by EPA Method 9012 and Standard Methods 335.2 • Nitrate by Standard Methods 353.2

3.0 INVESTIGATION RESULTS

3.1 Site Geology and Hydrology

Based on observations made during sampling, the sampled harbor bottom consisted of fine grained, poorly consolidated mud. The eastern-most sample (CK-10) consisted of fine grained sand with live clams and shells.

3.2 Analytical Results and Evaluation

Laboratory analytical results for the sediment samples are summarized in Table 1. The

laboratory analytical data reports are included in Appendix A.

Sediment analytical results were compared to limiting RECAP screening standards. The

limiting RECAP screening standard for each COC is the more conservative of Soil_SSni (protective of a residential scenario) and Soil_SSGW (protective of the soil to groundwater risk pathway). Arsenic and lead were detected in excess of limiting RECAP screening standards in four samples. No other analyzed COCs were detected in excess of limiting RECAP screening standards.

Arsenic was detected at CK-2 at 14 milligrams per kilogram (mg/kg), which exceeds the

RECAP Soil_SSni concentration of 12 mg/kg. Because the RECAP Soil_SSni is based on a background concentration, RECAP allows for the mean concentration of the analyzed arsenic concentrations to be compared to the standard. The mean of the 11 collected

samples is 9.07 mg/kg, which is below the limiting RECAP screening standard concentration for arsenic.

Lead was detected in excess of the RECAP Soil_SSGW in three samples (CK-1, CK-1 Dup, and CK-3). A Synthetic Precipitation Leaching Procedure (SPLP) analysis of the sample exhibiting the highest lead concentration (CK-1) was conducted. The SPLP result was compared to the RECAP Groundwater Class 1 (GWl) standard multiplied by 20 in

2 CK Associates


Sediment Sampling and Analysis

accordance with RECAP guidance. The results are summarized in Table 2. The detected SPLP concentration of 0.025 milligrams per liter (mg/L) does not exceed the GWl x 20 value of 0.3 mg/L; therefore, the detected lead concentrations can be compared to the limiting Soil_SSni standard of 400 mg/kg. Lead concentrations do not exceed 400 mg/kg in any of the sampled sediment.

Due to the high moisture content of the samples (ranging from 24.9% at CK-10 to 79.1% at CK-4), detected concentrations were reported on a dry weight basis. The adjustment for moisture content caused elevated reporting limits in some samples for some COCs. None of these COCs were detected. The elevated reporting limits exceed the Soil_SSGW for 1,1,2,2-tetrachloroethane, 1,1,2-trichloroethane, 1,1-dichloroethene, l,2-dibromo-3-chloropropane, methylene chloride, and aniline. The reporting limit for thallium exceeds the Soil_SSni for most of the samples.

4.0 SUMMARY AND CONCLUSIONS

CK performed sediment sampling and analysis at the New Orleans Municipal Yacht Harbor in order to determine current concentrations of potential COCs within the material to be dredged.

Arsenic was detected in one sample in excess of the limiting screening standard concentration, but the average of all samples did not exceed the limiting screening standard.

Lead was detected in three samples in excess of the limiting screening standard concentration (Soil_SSGW). The sample exhibiting the highest lead concentration was further analyzed for SPLP lead. The results of the SPLP analysis indicated that the lead concentration is protective of the soil to groundwater risk pathway. None of the samples contained lead concentrations in excess of the Soil_SSni standard.

Seven COCs were reported as not detected at a reporting limit that exceeded the RECAP limiting standard. The reporting limits were elevated due to the dry weight correction applied to the analytical results. There is no indication that these COCs are present in the sampled material.

The sediment sampling and analyses indicate that the sampled sediment does not contain any analyzed COCs in excess of RECAP limiting screening standards. Concentrations present in the sampled material are protective of potential receptors in a non-industrial use scenario.

3 CK Associates

FIGURES

Moffat & Nichol Baton Rouge, Louisiana


Orkans P<lrish Site Location Map

Orleans Parish

Drawn: CPVAMl0.4 Checked: JAL

0 3,000 6,000

Feet • esri CK ASSOCIATES

i,~,\-{,Off.~O"i (,,,,,,,!>eh

:::: ""'.'.:::""~

A roved: JAL

Date:

f)i.vg. No.:

01/31/20_"!_? ___ "'

A14436-0l

Reference: U.S.G.S 24K Series Quad Map, Spanish Fort, lA. Figure 1

Legend

,t;? Sample Points

Dredge Limits

0 225

Feet

Imagery: USDA FSA, NA!P 2015.

4$0

N

+ s

• esri P•t\o.,

N~h'"''" ""'"

Moffat & Nichol Baton Rouge, Louisiana


Sample Location Map

Orleans Parish

Drawn: CPVAMl0.11 Checked: JAL

A roved: JAL

Daw: 01/31/2017

Dwg. No.: A14436-02

Figure 2

TABLES

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Analyte Units Xylenes, Total mg/Kg

Zinc mg/Kg

Fl: MS and/or MSD Recovery Is outside accept~nce limits.

fZ, MS/MSD RPO exceeds control limits

•: LCS or LCSO i$ outside acceptance limits.

Soll_SSGW

''° 2800

J: Detected concentration is between the MDL and RDL; value is estimated

bold font Indicates a detected COC

highlighed concentrations ~ceed R~CAP limiting standard

CK-l

l/ll/2017 Soil_S$ni ll;lOAM

" <:0.0070

2300 ''°

Tablo l New Or!oan$ Municipal Yacht Harbor

S11dlm•mt Analyti~al Summary

CK·l Oupli<:ato CK·2 CK·3

l/ll/2017 l/ll/2017 1/11/2017 12:00 PM ll:40AM 12:15 PM

<:0.0069 <:0.0098 <:0.0078

'" "' '"

CK~ CK·S CK·G CK-7 CK-S CK·9 CK·lO

1/11/2017 1/11/2017 1/13/2017 l/13/2017 l/13/2017 1/13/2017 1/13/2017

12:30 PM l:lS PM 9:30AM 9:4SAM 10:10 AM l0'.2SAM 10'.45 AM

<:0.0099 <:0.16 <:0.0049 <:0.0080 <:0.0039 <0.0049 <0.0026

'" 150 ''° 200 " 93 "

Page S of S

Analyte Units

CK-1 RECAP GWl 1/11/2017

x20 ll:lOAM

Table 2


SPLP Summary

J: Detected concentration is between the MDL and RDL; value is estimated

APPENDIX A

LABORATORY REPORTS

The tparaand at th

This inten

Resu

est results in this repoit meet all 2003 NELAC and 2009 TN! requirements for accredited meters, exceptions are noted in this report. This repott may not be reproduced except in fufl, with Vfritten approval front the laboratory For questions please contact the Project Alfanager e e-mail address or telephone number fisted on this page.

report has been electronically signed and authorized by the signato1y. Electronic signature is ded to be the legally binding eqwVafent of a traditionally handwritten signature.

lts relate only to the items tested and tile san1pfe(s) as received by tile Jaboraloty.

THE LEADER IN ENVIRONMENTAL TESTING

ANAL YTICAl REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola 3355 Mclemore Drive Pensacola, FL 32514 Tel: (850)474-1001

TestArnerica Job ID: 400-132540-1 Client Project/Site: Moffat & Nichol

For: C-K Associates 17170 Perkins Road Baton Rouge, Louisiana 70810

Attn: Jennifer Lindquist

C}--W~ Authorized for release by: 21112017 3:17:01 PM

Jason Wilson, Project Manager I (251 )706-3217 [email protected]

Client: C-K Associates Project/Site: Moffat & Nichol

Table of Contents

TestAmerica Job ID: 400-132540-1

Cover Page .................. _ . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 Chronicle .. _ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124 Certification Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135 Chain of Custody. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136

Page 2 of 140 TestAmerica Pensacola

2/1/2017


Job ID: 400-132540-1

Laboratory: Tes!America Pensacola

Narrative

Comments No additional comments.

Receipt The samples were received on 1/12/2017 9:21 AM, 1/12/2017 4:57 PM and 1/14/2017 8:32 AM: the samples arrived in good condition, properly preserved and, \vhere required, on ice. The ten1peratures of the 8 coolers at receipt time were 1.0° C, 1.9° C, 2.0° C, 2.1° C, 2.2° c, 2.4° C, 2.7° C and 4.0° C.

GC/MSVOA Method(s) 8260C: The laboratory control sample (LCS) for analytical batch 400-338529 recovered outside control limits for one analyte. This analyte was biased high in the LCS and was not detected in the associated samples: therefore, the data have been reported.

Method(s) 8260C: Sample RB-2 (400-132650-6) contains met11ylene chloride. Reanalysis was performed with concurring results.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA Method(s) 8270D: The method blank for preparation batch 400-338284 and analytical batch 400-338574 contained Diethyl phthalate, Bis(2-ethylhexyl) phthalate and Di-n-octyl phthalate above the method detection limit. This target analyte concentration was less than the reporting limit {RL); therefore, re-extraction andfor re-analysis of samples was not performed.

Method(s) 8270D: The %RPD of the laboratory control standard duplicate (LCSD) for preparation batch 400-338284 recovered outside control limits for the following analytes: 2,4-0initrophenol and Pentachlorophenol.

Method(s) 8270D: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-338556 and analytical batch 400-3387 41 were outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.CK-5 (400-132588-6[MS]) and CK-5 (400-132588-6[MSD))

Method(s) 8270D: The method blank for preparation batch 400-340079 and analytical batcll 400-340421 contained Di-n-octyl phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction andfor re-analysis of samples was not performed.

Method(s) 8270D: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 400-340079 recovered outside control limits for the following analytes: 2,4-Dinitrophenol.

Method(s) 8270D: The laboratory control sample duplicate (LCSD) for preparation batch 400-339125 and 400-340079 and analytical batch 400-339188 recovered outside control limits for the flagged ana!ytes. The associated sample(s) was re-prepared andtor re-analyzed outside holding time. Both sets of data have been reported.

Method(s) 8270D: The method blank for preparation batch 400-339125 and analytical batch 400-339188 contained Diethyl phthalate and Di-n-octyJ phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re~analysis of samples was not performed.

Method(s) 82700 LL: Three surrogates are used for thls analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without performing re-extractionfre-analysis. The following sample contained an allowable nun1ber of surrogate compounds outside limits: (MB 400-33828411-A). These results have been reported and qualified.

No additional analytical or quality issues were noted, other than those described above or in the Definitions!Glossary page.

GCVOA No analytical or quality issues were noted, other than those described in the DefinitlonstGlossary page.

Case Narrative

Job Narrative 400-132540-1



211/2017

Client: C-K Associates ProjecUSite: Moffat & Nichol

Job ID: 400-132540-i (Continued)

Laboratory: TestAmerica Pensacola (Continued)

Case Narrative TestAmerica Job ID: 400-132540-1

GC Semi VOA Method(s) 80818: Physical properties (viscosity, color, odor) of the following sample(s) extract preclude concentrated analysis \Vhich would jeopardize instrumentation. Minimal dilution with elevated Rls is reported. CK-1 (400-132588-1), CK-2 (400-132588-2), Duplicate (400-132588-3), CK-3 (400-132588-4) and CK-4 (400-132588-5).

Method{s) MA-EPH: The fractionation surrogates 2-Bromonaphthalene and/or 2-Fluorobiphenyl are outside control limits for the following samples: RINSATE 1 (400-132540-1 ), RB-2 (400-132650-6) and (LCSD 400-33926213-A). These surrogates are used only to indicate separation between the aliphatic and aromatic phases of the fractionation process and do not reflect recoveries from the extractions process. As these surrogates are present in the aromatic samples and not present in the aliphatic, these results have been reported.

No additional ana!yUcal or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals Method(s) 60108, 6010C: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-338528 and analytical batch 400-338847 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.


General Chemistry Method(s) 353.2: The matrix spike I matrix spike duplicate (MSIMSD) recoveries for preparation batch 400-338576 and analytical batch 400·338609 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample {LCS) recovery was within acceptance limits.

Method(s) 353.2: The sample duplicate precision for the following san1ple associated with preparation batch 400-338576 and analytical batch 400-338609 was outside control limits: CK-5 (400-132588-6[MSD]) and (400-132588-L-1-C MSD).

Method(s) 353.2: The following sample showed a negative result greater than the absolute value of the reporting limit for CK-7 (400-132650·2). These samples were re.analyzed with a dilution and were non-detect. The diluted sample is reported as the primary analysis with the undiluted sample being reported as a secondary result.

Method(s) 7196A: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-339244 and analytical batch 400·339470 were outside control limits. sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample {LCS) recovery was within acceptance limits.

Method(s) 90128: The matrix spike duplicate (MSD) recoveries for preparation batch 400-339068 and analytical batch 400-339005 were outside control limits. Non-homogeneity is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.


Organic Prep Method(s} 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-338429.

Method{s) 3520C: Insufficient sample volume \Vas available to perform a matrix spike/matrix spike duplicate/sample duplicate (MSIMSDIDUP) associated with preparation batch 400-339262.

Method(s) 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-339262.

Method(s) 3520C: Insufficient sample volume \vas available to perform a matrix splke/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-338239.

Method(s) 3520C: Insufficient sample volume was available to perfonn a matrix spike/matrix spike duplicate/sample duplicate

Page 4of140 T estAmerica Pensacola

2/112017

Case Narrative Client: C-K Associates ProjecUSite: Moffat & Nichol


Job ID: 400-132540-1 (Continued)

Laboratory: TestAmerica Pensacola (Continued)

(MS/MSD/DUP) associated with preparation batch 400-338284.

Method(s) 3520C: Insufficient sample volume \Vas available to perfonn a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-339054.

Method(s) 3520C: Insufficient sample volume \Vas available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-339125.

Method(s) 3520C: Insufficient sample volume \Vas available to perforn1 a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-340079.

Method(s) 3520C: The following sample was re-prepared outside of preparation holding time due to low LCSD: RB-2 (400-132650-6).


VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Lab Admin No analytical or quality issues were noted, other than those described ln the Definitions/Glossary page.


2/112017


Sample Summary TestAmerica Job ID: 400-132540-1

Lab Sample ID Client Sarnple ID Matrix Collected Received 400-132540-1 RINSATE 1 Water 01/11/1713:20 01112117 09:21

400-132588-1 CK-1 Solid 01/11/1711:10 01/12117 16:57

400-132588-2 CK-2 Solid 01/11117 11:40 01112117 16:57

400-132588-3 Duplicate Solid 01/11/17 12:00 01112117 16:57

400-132588-4 CK-3 Sol!d 01/11/17 12:15 01/12117 16:57 400-132588-5 CK-4 Solid 01/1111712:30 01/1211716:57

400-132588-6 CK-5 Solid 01/11117 13:15 01/1211716:57

400-132650-1 CK-6 Solid 01/13117 09:30 01/14/17 08:32

400-132650-2 CK-7 Solid 01/13117 09:45 01/14117 08:32 400-132650-3 CK-8 So!id 01113117 10:10 01/14117 08:32

400-132650-4 CK-9 Solid 01/13/17 10:25 01114117 08:32

400-132650-5 CK-10 Solid 01/13117 10:45 01114117 08:32

400-132650-6 RB-2 Water 01/1311711:00 01114117 08:32

Page 6 of 140

TestAmerica Pensacola

2/112017

m

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project!Site: Moffat & Nichol

Client Sample ID: RINSATE 1 Lab Sample ID: 400-132540-i Date Collected: 01111/17 13:20 Matrix: Water Date Received: 01112117 09:21

Method: 8260C - Volatile Organic Compounds by GCIMS E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

1, 1, 1,2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01/16/17 09:43 1

1, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43

1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43

1, 1,2-Trich!oroethane <0.00050 0.0050 0.00050 mg/L 01/16/17 09:43

1, 1-Dich!oroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:43

1, 1-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/16117 09:43

1,2,4-Trichlorobenzene <0.00082 0.0010 0.00082 mg IL 01116/17 09:43

1,2-0ibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01116/17 09:43

1,2-Dich!orobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:43

1,2-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/16117 09:43

1,2-Dichloropropane <0.00050 0.0010 0.00050 mg/L 01116/17 09:43

1,3-Dich!orobenzene <0.00054 0.0010 0.00054 mg/L 01116/17 09:43

1,4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01116117 09:43

2-Butanone (MEK) <0.0026 0.025 0.0026 mg/L 01/16/17 09:43

4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg IL 01116117 09:43

Acetone <0.010 0.025 0.010 mg/L 01116117 09:43

Benzene <0.00038 0.0010 0.00038 mgll 01/16/17 09:43

Bromoform <0.00071 0.0050 0.00071 mg/L 01116117 09:43

Bromomethane <0.00098 0.0010 0.00098 mg/L 01116/17 09:43

Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01116117 09:43

Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/16117 09:43

Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01116/17 09:43

Ch!orodibromomethane <0.00050 0.0010 0.00050 n1g/L 01116117 09:43

Chloroethane <0.00076 0.0010 0.00076 mg IL 01116/17 09:43

Chloroform <0.00060 0.0010 0.00060 mg/L 01116/17 09:43

Ch!oromethane <0.00083 0.0010 0.00083 mg IL 01116/17 09:43

cis· 1,2·Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:43

cis-1,3·Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/16/17 09:43

Oich/orobromomethane <0.00050 0.0010 0.00050 mg/L 01116117 09:43

Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/16117 09:43

lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/16/17 09:43

Methyl tert·butyl ether <0.00074 0.0010 0.00074 mg/L 01/16117 09:43

Methylene Chloride <0.0030 0.0050 0.0030 mg/L 01/16117 09:43

Styrene <0.0010 0.0010 0.0010 mg/L 01116/17 09:43

Tetrach!oroethene <0.00058 0.0010 0.00058 mg IL 01116117 09:43

Toluene <0.00070 0.0010 0.00070 mg/L 01116/17 09:43

trans· 1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43

trans· 1,3·Dich!oropropene <0.00050 0.0050 0.00050 mg/L 01116117 09:43

Trichloroethene <0.00050 0.0010 0.00050 mg/L 01116/17 09:43

Trich!orofluoromethane <0.00052 0.0010 0.00052 mg IL 01116/17 09:43

Vinyl chloride <0.00050 0.0010 0.00050 mg IL 01116117 09:43

Xy!enes, Total <0.0016 0.010 0.0016 mg/L 01116117 09:43

Surrogate %Recovery Qualifier Lltnlts Prepared Analyzed DI/ Fae

4-Bromoffuorobenzene 101 78-118 0111611709:43 1

Dibromofluoromethane 103 81 - 121 0111611709:43

Toluene-dB (Surr) 102 80.120 01116117 09:43


Page 7 of 140 2/1/2017

Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol

Client Sample ID: RINSATE 1 Date Collected: 01111/1713:20 Date Received: 01/12/17 09:21

Method: 82700 LL. Semivolatile Organic Compounds by GCIMS ·Low Level Analyte Result Qualifier RL MDL Unit Acenaphthene <0.000030 0.00019 0.000030 mgfl

Acenaphthylene <0,000042 0.00019 0.000042 mg/L

Anthracene <0.000030 0.00019 0.000030 mg/L

Benzo[a]anthracene <0.000043 0.00019 0.000043 mg/L Benzo[a]pyrene <0.000040 0.00019 0.000040 mg/L

Benzo[b}fluoranthene <0.000032 0.00019 0.000032 mg/L

Benzo[k]fluoranthene

Chrysene

Dibenz(a,h)anthracene

Fluoranthene

Fluorene

lndeno[1,2,3-cd]pyrene

2-Methylnaphtha!ene

Naphthalene

Phenanthrene

Pyrene

Surrogate 2·Fluorobiphenyl

Nitrobenzene-d5 Terphenyi-d14

<0.000094 <0.000070 <0.000047

<0.000064 <0.00010

<0.000041

<0.000057 <0.000089 <0.000034

<0.000038

%Recovery Qual/fier

92

84 107

0.00019

0.00019 0.00019

0.00019 0.00019 0.00019

0.00019 0.00019 0.00019 0.00019

Ll1nlts 15-122

19-130

33-138

Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Anillne <-0.,0036 0.0094

1, 1'-Biphenyl <0.00016 0.0094 Bis(2·ch!oroethyl)ether

bis (2-ch!oroisopropyl) ether

Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate

4-Chloroaniline

2-Chloronaphthalene

2-Ch!oropheno!

Dibenzofuran

3,3'-Dichlorobenzidine

2,4-Dichlorophenol

Diethyl phthalate 2,4-Dimethylpheno!

Dimethyl phtha!ate

1,3-Dinitrobenzene

2,4-Dinitrophenot

2.4-Dinitrotoluene

2,6-Dinitrotoluene

Oi-n-octyl phthafate Hexachlorobenzene

Hexachlorobutadiene

Hexach!orocyclopentadiene

Hexachloroethane

lsophorone

2-Nitroaniline

<0.0025

<0.00015

0.0064 J B <0.00018

<0.0032

<0.00013 <0.0021

<0.00016

<0.0025

<0.0028

0.00067 J B <0.0033

<0.00016 <0.00094 <0.0032

<0.0018 <0.0018

0.00019 J B <0.00016

<0.00052

<0.0025 <0.0040

<0.00013 <0.0021

0.0094 0.0094

0.0094 0.0094 0.0094 0.0094

0.0094 0.0094

0.0094 0.0094

0.0094 0.0094 0.0094

0.0094 0.028

0.0094 0.0094

0.0094 0.0094

0.0094 0.019

0.0094

0.0094 0.0094

0.000094 mg/L

0.000070 m9/L 0.000047 m9/L

0.000064 m9/L 0.00010 m9/L

0.000041 mg/L

0.000057 mg/L 0.000089 mg/L 0.000034 mg/L

0.000038 m9/L

MDL Unit 0.0036 mg/L

0.00016 mg/L 0.0025 mg/L

0.00015 mg/L

0.0019 mg/L

0.00018 mg/L 0.0032 mg/L

0.00013 mgiL 0.0021 mg/L

0.00016 mg/L

0.0025 mg/L 0.0028 mg/L

0.00023 mg/L 0.0033 mg/L

0.00016 mg/L

0.00094 mg/L 0.0032 mg/L 0.0018 mg/L

0.0018 mg/L 0.00016 mg/L 0.00016 mg/L

0.00052 mg/L 0.0025 mglL 0.0040 mg/L

0.00013 mg/L 0.0021 mg/L

Page 8 of 140


Lab Sample ID: 400-132540-1 Matrix: Water

D Prepared

01112117 16:23 0111211716:23

Analyzed

01116/17 18:58 01116/17 18:58

0111211716:23 01/16/1718:58

0111211716:23 01/1611718:58 01/1211716:23 01/16/17 18:58 01/1211716:23 0111611718:58

01/12117 16:23 01116117 18:58 01/12117 16:23 0111611718:58 01/12117 16:23 0111611718:58 01112117 16:23 01116/17 18:58

01112117 16:23 01/16117 18:58 0111211716:23 01/16/1718:58

01/12117 16:23 01/16/17 18:58 01/1211716:23 01/16/17 18:58 01/12117 16:23 01/16/1718:58

01/1211716:23 01/1611718:58

Prepared

0111211716:23

0111211716:23

Analyzed

0111611718:58

0111611718:58

0111211716:23 0111611718:58

Oil Fae

1

1

Oil Fae

1

D Prepared Analyzed 01116/17 21:32

01116/17 21:32

Oii Fae

1 01/1211716:23

01/1211716:23 01/1211716:23 01116117 21:32 0111211716:23 01116117 21:32

0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 01/1211716:23 01116/17 21:32 01/12/1716:23 01/16/17 21:32

0111211716:23 01/16/17 21:32 01/1211716:23 01/16/17 21:32

0111211716:23 01116117 21:32 0111211716:23 01/16/17 21:32

01/1211716:23 01116117 21:32 01112117 16:23 01116117 21:32

01/1211716:23 01116117 21:32 0111211716:23 01116117 21:32 01/1211716:23 01116/17 21:32

01/1211716:23 01116/17 21:32 01/1211716:23 01/16/17 21:32

01112117 16:23 01/16/17 21:32 01/1211716:23 01/16/17 21:32

0111211716:23 0111611721:32 0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 0111211716:23 0111611721:32

T estAmerica Pensacola

2/1/2017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol

Client Sample ID: R!NSATE 1 Lab Sample ID: 400-132540-1 Date Collected: 01/11/i? 13:20 Matrix: Water Date Received: 01/12117 09:21

Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

3-Nitroaniline <0.0017 0.0094 0.0017 mg/L 01/1211716:23 01/16/17 21:32 1 4-Nitroani!ine <0.0014 0.0094 0.0014 m9/L 01/12117 16:23 01/16117 21:32

Nitrobenzene <0.00012 0.0094 0.00012 mg/L 01/1211716:23 01/16/17 21:32

4-Nitropheno1 <0.0020 0.0094 0.0020 m9/L 01/12117 16:23 01/16117 21:32 N-Nitrosodi-n-propylamine <0.0031 0.0094 0.0031 mg/L 01/1211716:23 01/16/17 21:32

N-Nitrosodiphenylamine <0.00017 0.0094 0.00017 mg/L 01/1211716:23 01116117 21:32

Pentachloropheno! <0.0013 0.019 0.0013 mg/L 01/12117 16:23 01116/17 21:32

Phenol <0.0025 0.0094 0.0025 mg/L 01 /12117 16:23 01116/17 21:32

1,2,4,5-T etrachlorobenzene <0.00017 0.0094 0.00017 mg/L 01/1211716:23 01/16117 21:32

2,3,4,6-T etrachlorophenol <0.0015 0.0094 0.0015 mg/L 01/12117 16:23 01/1611721:32

1,2,4-Trichlorobenzene <0.00017 0.0094 0.00017 m9/L 01112117 16:23 01/16117 21:32 2,4 ,5-Trichlorophenol <0.0035 0.0094 0.0035 mg IL 01112117 16:23 01116/17 21:32

2,4 ,6-Trichlorophenol <0.0033 0.0094 0.0033 mg/L 01/1211716:23 01/16/17 21:32

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae

2-Ffuorobiplienyl 72 46-124 0111211716:23 01116117 21:32 1 2-Fluorophenol 47 13-113 0111211716:23 01116117 21:32

Nitrobenzene-d5 73 36- 126 0111211716:23 01116117 21:32

Phenol-d5 66 17 -127 0111211716:23 01116117 21:32 Terphenyl-d14 98 44 - 149 01112117 16:23 01116117 21:32

2,4, 6-T ribromophenol 70 26-150 0111211716:23 01116117 21:32

Method: MAVPH. Massachusetts• Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C6-C8 A!iphatics <0.030 0.030 0.030 mg/L 01/19/17 22:24

C8-C 10 AHphatics <0.050 0.050 0,050 mg/L 01/19/17 22:24

C8-C10 Aromatics <0.025 0.025 0.025 m9/L 01/19/17 22:24

Surrogate %Recovery Qualifier Lim/ls Prepared Analyzed DJ/ Fae 8,a,a-Trifluorotoluene (fid) 101 70-130 01119117 22:24 1

a,a,a-Trifluorotoluene (pid) 103 70-130 01119117 22:24 1

Method: 8011 • EDB, DBCP, and 1,2,3-TCP (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 1,2-Dibromo-3-Ch!oropropane <D.0000056 0.000031 0.0000056 mg/L 01/23/1716:25 01127/17 00:09 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae 4-Bron1ofluorobenzene 113. 51-149 0112311716:25 01127117 00:09 1

Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Aldrin <0.0000012 0.000019 0.0000012 mg/L 01/1211716:15 01/19/1713:41 1

alpha-BHC 0.0000042 J B 0.000019 0.0000014 m9/L 01/1211716:15 01/19/1713:41 1 beta-BHC <0.0000012 0.000019 0.0000012 m9/L 0111211716:15 01/19/17 13:41

delta-BHC 0.0000084 JB 0.000019 0.0000008 mg/L 01/1211716:15 01/1911713:41

1 gamma-BHC (Undane) <0.0000096 0.000019 0.0000096 mg/L 01/1211716:15 01119/17 13:41

alpha-Chlordane <0.0000016 0.000019 0.0000016 mg/L 0111211716:15 01119117 13:41

gamin a-Chlordane 0.0000034 J 0.000019 0.0000012 mg/L 01/1211716:15 01119/1713:41 4,4'-DDD <0.0000012 0.000019 0.0000012 m9/L 01/1211716:15 01119/1713:41


Page 9of140 2/1/2017


Client Sample !D: RINSATE 1 lab Sample !D: 400-132540-1 Date Collected: 01111/1713:20 Matrix: Water Date Received: 01112/17 09:21

Method: 8081 B • Organochlorlne Pesticides (GC) (Continued)

Ee

1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fa

4,4'-DDE <0.00000085 0.000019 0.0000008 mg/L 01/12/1716:15 01/19/17 13:41

5 4,4'-DDT <0.0000015 0.000019 0.0000015 mg/L 01/12/1716:15 01/19/1713:41

Dieldrin 0.0000043 JB 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/1713:41

Endosu!fan I <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/17 13:41

Endosulfan H <0.0000028 0.000019 0.0000028 mg/L 01/12/1716:15 01/19/17 13:41

Endosulfan sulfate <0.00000081 0.000019 0.0000008 mg/L 01/12/1716:15 01/19/17 13:41 1

Endrin <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/1713:41

Endrin aldehyde <0.0000011 0.000019 0.0000011 mgll 01/12/1716:15 01/19117 13:41

Endrin ketone <0.0000015 0.000019 0.0000015 mg/L 01112/1716:15 0111911713:41

Heptachlor <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 0111911713:41

Heptach!or epoxide <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01119/17 13:41

Methoxychlor <0.0000016 0.000019 0.0000016 mg/L 01112/1716:15 01/19/17 13:41

Toxaphene <0.00012 0.0012 0.00012 mg/L 01/12/1716:15 0111911713:41

Surrogate %Recovery Qualifier Lin1its Prepared Analyzed Di/ Fae

DCB Decachforobiphenyl 55 10-130 0111211716:15 0111911713:41 1

Tetrachloro·m·xylene 99 43-130 0111211716:15 01119117 13:41

Method: MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C10-C12 A!iphatlcs <0.047 0.047 0.047 mg/L 01120/17 15:54 01126117 17:25 1

C12-C16 Aliphatics <0.047 0.047 0.047 mg/L 0112011715:54 01126117 17:25

(;16-C35 Aliphatics <0.047 0.047 0.047 mg/L 01120/1715:54 01/26117 17:25

C10·C12 Aromatics <0.047 0.047 0.047 mg IL 01/2011715:54 0112611719:59

C12-C16 Aromatics <0.047 0.047 0.047 mg/L 01/2011715:54 0112611719:59

C16-C21 Aromatics <0.047 0.047 0.047 mg/L 0112011715:54 01126117 19:59

C21-C35 Aromatics <0.047 0.047 0.047 mg IL 01/20/17 15:54 0112611719:59

Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae

1-Chlorooctadecane 89 40. 140 01120117 15:54 0112611717:25 1

o-Terphenyl 63 40.140 0112011715:54 01126117 19:59 1

2-Bromonapht/1alene 14 40-140 01120117 15:54 0112611719:59

2-Fluorobiphenyl 46 40.140 0112011715:54 0112611719:59

Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae Silver <0.0020 0.0050 0.0020 mg IL 01113117 08:50 01/16/1717:16 1

Arsenic <0.0040 0.010 0.0040 mg/L 01113/17 08:50 0111611717:16 1

Barium <0.0020 0.010 0.0020 mg/L 01113/17 08:50 01116117 17:16

Beryllium <0.0010 0.0030 0.0010 mg/L 01/13/17 08:50 01116117 17:16

Cobalt <0.0030 0.010 0.0030 mg/L 01113/17 08:50 01116117 17:16

Chromium <0.0020 0.010 0.0020 mg/L 01/13/17 08:50 01116117 17:16

Copper <0.0020 0.020 0.0020 mg/L 01/13/17 08:50 01116117 17:16

Nickel <0.0030 0.0050 0.0030 mg/L 01/13/1708:50 01/16117 17:16

Lead <0.0020 0.010 0.0020 mg/L 01113/17 08:50 01/16117 17:16

Selenium <0.0040 0.020 0.0040 mg/L 01113/17 08:50 01/16/1717:16

Tham um <0.0040 0.010 0.0040 mg/L 01113117 08:50 0111611717:16

Vanadium <0.0030 0.020 0.0030 mg IL 01/13/17 08:50 01/16/1717:16

Zinc <0.0080 0.020 0.0080 mg/L 01113/17 08:50 0111611717:16


Page 10of140 211/2017


Method: 7470A - Mercury {CVAA) Analyfe Result

Mercury <0.000070

General Chemistry Analyte Result

Cyanide, Total <0.0035

Nitrate Nitrite as N <0,018

Chromium, hexavalent <0.0065

Client Sample Results

Qualifier RL MDL Unit

0.00020 0.000070 mg/l


0.0050 0.0035 mg/L

0.050 0.018 mg/L

0.010 0.0065 mg/L

Page 11 of 140


D Prepared Analyzed Di! Fae

01113/17 08:15 01113117 12:58

E D Prepared Analyzed Oil Fae

01117117 09:30 01117117 14:18 1

01/13117 13:30 1

01112/17 10:56


21112017


Client Sample ID: CK-1 Date Collected: 01/11117 11:10 Date Received: 01/1211716:57

Method: 8260C • Volatile Organic Compounds by GCIMS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0092 1, 1, 1 -Trichloroethane 1, 1,2,2-T etrach!oroethane 1, 1,2-Trichloroethane 1, 1-Dlch!oroethane 1.1-Dichloroethene 1,2-Dibronio-3-Chloropropane

1,2-Dich!orobenzene 1,2-Dlchtoroethane 1,2-Dichloropropane

1,3-Dichlorobenzene 1,4-Dich!orobenzene Acetone Benzene Bromoform Bromomethane Carbon disulfide

Carbon tetrachloride

Ch!orobenzene Chtorodibromomethane

Chloroethane Chloroform Chloromethane

cis-1,2-Dich!oroethene cis-1 ,3-Dichloropropene Dichlorobromomethane

Ethylbenzene Methyl tert-butyl elher Methylene Chloride 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK)

Styrene Tetrachloroethene

Toluene trans, 1 ,2-Dich!oroethene

trans· 1, 3·Dlchf oropropene Trich!oroethene

Trichlorofluoromethane

Vinyl chloride Xy!enes, Total 1,2,4-Trichlorobenzene

lsobutyl alcohol

Surrogate 4-Bromoffuorobenzene Dibromoffuoromethane

Toluene-dB (Surr)

<0.0040

<0.0092

<0.0092

<0.0031 <0.0092

<0.012

<0.0026 <0.0030

<0.0092 <0.0035 <0.0092

0.20 <0.0025 <0.0092 <0.0092

<0.0092 <0.0062

<0.0019

<0.0092 <0.0092

<0.0092 <0.0037 <0.0028

<0.0044 <0.0092

<0.0022

<0.0037 <::0.037

0.030 J <0.018

<0.0037

<0.0092 <0.0037

<0.0092 <0.0092 <0.0037

<0.0092

<0.0092 <0.0070 <0.0074 <0.037

%Recovery Qualifier

100

102

94

RL 0.018 0.018 0.018

0.018 0.018 0.018

O.D18

0.018 0.018 0.018

0.018 0.018 0.092

0.018

0.018 0.018

0.018 O.D18

0.018 0.018 0.018

0.018 0.018

0.018 0.018 0.018

0.018 0.018

0.055 0.092 0.092

0.018 0.018

0.018

0.018

0.018 0.018

0.018 0.018

0.037 0.018 0.092

Li1nils

72-122

79-123

80-120

Page 12of140

MOL Unit 0.0092 mg/Kg 0.0040 mg/Kg

0.0092 mg/Kg 0.0092 mg/Kg

0.0031 mg/Kg 0.0092 mg/Kg

0.012 mg/Kg 0.0026 mg/Kg 0.0030 mg/Kg 0.0092 mg/Kg

0.0035 mg/Kg 0.0092 mg/Kg

0.027 mg/Kg

0.0025 mg/Kg

0.0092 mg/Kg 0.0092 mg/Kg

0.0092 mg/Kg


0.0092 mg/Kg 0.0037 mg/Kg 0.0028 mg/Kg

0.0044 mg/Kg 0.0092 mg/Kg 0.0022 mg/Kg


0.0037 mg/Kg 0.0092 mg/Kg 0.0037 mg/Kg

0.0092 mg/Kg

0.0092 mg/Kg 0.0037 mg/Kg

0.0092 mg/Kg

0.0092 mg/Kg 0.0070 mg/Kg 0.0074 mg/Kg

0.037 mg/Kg

TestAmerica Job ID 400-132540-1

Lab Sample ID: 400-132588-1 Matrix: Solid

Percent Solids: 31.8

D Prepared Analyzed " 01/22117 07:44 01/22117 11:25 <) 01/22/17 07:44 01/22/1711:25

" 01/22117 07:44 01/22/1711:25 " 01/22117 07:44 01/22117 11:25

" 01/2211707:44 01/2211711:25 0 01/2211707:44 01/2211711:25

" 01/2211707:44 01/22/1711:25

" 01/22117 07:44 01/22117 11:25 ::> 01/22117 07:44 01/22117 11:25

" 01/22117 07:44 01/22/1711:25

'" 01/22117 07:44 01/22/1711:25 " 01/22117 07:44 01/2211711:25

" 01122117 07:44 01/2211711:25 " 01/22117 07:44 01/2211711:25

" 01/22117 07:44 01/2211711:25

"' 01/22117 07:44 01/2211711:25 ,, 01/2211707:44 01/2211711:25

" 01/22117 07:44 01/22/17 11:25 " 01/22117 07:44 01/22117 11:25 "' 01/22117 07:44 01/2211711:25 ,,, 01/22117 07:44 01/22117 11:25

" 01/22117 07:44 01/2211711:25 '" 01/22117 07:44 01/22117 11:25 " 01/22117 07:44 01/2211711:25

" 01/22117 07:44 01/22/17 11:25 " 01/2211707:44 01/2211711:25

" 01/22117 07:44 01/22117 11:25

"' 01/2211707:44 01/2211711:25 " 01/2211707:44 01/22/1711:25 " 01/2211707:44 01/2211711:25 ::: 01/22117 07:44 01/22117 11:25

" 01/22117 07:44 01/22/17 11:25 " 01/2211707:44 01/2211711:25

" 01/22117 07:44 01/2211711:25 ,, 01/22117 07:44 01/22117 11:25

(< 01/22117 07:44 01/22117 11:25 " 01/22117 07:44 01/22117 11:25 ,, 01/2211707:44 01/2211711:25

1) 01/2211707:44 01/2211711:25

"' 01/2211707:44 01/2211711:25 D 01/2211707:44 01/2211711:25

" 01/2211707:44 01/2211711:25

Prepared Analyzed

01122/1707:44 0112211711:25

0112211707:44 0112211711:25

0112211707:44 0112211711:25

Oil Fae

1

1

1 1

Di/ Fae

1


2/112017


Client Sample ID: CK-1 Date Collected: 01111/1711:10 Date Received: 01/12/17 16:57

Method: 82700 - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene

Acenaphthylene

Aniline Anthracene Benzo[a]anthracene

Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,ijperylene Benzo[k]fluoranthene

1, 1 '-Biphenyl Bis(2-chloroethy!)ether bis (2-ch!oroisopropyl) ether

Bis(2-ethylhexyl) phlhalate

Butyl benzyl phthalate 4-Chloroaniline 2-Ch!oronaphtha!ene

2-Chlorophenol

Chrysene Dibenz(a,h)anthracene

Dibenzofuran 3,3'-Dlchlorobenzidine

2,4-Dich!oropheno1 Diethyl phthalate 2,4-Dimethylphenol

Dimethyl phthalate 1,3-Dinllrobenzene 2,4-Dinitrophenol

2,4-Dinitroto!uene 2,6-Dinltrotoluene Di-n-octyl phthalate

Fluoranthene

Fluorene Hexachlorobenzene

Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane

lndenof1 ,2,3-cdJpyrene

lsophorone 2-Methylnaphthalene Naphthalene 2-Nitroani!ine

3-Nitroaniline 4-Nitroaniline

Nitrobenzene 4-Nitropheno! N-Nitrosodi-n-propy!amine N-Nitrosodiphenylan1ine

Pentach!orophenol

Phenanthrene

<0.10

<0.10

<0.13

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.89

<0.10

<0.10

<0.10

<0.10

<0.10

<0.31

<0.10

<0.20

<0.31

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

<0.34

<0.34

<0.10

<0.20

<0.10

1.0 1.0 1.0

1.0 1.0

1.0 1.0

1.0 1.0 1.0

1.0 1.0 1.0 1.0 1.0

1.0 1.0

1.0 1.0

1.0

1.0

1.0 1.0

1.0 1.0 1.0

3.0 1.0 1.0 1.0

1.0 1.0 1.0

1.0 1.0 1.0 1.0

1.0

1.0 1.0

1.0

1.0 1.0

1.0 1.0 1.0

1.0 2.0 1.0

Page 13of140

MDL Unit

0.10 mg/Kg 0.10 mg/Kg 0.13 mg/Kg

0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg


0.10 mg/Kg 0.10 mg/Kg


0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg

0.89 mg/Kg 0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg 0.31 mg/Kg 0.10 mg/Kg

0.20 mg/Kg 0.31 mg/Kg 0.10 mg/Kg


0.10 mg/Kg 0.10 mg/Kg

0.10 mg/Kg

0.34 mg/Kg 0.34 mg/Kg 0.10 mg/Kg 0.20 mg/Kg 0.10 mg/Kg




D Prepared Analyzed " 01/16/1709:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05

" 01/16/17 09:16 01/18/17 16:05 "' 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 ':' 01/16/17 09:16 01/18/17 16:05 ;) 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 ,, 01/16/17 09:16 01/18/17 16:05 ,,, 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 ,, 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/1716:05 ;:; 01/16/17 09:16 01/18/1716:05

" 01/16117 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/1716:05 ,, 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05

'" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05

" 01116/17 09:16 01/18/1716:05 ,, 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/1716:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05

" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05 l'.l. 01/16/17 09:16 01/18/1716:05

" 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05

" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05

Dllfac E 1

1


2/1/2017


Client Sample ID: CK-1 Date Collected: 0111111l 11 :i O Date Received: 0111211716:57

Method: 82700 • Semivolatile Organic Compounds (GCIMS) (Continued) Analyte Result Qualifier RL MDL Unit Phenol <0.10 1.0 0.10 mg/Kg

Pyrene 1,2,4, 5-T etrachlorobenzene

2,3,4,6-T etrachlorophenol 1,2 ,4-TrlchJorobenzene 2,4,5-Trichlorophenol 2,4,6-Trich!orophenol

Surrogate 2-Fluorobiphenyl 2-F/uorophenol

Nitrobenzene-d5 Phenol-d5 Teiphenyl-d14

2, 4,6-Ttibromophenol

<0.10

<0.10

<0.10

<0.10

<0.10

<0.10

%Recovery Qualifier

92

94

82

89 109

122

1.0 1.0

1.0

1.0

1.0

1.0

Limits 27-127

25-128

15- 136

29-130

24-146

10-150

0.10 mg/Kg

0.10 mg/Kg

0.10 mg/Kg

0.10 mgiKg

0.10 mg/Kg

0.10 n1g/Kg

Method: MAVPH. Massachusetts. Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit C6-C8Atiphatics <17 17 17 mg/Kg C8-C 10 Aliphatics <29 29 29 mg/Kg

C8-C10 Aromatics

Surrogate

a,a,a-Trifluorotoluene (fid) a,a,a-Trifluorototuene (pid)

<14

%Recovery Quallfler

77

80

Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier

Aldrin <O .0095 alpha-BHC <0.0037

beta-BHC

delta-BHC

gamma-BHC (Undane) alpha-Chlordane gamma-Chlordane

4,4'-DDD

4,4'-DDE

4,4'-DDT

Dleldrin Endosulfan I Endosulfan II Endosu!fan sulfate

Endrin Endrin aldehyde

Endrin ketone Heptachlor Heptachlor epoxide Methoxychlor

Toxaphene

<0.0078

<0.0050 <0.0034

<0.0044

<0.0042

<0.0030

<0.0042

<0.012

<0.0056

<0.0033

<0.0036

<0.0033

<0.0030

<0.0045

<0.0054

<0.0037

<0.0070

<0.0051

<0.45

14

Limits 70-130

70-130

RL 0.026

0.026

0.026

0.026

0.026

0.026 0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

0.026

1.6

Page 14 of 140

14 mg/Kg

MDL Unit 0.0095 mg/Kg

0.0037 mg/Kg

0.0078 mg/Kg

0.0050 mg/Kg

0.0034 mg/Kg

0.0044 mg/Kg

0.0042 mg/Kg

0.0030 mg/Kg

0.0042 mg/Kg

0.012 mg/Kg

0.0056 mg/Kg

0.0033 mg/Kg

0.0036 mg/Kg

0.0033 mg/Kg

0.0030 mg/Kg

0.0045 mg/Kg

0.0054 mg/Kg

0.0037 mg/Kg

0.0070 mg/Kg

0.0051 mg/Kg

0.45 mg/Kg




D Prepared

" 01116117 09:16 ,, 01116117 09:16

Analyzed 01118117 16:05

01118/17 16:05

" 01116117 09:16 01118117 16:05

" 01116117 09:16 01118117 16:05 !) 01116117 09:16 01118117 16:05

" 01116117 09:16 0111811716:05

" 01116117 09:16 01118117 16:05

Prepared Analyzed

01118117 09:16 01/18/1716:05

0111811709:16 0111811716:05

0111811709:16 0111811716:05

01118117 09:16 01118117 16:05 01118117 09:16 01/18117 16:05

0111811709:16 0111811716:05

D Prepared Analyzed

" 0111611711:00 0111611718:19

" 0111611711:00 01116117 18:19

" 0111611711:00 0111611718:19

Prepared Analyzed

0111811711:00 01118117 18:19

01116117 11:00 01118117 18:19

O Prepared Analyzed ~ 01116117 09:24 0111711718:11

" 01116117 09:24 01117117 18:11

l) 01116117 09:24 01117/17 18:11

l) 01116117 09:24 01117117 18:11

" 01116117 09:24 0111711718:11

" 01116117 09:24 01117117 18:11

1:1 01116117 09:24 01117117 18:11

" 01116117 09:24 01117117 18:11

" 0111611709:24 0111711718:11

" 01116117 09:24 0111711718:11

" 01116117 09:24 0111711718:11

l) 01116117 09:24 0111711718:11

" 01116117 09:24 0111711718:11

"' 01116117 09:24 01117117 18:11

l'.I 0111611709:24 0111711718:11

" 01116117 09:24 01117117 18:11

" 01116117 09:24 0111711718:11

,, 01116117 09:24 0111711718:11

" 01116117 09:24 01117117 18:11

" 0111611709:24 0111711718:11

" 01116117 09:24 0111711718:11

DltFac E 1

DJ/ Fae 1

1

DU Fae 50

50

50

DI/ Fae

50 50

Oil Fae 5 5 5 5 5

5

5 5 5 5 5 5 5 5 5 5 5 5 5

5 5


21112017


Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date Collected: 0111111712:30 Matrix: Solid Date. Received: 0111211716:57 Percent Solids: 20.9

Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae

Phenol <0.16 1.6 0.16 mg/Kg 0:1 01116117 09:16 01117117 14:21 1

Pyrene 0.16 J 1.6 0.16 mg/Kg " 01/16117 09:16 01/17117 14:21 1

1,2,4,5-T etrachtorobenzene <0.16 1.6 0.16 mg/Kg " 01/16117 09:16 01/17/17 14:21

2,3,4,6-T etrachlorophenol <0.16 1.6 0.16 mg/Kg " 01116/17 09:16 01117/17 14:21

1,2,4-Trichtorobenzene <0.16 1.6 0.16 mg/Kg ;) 01/16/17 09:16 01/17/17 14:21

2,4,5-Trichlorophenol <0.16 1.6 0.16 mg/Kg f; 01/16/17 09:16 01/17117 14:21

2,4 ,6-Trichlorophenol <0.16 1.6 0.16 mg/Kg " 01/16/17 09:16 01/17117 14:21

Surrogate %Recovery Qualifier Lin1its Prepared Analyzed Di/ Fae

2-Ffuorobiphenyl 52 27 -127 01116117 og:16 0111711714:21 1

2-Fluorophenol 71 25-128 01116117 og:16 01117117 14.·21 1

Nitrobenzene-d5 56 15-136 0111611709:16 01117117 14:21 1

Pheno!-d5 73 29-130 01116117 og:16 01117117 14:21 1

Terphenyl-d14 56 24-146 01116117 og:16 01117117 14:21

2,4, 6· Tribromopflenof 75 10-150 01116117 og:16 01117117 14:21

Method: MAVPH ·Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C6HC8 AHphatics <26 26 26 mg/Kg " 01/16/1711:00 01/16/17 22:17 50

C8-C10 Aliphatics <43 43 43 mg/Kg " 0111611711:00 01/16/17 22:17 50

C8·C10 Aromatics <21 21 21 mg/Kg l) 01/1611711:00 01/16/17 22:17 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae

a,a,a-Trifluorotoluene (fid) 75 70-130 0111611711:00 01116117 22:17 50

a,a,a· Trifluorotoluene (pid) 75 70-130 0111611711:00 01116117 22:17 50

Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Aldrin <0.014 0.040 0.014 mg/Kg " 01/16117 09:24 01/17117 20:12 5

alpha-BHC <0.0056 0.040 0.0056 mg/Kg n 01/16/17 09:24 01/17117 20:12 5

beta-BHC <0.012 0.040 0.012 mg/Kg ;) 01/16117 09:24 01/17/17 20:12 5

delta-BHC <0.0075 0.040 0.0075 mg/Kg l) 01/16117 09:24 01/17/17 20:12 5

gammaHBHC (Undane} <0.0051 0.040 0.0051 mg/Kg " 01116117 09:24 01/17117 20:12 5

alpha-Chlordane <0.0065 0.040 0.0065 mg/Kg " 01/16/17 09:24 01117117 20:12 5

gamma-Chlordane <0.0063 0.040 0.0063 mg/Kg >:i 01116/17 09:24 01117117 20:12 5

4,4'-DDD <0.0044 0.040 0.0044 mg/Kg l) 01116/17 09:24 01/17117 20:12 5

4,4'-DDE <0.0063 O.D40 0.0063 mg/Kg " 01/16/17 09:24 01/17117 20:12 5 4,4'-DDT <0.018 0.040 0.018 mg/Kg -l) 01/16/17 09:24 01/17/17 20:12 5

Dieldrin <0.0084 0.040 0.0084 mg/Kg l~ 01116/17 09:24 01117/17 20:12 5

Endosulfan t <0.0049 0.040 0.0049 mg/Kg " 01/16117 09:24 01/17/17 20:12 5

Endosulfan H <0.0054 0.040 0.0054 mg/Kg ,, 01/16/17 09:24 01/17117 20:12 5

Endosu!fan sulfate <0.0049 0.040 0.0049 mg/Kg -l'.l 01/16117 09:24 01/17/17 20:12 5

Endrln <0.0044 0.040 0.0044 mg/Kg » 01116117 09:24 01/17117 20:12 5

Endrln aldehyde <0.0068 0.040 0.0068 mg/Kg l) 01116117 09:24 01117117 20:12 5

Endrin ketone <0.0082 0.040 0.0082 mg/Kg ~ 01/16117 09:24 01117117 20'.12 5

Heptachlor <0.0056 0.040 0.0056 mg/Kg 1.'I 01/16/17 09:24 01/17117 20:12 5

Heptachlor epoxide <0.011 0.040 0.011 mg/Kg l) 01116/17 09:24 01/17117 20:12 5

Methoxychlor <0.0077 0.040 0.0077 mg/Kg l) 01116/17 09:24 01117117 20:12 5

Toxaphene <0.68 2.3 0.68 mg/Kg " 01116/17 09:24 01/17/17 20:12 5


Page 30 of 140 21112017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol

Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date Collected: 01/11/1712:30 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 20.9

Surrogate %Recovery Qualifier Lfrnlts Prepared Analyzed DI/ Fae E DCB Decachlorobipheny/ 41 26- 129 01116117 09:24 01117117 20:12 5 Tetrachforo-m-xylene 41 31-122 01116117 09:24 01117117 20:12 5

Method; MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MOL Unit 0 Prepared Analyzed Oil Fae c10-c12 Aliphatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 18:59 1

C10-C12 Aromatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 23:11 C12-C16 Aliphatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 18:59

C12-C16 Aromatics <7.5 7.5 7.5 mg/Kg ;;i 01/19/17 07:20 01/24/17 23:11

C16-C35 Aliphatics 34 7.5 7.5 mg/Kg "' 01/19/17 07:20 01/24/17 18:59

C21-C35 Aromatics <7.5 7.5 7.5 mg/Kg ':' 01/19/17 07:20 01/24/17 23:11

C16-C21 Aromatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 23:11

Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae 1-Clllorooctadecane 80 40-140 0111g117 07:20 0112411718:59 1

o-Terphenyl 84 40-140 0111g117 07:20 01124117 23:11 1

Method; 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae

Silver <0.93 2.3 0.93 mg/Kg ,, 01/15/1711:30 01/16/1716:08 1

Arsenic 12 4.7 1-9 mg/Kg ,, 01/15/1711:30 01/16/17 16:08 1

Barium 150 4.7 0.93 mg/Kg ,, 01115/1711:30 01/16/17 16:08

Beryllium 0.85 J 1-4 0-47 n1g/Kg l) 01/15/1711:30 01/16/17 16:08

Cobalt 9.9 4.7 1.4 mg/Kg " 01/15/1711:30 01116/17 16:08

Chromium 24 4.7 0.93 mg/Kg " 01/15/1711:30 01/16117 16:08

Copper 98 9.3 0.93 mg/Kg " 01/15/17 11:30 01/16/1716:08

Nickel 28 2.3 1-4 mg/Kg " 01/15/1711:30 01/16/1716:08

Lead 75 4-7 0.93 mg/Kg l) 01/15/1711:30 01/16/17 16:08

Selenium 2-1 J 9.3 1.9 mg/Kg ,, 01115/1711:30 01/16/17 16:08

Thallium <1.9 4.7 1.9 mg/Kg " 01/15/17 11 :30 01/16/17 16:08

Vanadium 29 9.3 1-4 mg/Kg " 01/15/1711:30 01/16/17 16:08

Zinc 250 9.3 3.7 mg/Kg " 0111511711:30 01/16/1716:08

Method: 7471A - Mercury (CVAA) Analyte Result Qualifier RL MOL Unit D Prepared Analyzed Oil Fae

Mercury 0.047 0.013 0.0077 mg/Kg 01/15/17 12:43 01/16/17 09:56 1

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Chromium, hexavalent <12 18 12 mg/Kg -r.1 01120/1717:00 01/23/17 12:07 1

Cyanide, Total <D.62 1.2 0.62 mg/Kg " 01/18/1710:53 01/18/17 17:37 1

Percent Moisture 79.1 0.1 0.1 % 01/16/1712:37

General Chemistry. Soluble Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae Nitrate Nitrite as N <1.7 4.8 1.7 n1g/Kg " 01116/17 12:21 1


Page 31 of 140 21112017


Client Sample ID: CK-5 Date Collected: 0111111713:15 Date Received: 01112/1716:57

Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane

1, 1, 1-Trichforoethane

1, 1,2,2-Tetrachloroethane

1, 1.2-Trichloroethane

1, 1-Dichloroethane

1, 1-Dichloroethene

1,2-Dibromo-3-Chforopropane

1,2-Dich!orobenzene

1,2-Dichloroethane

1.2-Dichloropropane

1,3-Dichlorobenzene 1,4-Dichlorobenzene

Acetone

Benzene Bromoform

Bromomethane

Carbon disulfide


Chlorobenzene Ch!orodibromomethane

Chloroethane

Chloroforn1 Chloromethane

cis-1,2-Dichloroelhene

cis-1,3-Dich!oropropene

Dichlorobromomethane

Ethy!benzene

Methyl tert-buty! ether

Methylene Chloride

2-Butanone (MEK)

4-Methyl-2·pentanone (MIBK)

Styrene

Tetrachloroethene

Toluene trans-1,2-Dichloroethene

trans-1,3-Dlch!oropropene

Trich!oroethene

Trichlorofluoromethane

Vinyl chloride

Xylenes. Total 1,2,4-Trichlorobenzene

tsobutyl alcohol

Surrogate

4-Bromof/uorobenzene Dibromoffuoromet/Jane

Toluene-dB (Surr)

<0.21

<0.093

<0.21

<0.21

<0.070

<0.21 <0.28

<0.060

<0.069

<0.21

<0.080 <0.21

<0.61

<0.056

<0.21

<0.21

<0.21

<0.14

<0.044 <0.21

<0.21

<0.21 <0.084

<0.064

<0.10

<0.21

<0,051

<0.084

<0.84 <0.50

<0.42

<0.084

<0.21

0.62 <0.21

<,0.21

<0.084

<0.21

<0.21

<0.16

<0.17

<0.84

%Recovery Quallfler

98

95

104

RL 0.42 0.42

0.42

0.42

0.42

0.42

0.42

0.42 0.42

0.42

0.42

0.42

2.1

0.42

0.42 0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

1.3 2.1

2.1

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.42

0.84

0.42

2.1

Lllnlts

72-122

79-123

80-120

Page 32 of 140

MDL Unit 0.21 mg/Kg

0.093 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.070 mg/Kg

0.21 mg/Kg

0.28 mg/Kg

0.060 mg/Kg

0.069 mg/Kg

0.21 mg/Kg

0.080 mg/Kg 0.21 mg/Kg

0.61 mg/Kg

0.056 mg/Kg

0.21 mg/Kg 0.21 mg/Kg

0.21 mg/Kg

0.14 mg/Kg

0.044 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.084 mg/Kg

0.064 mg/Kg

0.10 mg/Kg

0.21 mg/Kg

0.051 mg/Kg

0.084 mg/Kg

0.84 mg/Kg

0.50 mg/Kg

0.42 mg/Kg

0.084 mg/Kg 0.21 mg/Kg

0.084 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.084 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.16 mg/Kg 0.17 mg/Kg

0.84 mg/Kg




D Prepared

" 01119117 08:59

" 01119117 08:59

Analyzed 01119/17 12:21

01119117 12:21

" 01119117 08:59 01119117 12:21 0 01119117 08:59 01119/17 12:21

:) 01119/17 08:59 01119117 12:21 <) 01119/1708:59 0111911712:21

,, 01119/17 08:59 01119/1712:21

" 01119/17 08:59 01119/17 12:21 " 01/19/17 08:59 01/19117 12:21

0 01119/17 08:59 01119/17 12:21

" 01119/17 08:59 01119/1712:21 ,,, 01/19/17 08:59 01/19/17 12:21

" 01/19/17 08:59 01/19/1712:21

" 01119/17 08:59 01119/17 12:21

" 01/19/17 08:59 01/19/17 12:21

" 01/19/17 08:59 01/19/17 12:21

" 01/19/17 08:59 01/19/17 12:21

" 01119/17 08:59 01/19/17 12:21

" 01119/17 08:59 01119/17 12:21 " 01119117 08:59 01/1911712:21

" 01/19/17 08:59 01119117 12:21

<) 01/19/17 08:59 01/19/1712:21

" 01119117 08:59 01/19117 12:21

" 01/19/17 08:59 01/19/17 12:21 ,, 01/19/17 08:59 01/19/17 12:21

" 01/19/17 08:59 01/19/17 12:21

:) 01/19/17 08:59 01/19/1712:21

" 01119/17 08:59 01/19/17 12:21 J) 01119/17 08:59 01/1911712:21

" 01/19/17 08:59 01/19/1712:21

" 01119/17 08:59 01119117 12:21

" 01119/17 08:59 0111911712:21

" 01119/17 08:59 01119117 12:21

·O 01/19/17 08:59 01/19117 12:21

" 01/19/17 08:59 01/19/1712:21

" 01/19/17 08:59 01/19117 12:21

Q 01/19/17 08:59 01/19/17 12:21 ,,, 01/19/17 08:59 01/19/17 12:21

{: 01/19/17 08:59 01/19/17 12:21

" 01119117 08:59 01/19117 12:21

" 01/19/17 08:59 01/1911712:21

" 01119117 08:59 01119/17 12:21

Prepared

01119117 08:59

01119117 08:59

Analyzed

01119117 12:21

0111911712:21

01119117 08:59 0111911712:21

DU Fae 50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50 50

50

50

50

50

50

50 50

50

50 50

50

50

50 50

50

50

50

50

50

Dlf Fae

50

50

50


2/1/2017


Client Sample ID: CK-5 Date Collected: 01/11/1713:15 Date Received: 01/12/1716:57

Method: 82700 • Semivolatife Organic Compounds (GC/MSJ Analyte Result Qualifier RL

Acenaphthene <0.066 0.66

AcenaphthyJene

Aniline Anthracene

Benzo[a]anthracene

Benzo{a]pyrene

Benzo[b ]fluoranthene Benzo[g,h,iJpery!ene Benzo[k]fluoranthene

1, 1 '-Biphenyl Bis(2-ch!oroethy!)ether bis (2-ch!oroisopropyf) ether Bis(2-ethylhexyl) phthalate

Butyl benzyl phthalate

4-Ch!oroaniline 2-Chloronaphlhalene

2-Chlorophenol

Chrysene Dibenz{a,h)anthracene

Dibenzofuran 3,3'-0ich!orobenzidine

2,4-Dichlorophenor Diethyl phthalate 2,4-Dimethylpheno!

Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dinitropheno!

2,4-Din!trotoluene 2,6-Dinitroto!uene Di-n-octyl phthalate

Fluoranthene

Fluorene Hexach!orobenzene

Hexachlorobutadiene Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cdJpyrene

lsophorone

2-Methylnaphlhalene Naphthalene

2-Nitroaniline 3-Nitroanmne 4-Nitroaniline

Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine

Pentachlorophenol Phenanthrene

<0,066

<0.086

<0.066

0.084 J 0.11 J 0.26 J

<0.066 <0.066

<0.066

<0.066

<0.066 <0.066

<0.066 <0.066

<0.066

<0.066

0.13 J <0.066

<0.066

<0.066

<0.066 <0.066 <0.066

<0.066

<0.066

<0.58 F2 F1 <0.066 <0.066

<0.066

0.27 J <0.066 <0.20

<0.066 <0.13 F1

<020 <0.066 <0.066

<0.066 <0.066

<0.066

<0.066

<0.066 <0.066

<0.22

<0.22 <0.066

<0.13

<0.066

0.66

0.66 0.66 0.66 0.66

0.66

0.66 0.66

0.66 0.66 0.66

0.66 0.66 0.66 0.66

0.66

0.66 0.66

0.66 0.66

0.66 0.66

0.66

0.66 0.66

2.0

0.66 0.66 0.66

0.66 0.66 0.66

0.66

0.66 0.66

0.66 0.66

0.66 0.66

0.66 0.66 0.66 0.66

0.66

0.66 0.66

1.3 0.66

Page 33 of 140

MDL Unit 0.066 mg/Kg 0.066 mg/Kg 0.086 mg/Kg

0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg


0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg


0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg

0.066 mg/Kg 0.20 mg/Kg

0.066 mg/Kg

0.13 mg/Kg 0.20 mg/Kg

0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg

0.066 mg/Kg

0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg

0.22 mg/Kg

0.22 mg/Kg 0.066 mg/Kg

0.13 mg/Kg 0.066 mg/Kg




D Prepared Analyzed Oii Fae E c 01/16/17 09:16 01/17/17 14:54

" 01/16/17 09:16 01/17/17 14:54 ,, 01/16/17 09:16 01/17/1714:54

!) 01/16/17 09:16 01/1711714:54 ,, 01/16/1709:16 01/17/1714:54

... 01/16/1709:16 01/17/17 14:54

0 01/16/17 09:16 01/17/17 14:54 ::: 01/16/17 09:16 01/17/1714:54 •:: 01/16/17 09:16 01/17/1714:54 :;; 01/16/17 09:16 01/17/17 14:54

b 01/16/17 09:16 01/1711714:54 ,,, 01/16/1709:16 01/17/1714:54

,, 01/16/17 09:16 01/1711714:54

;) 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/17 14:54 0 01/16/17 09:16 01/17/17 14:54

'" 01/16/17 09:16 01/17117 14:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54 ,, 01/16/17 09:16 01/17/1714:54

,, 01/16/1709:16 01/17/1714:54

" 01/16/17 09:16 01/17/17 14:54 " 01/16/17 09:16 01/17/17 14:54

" 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54

" 01/16/17 09:16 01/17/1714:54 :;' 01/16/17 09:16 01/17/1714:54

'" 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54

'" 01/16/17 09:16 01/17/1714:54 ,, 01/16/17 09:16 01/1711714:54

" 01/16/17 09:16 01/1711714:54 <) 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54

" 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54

" 01/16117 09:16 01/17/1714:54 " 01/16/17 09:16 01117/1714:54 " 01/16/17 09:16 01/1711714:54

" 01116/17 09:16 01/1711714:54 " 01116/17 09:16 01/17/1714:54

'" 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54

" 01/16/17 09:16 01/1711714:54 p 01/16/17 09:16 01/17/1714:54

1

1


2/1/2017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1

Project/Site: Moffat & Nichol

Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 0111111713:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8

Method: 8270D - Semivolalile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Phenol <0.066 0.66 0.066 mg!Kg >,\ 01116117 09:16 01117117 14:54 1

Pyrene 0.23 J 0.66 0.066 mg/Kg "' 01116/17 09:16 01117117 14:54

1,2,4 ,5-T etrachlorobenzene <0.066 0.66 0.066 mg/Kg i) 01116117 09:16 01117117 14:54

2,3 ,4, 6-T etrachlorophenol <0.066 0.66 0.066 mg/Kg " 01116/17 09:16 01117/17 14:54

1,2,4-Trichlorobenzene <0,066 0,66 0.066 mg/Kg (> 01116/17 09:16 01117117 14:54

2,4,5-Trich!orophenol <0.066 0,66 0.066 mg/Kg {l 01116/17 09:16 01117117 14:54 1

2,4,6-Trlchforopheno! <0.066 0.66 0.066 mg/Kg 0 01116/17 09:16 01117117 14:54 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed DiJ Fae 2-Fluorobip/Jenyl 58 27-127 011161170g_16 0111711714:54 1

2-Fluorophenol 72 25-128 01116117 09:16 01117117 14:54 1

Nitrobenzene-d5 57 15-136 01116117 og:16 01117117 14:54 1

Phenol-d5 74 29-130 011161170g:16 0111711714:54

Terpheny/-d14 65 24-146 01116117 og:16 0111711714:54

2,4,6c Tribromopbenol 82 10-150 011161170g:16 01117117 14:54

Method: MAVPH - Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C6-C8 Aliphatics <7.3 7.3 7.3 mg/Kg ,, 0111611711:00 01117/1710:52 50

C8-C 10 A!lphatics <12 12 12 mgiKg ,, 0111611711:00 01117117 10:52 50

C8-C10 Aromatics <6.1 6.1 6.1 mg/Kg " 0111611711:00 01117117 10:52 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae a,a,a-Trifluorotoluene (fid) 79 70-130 0111611711:00 01117117 10:52 50

a,a,a· Trifluorotoluene (pid) 81 70-130 0111611711:00 0111711710:52 50

Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dilfac

Aldrin <0.0024 0.0068 0.0024 mg/Kg " 01116117 09:24 01117117 21:10 2 alpha·BHC <0.00096 0.0068 0.00096 mg/Kg " 01116117 09:24 01117117 21:10 2 bela-BHC <0.0020 0.0068 0.0020 mg/Kg " 01116117 09:24 01117117 21:10 2

della-BHC <0.0013 0.0068 0.0013 mg/Kg '" 01116117 09:24 01117117 21:10 2

gamma-BHC (Undane) <0.00088 0.0068 0.00088 mg/Kg n 01116/17 09:24 01117117 21:10 2

alpha-Chlordane 0.0014 J 0.0068 0.0011 mg/Kg 0 01116117 09:24 01117117 21:10 2

gamma-Chlordane 0.0025 J 0.0068 0.0011 mg/Kg '" 01116/17 09:24 01117117 21:10 2

4,4'-DDD <0.00076 0.0068 0.00076 mg/Kg " 01116117 09:24 01117117 21:10 2 4,4'-DDE <0.0011 0.0068 0.0011 mg/Kg " 01116117 09:24 01117117 21:10 2

4.4'-DDT <0.0031 0.0068 0.0031 mg/Kg ;) 01116117 09:24 01117117 21:10 2

Dieldrin <0.0014 0.0068 0.0014 mg/Kg i:I 01116117 09:24 01117117 21:10 2

Endosulfan I <0.00084 0.0068 0.00084 mg/Kg n 01116/17 09:24 01117117 21:10 2

Endosu!fan II <0.00092 0.0068 0.00092 mg/Kg " 01116/17 09:24 01117117 21:10 2

Endosutfan sulfate <0.00084 0.00!38 0.00084 mg/Kg ;) 01116/17 09:24 01117117 21:10 2

Endrin <0.00076 0.0068 0.00076 mg/Kg ,, 01116/17 09:24 01117117 21:10 2

Endrin aldehyde <0.0012 0.0068 0.0012 mg/Kg ~l 01116117 09:24 01117117 21:10 2

Endrin ketone <0.0014 0.0068 0.0014 mg/Kg 0 01116117 09:24 01117/17 21:10 2

Heptachlor <0.00096 0.0068 0.00096 mg/Kg ,, 01116117 09:24 01117/17 21:10 2

Heplachlor epoxide <0.0018 0.0068 0.0018 mg/Kg " 01116117 09:24 01117117 21:10 2

Methoxychlor <0.0013 0.0068 0.0013 mg/Kg n 01116117 09:24 01117117 21:10 2

Toxaphene <0.12 0.40 0.12 mg/Kg " 01116117 09:24 01117117 21:10 2


Page 34 of 140 2/112017


Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01111117 13:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8

Surrogate %Recovery Quallfler Lltnfts Prepared Analyzed DJ/ Fae El DCB Decachlorobiphenyl 62 26-129 01116117 09:24 01117117 21:10 2

Tetrach/oro-m-xylene 62 31- 122 01116117 09:24 01117117 21:10 2

Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C1O-C12 A!iphatics <3.3 3.3 3.3 mg/Kg ., 01119/17 07:20 01124117 18:02 1

C10-C12 Aromatics <3.3 3.3 3.3 mg/Kg " 01119117 07:20 01124117 22:14

C12-C16 Aliphatics <3.3 3.3 3.3 mg/Kg ::1 01/19117 07:20 01124/1718:02

C12-C16 Aromatics <3.3 3.3 3.3 mg/Kg z:: 01/19/17 07:20 01124117 22:14

C16-C35 Aliphatics 11 3.3 3.3 mg/Kg ::1 01119117 07:20 01/24/17 18:02

C21 ·C35 Arornatics 3.5 3.3 3.3 mg/Kg n 01119117 07:20 01124117 22:14

C16-C21 Aromatics <3.3 3.3 3.3 rng/Kg 0 01119117 07:20 01/24117 22:14

Surrogate %Recovery Qualifier Limits Prepared Analyzed D/I Fae 1-Chlorooctadecane 83 40-140 01119117 07:20 0112411718:02 1

o-Terphenyl 70 40-140 01119117 07:20 01124117 22:14

Method: 6010C - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Silver <0.37 0.93 0.37 mg/Kg D 01/1511711:30 0111611716:11 1

Arsenic 12 1.9 0.74 mg/Kg :) 01/1511711:30 01116117 16:11

Barium 120 1.9 0.37 mg/Kg ,, 0111511711:30 0111611716:11

Beryllium 0.33 J 0.56 0.19 mg/Kg '" 0111511711:30 01116/1716:11

Cobalt 4.8 1.9 0.56 mg/Kg 0 0111511711:30 0111611716:11

Chromium 26 1.9 0.37 mg/Kg (.) 01115/1711:30 01/1611716:11

Copper 44 3.7 0.37 mg/Kg ,,

0111511711:30 0111611716:11

Nickel 12 0.93 0.56 mg/Kg '" 0111511711:30 01116117 16:11

Lead 64 1.9 0.37 mg/Kg 1:i 0111511711:30 01116117 16:11

Selenium 1.3 J 3.7 0.74 mg/Kg "' 01/15/1711:30 01/16117 16:11

Thallium <0.74 1.9 0.74 mg/Kg " 0111511711:30 01/1611716:11 1

Vanadium 14 3.7 0.56 mg/Kg q 01/1511711:30 0111611716:11

Zinc 150 3.7 1.5 mg/Kg " 01/1511711:30 0111611716:11

Method: 7471A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Merc_ury 0.052 0.012 0.0074 mg/Kg 01115117 12:43 01116117 09:57 1

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae

Chromium, hexavalent <5.8 F1 8.3 5.8 mg/Kg ~\ 01120/1717:00 01123/17 12:03 1

Cyanide, Total <0.27 F1 0.51 0.27 mg/Kg o;:- 01/1811710:53 01/18117 17:30

Percent Moisture 51.2 0.1 0.1 % 0111611712:37

General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Nitrate Nitrite as N <0.74 F1 F2 2.1 0.74 mg/Kg " 01/1611712:22 1

Tes!America Pensacola

Page 35 of 140 2/112017

Client Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol

Client Sample ID: CK-6 Date Collected: 01/13/17 09:30 Date Received: 01/14/17 08:32

Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0065 1, 1, 1-Trichloroethane <0.0029

1,1,2,2-Tetrach!oroethane

1, 1,2-Trichforoethane

1, 1-Dich!oroethane 1, 1-0ich!oroethene

1,2-Dibromo-3-Ch loropropane

1,2-Dlchlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene 1,4-Dich!orobenzene

Acetone Benzene

Bromofonn Bromomethane

Carbon disulfide Carbon tetrachloride

Chlorobenzene

Chlorodibromomethane

Chloroethane

Chforofom1 Chloromethane

cis-1,2-Dichloroethene

cis-1,3-Dichloropropene Dichlorobromomethane

Ethylbenzene

Methyl tert-butyl ether

Methylene Chloride

2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK)

Styrene Tetrach!oroethene

Toluene trans..:1,2-Dich!oroethene

trans· 1,3·Dichloropropene

Trichloroethene

Trichlorofluoron1ethane

Vinyl chloride

Xy!enes, Total 1,2,4-Trichf orobenzene

lsobutyl alcohol

Surrogate

4-Bromonuorobenzene

Dibromoffuoromethane

Toluene-dB (Surr)

<0.0065 <0.0065

<0.0022 <0.0065

<0.0086

<0.0018

<0.0021 <0.0065

<0.0025 <0.0065

0.30 <0.0017

<0.0065

<0.0065

0.023 <0.0044

<0.0014

<0.0065

<0.0065 <0.0065 <0.0026 <0.0020

<0.0031 <0.0065

<0.0016

<0.0026

<0.026

0.022 J <0.013

<0.0026 <0.0065

0.0037 J <0.0065 <0.0065

<0.0026 <0.0065

<0.0065 <0.0049 <0.0052

<0.026

%Recovery Qualifier

104

96

111

RL 0.013 0.013

0.013 0.013

0.013 0.013 0.013

0.013 0.013 0.013

0.013 0.013 0.065 0.013

0.013 0.013

0.013

0.013 0.013 0.013

0.013

0.013 0.013

0.013 0.013 0.013

0.013 0.013

0.039 0.065

0.065

0.013 0.013

0.013 0.013

0.013 0.013 0.013

0.013 0.026 0.013 0.065

Lim/rs

72-122

79-123

80.120

Page 36of140

MOL Unit 0.0065 mg/Kg 0.0029 mg/Kg

0.0065 mg/Kg 0.0065 mg/Kg

0.0022 mg/Kg 0.0065 mg/Kg

0.0066 mg/Kg 0.0016 mg/Kg 0.0021 mg/Kg



0.0044 mg/Kg 0.0014 mg/Kg 0.0065 mg/Kg

0.0065 mg/Kg

0.0065 mg/Kg 0.0026 mg/Kg

0.0020 mg/Kg

0.0031 mg/Kg 0.0065 mg/Kg

0.0016 mg/Kg


0.0026 mg/Kg 0.0065 mg/Kg

0.0026 mg/Kg


0.0065 mg/Kg

0.0049 mg/Kg 0.0052 mg/Kg

0.026 mg/Kg


Lab Sample ID: 400-132650-i Matrix: Solid


O Prepared

" 01119/17 06:59 Q 01/19/17 06:59

Analyzed 01/19/17 15:35 01/19/1715:35

" 01119111 o8·.59 0111911115:35 " 01/19/17 08:59 01/19/17 15:35 ;) 01/19/1708:59 01/1911715:35 ;) 01/19/17 08:59 01119117 15:35

" 01/19/1708:59 01/19/1715:35

" 01/19/17 08:59 01/19/17 15:35 {l 01/19117 08:59 01/19/1715:35

;) 01/19/17 08:59 01/19/1715:35 l) 01/19/17 08:59 0111911715:35 ;;, 01119/17 08:59 01/19/17 15:35

" 01119/17 06:59 01/19117 15:35 " 01/19/17 08:59 01/19/17 15:35

" 01119117 08:59 01/19/17 15:35 " 01/19/17 08:59 01/19/17 15:35

" 01119117 08:59 01/19/17 15:35

" 01/19/17 08:59 01/19/1715:35 " 01119/1708:59 01/19/1715:35 ;) 01119/1706:59 01/1911715:35

0 01/19/17 06:59 01/19/17 15:35

I) 01119117 08:59 01/1911715:35 ·(.\ 01/19/17 08:59 01/19/1715:35

;) 01/19117 08:59 01/19/1715:35

" 01/19117 08:59 01/19/1715:35 ,, 01/19/17 08:59 01/19117 15:35

" 01119/17 08:59 01/19/17 15:35 ,, 01119/1708:59 0111911715:35

Q 01119/1706:59 01/1911715:35 " 01119/17 08:59 01119/17 15:35 ,,, 01119/17 08:59 01/19117 15:35

,,, 01/19/17 06:59 01/19117 15:35 " 01/19117 08:59 01/19/17 15:35

i) 01/19117 08:59 01119117 15:35 ,, 01119/17 08:59 01/19/1715:35

" 01119/17 08:59 01/19/17 15:35 " 01/19/17 08:59 01/19117 15:35 1) 01/19/1708:59 01/19/1715:35 ;) 01/19/1706:59 01/1911715:35

" 01/19117 08:59 01/19/17 15:35 ,, 01/19117 06:59 01/19/1715:35

" 01/19117 08:59 01/19/1715:35

Prepared Analyzed

0111911708:59 0111911715:35

01119117 08:59 0111911715:35

01119117 08:59 0111911715:35

Oil Fae 1

1

1

DI/ Fae

1


2/1/2017

Client Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol

Client Sample ID: CK-6 Date Collected: 01113/17 09:30 Date Received: 01114/17 08:32

Method: 82700 - Semivotatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene

Aniline Anthracene

Benzo[a]anthracene

Benzofa]pyrene Be nzo{b ]flu o ra nthe ne Be nzo[g ,h, i] pery le ne Benzo[k]fluoranthe_ne 1, 1'-Biphenyl

Bis(2-ch!oroethyl)ether bis (2-ch!oroisopropyl) ether

Bis(2-<1thylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanmne 2-Chloronaphlhalene

2-Chlorophenol


Oibenzofuran 3,3'-Dichlorobenzidine

2,4-Dich!orophenol Diethyl phthalate

2,4-Dimethylpheno!

Dimethyl phtha!ate 1,3-Dinitrobenzene

2,4-Dinitrophenol 2,4-Dinitrototuene 2,6-Dinitrotoluene

Oi-n-octyl phthalate

Fluoranthene Fluorene

Hexachforobenzene

Hexachlorobuladiene

Hexach!orocycJopeotadiene Hexachforoethane

lndeno[1,2,3-cd]pyrene lsophorone 2-Methylnaphlha!ene Naphthalene 2-Nitroaniline

3-NitroanU!ne 4-Nitroanillne

Nitrobenzene

4-Nitrophenol N-Nitrosodi-n-pfqpylamine N-Nitrosodiphenylamine

Pentachforophenol

Phenanthrene

<0.063

<0.063

<0.082

<0.063 <0.063

0.28 J 0.38 J 0.16 J 0.15 J

<0.063

<0.063

<0.063

0.15 J 0.071 J

<0.063

<0.063

<0.063

0.25 J <0.063

<0.063

<0.063

<0.063 <0.063

<0.063

<0.063

<0.063 <0.55

<0.063

<0.063

<0.063

0.44 J <0.063

<0.19

<0.063

<0.13

<0.19

0.15 J <0.063

<0,063

<0.063

<0.063

<0.063

<0.063 <0.063

<0.21

<0.21

<0.063

<0.13

0.18 J

0.63

0.63

0.63

0.63 0.63

0.63 0.63

0.63 0.63

0.63 0.63

0.63

0.63

0.63 0.63

0.63

0.63

0.63 0.63

0.63

0.63

0.63 0.63

0.63

0.63

0.63

1.9

0.63

0.63

0.63

0.63

0.63 0.63

0.63

0.63 0.63

0.63

0.63 0.63

0.63 0.63

0.63 0.63

0.63 0.63

0.63 0.63

1.3 0.63

Page 37 of 140


0.063 mg/Kg

0.082 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.55 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.19 mg/Kg

0.063 mg/Kg

0.13 mg/Kg

0.19 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg

0.21 mg/Kg

0.21 mg/Kg

0.063 mg/Kg

0.13 mg/Kg

0.063 mg/Kg

T estAmerica Job ID 400-132540-1



D Prepared

" 01/18/17 09:33 " 01/18117 09:33

Analyzed

01119117 00:09

01119117 00:09

" 01/16/17 09:33 01119117 00:09

" 01/18/17 09:33 01119117 00:09 " 0111811709:33 01119117 00:09 ,, 01118/1709:33 01/19117 22:14

"' 01118/17 09:33 01119117 22:14

:) 01/18/17 09:33 01119/17 22:14 n 01118117 09:33 01/19/17 22:14

l) 01/16117 09:33 01119/17 00:09

" 01/18/17 09:33 01119117 00:09 :) 01/18117 09:33 01119117 00:09 {> 01/18117 09:33 01119117 00:09

,, 0111811709:33 01119117 00:09

" 01118/1709:33 01119117 00:09

" 01118117 09:33 01119117 00:09 ,, 01/18/17 09:33 01/19/17 00:09

,, 01/18117 09:33 01/19/17 00:09

" 01118/17 09:33 01/19117 22:14 :) 01/18117 09:33 01/19/17 00:09 ,, 01118117 09:33 01119117 00:09

" 01118/17 09:33 01119117 00:09 D 01118/17 09:33 01119117 00:09

" 01/18117 09:33 01/19117 00:09

"' 01/18/17 09:33 01/19117 00:09

" 01/18117 09:33 01119117 00:09 " 01118117 09:33 01/19117 00:09

" 01/18117 09:33 01119/17 00:09

" 01/18117 09:33 01119117 00:09

" 01/18/17 09:33 01119117 00:09

" 01118117 09:33 01119117 00:09

"' 01118117 09:33 01/19117 00:09 p 01118/17 09:33 01/19117 00:09

" 01118/1709:33 01/19117 00:09 i) 01/18117 09:33 01/19/17 00:09 " 01/18/17 09:33 01119117 00:09 p 01/18/17 09:33 01119117 22:14

0 01118/17 09:33 01119/17 00:09

'" 01/18117 09:33 01119117 00:09 0 01118/17 09:33 01119117 00:09

" 01118/17 09:33 01119117 00:09 " 01118/17 09:33 01/19117 00:09

" 01118/17 09:33 01/19/17 00:09 "' 01/18/17 09:33 01119/17 00:09 ,, 01/18/17 09:33 01119/17 00:09

" 01118117 09:33 01/19/17 00:09 " 01118/17 09:33 01119117 00:09

" 01118/17 09:33 01119117 00:09 n 01118/17 09:33 01119117 00:09

Dilfac E 1

1

1


211/2017


Client Sample ID: CK-6 Lab Sample ID: 400·-132650-1 Date Collected: 01113117 09:30 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 51.9

Method: 82700 • Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Di! Fae

Phenol <0.063 0.63 0.063 mg/Kg " 01 /18/17 09:33 01/19/17 00:09 1

Pyrene 0,58 J 0.63 0.063 mg/Kg "' 01/18/17 09:33 01/19/17 00:09

1,2,4,5-T etrach!orobenzene <0.063 0.63 0.063 mg/Kg "' 01/18/17 09:33 01/19/17 00:09

_2,3, 4, 6-T etrachf orophenol <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/17 00:09

1,2,4-Trichlorobenz:ene <0.063 0.63 0.063 mg/Kg r; 01/18/1709:33 01/19/17 00:09

2,4 ,5· Trichlorophenot <0.063 0.63 0.063 mg/Kg ,, 01/18/17 09:33 01/19/17 00:09

2,4 ,6-Trichlorophenol <0.063 0.63 0.063 mg/Kg '" 01/18/17 09:33 01/19/17 00:09

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae

2-Fluorobiphenyl 51 27. 127 01118117 09:33 01119117 00:09 1

2-Fluorophenol 57 25.128 01118117 09:33 01119117 00:09 1

Nitrobenzene-d5 45 15.136 01118117 09:33 01119117 00:09

P/1enof-d5 57 29-130 01118117 09:33 01119117 00:09 1

Terpheny!-<114 75 24-146 01118117 09:33 01119117 00:09

2,4,6-Tribromophenof 61 10-150 01118117 09:33 01119117 00:09

Method: MAVPH • Mas.sachusetts ·Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Di! Fae C6-C8 A!iphatics <12 12 12 mg/Kg " 01/16/17 11:30 01/17/17 00:17 50

C8-C10 Aliphatics <20 20 20 mg/Kg -t,; 01/16/1711:30 01117117 00:17 50

C8-C10 Aromatics <10 10 10 mg/Kg " 01/16/1711:30 01/17117 00:17 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI! Fae

a,a,a-Trifluorotoluene (fid) 79 70.130 0111611711:30 01117117 00:17 50

a,s,a-Trif/uorotoluene (pid) 78 70-130 01116117 11:30 01117117 00:17 50

Method: 80816 • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Aldrin <0.0023 0.0064 0.0023 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

alpha-BHC <0.00090 0.0064 0.00090 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

beta-BHC <0.0019 0.0064 0.0019 mg/Kg ') 01/18/1712:42 01/19/17 21:49 2

delta-BHC <0.0012 0.0064 0.0012 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

gamma-BHC {Lindane) <0.00083 0.0064 0.00083 mg/Kg !) 01/18/1712:42 01/19/17 21:49 2

alpha-Chlordane 0.0028 J 0.0064 0.0011 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

gamma-Chlordane 0.0080 0.0064 0.0010 mg/Kg J::I 01/18/1712:42 01/19/17 21:49 2

4,4'-DDD 0.0020 J 0.0064 0.00071 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2

4,4'-DDE 0.0019 J 0.0064 0.0010 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2

4.4'-DDT <0.0029 0.0064 0.0029 mg/Kg ,, 01/18/1712:42 01/19/17 21:49 2

Dieldrin 0.0038 J 0.0064 0.0014 mg/Kg i) 01/18/1712:42 01/19/17 21:49 2

Endosulfan I <0.00079 0.0064 0.00079 mg/Kg " 01/18/1712:42 01/19/1721:49 2

Endosulfan II <0.00086 0.0064 0.00086 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2

Endosulfan sulfate <0.00079 0.0064 0.00079 mg/Kg ,, 01/18/1712:42 01/19/17 21:49 2

Endrin <0.00071 0.0064 0.00071 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2

Endrin aldehyde <0.0011 0.0064 0.0011 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

Endrin ketone <0.0013 0.0064 0.0013 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

Heptachlor <0.00090 0.0064 0.00090 mg/Kg ,, 01/18/17 12:42 01/19/17 21:49 2

Heptachlor epoxide <0.0017 0.0064 0.0017 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2

Methoxychlor <0.0012 0.0064 0.0012 mg/Kg " 01/18/1712:42 01/19/17 21:49 2

Toxaphene <0.11 0.38 0.11 mg/Kg ,, 01/18/17 12:42 01/19/17 21:49 2


Page 38 of 140 2/1/2017


Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01113117 09:30 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9

Surrogate %Recovery Qua/If/er Limits Prepared Analyzed DJ/ Fae E DCB Decachlorobiphenyl 45 26- 129 01118117 12:42 01119117 21:49 2

Tetrachloro-m-xylene 41 31-122 0111811712:42 01119117 21:49 2

Method: MA·EPH ·Massachusetts. Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DH Fae C10-C12 A!iphatics <3.0 3.0 3.0 mg/Kg '" 01/19/17 07:20 01/24/17 19:57 1

C10-C12 Aromatics <3.0 3.0 3.0 mg/Kg '" 01/19/17 07:20 01/25/17 00:08

C12-C16 A!iphatics <3.0 3.0 3.0 mg/Kg ,, 01/19/17 07:20 01/24117 19:57

C12-C16 Aromatics <3.0 3.0 3.0 mg/Kg Q 01/19/17 07:20 01/25/17 00:08

C16-C35 Aliphatics 45 3.0 3.0 mg/Kg " 01/19/17 07:20 01/24/17 19:57

C21~C35_Aromatics 21 3.0 3.0 mg/Kg '" 01/19/17 07:20 01125/17 00:08

C16~C21 Aromatics 5.2 3.0 3.0 n1g/Kg 1:1 01/19/17 07:20 01/25/17 00:08


1-Chlorooctadecane 98 40-140 01119117 07:20 0112411719:57 1

o-Terphenyl 98 40-140 01119117 07:20 01125117 00:08

Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae

Silver <0.35 0.88 0.35 mg/Kg l) 01116/17 08:55 01/17/1713:01 1

Arsenic 7.1 1.8 0.71 mg/Kg " 01/16/17 08:55 01/17/17 13:01

Barium 87 F1 1.8 0.35 mg/Kg l) 01/16/17 08:55 01/17/1713:01

Beryllium 0.37 J 0.53 0.18 mg/Kg l) 01/16/17 08:55 01/17/17 13:01

Cobalt 4.1 1.8 0.53 mg/Kg l) 01/16/17 08:55 01/17/17 13:01

Chromium 11 1.8 0.35 mg/Kg " 01/16/17 08:55 01/17/17 13:01

Copper 37 3.5 0.35 mg/Kg " 01/16117 08:55 01/17/17 13:01

Nickel 12 0.88 0.53 mg/Kg " 01/16/17 08:55 01/17/1713:01

Lead 42 1.8 0.35 mg/Kg ,, 01/16/17 08:55 01/17/17 13:01

Seleniun1 0.87 J 3.5 0.71 mg/Kg " 01/16/17 08:55 01117/17 13:01

Thallium <0.71 1.8 0.71 mg/Kg " 01/16/17 08:55 01/17/17 13:01

Vanadium 11 3.5 0.53 m9IK9 " 01/16/17 08:55 01/17/1713:01

Zinc 130 3.5 1.4 mg/Kg " 01/16/17 08:55 01/17/17 13:01

Method: 7471A. Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae

Mercury 0.066 0.013 0.0078 mg/Kg 01/15/17 12:43 01/16/17 12:14

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Chro1nlun1, hexavalent <4.4 6.3 4.4 n1g/Kg " 01/20/17 17:00 01/23/17 12:07 1

Cyanide, Total <0.24 0.46 0.24 mg/Kg ;" 01/1811710:53 01/18/17 17:37

Percent Moisture 48.1 0.1 0.1 % 01/17/17 14:08

General Chemistry ·Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Nitrate Nitrite as N <0.69 1.9 0.69 mg/Kg ,, 01/16/17 12:26 1


Page 39 of 140 2/1/2017


Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 23.3

Method: 8260C. Volatile Organic Compounds by GCIMS E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 1, 1, 1,2-Tetrach!oroethane <0.010 0.021 0.010 mg/Kg " 01/19/17 08:59 01/19/1715:58 1 1. 1, 1-Trichloroethane <0.0046 0.021 0.0046 mg/Kg 0 01/19/17 08:59 01/19/1715:58

1, 1 ,2 ,2-Tetrachloroethane <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58

1, 1,2-Trichforoethane <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58

1, 1-Dich!oroethane <0.0035 0.021 0.0035 mg/Kg 0 01/19/17 08:59 01/19/17 15:58

1, 1-Dich!oroethene <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58

1,2-Dibromo-3-Chloropropane <0.014 0.021 0.014 mg/Kg ,, 01/19/17 08:59 01/19/17 15:58

1.2-Dichlorobenzene <0.0030 0.021 0.0030 mg/Kg (.J: 01/19/17 08:59 01/19/17 15:58

1,2-Dich!oroethane <0.0034 0.021 0.0034 mg/Kg o:i 01/19/17 08:59 01/19/17 15:58

1,2-Dichloropropane <0.010 0.021 0.010 mg/Kg ;:; 01/19/17 08:59 01/19/1715:58

1,3-Dichlorobenzene <0.0040 0.021 0.0040 mg/Kg " 01119/17 08:59 01/19/1715:58

1,4-Dich!orobenzene <0.010 0.021 O.D10 mg/Kg 1;1 01/19/17 08:59 01/19/17 15:58

Acetone 0.16 0.10 0,031 mg/Kg 0 01/19/17 08:59 01/19/1715:58

Benzene 0.0031 J 0.021 0.0028 mg/Kg " 01 /19/17 08:59 01/19/1715:58

Bromoform <0.010 0.021 0.010 mg/Kg n 01/19/17 08:59 01/19/17 15:58

Bromomethane <0.010 0.021 0.010 mg/Kg -[,< 01 /19117 08:59 01/19/17 15:58

Carbon disulfide 0.011 J 0.021 0.010 mg/Kg p 01/19/17 08:59 01/19/17 15:58

Carbon tetrachloride <0.0071 0.021 0.0071 mg/Kg l:i' 01/19/17 08:59 01/19/1715:58

Chlorobenzene <0.0022 0.021 0.0022 mg/Kg " 01119/17 08:59 01/19/1715:58

Ch!orodibromomethane <0.010 0.021 0.010 mg/Kg 0. 01/19/17 08:59 01/19/17 15:58

Chloroethane <0.010 0.021 0.010 mg/Kg p 01119/17 08:59 01/19/17 15:58

Chloroform <0.010 0.021 omo mg/Kg l'.\ 01/19/17 08:59 01/19/1715:58

Ch!oromethane <0.0042 0.021 0.0042 mg/Kg ·r,! 01/19/17 08:59 01/19/17 15:58

cis-1,2-Dichloroethene <0.0032 0.021 0.0032 mg/Kg '" 01/19117 08:59 01/19/17 15:58

cis-1,3-Dichloropropene <0,0050 0.021 0.0050 mg/Kg " 01 /19/17 08:59 01/19/17 15:58

Dichlorobromomethane <0.010 0.021 0.010 mg/Kg ,,, 01 /19117 08:59 01/19/17 15:58

Ethylbenzene <0.0026 0.021 0.0026 mg/Kg ~ 01119/17 08:59 01/19/17 15:58

Methyl tert-butyl ether <0.0042 0.021 0.0042 mg/Kg -i:i 01119117 08:59 01/19/17 15:58

Methylene Chloride <0,042 0.063 0.042 mg/Kg ,, 01/19/17 08:59 01/19/1715:58

2-Butanone (MEK) <0.025 0.10 0.025 mg/Kg 1.1 01/19/17 08:59 01/19/1715:58

4-Methyl-2-pentanone (MIBK} <0.021 0.10 0.021 mg/Kg ·J:i 01/19/17 08:59 01/19/1715:58

Styrene <0.0042 0.021 0.0042 mg/Kg {l; 01/19/17 08:59 01/19/17 15:58 T etrachloroethene <0.010 0.021 0.010 mg/Kg p 01/19/17 08:59 01/19117 15:58

Toluene 0,0050 J 0.021 0.0042 mg/Kg ·f.< 01/19/17 08:59 01119/1715:58

trans-1,2-Dichloroethene <0.010 0.021 0.010 mg/Kg i,! 01/19117 08:59 01/19/17 15:58

trans-1,3-Dlch!oropropene <0.010 0.021 omo mg/Kg " 01/19/17 08:59 01/19/17 15:58

Trichloroethene <0.0042 0.021 0.0042 mg/Kg " 01/19/17 08:59 01/19/17 15:58

Trich!orofluoromethane <0,010 0.021 0.010 mg/Kg l) 01/19117 08:59 01/19/17 15:58

Vinyl chloride <0.010 0.021 0.010 mg/Kg '" 01/19/17 08:59 01/19/17 15:58

Xylenes, Total <0,0080 0.042 0.0080 mg/Kg " 01119117 08:59 01/19/1715:58

1,2,4-Trichlorobenzene <0.0084 0.021 0.0084 mg/Kg .;;i: 01/19/17 08:59 01/19/1715:58

lsobuty1 alcohol <0.042 0.10 0.042 mg/Kg ·l;! 01/19/17 08:59 01/19/1715:58


4-Bromof/uorobenzene 112 72-122 01119117 08:59 0111911715:58 1

Dibromofluorometl1ane 97 7g_123 01119117 08:59 01119117 15:58 1

Toluene-dB (Surr) 108 BO- 120 01119117 08:59 0111911715:58


Page 40 of 140 2/1/2017


Client Sample ID: CK-7 Date Collected: 01/13/17 09:45 Date Received: 01/14/17 08:32

Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene


Benzo[a]pyrene Benzo[b }flu o ra nthene Benzo[g,h,i]perylene Benzo[k]fluoranthene

1, 1 '-Biphenyl 81s(2-chloroethyl}ether

bis (2-chloroisopropyl) ether

Bis(2-ethylhexyl) phthalate Butyl benzyl phtha!ate

4-Chloroaniline

2-Ch!oronaphthalene

2-Chloropheno!

Chrysene Oibenz{a,h)anthracene

Oibenzofuran

3,3'-Dichlorobenzidine

2,4-Dlchlorophenol

Diethyl phthalate

2,4-Dimethylpheno!

Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dfnitropheno! 2,4-Dlnitroto!uene

2,6-0inltrotoluene Di·n-octyl phthalate

Fluoranthene Fluorene Hexachlorobenzene

Hexach!orobutadiene

HexachJorocyclopentadiene Hexachloroethane

Jndeno[1,2,3-cdJpyrene

lsophorone 2-Methylnaphthalene Naphthalene

2-Nitroaniline

3-Nitroanifine 4-Nltroaniline Nitrobenzene

4-Nitrophenol N-Nitrosodi-n-propy!amine N-Nitrosodiphenylamine

Pentach1orophenol

Phenanthrene

<0.14

<0.14

<0.18

<0.14

<0.14

0.21 J 0.27 J

<0.14

<0.14

<0.14

<0.14

<0.14

0.53 J <0.14 <0.14

<0.14

<0.14

<0.14

<D.14

<0.14

<0.14

<0.14

<0.14

<0.14

<0.14

<0.14

<1.2

<D.14

<0.14

<0.14

0.34 J <0.14 <D.42

<0.14

<0.28

<0.42

<0.14

<0.14

<0.14

<0.14

<0.14

<0.14 <0.14

<0.14

<D.46

<0.46

<0.14

<0.28

0.23 J

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4 1.4

1.4

1.4 1.4

1.4

1.4 1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4 1.4

1.4

1.4

1.4

4.1

1.4

1.4

1.4

1.4

1.4 1.4

1.4

1.4

1.4 1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4

2.8

1.4

Page 41of140

MDL Unit 0.14 mg/Kg

0.14 mg/Kg

0.18 mg/Kg

0.14 mg/Kg 0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg 0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg 0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

1.2 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg 0.42 mg/Kg

0.14 mg/Kg

0.28 mg/Kg 0.42 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.14 mg/Kg

0.46 mg/Kg

0.46 mg/Kg 0.14 mg/Kg

0.28 mg/Kg

0.14 mg/Kg




D Prepared Analyzed " 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 00:41

0 01/18/17 09:33 01/19/17 00:41

n 01/18/17 09:33 01/19/17 00:41

"' 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 22:44

l) 01/18/17 09:33 01/19/17 22:44

" 01/18/17 09:33 01/19/17 22:44 r:r 01/18/17 09:33 01/19/17 22:44

"' 01/18/17 09:33 01/19/17 00:41 n 01/18/1709:33 01/19/1700:41

.o 01/18/17 09:33 01/19/17 00:41

,, 01/18/17 09:33 01/19/17 00:41

:.\ 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

"' 01/18/17 09:33 01/19/17 00:41

,, 01/18/17 09:33 01/19/17 00:41

l) 01/18/17 09:33 01/19/17 00:41 01/18/17 09:33 01/19/17 22:44

,, 01/18/17 09:33 01/19/17 00:41

... 01/18/17 09:33 01/19/17 00:41

p 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

() 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01119/1700:41

" 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

,, 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

1:, 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 22:44

"' 01/18/17 09:33 01/19/17 00:41 " 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

"' 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/1700:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

" 01/18/17 09:33 01/19/17 00:41

p 01/18/17 09:33 01/19/17 00:41

DllFac E 1


2/1/2017

Client Sample Results Client: C-K Associates Tes!America Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol

Client Sample ID: Cl<-7 Lab Sample ID: 400-132650-2 Date Collected: 01113/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3

Method: 8270D • Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Phenol <0.14 1.4 0.14 mg/Kg r:i 01/18/17 09:33 01/19/17 00:41 1

Pyrene 0.39 J 1.4 0.14 mg/Kg 0::< 01/18/17 09:33 01/19/17 00:41

1,2, 4, 5-T etrachlorobenzene <0.14 1.4 0.14 mg/Kg " 01/18/17 09:33 01/19/17 00:41

2,3,4,6-T etrachlorophenol <0.14 1.4 0.14 mg/Kg t; 01/18/17 09:33 01/19/17 00:41

1,2,4-Trichlorobenzene <0.14 1.4 0.14 mg/Kg {! 01/18/17 09:33 01/19/17 00:41 1

2,4 ,5· Trichlorophenol <D.14 1.4 0.14 mg/Kg " 01/18/17 09:33 01/19/17 00:41

2,4,6-Trichloropheno! <0.14 1.4 0.14 mg/Kg 0 01/18/17 09:33 01/19/17 00:41

Surrogate %Recovery Qualifier Limits Prepared Analyzed DH Fae

2-Fluorobiphenyl 56 27 -127 01118117 09:33 01119117 00:41 1

2-F/uorophenof 64 25-128 0111811709:33 01119117 00:41 1

Nitrobenzene-d5 54 15-136 01118117 09:33 01119117 00:41 1

Phenol-d5 67 29-130 01118117 09:33 01119117 00:41 1

Terphenyl·d14 82 24-146 01118117 09:33 01119117 00:41

2,4,6-Tribromophenol 76 10-150 01118117 09:33 01119117 00:41

Method: MAVPH ·Massachusetts· Vol_atile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DU Fae

C6-C8 Aliphatics <25 25 25 mg/Kg '" 01/16/1711:30 01/17/17 01:16 50

C8-C10 Afiphatics <42 42 42 mg/Kg -):! 0111611711:30 01/17/17 01:16 50

C8-C10 Aromatics <21 21 21 mg/Kg " 01116/1711:30 01/17117 01:16 50



a,e,a-Trifluorotoluene (pid) 74 70-130 0111611711:30 01117117 01:16 50

Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DU Fae

Aldrtn <0.0026 0.0072 0.0026 mg/Kg " 01/23117 08:05 01/2611715:18 1

alpha-BHC <0.0010 0.0072 0.0010 mg/Kg n 01123117 08:05 01/26117 15:18

beta-BHC <0.0021 0.0072 0.0021 mg/Kg -;) 01 /23/17 08:05 01/26/17 15:18

della-BHC <0.0014 0.0072 0.0014 mg/Kg " 01/23/17 08:05 01/26/1715:18

gamma-BHC (Lindane) <0.00094 0.0072 0.00094 mg/Kg " 01/23/17 08:05 01/26/1715:18

alpha-Chlordane 0.0062 J 0.0072 0.0012 mg/Kg " 01/23/17 08:05 01126117 15:18

gamma-Chlordane 0.010 0.0072 0.0011 mg/Kg :::i 01/23/17 08:05 01/26/17 15:18

4,4'-000 0.0045 J 0.0072 0.00081 mg/Kg " 01/23/17 08:05 01/26/1715:18

4,4'-DDE 0.0060 J 0.0072 0.0011 mg/Kg " 01/23/17 08:05 01/26/17 15:18

4.4'-DDT <0.0033 0.0072 0.0033 mg/Kg .r,1 01/23117 08:05 01/26/1715:18

Dieldrin 0.011 0.0072 0.0015 mg/Kg '·~ 01 /23/17 08:05 01/26/17 15:18

Endosulfan l <0.00089 0.0072 0.00089 mg/Kg " 01/23/17 08:05 01/26/1715:18

Endosu!fan II <0.00098 0.0072 0.00098 mg/Kg " 01/23/17 08:05 01/26/1715:18 1

Endosulfan sulfate <0.00089 0.0072 0.00089 mg/Kg r,, 01 /23117 08:05 01/26/17 15:18 1

Endrin <0.00081 0.0072 0.00081 mg/Kg " 01/23/17 08:05 01/26/1715:18

Endrln aldehyde <0.0012 0.0072 0.0012 mg/Kg " 01/23/17 08:05 01/26/17 15:18

Endrin ketone <0.0015 0.0072 0.0015 mg/Kg " 01/23/17 08:05 01/26/1715:18

Heptachlor <0.0010 0.0072 0.0010 mg/Kg ;;1 01/23/17 08:05 01/26/17 15:18

~eplachlor epoxide <0.0019 0.0072 0.0019 mg/Kg " 01/23/17 08:05 01126117 15:18

MethoxYchlor <0.0014 0.0072 0.0014 mg/Kg p 01/23/17 08:05 01/26/17 15:18

Toxaphene <0.12 0.43 0.12 mg/Kg " 01/23/17 08:05 01/26/17 15:18


Page 42 of 140 2/1/2017

Client Sample Results Client C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3

Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae E DCB Decachlorobipf)enyl 44 26-129 01123117 08:05 01/26117 15:18 1

Tetrachloro-m-xylene 49 31-122 01123117 08:05 01126117 15:18

Method: MA-EPH -Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL .Unit D Prepared Analyzed Oil Fae

C10-C12 Aliphatics <6.9 6.9 6.9 mg/Kg f) 01/19/17 07:20 01/24/17 20:07 1

C10-C12 Aromatics <6.9 6.9 6.9 mg/Kg {) 01/19/17 07:20 01/25/17 00:18 1

C12-C16 Aliphatics <6.9 6.9 6.9 mg/Kg t:l 01/19/17 07:20 01/24/17 20:07

C12-C16 Aromatics <6.9 6.9 6.9 mg/Kg {.l 01/19/17 07:20 01/25/17 00:18

C16-C35 Aliphatics 75 6.9 6.9 mg/Kg n 01/19/17 07:20 01/24/17 20:07

C21.C35 Aro1natics 12 6.9 6.9 mg/Kg {l 01/19/17 07:20 01/25/17 00:18

C16-C21 Aromatics <6.9 6.9 6.9 mg/Kg ;) 01/19/17 07:20 01/25/17 00:18

Surrogate %Recove:ry Qualifier Lirnlts Prepared Analyzed DH Fae 1-Chlorooctadecane 86 40-140 01119117 07:20 01124117 20:07 1

crTerphenyl 81 40-140 01119117 07:20 01125117 00:18 1

Method; 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Silver <0.80 2.0 0.80 mg/Kg n 01/16/17 08:55 01/17/17 13:16

Arsenic 9.4 4.0 1.6 mg/Kg '" 01/16/17 08:55 01/17/1713:16

Bariun1 310 4.0 0.80 mg/Kg 1) 01/16/17 08:55 01/17/17 13:16

Beryllium 0.71 J 1.2 0.40 mg/Kg i:1 01/16/17 08:55 01/17/17 13:16

Cobalt 9,9 4.0 1.2 mg/Kg \) 01/16/17 08:55 01/17/17 13:16

Chromium 22 4_.o 0.80 mg/Kg " 01/16/17 08:55 01/17/17 13:16

Copper 68 8.0 0.80 mg/Kg " 01/16/17 08:55 01/17/1713:16

Nickel 24 2.0 1.2 mg/Kg l) 01/16/17 08:55 01/17/1713:16

Lead 90 4.0 0.80 mg/Kg ::t 01/16/17 08:55 01/17/17 13:16

Selenium 2.3 J 8.0 1.6 mg/Kg " 01/16/17 08:55 01/17/1713:16

Thallium <1.6 4.0 1.6 mg/Kg " 01/16/17 08:55 01/17/1713:16

Vanadium 27 8.0 1.2 mg/Kg " 01/16/17 08:55 01117/17 13:16

Zinc 200 8.0 3.2 mg/Kg J) 01/16/17 08:55 01/17/17 13:16

Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Mercury 0.043 0.013 0.0078 mg/Kg 01/15/1712:43 01/16/17 12:16 1

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Chromium, hexavalent <11 15 11 mg/Kg <> 01/20/1717:00 01/23/17 12:07 1

Cyanide, Total <0.56 1.1 0.56 mg/Kg .;:; 01/18/1710:53 01/18/17 17:37 1

Percent Moisture 76.7 0.1 0.1 % 01/17/17 14:08

General Chemistry • Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae

Nitrate Nitrite as N <1.5 4.3 1.5 mg/Kg n 01/16/1712:27 1

Nitrate Nitrite as N <7.7 21 7.7 mg/Kg \;!' 01/16/17 12:32 5


Page 43 of 140 2/112017


Client Sample ID: CK-8 Date Collected: 01/1311710:10 Date Received: 01/14117 08:32

Method: 8260C ·Volatile Organic Compounds by GC/MS Analyte Result Qualifier

1, 1, 1,2-Tetrach!oroethane <0.0052

1, 1, 1-Trlchloroethane 1,1,2,2-Tetrachloroethane

1, 1,2-Trichloroethane

1, 1-Dich!oroethane 1, 1-Dichloroethene 1,2-Dibromo-3-Chloropropane

1,2·Dichlorobenzene 1,2-Dich!oroethane

1,2-Dichloropropane

1,3-Dichlorobenzene 1,4-Dich!orobenzene

Acetone Benzene Brornoform Bromomethane

Carbon disulfide


Ch!orobenzene

Chlorodibromomethane

Chloroethane

Chloroform Chlorornethane cis-1,2-Dichloroethene

cis-1,3-Dichloropropene

Dlchlorobromomethane

Ethylbenzene


Methylene Chloride 2-Butanone (MEK)

4-Methyl-2-pentanone (MIBK)

Styrene T etrachtoroethene

Toluene

trans-1,2-Dich!oroethene

trans-1,3-Dichloropropene

Trich!oroethene Trichtorofluoromethane

Vinyl chloride

Xylenes, Total 1,2 ,4-Trichlorobenzene

lsobutyl alcohol

Surrogate

4-Bromofluorobenzene Dibromof/uorometl1ane

Toluene-dB (Surr)

<0.0023

<0.0052 <0.0052

<0.0017 <0.0052

<0.0068

<0.0015

<0.0017

<0.0052

<0.0020

<0.0052

0.064 <0.0014

<0.0052 <0.0052

<0.0052 <0.0035

<0.0011

<0.0052

<0.0052 <0.0052 <0.0021

<0.0016

<0.0025

<0.0052 <0.0013

<0.0021 <0.021

<0.012

<0.010

<0.0021

<0.0052

<0.0021 <0.0052

<0.0052 <0.0021

<0.0052

<0.0052 <0.0039

<0.0041 <0.021

%Recovery Qualifier

101

102

95

RL 0.010 0.010

0.010 0.010

0.010 0.010

0.010 0.010 0.010

0.010 0.010 0.010

0.052 0.010

0.010 0.010 0.010

0.010

0.010 0.010

0.010

0.010 0.010

0.010

0.010 0.010

0.010

0.010 0.031 0.052

0.052 0.010 0.010

0.010 0.010 0.010

0.010 0.010 0.010

0.021 0.010

0.052

Lllnlts

72-1.22

79-123

80-120

Page 44 of 140

MDL Unit


0.0017 mg/Kg 0.0052 mg/Kg 0.0068 mg/Kg

0.0015 mg/Kg 0.0017 mg/Kg

0.0052 mg/Kg

0.0020 mg/Kg 0.0052 mg/Kg

0.015 mg/Kg 0.0014 mg/Kg

0.0052 mg/Kg 0.0052 mg/Kg

0.0052 mg/Kg


0.0052 mg/Kg 0.0021 mg/Kg 0.0016 mg/Kg

0.0025 mg/Kg 0.0052 mg/Kg

0.0013 mg/Kg

0.0021 mg/Kg

0.021 mg/Kg 0.012 mg/Kg

0.010 mg/Kg

0.0021 mg/Kg 0.0052 mg/Kg

0.0021 mg/Kg






D Prepared

" 01/22117 07:44 " 01/22117 07:44

Analyzed 01/2211713:31 01/22117 13:31

" 01/22117 07:44 01122117 13:31 " 01/22117 07:44 01/22117 13:31

" 01/22117 07:44 01122117 13:31 ,, 01/22117 07:44 01/2211713:31

" 01/22117 07:44 01/2211713:31 v 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/2211713:31

" 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/17 13:31 ;) 01/22117 07:44 01/22117 13:31

" 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/2211713:31

" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/1713:31

" 01/22117 07:44 01/22/1713:31 " 01/22117 07:44 01/22/17 13:31 " 01122117 07:44 01/22117 13:31 " 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22117 13:31

1:1 01/22117 07:44 01/22117 13:31 (; 01/22117 07:44 0112211713:31

" 01122117 07:44 01/2211713:31 "' 01/22117 07:44 01/22/17 13:31 ,, 01/22117 07:44 01/22117 13:31

i) 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/1713:31

" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/2211713:31

" 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/22/17 13:31 ,, 01/22117 07:44 01/2211713:31

,, 01/22117 07:44 01122117 13:31

;) 01122117 07:44 01/22117 13:31

" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/22117 13:31

" 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/22117 13:31

Prepared

01122117 07:44

01122117 07:44

Analyzed

01122117 13:31

0112211713:31

01122117 07:44 0112211713:31

Oii Fae

1

DI/ Fae

1


2/112017


Client Sample ID: CK-8 Date Collected: 01/13/1710:10 Date Received: 01114117 08:32

Method: 82700 • Semivolatlle Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene <0.069 0.69 Acenaphthylene

Aniline Anthracene Benzo[aJanthracene Benzo[a]pyrene

Benzo{b ]fluoranthene Benzo[g,h,iJperylene BenzofkJfluoranthene 1, 1'-Biphenyl Bis(2-ch!oroethyl)ether bls (2-chloroisopropyl) ether

Bis(2-ethylhexyl).phthalate Butyl benzyl phthalate 4-ChloroaniHne 2-Chloronaphtha!ene

2-Ch!orophenol

Chrysene Oibenz{a,h)anthracene

Dibenzofuran 3,3'-Dichlorobenzidine


2.4-Dime!hylphenol

Dimethyl phthalate 1,3-Dinitrobenzene

2,4-Dinitrophenol 2,4-Dlnitroto!uene 2,6-Dinitrotofuene

Di-n-octyl phthalate Fluoranthene

Fluorene Hexach!orobenzene

Hexachlorobutactiene

Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cd]pyrene

lsophorone 2-Methylnaphthalene Naphthalene 2-Nltroani!ine

3-Nitroani!ine 4-Nitroaniline

Nitrobenzene

4-Nitropheno! N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine

Pentachlorophenol

Phenanthrene

<0.069

<0.091 <0.069 <0.069

<0.069

0.086 J <0.069

<0.069

<0.069

<0.069

<0.069

0.093 J <0.069

<0.069

<0.069

<0.069

<0.069 <0.069

<0.069

<0,069

<0.069

<:0.069

<:Q.069

<0.069 <0.069 <:0.61

<0.069

<0.069 <0.069 <0.069

<0.069

<:0.21

<0.069

<0.14

<:0.21

<0.069 <0.069 <0.069

<0.069

<0.069 <0.069

<0.069

<0.069

<0.23

<0.23 <0.069

<0.14

<0.069

0.69

0.69

0.69 0.69

0.69 0.69

0.69 0.69 0.69

0.69 0.69

0.69 0.69 0.69 0.69

0.69

0.69 0.69

0.69 0.69

0.69 0.69 0.69

0.69 0.69

2.1

0.69 0.69 0.69 0.69

0.69 0.69

0.69 0.69 0.69 0.69

0.69

0.69 0.69

0.69 0.69 0.69 0.69

0.69 0.69 0.69

1.4

0.69

Page 45 of 140

MDL Unit 0.069 mg/Kg 0.069 mg/Kg


0.069 mg/Kg

0.069 mg/Kg 0.069 mg/Kg

0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg



0.069 mg/Kg

0.069 mg/Kg 0.069 mg/Kg

0.069 mg/Kg

0.069 mg/Kg 0.069 mg/Kg

0.61 mg/Kg

0.069 mg/Kg 0.069 mg/Kg

0.069 mg/Kg 0.069 mg/Kg

0.069 mg/Kg 0.21 mg/Kg

0.069 mg/Kg

0.14 mg/Kg 0.21 mg/Kg

0.069 mg/Kg


0.069 mg/Kg 0.069 mg/Kg

0.069 mg/Kg 0.23 mg/Kg

0.23 mg/Kg 0.069 mg/Kg 0.14 mg/Kg

0.069 mg/Kg

Tes!America Job ID: 400-132540-1

Lab Sample ID: 400-132650.-3 Matrix: Solid


D Prepared Analyzed Oil Fae IIl) 01/1811709:33 01/19/17 01:14 ;) 01/18117 09:33 01119/17 01:14

" 01/16/17 09:33 01/19/17 01:14 ~ 01118/17 09:33 01/19117 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01/18/1709:33 01/19/17 23:14 " 01118/1709:33 01119117 23:14 ,, 01118/17 09:33 01119117 23:14 ,,, 01/18/17 09:33 01119117 23:14 ,, 01/18/17 09:33 01119/17 01:14

" 01118/17 09:33 01/19/17 01:14 1) 01118/17 09:33 01/19/17 01:14

•:• 01/18/17 09:33 01/19117 01:14

" 01118/17 09:33 01/19117 01:14 " 01118/1709:33 01/19/17 01:14 ,, 01/18/1709:33 01/19/17 01:14

'" 01/18/17 09:33 01/19/17 01:14 " 01/18/1709:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 23:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01118/17 09:33 01/19117 01:14 " 01116117 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01/1811709:33 01/19/17 01:14 " 01/18/1709:33 01119/17 01:14 " 01/18/17 09:33 01/19/17 01:14 :) 01/18/17 09:33 01/19/17 01:14

" 01118/17 09:33 01119/17 01:14 " 01/18/17 09:33 01119/17 01:14 " 01/18/1709:33 01/19/1701:14

'" 01/18/17 09:33 01119/17 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01/18/17 09:33 01/19/17 01:14 " 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01/18/17 09:33 01119/17 23:14 " 01/18/1709:33 01119/1701:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14

" 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14 " 01118/17 09:33 01/19117 01:14 " 01/16/17 09:33 01/19/17 01:14

" 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01 :14 " 01/18/17 09:33 01/19/17 01:14

" 01118/17 09:33 01/19/17 01:14


211/2017


Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 0111311710:10 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 46.4

Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Phenol <0.069 0.69 0.069 mg/Kg ,, 01118117 09:33 01119117 01:14 1

Pyrene 0.069 J 0.69 0.069 mg/Kg ,, 01118/17 09:33 01/19/17 01:14

1,2,4,5-Tetrachlorobenzene <0,069 0.69 0.069 mg/Kg " 01/18117 09:33 01/19/17 01:14

2,3,4,6-T etrachlorophenol <0.069 0.69 0.069 mg/Kg " 01/18/17 09:33 01119117 01:14 1,2,4-Trichlorobenzene <0,069 0.69 0.069 mg/Kg •:• 01/18117 09:33 01/19/17 01:14

2.4 ,5-Trichlorophenol <0.069 0.69 0.069 mg/Kg '" 01/18/1709:33 01/19117 01:14

2,4,6-Trichlorophenol <0.069 0.69 0.069 mg/Kg " 01118117 09:33 01119117 01:14

Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae 2-Fluorobiphenyl 51 27 -127 01118117 09:33 01119117 01:14 1

2-Ffuorophenol 59 25-128 01118117 09:33 01119117 01:14

Nitrobenzene-d5 47 15 -136 01118117 09:33 01119117 01:14

P/1enol-d5 61 29-130 01118117 09:33 01119117 01:14

Terphenyl-d14 76 24- 146 01118117 09:33 01119117 01:14

2,4,6-Tribromopflenol 63 10-150 01118117 09:33 01119117 01:14

Method: MAVPH - Ma.ssachusetts - Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae C6-C8 Aliphatics <12 12 12 mg/Kg " 01/16/1711:30 01117117 02:16 50 CB-C 10 Aliphatics <19 19 19 mg/Kg " 01116/1711:30 01117117 02:16 50

C8-C10 Aromatics <9.7 9.7 9.7 mg/Kg J) 01116/1711:30 01117117 02:16 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae a,a,a-Trifluorotoluene (fid) 83 70-130 0111611711:30 01/17117 02:16 50

a,a,a-Tn"fluorotoluene (pid) 86 70-130 0111611711:30 01117117 02:16 50

Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Aldrin <0.0026 0.0073 0.0026 mg/Kg " 01/1811712:42 01/19/17 22:50 2

alpha-BHC <0.0010 0.0073 0.0010 mg/Kg " 01118117 12:42 01119/17 22:50 2 beta-BHC <0.0021 0.0073 0.0021 mg/Kg ,, 01118/1712:42 01/19/17 22:50 2

della·BHC <0.0014 0.0073 0.0014 mg/Kg " 0111811712:42 01119117 22:50 2

-gamma-BHC (Undane) <0.00094 0.0073 0.00094 mg/Kg " 01118/1712:42 01119117 22:50 2 alpha-Chlordane <0.0012 0.0073 0.0012 mg/Kg " 01118/17 12:42 01119117 22:50 2

gamma-Chlordane <0.0012 0.0073 0.0012 mg/Kg ;:i 01118117 12:42 01119117 22:50 2

4,4'-DDD 0.00084 J 0.0073 0.00082 mg/Kg " 01118/1712:42 01/19/17 22:50 2

4,4'-DDE <0.0012 0.0073 0.0012 mg/Kg " 01/18/17 12:42 01119/17 22:50 2

4,4'-DDT <0.0033 0.0073 0.0033 mg/Kg " 01/18/1712:42 01119/17 22:50 2 Dieldrin <0.0015 0.0073 0.0015 mg/Kg ;) 01/18/1712:42 01119117 22:50 2

Endosulfan I <0.00090 0.0073 0.00090 mg/Kg " 01/18/1712:42 01119/17 22:50 2

Endosu!fan II <0.00099 0.0073 0.00099 mg/Kg " 01/1811712:42 01/19/17 22:50 2

Endosulfan sulfate <0.00090 0.0073 0.00090 mg/Kg l'J 01118/1712:42 01/19117 22:50 2

Endrin <0.00082 0.0073 0.00082 mg/Kg " 01118/1712:42 01119117 22:50 2

, Endrin aldehyde <0.0012 0.0073 0.0012 mg/Kg J) 01/18/1712:42 01/19/17 22:50 2 Endrin ketone <0.0015 0.0073 0.0015 mg/Kg " 01/18/1712:42 01119117 22:50 2

Heptachlor <0.0010 0.0073 0.0010 mg/Kg ,, 01118/1712:42 01/19117 22:50 2

Heptachlor epoxide <0.0019 0.0073 0.0019 mg/Kg " 01/18/1712:42 01119117 22:50 2

Methoxychlor <0.0014 0.0073 0.0014 mg/Kg " 01118/1712:42 01119117 22:50 2 Toxaphene <0.12 0.43 0.12 mg/Kg 0 01118/1712:42 01/19117 22:50 2


Page 46 of 140 2/112017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 01/13/1710:10 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 46.4

Surrogate %RecovetY Qua/If/er Limits Prepared Analyzed Dil Fae E DCB Decachlorobiphenyl 58 26-129 0111811712;42 01119117 22:50 2

Tetrachloro-m·xylene 52 31-122 01118117 12:42 01119117 22:50 2

Method: MA-EPH - Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

c10.c12 A!iphatlcs <3.4 3.4 3.4 mg/Kg ,, 01/19/17 07:20 01/24/17 20:17 1

C10-C12 Aromatics <3.4 3.4 3.4 mg/Kg "' 01/19/17 07:20 01/25/17 00:27 1

C 12-C 16 AHphatics <3.4 3.4 3.4 mg/Kg " 01/19/17 07:20 01/24/17 20:17


C16-C35 Aliphatics 17 3.4 3.4 mg/Kg n 01/19/17 07:20 01/24/17 20:17

C21-C35 Aromatics <3.4 3.4 3.4 mg/Kg n 01/19117 07:20 01 /25/17 00:27


Surrogate %Recovery Qualifier L/111/ts Prepared Analyzed Di/ Fae

1-Clllorooctadecane 85 40-140 0111911707:20 01124117 20:17 1

o-Terphenyl 78 40-140 01119117 07:20 01125117 00.27

Method: 601 OC - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Silver <0.40 1.0 0.40 mg/Kg 0 01/16/17 08:55 01/17/1713:20 1

Arsenic 4.3 2.0 0.80 mg/Kg ,, 01/16/17 08-.55 01/17/1713:20

Barium 88 2.0 0.40 mg/Kg " 01/16/17 08:55 01/17/1713:20

Beryllium 0.36 J 0.60 0.20 mg/Kg " 01/16/17 08:55 01/17/1713:20

Cobalt 5.0 2.0 0.60 mg/Kg " 01/16/1708:55 01/17/17 13:20

Chromium 11 2.0 0.40 mg/Kg " 01/16/1708:55 01/17117 13:20

Copper 19 4.0 0.40 mg/Kg u 01/16/17 08:55 01/17/17 13:20

Nickel 12 1.0 0.60 mg/Kg " 01/16/17 08:55 01/17/17 13:20

Lead 30 2.0 0.40 mg/Kg " 01/16/17 08:55 01/17/17 13:20

Selenium <0.80 4.0 0.80 mg/Kg " 01 /16/17 08:55 01/1711713:20

Thallium <D.80 2.0 0.80 mg/Kg " 01/16/17 08:55 01/17/1713:20

Vanadium 1Z 4.0 0.60 mg/Kg " 01/16/17 08:55 01/17/1713:20

Zinc 84 4.0 1.6 mg/Kg ,, 01/16/17 08:55 01/17/1713:20

Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Mercury 0.031 0.012 0.0075 mg/Kg 01/15/1712:43 01/16/1712:17 1

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Chromium, hexavalent <5.5 7.9 5.5 mg/Kg ,,, 01/20/17 17:00 01/23/1712:07 1

Cyanide, Total <0.29 0.55 0.29 mg/Kg " 01/18/1710:53 01/18/1717:37

Percent Moisture 53.6 0.1 0.1 % 01/1711714:08

General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Nitrate Nitrite as N 0.99 J 2.2 0.78 mg/Kg ,, 01/16/17 12:28 1


Page 47 of 140 211/2017


Client Sample ID: CK-9 Date Collected: 01/13/1710:25 Date Received: 01114/17 08:32

Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL 1, 1, 1,2-Tetrachloroethane <0.0064 0_013

1, 1, 1-Trichloroethane 1,1,2,2-Tetrachloroethane

1, 1,2-Trich!oroethane 1, 1-Dichloroethane 1, 1-Dichloroethene 1.2-Dibromo-3-Ch!oropropane

1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane

1,3-Dlch!orobenzene 1.4-Dichlorobenzene

Acetone Benzene Bromoforrn Bromomethane


Chlorobenzene Chlorodibromomethane

Chloroethane

Chloroform Chloromethane

cis-1,2-Dichloroethene cis-1,3-Dich!oropropene Dichlorobromomethane

Ethylbenzene Methyl tert-butyl ether



Styrene T etrach!oroethene

Toluene trans-1,2-Dichloroethene trans-1,3-Dich!oropropene Trichloroethene Trich!orofluoromethane

Vinyl chloride Xylenes, Total 1,2.4-Trichlorobenzene

lsobutyl alcohol

Surrogate

4-Bromofluorobenzene Dibromofluorometl1ane

Tofuene-08 (Sun-)

<0.0028

<0.0064 <0.0064

<0.0021 <0.0064

<0.0085 <0.0018

<0.0021 <0.0064

<0.0024 <0.0064

0.15 <0.0017 <0.0064

<0.0064

0.0078 J <0.0044 <0.0013

<0.0064 <0.0064 <0.0064

<0.0026

<0.0019

<0.0031 <0.0064

<0.0016

<0.0026 <0.026 <0.015

<0.013

<0.0026 <0.0064 <0.0026

<0.0064

<0.0064 <0.0026

<0.0064 <0.0064 <0,0049

<0.0051 <0.026

%Recovery Qualifier

117

93

112

0.013

0.013 0.013

0.013 0.013 0.013

0.013 0.013 0.013 0.013 0.013

0.064 0.013

0.013 0.013

0.013

0.013 0.013 0.013

0.013 0.013 0.013 0.013

0.013 0.013 0.013

0.013

0.038 0.064 0.064 0.013 0.013

0.013 0.013

0.013 0.013

0.013

0.013 0.026 0.013 0.064

Llfnits 72-122

79-123

80-120

Page 48 of 140


0.0064 mg/Kg

0.0021 mg/Kg 0.0064 mg/Kg

0.0085 mg/Kg 0.0018 mg/Kg 0.0021 mg/Kg

0.0064 mg/Kg 0.0024 mg/Kg 0.0064 mg/Kg

0.019 mg/Kg


0.0044 mg/Kg

0.0013 mg/Kg 0.0064 mg/Kg

0.0064 mg/Kg

0.0064 mg/Kg 0.0026 mg/Kg

0.0019 mg/Kg

0.0031 mg/Kg 0.0064 mg/Kg

0.0016 mg/Kg


0.0026 mg/Kg 0.0064 mg/Kg

0.0026 mg/Kg


0.0064 mg/Kg

0.0049 mg/Kg 0.0051 mg/Kg

0.026 mg/Kg




O Prepared Analyzed " 01/19/17 08:59 01119/17 16:47 Q 01/19/17 08:59 01119117 16:47

" 01/19/17 08:59 01/19/17 16:47

" 01/19/17 08:59 01/19/1716:47 l) 01/19/17 08:59 01/19117 16:47

" 0111911708:59 01/19/1716:47

'" 01119117 08:59 01/19/17 16:47 " 01119/17 08:59 01/19/1716:47 l) 01119/17 08:59 01/19117 16:47

i:i 01119/17 08:59 01/19/1716:47

" 01/19/17 08:59 01/19/1716:47 l) 01/19/17 08:59 01/19/17 16:47

" 01/19/17 08:59 01/19/17 16:47

" 01/19/17 08:59 01119/17 16:47 " 01/19/17 08:59 01119/1716:47 " 01/19/17 08:59 01/19117 16:47 " 01/19/17 08:59 01/1911716:47

" 01/19/17 08:59 01/19/17 16:47 " 01119117 08:59 01/19/17 16:47 n 01/19/17 08:59 01/19/17 16:47

" 01119/17 08:59 01/19/17 16:47 l) 01119/17 08:59 01/19/17 16:47

" 01/19/17 08:59 01/19/17 16:47

" 01/19/17 08:59 01/19/17 16:47 Q 01119/17 08:59 01/19/17 16:47 " 01/19/17 08:59 0111911716:47

" 01/19/17 08:59 01119/1716:47 " 01/19/17 08:59 01/1911716:47 l) 01/19117 08:59 01119/1716:47 " 01/19/17 08:59 01/19/17 16:47

"' 01/19/17 08:59 01/19/17 16:47 ,, 01119117 08:59 01/19/1716:47

" 01/19/17 08:59 01/19/17 16:47 :) 01/19/1708:59 01/19/1716:47

" 01/19/17 08:59 01/19/17 16:47 '" 01/19/17 08:59 01/19/17 16:47 " 01/1$117 08:59 01/19/1716:47 ,, 01/19/17 08:59 01/19/1716:47

"' 01/19/17 08:59 01/19117 16:47 " 01119/17 08:59 0111911716:47 " 01/19117 08:59 01/19/1716:47 ,, 01/19117 08:59 01119117 16:47

Prepared 01119117 08:59

01119117 08:59

Analyzed 01119117 16:47

0111911716:47

01119117 08:59 01119117 16:47

Oil Fae

1

DJ/ Fae

1


2/1/2017


Client Sample ID: CK-9 Dat<l Collected: 0111311710:25 Date Received: 01114/17 08:32

Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene <0.063 0.63 Acenaphthylene


Benzo[a]pyrene Benzo[b ]flu ora nthene Benzo[g,h,i]perylene

Benzo[k]fluoranthene 1, 1 '-Biphenyl

8is(2-chloroethy!)ether bis {2-chloroisopropyl) ether

Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanilfne 2-Chloronaphtha!ene

2-Ch!orophenol

Chrysene Dibenz(a.h}anthracene Dibenzofuran

3,3'-Dlch!orobenzidine 2,4-Dichforophenol Diethyl phthalate 2,4-Dimethy!phenol

Dimethyl phthalate 1,3-Dlnltrobenzene 2,4-Dinitropheno!

2,4-Dlnitrotoluene 2,6-Dinitroto!uene

Oi~n·octyl phthalate

Fluoranthene


Hexachlorobutad!ene

Hexach!orocyclopentadiene Hexachloroethane

lndeno[1,2,3-cd]pyrene lsophorone 2-Methylnaphtha!ene Naphthalene 2-Nitroani!ine 3-Nitroaniline 4-Nltroaniline

Nitrobenzene 4-Nitrophenol

N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine

Pentachlorophenol

Phenanthrene

<0.063

<0.082

<0.063

<0.063

0.18 J 0.24 J 0.10 J 0.12 J

<0.063

<0.063 <0.063

0.089 J <0.063

<0.063

<0.063

<0.063

0.14 J <0.063

<0.063

<0.063

<0.063 <0.063 <0.063

<0.063

<0.063

<0.55 <0.063 <0.063

0.073 J 0.29 J

<0.063

<0.19

<0.063 <0.13

<0.19

0.091 J <0.063

<0.063

<0.063

<0.063

<0.063

<0.063 <0.063

<0.21

<0.21

<0.063 <0.13

0.12 J

0.63

0.63 0.63 0.63

0.63

0.63 0.63 0.63

0.63 0.63 0.63 0.63

0.63 0.63

0.63

0.63 0.63 0.63 0.63

0.63

0.63 0.63

0.63

0.63 0.63

1.9 0.63 0.63

0.63 0.63

0.63 0.63

0.63

0.63 0.63 0.63 0.63

0.63 0.63 0.63

0.63 0.63

0.63 0.63

0.63 0.63

1.3 0.63

Page 49of140


0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg


0.063 mg/Kg

0.063 mg/Kg

0.063 mg/Kg


0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg

0.55 mg/Kg 0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.19 mg/Kg

0.063 mg/Kg

0.13 mg/Kg 0.19 mg/Kg

0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.063 mg/Kg

0.063 mg/Kg 0.21 mg/Kg

0.21 mg/Kg 0.063 mg/Kg

0.13 mg/Kg 0.063 mg/Kg


Lah Sample ID: 400-132650-4 Matrix: Solid


0 Prepared Analyzed

r; 01118/17 09:33 01/19/17 01:47 :: 01118/17 09:33 01/19117 01:47

" 01118117 09:33 01119117 01:47 0 01/18/17 09:33 01/19/1701:47 ,, 01118117 09:33 01/19117 01:47

,, 01118/17 09:33 01/19117 23:44

0 01118117 09:33 01119117 23:44 ,, 01118/17 09:33 01119/17 23:44 ,, 01118/17 09:33 01119117 23:44

,, 01118/17 09:33 01/19/17 01:47

" 01118/17 09:33 01/19/17 01:47 " 01118/17 09:33 01/19/17 01:47 :) 01118/17 09:33 01/19/17 01:47 ,, 01118/17 09:33 01/19117 01:47 ,, 01/18117 09:33 01/19/17 01:47

" 01/18/17 09:33 01119117 01:47 ,, 01/18/17 09:33 01/19/17 01:47

!) 01118/17 09:33 01119117 01:47 " 01/18/17 09:33 01119117 23:44 ,, 01118/17 09:33 01119117 01:47

,,, 01118/17 09:33 01/1911701:47

" 01118117 09:33 01119/17 01:47 " 01/18/17 09:33 01/19/17 01:47 " 01/18/17 09:33 01/19117 01:47 ,, 01118/17 09:33 01/19/17 01:47

" 01/18117 09:33 01119/17 01:47 " 01118/1709:33 01/19/1701:47 ,, 01118/17 09:33 01/19/17 01:47 (j 01/18/17 09:33 01/19/17 01:47

" 01/18117 09:33 01/19/17 01:47 " 01118/17 09:33 01119117 01:47

" 01/18/17 09:33 01119/17 01:47 " 01118117 09:33 01119/17 01:47

" 01/18/17 09:33 01/1911701:47 {j 01/18117 09:33 01/19/17 01:47 ,, 01118/17 09:33 01119/17 01:47

" 01/18/17 09:33 01119117 23:44 {j 01118/17 09:33 01119/17 01:47 " 01118/17 09:33 01/19/1701:47 ,, 01118/17 09:33 01119/17 01:47

" 01/18/17 09:33 01/19/1701:47 " 01/18/1709:33 01/1911701:47 " 01118/17 09:33 01/19/17 01 :47 " 01/18117 09:33 01/19/17 01:47

" 01118117 09:33 01/19/17 01:47

" 01/18117 09:33 01/19/17 01:47 " 01118117 09:33 01119/17 01:47

" 01118/17 09:33 01/19117 01:47 " 01/18/17 09:33 01/19117 01:47

Ollfac E 1

1

1

1

1


2/1/2017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol

Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01113117 10:25 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 52.0

e

1 E Method: 8270D • Semivotatite Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fa

Phenol <0.063 0.63 0.063 mg/Kg ::1 01/18/17 09:33 01/19/17 01:47

Pyrene 0.37 J 0.63 0.063 mg/Kg ::: 01/18/17 09:33 01/19/17 01:47

1,2,4, 5-T etrach1orobenzene <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/17 01:47

2,3,4,6-T etrachlorophenol <0.063 0.63 0.063 mg/Kg f) 01/18/17 09:33 01/19/17 01 :47

1,2,4-Trichlorobenzene <0.063 0.63 0.063 mg/Kg (l 01/18/17 09:33 01/19/17 01:47

2.4,5-Trichlorophenol <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/1701:47

2,4 ,6-Trichlorophenol <0.063 0.63 0.063 mg/Kg D 01/18/17 09:33 01/19/17 01:47


2-Fluorobiphenyl 67 27 -127 0111811709:33 01119117 01:47 1

2-Fluorophenol 68 25-128 01118117 og:33 01119117 01:47 1

Nitrobenzene-d5 56 15-136 0111811709:33 01119117 01:47 1

PJJenol-d5 68 29-130 01118117 09:33 01119117 01:47 1

Teiphenyl-d14 111 24-146 01118117 09:33 01119117 01:47

2,4,6· Tribromophenot 67 10-150 01118117 09:33 01119117 01:47

Method: MAVPH ·Massachusetts· Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C6·C8 A!iphatics <15 15 15 mg/Kg " 01/16/17 11 :30 01/17/17 03:16 50

CB-C10 Al!phatics <26 26 26 mg/Kg :) 01116/1711:30 01/17/17 03:16 50

C8-C10 Aromatics <13 13 13 mg/Kg " 01/16/1711:30 01/17/17 03:16 50



a,a,a-Trifluorotoluene (pid) 92 70-130 0111611711:30 0111711703:16 50

Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DllFac

Aldrin <0.0023 0.0065 0.0023 mg/Kg (~ 01/18/1712:42 01/19/17 23:20 2

alpha-BHC <0.00092 0.0065 0.00092 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

beta-BHC <0.0019 0.0065 0.0019 mg/Kg ,,, 01/18/1712:42 01/19/17 23:20 2

della-BHC <0.0012 0.0065 0.0012 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

gamma-BHC (Undane) <0.00085 0.0065 0.00085 mg/Kg n 01/18/1712:42 01/19/17 23:20 2

alpha-Chlordane <0.0011 0.0065 0.0011 mg/Kg 0 01/18/1712:42 01/19/17 23:20 2

gamma-Chlordane 0.0010 J 0.0065 0.0010 mg/Kg 0 01/18/1712:42 01119117 23:20 2

4,4'-DDD 0.00085. J 0.0065 0.00073 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

4,4'-DDE 0.0010 J 0.0065 0.0010 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

4,4"-DDT <0.0030 0.0065 0.0030 mg/Kg " 01/18/1712:42 01119/17 23:20 2

Dieldrin <0.0014 0.0065 0.0014 mg/Kg ,,, 01/18/1712:42 01/19/17 23:20 2

Endosulfan I <0.00081 0.0065 0.00081 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

Endosulfan II <0.00089 0.0065 0.00089 mg/Kg " 01118/1712:42 01/19/17 23:20 2

Endosulfan sulfate <0.00081 0.0065 0.00081 mg/Kg ,, 01/18/1712:42 01/19/17 23:20 2

Endr!n <0.00073 0.0065 0.00073 mg/Kg ,, 01/18/1712:42 01/19/17 23:20 2

Endrin aldehyde <0.0011 0.0065 0.0011 mg/Kg " 01/18/1712:42 01/19/17 23:20 2

Endrin ketone <0.0013 0.0065 0.0013 mg/Kg 0 01/18/17 12:42 01/19/17 23:20 2

Heptach!or <0.00092 0.0065 0.00092 mg/Kg o;i 01/18/17 12:42 01/19/17 23:20 2

Heptach!or epoxide <0.0017 0.0065 0.0017 mg/Kg " 01/18/17 12:42 01/19/17 23:20 2

Methoxychlor <0.0013 0.0065 0.0013 mg/Kg " 01/18/17 12:42 01/19/17 23:20 2

Toxaphene <0.11 0.38 0.11 mg/Kg t,1 01/18/1712:42 01/19/17 23:20 2


Page 50 of 140 211/2017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1

ProjecVSite: Moffat & Nichol

Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01113/17 10:25 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 52.0

e

a

2

2

ae

m Surrogate %Recovery Qua/If/er Limits Prepared Arralyzed DI/ F

DCB Decar;hlorobiphenyl 57 26- 129 01118117 12:42 01119117 23:20

Tetrachloro-m-xylene 52 31-122 0111811712:42 01119117 23:20

Method: MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MOL Unit 0 Prepared Analyzed Oil F

C10-C12Aliphatics <3.1 3.1 3.1 mg/Kg ,, 01/19/17 07:20 01/24/17 20:37 1C10-C12 Aromatics <3.1 3.1 3.1 mg/Kg ;) 01/19/17 07:20 01/25/17 00:46

C12-C16 AHphatics <3.1 3.1 3.1 mg/Kg l) 01/19/17 07:20 01/24/17 20:37 C12-C16 Aromatics <3.1 3.1 3.1 mg/Kg 0 01/19/17 07:20 01/25/17 00:46

C16-C35 Aliphatics 20 3.1 3.1 mg/Kg ;) 01/19/17 07:20 01/24/17 20:37

C21-C35 Aro1natics 10 3.1 3.1 mg/Kg ;:< 01119/17 07:20 01/25/17 00:46

C-16-C21 Aromatics 4.3 3.1 3.1 mg/Kg " 01119/17 07:20 01/25/17 00:46

Surrogate %Recovety Qualifier Limits Prepared Analyzed Di/ Fae

t~Chlorooctadecanc 86 40-140 01119117 07:20 01124117 20:37 1

o-Terphenyl 74 40-140 01119117 07:20 01125117 00:46

Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae

Silver <0.36 0.89 0.36 mg/Kg 0 01/16/17 08:55 01/17/17 13:23 1

Arsenic 4.5 1.8 0.72 mg/Kg " 01/16/17 08:55 01/17117 13:23 1

Barium 100 1.8 0.36 mg/Kg ,, 01/16/17 08:55 01/17/17 13:23

Beryllium 0.37 J 0.54 0.18 mg/Kg !;! 01/16/17 08:55 01/17/17 13:23

Cobalt 5.4 1.8 0.54 mg/Kg " 01/16117 08:55 01/17/17 13:23

Chromium 12 1.8 0.36 mg/Kg ,".} 01/16/1708:55 01/17/1713:23

Copper 23 3.6 0.36 mg/Kg ,, 01/16/17 08:55 01/17/1713:23

Nickel 12 0.89 0.54 mg/Kg ,,, 01/16/17 08:55 01/17/17 13:23

Lead 37 1.8 0.36 mg/Kg ::: 01/16/17 08:55 01/17/17 13:23

Selenium 0.83 J 3.6 0.72 mg/Kg (l 01/16/17 08:55 01/17/17 13:23

Thallium <0,72 1.8 0.72 mg/Kg n 01/16/17 08:55 01/17/17 13:23 1

Vanadium 13 3.6 0.54 mg/Kg n 01/16/17 08:55 01/17/17 13:23

Zinc 93 3.6 1.4 mg/Kg "' 01/16/17 08:55 01/17/17 13:23

Method: 7471A - Mercury (CVAAJ Analyte Result Qualifier RL MOL Unit D Prepared Analyzed Dll Fae

Mercury 0.053 0.013 0.0078 mg/Kg 01/15117 12:43 01/16/1712:19 1

General Chemistry Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae Chromium, hexava!ent <5.2 7.5 5.2 mg/Kg ,, 01/20/1717:00 01/23/17 12:07 1

Cyanide, Total <0.23 0.45 0.23 mg/Kg ;;i 01/18/17 10:53 01/18/17 17:37 1

Percent Moisture 48.0 0.1 0.1 % 01/17/17 14:08 1

General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oii Fae

Nitrate Nitrite as N 1.1 J 1.9 0.69 mg/Kg i:1 01/16/17 12:29 1


Page51 of140 2/1/2017


Client Sample ID: CK-10 Date Collected: 01/13/1710:45 Date Received: 01/14/17 08;32

Method: 8260C - Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0034 1,1,1-Trich!oroethane <0.0015

1,1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dlch!oroethene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dich!oroethane 1,2-Dlchloropropane

1,3-Dichlorobenzene 1.4-Dich!orobenzene

Aceto_ne Benzene Bromofonn Bromomethane

Carbon-disulfide Carbon tetrachloride


Chloroethane

Chlorofom1 Ch!oromethane

cis-1,2-Dlchloroethene

cis-1,3-Dichloropropene Dichlorobromomethane

Ethylbenzene Methyl tert-butyl ether



Styrene Telrachloroethene

Toluene trans--1,2-Dich!oroethene trans-1,3-Dlchf oropropene Trichloroethene Trich!orofluoromethane

Vinyl chloride Xy!enes, Total 1, 2,4· Trichlorobenzene

lsobutyl alcohol

Surrogate 4-Bromofluorobenzene Dibromofluoromethane Toluene-dB (Surr)

<0.0034 <0.0034

<0.0011

<0.0034

<0.0045

<0.00098 <0.0011

<0.0034

<0.0013 <0.0034

0.036 <0.00092

<0.0034

<0.0034

0.015 <0.0023

<0.00071

<0.0034 <0.0034

<0.0034 <0.0014

<0.0010

<0.0016

<0.0034

<0.00084

<0.0014

<0.014

<0.0082

<0.0069

<0.0014 <0.0034

<0.0014 <0.0034

<0.0034

<0.0014 <0.0034

<0.0034 <0.0026

<0.0027

<0.014

%Recovery Qualifier 107

109

101

RL 0.0069 0.0069

0.0069

0.0069

0.0069 0.0069

0.0069

0.0069

0.0069 0.0069

0.0069 0.0069

0.034

0.0069

0.0069 0.0069

0.0069

0.0069

0.0069

0.0069 0.0069

0.0069

0.0069

0.0069

0.0069 0.0069

0.0069

0.0069

0.021

0.034

0.034

0.0069 0.0069

0.0069

0.0069

0.0069 0.0069

0.0069 0.0069

0.014 0.0069

0.034

Lfmlts 72-122

79-123

80-120

MDL Unit

0.0034 mg/Kg 0.0015 mg/Kg

0.0034 mg/Kg

0.0034 mg/Kg

0.0011 mg/Kg 0.0034 mg/Kg

0.0045 mg/Kg 0.00098 mg/Kg

0.0011 mg/Kg 0.0034 mg/Kg

0.0013 mg/Kg 0.0034 mg/Kg

0.010 mg/Kg

0.00092 mg/Kg

0.0034 mg/Kg 0.0034 mg/Kg

0.0034 mg/Kg

0.0023 mg/Kg

0.00071 mg/Kg

0.0034 mg/Kg

0.0034 mg/Kg

0.0034 mg/Kg

0.0014 mg/Kg

0.0010 mg/Kg 0.0016 mg/Kg

0.0034 mg/Kg

0.00084 mg/Kg

0.0014 mg/Kg

0.014 mg/Kg

0.0082 mg/Kg

0.0069 mg/Kg

0.0014 mg/Kg 0.0034 mg/Kg

0.0014 mg/Kg 0.0034 mg/Kg

0.0034 mg/Kg 0.0014 mg/Kg

0.0034 mg/Kg

0.0034 mg/Kg

0.0026 mg/Kg 0.0027 mg/Kg

0.014 mg/Kg

Page 52 of 140




O Prepared Analyzed " 01119117 08:59 0111911717:13 ,, 01119117 08:59 0111911717:13

l.l 01119117 08:59 0111911717:13 ,, 01119117 08:59 01119117 17:13

" 01119117 08:59 01119117 17:13 ,, 01119117 08:59 0111911717:13

p 01119117 08:59 0111911717:13

,, 01119117 08:59 0111911717:13 l) 01119117 08:59 0111911717:13

,, 01119117 08:59 0111911717:13

u 01119117 08:59 0111911717:13

::: 01119117 08:59 0111911717:13

" 01119117 08:59 01119117 17:13

" 01119117 08:59 01119117 17:13

" 01119117 08:59 0111911717:13

" 01119117 08:59 01119117 17:13

" 01119117 08;59 01119117 17:13

u 01119117 08:59 0111911717:13

" 01119117 08:59 0111911717:13 n 01119117 08:59 01119117 17:13

" 01119117 08:59 01119117 17:13

" 01119117 08:59 0111911717:13 " 01119117 08:59 0111911717:13

" 01119117 08:59 01119117 17:13 n 01119117 08:59 01119117 17:13

" 01119117 08:59 0111911717:13

l) 01119117 08:59 0111911717:13

" 01119117 08:59 0111911717:13 ;) 01119117 08:S9 0111911717:13 ,, 01119117 08:59 0111911717:13

i:: 01119117 08:59 0111911717:13

0 01119117 08:59 0111911717:13 " 01119117 08:59 01119117 17:13

0 01119117 08:59 0111911717:13

,, 01119117 08:59 0111911717:13

ll 01119117 08:59 0111911717:13

" 01119117 08:59 0111911717:13 ,,, 01119117 08:59 0111911717:13

,, 01119117 08:59 0111911717:13

" 01119117 08:59 0111911717:13 " 01119117 08:59 0111911717:13 i:i 01119117 08:59 0111911717:13

Prepared Analyzed

0111911708;59 0111911717:13

01119117 08:59 0111911717:13

01119117 08:59 0111911717:13

Oil Fae

1

1

1

Dfl Fae 1

1


211/2017


Client Sample ID: CK-10 Date Collected: 01/13/1710:45 Date Received: 01/14/17 08:32

Method: 82700 -.Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene


Benzofa]pyrene Be nzo{b ]flu ora nthe ne Benzofg,h,iJperylene Benzo[k]fluoranthene

1, 1 '-Biphenyl Bis(2-chloroethy!)ether bis (2-ch1oroisopropyl) ether Bis(2-ethylhexyl) phthalate

Butyl benzyl phthafate 4-Chloroaniline 2-Chloronaphtha!ene

2-Ch!orophenol


Dibenzofuran 3,3'-Dichlorobenzidine


2,4-Dimethylphenol

Dimethyl phthalate 1,3-Dlnitrobenzene 2,4-Dinitrophenol 2,4-Dinltrotoluene 2,6-Dinitroto!uene

Di-n-octyl phtha!ate

Fluoranthene Fluorene Hexachforobenzene

Hexachlorobutadiene

Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cd]pyrene

Jsophorone 2-Methylnaphthalene Naphthalene

2-Nitroaniline 3-Nitroanillne 4-Nitroaniline Nitrobenzene

4-Nitropheno! N-Nitrosodi-n-propyfamine N-Nitrosodiphenylamine Pentach!orophenol Phenanthrene

<0.043

<0.043

<0.055 <0.043

<0.043

0.058 J 0.076 J

<0.043 <0.043

<0.043 <0.043 <0.043

<0.043

<0.043 <0.043

<0.043

<0.043 <0.043

<0.043 <0.043

<0.043 <0.043

<0.043 <0.043

<0.043

<0.043

<0.37 <0.043 <0.043

<0.043

0.066 J <0.043

<0.13

<0.043

<0.085 <0.13

<0.043 <0.043 <0.043 <0.043 <0.043

<0.043

<0.043 <0.043

<0.14

<0.14

<0.043 <0.085 <0.043

0.43 0.43

0.43 0.43 0.43

0.43 0.43 0.43 0.43

0.43 0.43 0.43 0.43

0.43 0.43 0.43

0.43 0.43 0.43 0.43

0.43

0.43 0.43

0.43 0.43

0.43 1.3

0.43

0.43 0.43 0.43

0.43 0.43

0.43

0.43 0.43 0.43

0.43 0.43 0.43

0.43 0.43 0.43 0.43 0.43

0.43 0.43

0.85 0.43

Page 53 of 140


0.055 mg/Kg

0.043 mg/Kg 0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg


0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg

0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg

0.37 mg/Kg


0.043 mg/Kg 0.13 mg/Kg

0.043 mg/Kg 0.085 mg/Kg 0.13 mg/Kg

0.043 mg/Kg

0.043 mg/Kg

0.043 mg/Kg 0.043 mg/Kg


0.14 mg/Kg 0.14 mg/Kg

0.043 mg/Kg 0.085 mg/Kg

0.043 mg/Kg



Percent Solids: 75,1

D Prepared Analyzed

" 01/18117 09:33 01/19/17 02:20 " 01118/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20

" 01/18117 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/20/17 00:15

" 01/18/1709:33 01/20/17 00:15 01/18/17 09:33 01/20/17 00:15

" 01/18/17 09:33 01/20/17 00:15 ,, 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/1709:33 01/19/1702:20 ,, 01/18117 09:33 01/19/17 02:20

" 01/18117 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/20/17 00:15

" 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/1702:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/1709:33 01/19/17 02:20

,, 01/18/17 09:33 01/19/17 02:20

" 01118/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 1:> 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20

,, 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19117 02:20

" 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/20/17 00:15

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01119117 02:20 " 01/18/17 09:33 01119/17 02:20 " 01/18/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,,, 01/18/17 09:33 01/19/17 02:20

" 01118/17 09:33 01/19/17 02:20

" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20

DilFac E 1

1

1 1

1


2/1/2017


Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01/13/1710:45 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 75. 1

Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Phenol <0.043 0.43 0.043 mg/Kg ,, 01/18/17 09:33 01/19/17 02:20 1

Pyrene 0.094 J 0.43 0.043 mg/Kg ,,, 01/18/17 09:33 01/19/17 02:20

1,2, 4, 5-T etrach!orobenzene <0.043 0.43 0.043 mg/Kg n 01/18/17 09:33 01119/17 02:20

2,3,4,6-T etrachlorophenol <0.043 0.43 0.043 mg/Kg " 01/18/17 09:33 01119117 02:20

1,2,4-Trichtorobenzene <0.043 0.43 0.043 mg/Kg 0 01/18117 09:33 01/19117 02:20

2,4,5-Trichlorophenol <0.043 0.43 0.043 mg/Kg <) 01/18117 09:33 01119/17 02:20

2,4,6-Trichlorophenol <0.043 0.43 0.043 mg/Kg ~ 01118117 09:33 01/19/17 02:20


2-Fluorobipl1enyl 67 27 - 127 0111811709:33 01119117 02:20 1

2-Fluorophenol 76 25-128 01118117 09:33 01119117 02.·20

Nitrobenzene-d5 63 15-136 01118117 09:33 01119117 02:20

Phenol-d5 77 29-130 01118117 09:33 01119117 02:20 1

Teipheny/-d14 96 24-146 01118117 og:33 01119117 02:20

2, 4,6-Tribromopflenol 84 10-150 01118117 09:33 01119117 02:20

Method: MAVPH - Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C6-C8 AHphatics <11 11 11 mg/Kg " 01116117 11:30 01117117 04:15 50

CB-C 10 Atiphatics <18 18 18 mg/Kg -1:< 0111611711:30 01/17117 04:15 50

C8-C10 Aromatics <9.2 9.2 9.2 mg/Kg ,, 0111611711:30 01117117 04:15 50

surrogate %Recovery Quallfier Limits Prepared Analyzed Di/ Fae

a,a,a-Triffuorotoluene (fid) 113 70-130 01116117 11:30 01117117 04:15 50

a,a,a-Ttifluorotofuene (pid) 113 70-130 01116117 11:30 01117117 04:15 50

Method: 80816. Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Aldrin <0.0016 0.0045 0.0016 mg/Kg " 01118/17 12-.42 01119117 23:50 2

alpha-BHC <0.00063 0.0045 0.00063 mg/Kg " 0111811712:42 01119117 23:50 2

beta-BHC <0.0013 0.0045 0.0013 mg/Kg ,, 01118/17 12:42 01119/17 23:50 2

delta-BHC <0.00084 0.0045 0.00084 mg/Kg 0 01118117 12:42 01119/17 23:50 2

gamma-BHC (Lindane) <0.00058 0.0045 0.00058 mg/Kg " 01118117 12:42 01119117 23:50 2

alpha-Chlordane <0.00074 0.0045 0.00074 mg/Kg " 01/18/17 12:42 01119117 23:50 2

gamma-Chlordane 0.00078 J 0.0045 0.00071 mg/Kg '·' 01/1811712:42 01/19/17 23:50 2

4,4'-DDD 0.00055 J 0.0045 0.00050 mg/Kg " 01118117 12:42 01119117 23:50 2

4,4'-DDE <0,00071 0.0045 0.00071 mg/Kg ,, 01/1811712:42 01119117 23:50 2

4,4'-DDT <0.0020 0.0045 0.0020 mg/Kg ,, 01118/1712:42 01/19/17 23:50 2

Dieldrin <0.00095 0.0045 0.00095 mg/Kg i:i 0111811712:42 01119117 23:50 2

Endosulfan I <0.00055 0.0045 0.00055 mg/Kg " 01/18/1712:42 01119117 23:50 2

Endosulfan 11 <0.00061 0.0045 0.00061 mg/Kg " 01118/1712:42 01119117 23:50 2

Endosu!fan sulfate <0.00055 0.0045 0.00055 mg/Kg {l 01/18/1712:42 01119/17 23:50 2

Endrin <0.00050 0.0045 0.00050 mg/Kg :? 01118/1712:42 01/19/17 23:50 2

Endrin aldehyde <0.00076 0.0045 0.00076 mg/Kg " 01118117 12:42 01/19117 23:50 2

Endrin ketone <0.00092 0.0045 0.00092 rng/Kg " 01118/17 12:42 01119/17 23:50 2

Heptachlor <0.00063 0.0045 0.00063 mg/Kg 1:; 01/18117 12:42 01/19/17 23:50 2

Heptachlor epoxide <0.0012 0,0045 0.0012 mg/Kg 0 01118/17 12:42 01/19117 23:50 2

Methoxychtor <0.00087 0.0045 0.00087 mg/Kg p 01/18117 12:42 01/19117 23:50 2

Toxaphene <0.076 0.26 0.076 mg/Kg f.! 01/18117 12:42 01119117 23:50 2


Page 54 of 140 2/1/2017


Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01113/1710:45 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 75.1

Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae E DCB Decachlorobiphenyl 50 26-129 01118117 12:42 01119/17 23:50 2

Tetrachloro-m-xylene 45 31-122 0111811712:42 01119117 23:50 2

Method: MA-EPH. Massachu.setts ·Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

C10·C12 Aliphatics <2.1 2.1 2.1 mg/Kg " 01119117 07:20 01/24/17 20:47

C10-C12 Aromatics <2.1 2.1 2.1 mg/Kg i.' 01/19/17 07:20 01/25/17 00:55

C12-C16 Aliphatics <2.1 2.1 2.1 mg/Kg 0 01/19/1707:20 01/24/17 20:47


C16-C35 Aliphatics 10 2.1 2.1 mg/Kg "' 01/19/17 07:20 01/24117 20:47

C21 ·C35 Aro1natics 2.7 2.1 2.1 mg/Kg " 01/19/17 07:20 01/25/17 00:55



1-Chlorooctadecane 96 40-140 0111g/17 07:20 01124117 20:47 1

o~ Terphenyl 78 40-140 0111g117 07:20 01125117 00:55 1

Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Silver <0.25 0.62 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26

Arsenic 2.5 1.2 0.50 mg/Kg o. 01/16/17 08:55 01/17/17 13:26

Barium 58 1.2 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26

Beryllium 0.20 J 0.37 0.12 mg/Kg " 01/16/17 08:55 01/17/17 13:26

Cobalt 3.4 1.2 0.37 mg/Kg " 01/16/1708:55 01/17/17 13:26

Chromium 6.1 1.2 0.25 mg/Kg " 01/16/17 08;55 01/17/17 13:26

Copper 10 2.5 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26

Nickel 6.6 0.62 0.37 mg/Kg " 01/16/17 08:55 01/17/17 13:26

Lead 39 1.2 0.25 mg/Kg " 01/16/17 08:55 01/17/17 13:26

Selenium <0.50 2.5 0.50 mg/Kg " 01/16/17 08:55 01/17/1713:26

Thallium <0.50 1.2 0.50 mg/Kg " 01/16/17 08:55 01/17/1713:26

Vanadium 7.5 2.5 0.37 mg/Kg " 01/16/17 08:55 01/17/17 13:26

Zinc 61 2.5 0.99 mg/Kg ,, 01/16/17 08:55 01/17/1713:26

Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae

Mercury 0.041 0.013 0.0077 mg/Kg 01/15/1712:43 01/16/17 12:20 1

General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Chromium, hexavalent <3.4 F1 4.9 3.4 mg/Kg ,, 01/20/17 17:00 01/23/1712:07 1

Cyanide, Total <0.17 0.33 0.17 mg/Kg ,, 01/18/1710:53 01/18/1717:37 1

Percent Moisture 24.9 0.1 0.1 % 01117/1714:08

General Chemistry· Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Nitrate Nitrite as N <0.48 F1 1.3 0.48 mg/Kg " 01/16/17 12:30 1


Page 55 of 140 211/2017

Client Sample Results Client: C-K Associates Tes!America Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol

Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 0111311711:00 Matrix: Water

Date Received: 01114117 08:32

Method: 8260C ·Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OH Fae1, 1, 1.2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01/17/1716:13 11, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/l 01/17/17 16:13

1. 1 ,2,2-T etrach!oroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

1, 1,2-Trichloroethane <0.00050 0.0050 0.00050 mg/L 01/17/17 16:13

1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

1, 1-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

1,2,4-Trich!orobenzene <0.00082 0.0010 0.00082 mg/L 01/17/17 16:13

1, 2-Dibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01/17/17 16:13

1,2-Dichlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

1,2-Dich!oroethane <D.00050 0.0010 0.00050 mg/L 01/17/1716:13

1,2-Dich!oropropane <0.00050 0.0010 0.00050 mg/L 01/17/1716:13

1,3-0lchlorobenzene <0.00054 0.0010 0.00054 mg/L 01/17/1716:13

1.4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01/17/17 16:13

2-Butanone (MEK) <0.0026 0.025 0.0026 mg!L 01/17/17 16:13

4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg/L 01/17/17 16:13

Acetone <0.010 0.025 0.010 mg/L 01/17/17 16:13

Benzene <0.00038 0.0010 0.00038 mg/L 01117/17 16:13

Bromoform <0.00071 0.0050 0.00071 mg/L 01/17/17 16:13

Bromomethane <0.0009B 0.0010 0.00098 mg/l 01117/17 16:13

Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

Chlorodibromomethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

Ch!oroethane <0.00076 0.0010 0.00076 mg/L 01/17/17 16:13

Chloroform <0.00060 0.0010 0,00060 mg/L 01/17117 16:13

Ch1oromethane <0.00083 0.0010 0.00083 mg/L 01/17/17 16:13

cls-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

ds-1,3-Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/1711716:13

Dichlorobromomethane <0.00050 0.0010 0.00050 mg/L 01117/1716:13

Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/17/1716:13

lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/17/17 16:13

Methyl tert-butyl ether <0.00074 0.0010 0.00074 mg/L 01/17/1716:13

Methylene Chloride 0.0066 0.0050 0.0030 mg/L 01/17/17 16:13

Styrene <0.0010 0.0010 0.0010 mg/L 01/17/17 16:13

T e!rach!oroethene <0.00058 0.0010 0.00058 mg/L 01/17117 16:13

Toluene <0.00070 0.0010 0.00070 mg/L 01/17/1716:13

trans-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 0111711716:13

trans-1,3-Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/17/1716:13

Trichloroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13

Trich!orofluoromethane <0.00052 0.0010 0.00052 mg/L 01/17/17 16:13

Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01/17/1716:13

Xylenes, Total <0.0016 0.010 0.0016 mg/L 01/17/17 16:13

Surrogate %Recovery Qua/Iner Lilnits Prepared Analyzed DI/ Fae

4-Bromotluoro_benzene 98 78-118 01117117 16:13 1

Dibromoffuoromethane 105 81-121 0111711716:13

Toluene-dB (Surr) 99 80-120 0111711716:13


Page 56 of 140 2/1/2017

m

Client: C-K Associates ProjecVSite: Moffat & Nichol

Client Sample ID: RB-2 Date Collected: 0111311711:00 Date Received: 01/14/17 08:32


Method: 82700 LL. Semivolatlle Organic Compounds by GC/MS ·Low Level Analyte Result Qualifier RL MDL Unit Acenaphthene <0.000031 0.00019 0.000031 mg/l Acenaphthylene <0.000043 0.00019 0.000043 mg/L

Anthracene Benzo[a]anthracene Benzo[a]pyrene

Benzo[b]fluoranthene Benzo[k]fluoranthene

Chrysene Oibenz(a,h)anthracene

Fluoranthene Fluorene lndeno[1,2,3-cd]pyrene

2-Methylnaphtha!ene

Naphthalene Phenanthrene

Pyrene

Surrogate

2-F/uorobiphenyl Nitrobenzene-d5 Terphenyl-d14

<0.000031

<0.000044 <0.000040

<0.000033

<0.000096 <0.000071 <0.000048

<0.000065

<0.00011 <0.000041

<0.000058 <0.000090 <0.000035 <0.000038


77

110

0.00019 0.000031 mg/L 0.00019 0.000044 mg/L 0.00019 0.000040 mg/L 0.00019 0.000033 mg/L

0.00019

0.00019 0.00019 0.00019

0.00019 0.00019

0.00019 0.00019 0.00019

0.00019

Limits 15-122

19-130

33-138

0.000096 mgfl

0.000071 mg/L 0.000048 mg/L 0.000065 mg/L

0.00011 mg/L 0.000041 mglL 0.000058 mg/L

0.000090 mg/L 0.000035 mg/L

0.000038 mg/L

Method: 82700 • Semivola!ile Organic Compounds (GC/MS) Analyte Result Qualifier RL Aniline <0.0037 6.0096

1, 1'-Biphenyl <0.00016 0.0096 Bis(2-chloroethyl)ether <0,0026 0.0096

Pis (2-ch!oro!sopropyl) ether Bis(2-ethythexyl) phthalate

Butyl benzyl phthalate 4-Ch!oroaniline 2-Chloronaphthalene

2-Chlorophenol Olbenzofuran 3,3'-Dichlorobenzidine

2,4-Dtchlorophenol Diethyl phtha!ate 2,4-Dimethylphenol Dimethyl phthalate

1,3-Dinitrobenzene 2,4-Dinitropheno! 2,4-Dlnitrotoluene

2,6-Dinitroto!uene Di-n-octyl phthalate Hexachlorobenzene Hexachlorobutadiene

Hexach!orocyclopentadlene Hexachloroethane lsophorone 2-Nitroanifine

<0.00015 <0.0019

<0.00018 <0.0033

<0.00013

<0.0021 <0.00016

<0.0025

<0.0029

<0.00023 <0.0034

<0.00016 <0.00096

<0.0033

<0.0018 <0.0018

<0.00016 <0.00016

<0.00053

<0.0025 <0.0040

<0.00013 <0.0021

0.0096

0.0096 0.0096 0.0096 0.0096

0.0096 0.0096 0.0096

0.0096 0.0096 0.0096 0.0096

0.0096 0.029

0.0096

0.0096 0.0096 0.0096 0.0096

0.019 0.0096

0.0096 0.0096


0.00016 mg/L 0.0026 mg/L

0.00015 mg/L

0.0019 mg/L 0.00018 mg/L

0.0033 mg/L

0.00013 mg/L 0.0021 mg/L

0.00016 mg/L 0.0025 mg/L

0.0029 mg/L 0.00023 mglL

0.0034 mg/L 0.00016 mg/L

0.00096 mglL 0.0033 mg/L

0.0018 mg/L 0.0018 mg/L

0.00016 mg/L 0.00016 mg/L 0.00053 mg/L

0.0025 mg/L 0.0040 mg/L

0.00013 mg/L 0.0021 mg/L

Page 57 of 140



D Prepared Analyzed 01119/17 15:31 01124/17 16:27 01119/1715:31 01124117 16:27 0111911715:31 01124117 16:27

01119/1715:31 0112411716:27 0111911715:31 01124/1716:27

01119/1715:31 0112411716:27 01119/17 15:31 01124/17 16:27

01/19/17 15:31 0112411716:27 0111911715:31 01/24/17 16:27 01119/17 15:31 0112411716:27

01119/17 15:31 01124117 16:27 0111911715:31 01124117 16:27

01119/1715:31 01124117 16:27 01119117 15:31 01124117 16:27 01119/1715:31 01124/1716:27 01119/1715:31 01124117 16:27

Prepared

0111911715:31

0111911715:31

Analyzed

0112411716:27

0112411716:27

0111911715:31 0112411716:27

DllFac E 1

DH Fae

O Prepared Analyzed Oil Fae 0111911715:31 0112511710:06 01119/1715:31 0112511710:06 01119/1715:31 01125/1710:06

01119/1715:31 01125117 10:06 01119/1715:31 01125/1710:06

01119/1715:31 01125/17 .10:06 01119/1715:31 0112511710:06

01119/1715:31 0112511710:06

01119/1715:31 01/2511710:06 01/19/17 15:31 01125/1710:06

01119/17 15:31 01/25117 10:06

01119/1715:31 0112511710:06 0111911715:31 01125/1710:06 01119/1715:31 0112511710:06 0111911715:31 01/2511710:06

01119/1715:31 01125/1710:06 0111911715:31 01/2511710:06 01119/1715:31 01125/1710:06 01119/1715:31 0112511710:06

01119/1715:31 01125117 10:06 0111911715:31 01125/1710:06

01119/1715:31 01/25117 10:06

0111911715:31 01125117 10:06 0111911715:31 01125/1710:06 01119117 15;31 0112511710:06

01119/17 15:31 01125117 10:06


2/1/2017


Client Sample ID: RB-2 Date Collected: 01/13/1711:00 Date Received: 01 /14/17 08:32


Method: 8270D • Semivolatile Organic Compounds (GC/MSJ (Continued) Analyte Result Qualifier RL MDL Unit 3-Nftroaniline <0.0017 0.0096 0.0017 mg/L

4-Nitroanl!ine Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propy!amine N-Nitrosodiphenyramine Pentachlorophenot Phenol 1,2,4,5-Tetrachlorobenzene

2,3,4,6-Tetrachlorophenol 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trich!oropheno!

Surrogate 2-Fluorobiphenyl

2-Fluorophenol Nitrobenzene-dS

Pheno!-d5 Terphenyf-d14

2,4,6-Tribromophenol

<0.0014

<0.00013 <0.0020 <0.0032

<0.00017 <0.0013 <0.0025

<0.00017

<0.0015 <0.00017

<0.0036

<0.0034

%Recovery Qualifier

78 65 75

75 96

75

0.0096

0.0096 0.0096 0.0096

0.0096 0.019

0.0096 0,0096

0.0096 0.0096 0.0096

0.0096

Limits 46-124

13-113

36-126

17 -127

44-149

26-150

0.0014 mg/L

0.00013 mg/L

0.0020 mg/L 0.0032 mg/L

0.00017 mg/L 0.0013 mg/L

0.0025 mg/L 0.00017 mg/L 0.0015 mg/L

0.00017 mg/L 0.0036 mg/L

0.0034 mg/L

Method: 8270D - Semivolatile Organic Compounds (GCIMSJ • RERA Analyte Result Qualifier RL MDL Unit Aniline <0.0035 H Cl.0093 0.0035 mg/L

1,1'-Biphenyl <0.00016 H 0.0093 0.00016 mg/L Bis(2-chloroethyl)ether <0.0025 H 0.0093 0.0025 mg/L

bis (2-chloroisopropy!) ether

8is(2~ethylhexyl) phtha!ate Butyl benzyl phthalate 4-Chloroanmne 2-Ch!oronaphthalene 2-Chloropheno!

Dibenzofuran 3,3'-Dichlorobenzfdine 2,4-0ich!orophenol Diethyl phthalate 2.4-Dimethylphenol

Dimethyl phtha!ate 1,3-Dinitrobenzene 2,4-Dlnllrophenol

2,4-Dinitrototuene 2,6-Dinitrotoluene Di-n-octyl phthalate Hexach1orobenzene

Hexachlorobutadiene Hexach!orocyclopentadiene Hexachloroethane lsophorone

2-Nitroan!line

<0.00015 H

<0.0019 H <0.00018 H

<0.0031 H <0.00013 H

<0.0020 H <0.00016 H

<0.0024 H

<0.0028 H <0.00022 H

<0.0032 H

<0.00016 H <0.00093 H <0.0031 H'

<0.0018 H <0.0018 H

<0.00016 H

<0.00016 H <0.00051 H

<0.0024 H <0.0039 H

<0.00013 H <0.0020 H

0.0093

0.0093 0.0093

0.0093

0.0093 0.0093 0.0093

0.0093 0.0093 0.0093 0.0093

0.0093 0.0093 0.028

0.0093 0.0093 0.0093

0.0093

0.0093

0.019 0.0093 0.0093 0.0093

0.00015 mg/L

0.0019 rng/L 0.00018 mg/L

0.0031 mg/L

0.00013 mg/L

0.0020 mg/L 0.00016 mg/L

0.0024 mg/L

0.0028 mg/L 0.00022 rng/L

0.0032 mg/L 0.00016 mg/L

0.00093 mg/L 0.0031 mg/L 0.0018 mg/L 0.0018 mg/L

0.00016 mg/L 0.00016 mg/L

0.00051 mg/L

0.0024 mg/L 0.0039 mg/L

0.00013 mg/L

0.0020 mg/L

Page 58 of 140



D Prepared Analyzed OJI Fae E 01/19/1715:31 01/25/17 10:06

D

01/19/1715:31 01/25/1710:06

01/19/1715:31 01/25/1710:06 01/19/1715:31 01/25/1710:06 01/19/1715:31 01/2511710:06 01/1911715:31 01/25117 10:06

01/19/1715:31 01/25/17 10:06 01/19/17 15:31 01/25/17 10:06 01/1911715:31 01/25/1710:06

01/1911715:31 01125/1710:06 01119/1715:31 01/2511710:06 01/19/1715:31 01/25117 10:06

01/19/1715:31 01/25/1710:06

Prepared

0111911715:31

0111911715:31

Analyzed

01125117 10:06

0112511710:06

0111911715:31 0112511710:06

0111911715:31 0112511710:06

01119117 15:31 0112511710:06

0111911715:31 0112511710:06

Prepared 01/27/1711:20

01/27/1711:20

Analyzed 01/3111716:30

01/31/1716:30 01/27/1711:20 01/31/1716:30

01/27/1711:20 01/31/1716:30

01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/17 16:30

01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30

01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30

01127/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30 0112711711:20 01/31/17 16:30

01/27/1711:20 01/31/17 16:30 01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31117 16:30

01/27/1711:20 01/31/1716:30 01/2711711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30

01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30

01127/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30

01/27/1711:20 01/31/1716:30 01/27/1711:20 01/3111716:30

1

1

DI/ Fae

1

1

Oil Fae 1

1

1

1

1

1


2/1/2017

Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol

Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 01/13/1711 :00 Matrix: Water Date Received: 01/14/17 08:32

Method: 8270D • Semivolatile Organic Compounds (GC/MS). RERA (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 3-Nitroaniline <0.0017 H 0.0093 0.0017 mg/L 0112711711:20 01131/17 16:30 1

4-Nitroanjllne <0.0014 H 0.0093 0.0014 mg/L 0112711711:20 01131/17 16:30

Nitrobenzene <0.00012 H 0.0093 0,00012 mg IL 01127117 11:20 01131117 16:30

4-Nitrophenol <0.0019 H 0.0093 0.0019 mg IL 0112711711:20 01131117 16:30

N-Nitrosodi-n-propylamine <0.0031 H 0.0093 0.0031 mg/L 0112711711:20 01131117 16:30

N-Nitrosodfphenylamine <0.00017 H 0.0093 0.00017 mgll 0112711711:20 01131117 16:30

Pentach!orophenol <0.0013 H 0.019 0.0013 mg/L 01127117 11 :20 01131117 16:30

Phenol <0.0024 H 0.0093 0.0024 mg/L 01127/1711:20 01131117 16:30

1,2, 4 ,5-T etrach!orobenzene <0.00017 H 0.0093 0.00017 mg/L 0112711711:20 01131117 16:30

2,3 ,4, 6-T etrachlorophenol <0.0015 H 0.0093 0.0015 mg/L 01127/1711:20 01131117 16:30

1,2,4-Trichlorobenzene <0.00017 H 0.0093 0,00017 mg/L 01127/1711:20 01131117 16:30

2,4,5-Trich!oropheno! <0.0034 H 0.0093 0.0034 mg/L 01127/1711:20 0113111716:30

2,4,6-Trichloropheno! <0.0032 H 0.0093 0.0032 mg/L 01127/1711:20 01/31/17 16:30


2-Fluorobiphenyf 68 46- 124 0112711711:20 01131117 16:30 1

2-Fluorophenol 48 13-113 0112711711:20 0113111716:30 1

Nifrobenzene-d5 69 36-126 0112711711:20 0113111716:30

Phenol-d5 64 17-127 0112711711:20 01131117 16:30 1 Terpheny/-d14 87 44-149 0112711711:20 01131117 16:30 1

2,4,6-Tribromophenol 68 26-150 0112711711:20 0113111716:30

Method: MAVPH. Massachusetts - Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDI. Unit D Prepared Analyzed Oil Fae C6-C8 A!iphatics <0.030 0.030 0.030 mg IL 01/19117 23:24 1

C8-C10 Aliphatics <0.050 0.050 0.050 mgll 01/19117 23:24 C8-C10 Aromatics <0.025 0.025 0.025 mg/L 01/19/17 23:24

Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae a,a,a-Trifluorotoluene (fid) 101 70-130 01119117 23:24 1

a,a,a-Trifluoroto!uene (pid) 105 70-130 01119117 23:24

Method: 8011 • EDB, DBCP, and 1,2,3-TCP (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

1, 2-Dibromo-3-Chloropropane <0.0000056 0.000030 0.0000056 mg/L 01/2311716:25 01/27/17 00:38 1

Surrogate %Recovety Qualifier Limits Prepared Analyzed DJ/ Fae 4-Bromofluorobenzene 105 51-149 0112311716:25 01127117 00:38 1

Method: 80818 - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DllFae

Aldrin <0.0000011 0.000018 0.0000011 mg/L 01119/1710:03 01124117 13:06 1

alpha-BHC <0.0000013 0.000018 0.0000013 mg/L 01119/1710:03 01/24/17 13:06

beta-BHC <0.0000011 0.000018 0.0000011 mg IL 01/19/1710:03 01/24/17 13:06

de!ta-BHC <0.00000076 0.000018 0.0000007 mg/L 01/19/1710:03 01124/17 13:06

6 gamma-BHC (Undane) <0.0000091 0.000018 0.0000091 mg/L 01/19/1710:03 01/24117 13:06

alpha-Chlordane <0.0000015 0.000018 0.0000015 mg/L 01/19/1710:03 01/24/1713:06

gamma-Chlordane <0.0000012 0.000018 0.0000012 mg/L 01/1911710:0> 01124/1713:06

4.4'-DDD <0.0000011 0.000018 0.0000011 mg/L 01/19/1710:03 01/24/17 13:06


Page 59 of 140 2/112017


Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 01/13/1711 :OO Matrix: Water Date Received: 01/14/17 08:32

Method: 8081 B - Organochlorine Pesticides (GC) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

4,4'-DDE <0.00000080 0.000018 0.0000008 mg/L 01/19/1710:03 01/24/17 13:06 1 0

4,4'-DDT <0.0000014 0.000018 0.0000014 mg/L 01/19/17 10:03 01/24/1713:06

Dieldrin <0.0000011 0.000018 0.0000011 mg/L 01/19/1710:03 01/24/17 13:06

Endosulfan I <0.0000011 0.000018 0.0000011 mg/L 01/19/17 10:03 01/24/17 13:06

Endosu!fan II <0.0000027 0.000018 0.0000027 mg/L 01/19117 10:03 01/24/1713:06

Endosulfan sulfate <0.00000076 0.000018 0.0000007 mg/L 01/19/1710:03 01124/17 13:06 6

Endrln <0.0000011 0.000018 0.0000011 mg/L 0111911710:03 01/24/1713:06

Endrin aldehyde <0.0000010 0.000018 0.0000010 mg/L 01/19/1710:03 01/24117 13:06

Endrin ketone <0.0000014 0.000018 0.0000014 mg/L 01/19/17 10:03 01/24/1713:06

Heptachlor <0.0000011 0.000018 0.0000011 mg/L 01/19/17 10:03 01/24/1713:06

Heptach!or epoxlde <0.0000012 0.000018 0.0000012 mg/L 01/19/17 10:03 01/24/17 13:06

Methoxych!or <0.0000015 0.000018 0.0000015 mg/L 01/19/1710:03 01/24/1713:06

Toxaphene <0.00011 0.0011 0.00011 mg/L 01/19/1710:03 01/24/17 13:06


DCB Decachlorobiphenyl 48 10- 130 01119117 10:03 0112411713:06 1

Tetrachloro-m·xy/ene 64 43 .130 01119117 10:03 01124117 13:06

Meth.od: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C10-C12 Aliphatrcs <0.048 0.048 0.048 mg/L 01/2011715:54 01/26/17 17:34 1

C12-C16 A!iphatics <0.048 0.048 0.048 mg/L 01/20/1715:54 01/26/17 17:34

C16-C35 Alip_hatics <0.048 0.048 0.048 mg/L 01/2011715:54 01/26/1717:34

C10-G12 Aromatics <0.048 0.048 0.048 mg/L 01120117 15:54 01/26/17 20:09

C12-C16 Aromatics <0.048 0.048 0.048 mg/L 01/20/17 15:54 01/26/17 20:09

C16-C21 Aromatics <0.048 0.048 0.048 mg/L 01/20/1715:54 01/26/17 20:09

C21-C35 Aromatics <0.048 0.048 0.048 mg/L 01/20/17 15:54 01/26/17 20:09

Surrogate %Recovery Qualifier Limits Prepared Analyzed Oil Fae

1~Chlorooctadecane 97 40-140 01120117 15:54 0112611717:34 1

o-Terphenyl 81 40-140 0112011715:54 01126117 20:09 1

2-Bromonaphthalene 20 40-140 01120117 15:54 01126117 20:09

2-Ffuorobiphenyl 60 40-140 01120117 15:54 01126117 20:09

Method: 6010C - Metals (ICP) Analyte Result Qualifier RL MDL Vnlt D Prepared Analyzed Oil Fae

Silver <0.0020 0.0050 0.0020 mg/L 01/18/17 10:09 01/19/1716:25 1

Arsenic <0.0040 0.010 0.0040 mg/L 01/18/1710:09 01/19117 16:25

Barium 0.0026 J 0.010 0.0020 mg/L 01/18/17 10:09 01/19/17 16:25

Beryllium <0.0010 0.0030 0.0010 mg/L 01/18/1710:09 01/19/17 16:25

Cobalt <0.0030 0.010 0.0030 mg/L 01/18/1710:09 01/19/17 16:25

Chromium <0.0020 0.010 0.0020 m9/L 01/18/1710:09 01/19/1716:25

Copper <0.0020 0.020 0.0020 mg/l 01/18/1710:09 01/19/17 16:25

Nickel <0.0030 0.0050 0.0030 mg/L 01/18/1710:09 01/19/17 16:25

Lead <0.0020 0.010 0.0020 mg/L 01/18/17 10:09 01/19/1716:25

Selenium <0.0040 0.020 0.0040 mg IL 01/18/17 10:09 01/19/1716:25

Tham um <0.0040 0.010 0.0040 mg/L 01/18/17 10:09 01/19/1716:25

Vaqadium <0.0030 0.020 0.0030 mg/L 01/18/17 10:09 01/19/17 16:25

Zinc 0.020 0.020 0.0080 m9/L 01/18/17 10:09 01/19/17 16:25


Page 60 of 140 21112017


Method: 7470A ·Mercury (CVAA) Analyte Result

Mercury <0.000070

General Chemistry Analyte Result

Cyanide, Total <0.0035

Nitrate Nitrite as N <0.018

Chromium, hexava!ent <0.0065


Qual!fier RL MDL Unit 0.00020 0.000070 mg/L


0.0050 0.0035 mgll 0.050 O.D18 mg/L

0.010 0.0065 mg IL

Page 61 of 140


D Prepared Analyzed Oii Fae 01116117 16:27 01118117 13:46 1

El D Prepared Analyzed Dllfac 01117/17 09:30 01117117 14:24 1

01116117 09:36

01114117 09:18


2/1/2017

Definitions/Glossary Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Qualifiers

GC/MSVOA Qualifier Qualifier Description

LCS or LCSD is outside acceptance limlts.

J Result is less than Jhe RL but greater than or equal to the fl.1DL and the concentration is an approximate value.

GC/MS Semi VOA Quallfler Qualifier Description

RPO of the LCS and LCSO exceeds the control limits

8 Compound wasJound in the blank and sample.

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value,

F1 MS and/or MSD Recovery is outside acceptance limits.

F2 MSJMSD RPO exceeds control limits

LCS or LCSD is outside acceptance limits.

H Sample was prepped or analyzed beyond the specified holding time

x Surrogate is outside control limits

GCSemiVOA Quallfler Qualifier Description

B Compound was found in the blank and sample.

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

LCS or LCSD is outside acceptance limits.

Metals Qualifier Quallfler Description

J Result is less 'than ·the RL but greater than or equal to the MDL and the concenfration is an approximate va!Ue.

F1 MS andior MSD Recovery is outside acceptance limits.

General Chemistry Qualifier Qual_lfier Description

F1 MS and/or t.1SD Recovery is outside acceptance Hmits.

F2 MS/MSD RPO exceeds control limits

J Result ls Jess than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary

Abbreviation These commonly used abbreviations may or may not be present in this report.

• Listed under the "D" column to designate that the result Is reported on a dry weight basis

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Oil Fae Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re·analysis, Re·extraction, or additional lniUa! metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum dete'ctable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit {or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

Page 62of140


2/1/2017

Definitions/Glossary Client: C-K Associates ProjecVSite: Moffat & Nichol


Glossary (Continued)

Abbreviation These commonly used abbreviations may or may not be present In this report.

RPO Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEO Toxicity Equivalent Quotient (Dioxin)

Page 63of140


2/1/2017

Surrogate Summary Client: C-K Associates Project/Site: Moffat & Nichol


Method: 8260C - Volatile Organic Compounds by GGIMS Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID 400-132588-1 CK-1 400-132588-2 CK-2

400-132588-3 Duplicate 400-132588-4 CK-3

400-132588-5 CK-4 400-132588-6 CK-5

400-132588-6 MS CK-5

400-132588-6 MSD CK-5 400-132650-1 CK-6 400-132650-2 CK-7

400-132650-3 CK-8 400-132650-4 CK-9

400-132650-5 CK-10

LCS 400-339082/15-A Lab Control Sample

LCS 400-33933012-A Lab Control Sample MB 400-339082/14-A Method Blank

MB 400-33933011-A Method Blank

Surrogate Legend BFB = 4·Bromofluorobenzene DBFf\1 = Dibromofluoromethane

TOL = Tofuene·d8 (Surr)

Percent Surrogate Recovery (Acceptance Limits}

BFB DBFM TOL (72-122) (79-123) (80-120)

100 102 94 100 103 91

102 104 94 99 102 94 104 102 94 98 95 104

100 98 104 98 102 101 104 96 111 112 97 106

101 102 95 117 93 112

107 109 101

97 104 104

93 105 97 95 100 105

96 100 93

Method: 8260C - Volatile Organic Compounds by GGIMS Matrix: Water Prep Type: Total/NA

Lab Sample ID 400-132540-1

400-132650-6

LCS 400-33852911002

LCS 400-33877111002

MB 400-33852914

MB 400-338771/4

Surrogate Legend

Cllent Sample ID RINSATE 1 RB-2

Lab Control Sample

Lab Control Sample

Method Blank Method Blank

BFB = 4·Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene..c.fB (Surr)

BFB

(78-118) 101

98

97

93

98

99

Percent Surrogate Recovery (Acceptance Lin1its)

DBFM TOL

(81-121) (B0-120) 103 102

105

108

104

104

103

99

98

95 99

100

Method: 82700 • Semivolatile Organic Compounds (GCIMS) Matrix: Solid Prep Type: Total/NA

Lab Sample ID 400~ 132588~ 1 400-132588-2

400-132588-3

Client Sample JD CK-1 CK-2

Duplicate

Percent Surrogate Recovery (Acceptance Limits)

FBP

(27-127) 92

49 71

2FP (25-128)

94 73

74

Page 64 of 140

NBZ PHL TPH TBP (15-136) (29-130) (24-146) (10-150)

82 89 109 122

77 75

82

81

78

96

85 93


21112017

Surrogate Summary Client: C-K Associates ProjecVSite: Moffat & Nichol


Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) Matrix: Solid Prep Type: Total/NA


FSP 2FP NSZ

Lab Sample ID Client Sample ID (27-127} (25-128} (15-136}

400-132588-4 CK'3 75 80 67 400-132588-5 CK-4 52 71 56

400-132588-6 CK-5 58 72 57

400-132588-6 MS CK-5 77 78 68

400-132588-6 MSD CK-5 90 86 77 400-132650-1 CK-6 51 57 45 400-132650-2 CK-7 56 64 54 400-132650-3 CK-8 51 59 47 400-132650-4 CK-9 67 68 56 400-132650-5 CK-10 67 76 63

LCS 400-33855619-A Lab Control Sample 78 74 67

MB 400-338556110-A Method Blank 91 88 78

Surrogate Legend

FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol

NBZ = Nitroben2ene-d5 PHL = Phenol-d5

TPH = Terphenyl-d14

TSP= 2,4,6-Tribromophenol

Method: 82700 - Semivolatile Organic Compounds (GCIMS) Matrix: Water

PHL TPH TSP

(29-130) (24-146) (10-150}

82 87 98

73 56 75

74 65 82

78 96 98

87 113 112

57 75 61

67 82 76

61 76 63

68 111 67

77 96 84

75 100 99

89 118 104

Prep Type: Total/NA



400-132650-6

400-132650-6 - RERA

LCS 400-33828412-A

LCS 400-33912512-A

LCS 400-34007912-A

LCSD 400-33828413-A

LCSD 400-33912513-A

LCSD 400-34007913-A

MB 400-33828411-A

MB 400-33912511-A

MB 400-34007911-A

Surrogaie Legend FBP = 2-Fluorobipheny! 2FP = 2-Fluorophenol NBZ = Nitrobenzene-d5 PHL = Phenol-dS TPH = Terphenyl-d14

Client Sample ID RINSATE 1

RB-2

RB-2

Lab Control Sample Lab Control Sample

Lab Control Sample Lab Control Sample Dup

Lab Control Sample Dup

Lab Control Sample Oup Method Blank Method Blank

Method Blank

TSP = 2,4,6-Tribromophenol

FBP

(46-124)

72

78

68

69

85

64 74

91

74

76

91

66

2FP

(13-113}

47

65

48

48

66

30

60

35

58

61

42

38

Page 65 of 140

NBZ PHL TPH TSP

(36-126} (17-127) (44-149) (26-150}

73 66 98 70

75 75 96 75

69 64 87 68

70 67 92 80

81 57 95 95

66 58 76 68

75 74 101 88

85 42 107 53

78 76 90 79

76 73 104 78

88 54 112 61

69 57 88 28


2/1/2017



Method: 82700 LL - Semivolatile Organic Compounds by GCIMS ·Low Level Matrix: Water Prep Type: Total/NA


400-132650-6

LCS 400-33828412-A

LCS 400-33912512-A

LCSD 400-33828413-A

LCSD 400-339125/3-A

MB 400-338284/1-A

MB 400-33912511-A

surrogate Legend

FBP = 2~Fluorobiphenyl

NBZ ::::: Nitrobenzene-d5

TPH = Terphenyl-d14


RB-2

Lab Control Sample Lab Control Sample

Lab Control Sample Oup Lab Control Sample Dup Method Blank

Method Blank

FBP

(15-122)

92

92

80

114

86

105

108

116

Percent surrogate Recovery (Acceptance Lln1lts)

NBZ TPH

(19-130) (33-138)

M 107

77 110 91

100

92

91

100

101

89

132

92

117 140 x 135

Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA

Lab Sainple ID Client Sainple ID 400-132588-1 CK-1

400-132588-2 CK-2

400-132588-3 Duplicate 400-132588-4 CK-3

400-132588-5 CK-4

400-132588-6 CK-5

400-132588-6 MS CK-5

400-132588-6 MSD CK-5

400-132650-1 CK-6

400-132650-2 CK-7

400-132650-3 CK-8

400-132650-4 CK-9

400-132650-5 CK-10

LCS 400-33860412-A lab ContrQI Sample LCSD 400-33860413-A Lab Control Sample Oup

MB 400-338604/1-A Method Blank

Surrogate Legend

TFT = a,a,a-TrifJuoroto!uene (fid)

TFT2

(70-130)

77

74

79

76 75

79

79

94

79

72

83

93

113

107

100

75


TFT1

(70-130)

80

75

79

77

75

81

79

93

78

74

86

92

113

109

101

76

Method: MAVPH • Massacliusetts. Volatile Petroleum Hydrocarbons (GC) Matrix: Water Prep Type: Total/NA


400-132650-6

LCS 400-33905713

LCSD 400-339057/4

Client Sample IP RINSATE 1

RB-2

Lab Control Sample Lab Control Sample Dup

TFT2

(70-130)

101

101

107

105


TFT1

(70-130)

103

105

108

107


Page 66 of 140 2/112017

Surrogate Summary Client: C-K Associates ProjecVSite: Moffat & Nichol


Method: MAVPH • Massachusetts ·Volatile Petroleum Hydrocarbons (GC) (Continued) Matrix: Water Prep Type: Total/NA

Lab sample ID MB 400:339657/2

Surrogate Legend

Client Sample ID Method Blank

TFT = a,a,a-Trifluorotoluene (fid)

TFT2

(70-130)

106

Method: 8011. EDB, DBCP, and 1,2,3-TCP (GC) Matrix: Waler


400-132650-6

LCS 400-339493/2-A

LCSD 400-339493/3-A

MB 400-339493/1-A

Surrogate Legend


RB-2

Lab Control sample Lab Control Sample Dup Method Blank

BFB = 4-Bromofluorobenzene

BFB1

(51-149)

113

105

97

108

109

Method: 80818 • Organoch!orine Pesticides (GC) Matrix: Solid

Lab Sample ID Client Sample ID 400-132588-1 CK-1

400-132588-2 CK-2

400-132588-3 Duplicate 400-1325884 CK-3

400-132588-5 CK-4

400-132588-6 CK-5

400-132588-6 MS CK-5

400-132588-6 MSD CK-5

LCS 400-338557/9-A Lab Control Sample MB 400-338557/10-A Method Blank

Surrogate Legend

DCB = DCB Decachlorobiphenyl TCX = Tetrachloro-m-xylene

OCB1 (26-129)

53

46

62

48

41

62

81

67

86

99

Method: 8081 B • Organochlorine Pesticides (GC) Matrix: Solid

DCB2

Lab Sample 10 Client Sample ID (26-129)

400-132650-1 CK-6 45 400-132650-2 CK-7 44 400-132650-3 CK-8 58


TFT1

(70-130)

106

Prep Type: Total/NA


Prep Type: Total/NA

Percent Surrogate Recovery (Acceptance Limits} TCX1

(31-122)

46

44

52

42

41

62

83

68

85

95

Prep Type: Total/NA


TCX2 (31-122)

41

49

52


Page 67 of 140 2/112017

Surrogate Summary Client C-K Associates Projecl/Site: Moffat & Nichol


Method: 80818 • Organochlorine Pesticides (GC) (Continued) Matrix: Solid Prep Type: Total/NA

Lab Sample ID 400:1:i2sso-4

400-132650-5

Surrogate Legend

Client Sample ID CK-9

CK-10

DCB = DCB Decachtorobiphenyl

TCX = Tetrachloro-m-xylene

DCB2

(26-129)

57

50

Method: 80818 • Organochlorine Pesticides (GC) Matrix: Water

Lab Sample ID Client Sample ID 400-132540-1 RINSATE 1

400-1326.50-6 RB-2

LCS 400-33823912-A Lab Control Sample LCS 400-33905412-A Lab Control Sample LCSD 400-33823913-A Lab Control Sample Oup LCSD 400-33905413-A Lab Control Sample Dup MB 400-33823911-A Method Blank MB 400-33905411 ·A Method Blank

Surrogate Legend

DCB == DCB Decachlorobiphenyl

TCX = Tetrachloro-m-xylene

DCB1

(10-130)

55

48

67

53

52

106

56

93


TCX2

(31-122)

52

45

Prep Type: Total/NA


TCX1

(43-130)

99

64

88

77

91

68

99

69

Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA


1COD1

Lab Sample ID Client Sample ID (40-140)

400-132588-1 CK-1 88

400-132588-2 CK-2 86

400-132588-3 Duplicate 1.0J 400-132588-4 CK-3 96

400-132588-5 CK-4 80

400-132588-6 CK-5 83

400-132588-6 MS CK-5 88 400-132588-6 MSD CK-5 82

400-132650-1 CK-6 98

400-132650-2 CK-7 86 400-132650-3 CK-8 85

400-132650-4 CK-9 86

400-132650-5 CK-10 96 LCS 400-339010114-A Lab Control Sample 98

LCSD 400-339010115-A Lab Control Sample Dup 106

MB 400.-339010116-A Method Blank 95

Surrogate Legend


Page 68 of 140 2/1/2017



1COD = 1-Ch!orooctadecane

Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA

Percent Surrogate Recovery (Acceptance Limits) OTPH1

Lab Sample ID Cllent Sample ID (40-140)

400-132588-1 CK-1 66

400-132588-2 CK-2 79

400-132588-3 Duplicate 94

400-132588-4 CK-3 72

400-132588-5 CK-4 84

400-132588-6 CK-5 70

400-132588·6 MS CK-5 86

400-132588-6 MSD CK-5 99

400-132650-1 CK-6 98

400-132650-2 CK-7 81

400-132650-3 CK-8 78

400-132650-4 CK-9 74

400-132650-5 CK-10 78

LCS 400-339010/14-A Lab Control Sample 123

LCSD 400-339010/.15-A Lab Control Sample Oup 118

MB 400-339010/16-A Method Blank 83

Surrogate Legend

OTPH = o·Terphenyl

Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Water Prep Type: Total/NA

Percent surrogate Recovery (Acceptance Limits}


400-132650-6

LCS 400-339262/2-A

LCSD 400-339262/3-A

MB 400-33926211-A

Surrogate Legend


RB-2

Lab Control Sample Lab Control Sample Dup Method Blank

1 COD = 1-Chlorooctadecane

1COD1

(40-140)

89

97

84

81

79

Method: MA~EPH - Massachusetts - Extractable Petro.leum Hydrocarbons (GC) Matrix: Waler Prep Type: Total/NA



400-132650-6

LCS 400-339262/2-A

LCSD 400-339262/3-A

MB 400-339262/1-A

Surrogate Legend

Client Sample 10 RINSATE 1

RB-2

Lab Control San1ple Lab Control Sample Dup

Method Blank

OTPH1

(40-140)

63

81

85

83

73

2BN1 FBP1

(40-140) (40-140)

14 46

20 60

50 121

32 74

57 119

Page 69of140


2/1/2017


OTPH::: o-Terphenyl 2BN = 2-Bromonaphthalene FBP ::: 2-Fluorobipheny!

Surrogate Summary

Page 70 of 140



2/1/2017

QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Method: S260C - Volatile Organic Compounds by GC/MS

Lab Sample ID: MB 400-338529/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis.Batch: 338529

MB MB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dll Fae

1, 1, 1,2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01116117 09:19 1 1, 1, 1 -Trichloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19

1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19

1, 1,2-Trichloroethane <D.00050 0.0050 0.00050 mgll 01116117 09:19 E 1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19

1, 1-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:19

1,2-Dibron10-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01116117 09:19

1,2-0ich)orobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19

1,2-Dichloroethane <0.00050 0.0010 0.00050 mg IL 01116117 09:19

1,2-Dich!oropropane <0.00050 0.0010 0.00050 mg IL 01116117 09:19

1,3-Dichlorobenzene <0.00054 0.0010 0.00054 mg/L 01116117 09:19

1.4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01116117 09:19

Acetone <0.010 0.025 0.010 mg IL 01116117 09:19

Benzene <0.00038 0.0010 0.00038 mg/L 01116117 09:19

Bromofonn <0.00071 0.0050 0.00071 mg/L 01116117 09:19

Bromomethane <0.00098 0.0010 0.00098 mg/L 01116117 09:19

Carbon disulfide <0.00050 0.0010 0.00050 mg IL 01116117 09:19

Carbon tetrachloride <0.00050 0.0010 0.00050 mgll 01116117 09:19

Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19

Chlor.odib'romonlethane <0.00050 0.0010 0.00050 mg IL 01116117 09:19

Chloroethane <0.00076 0.0010 0.00076 mQIL 01116117 09:19

Chloroform <0.00060 0.0010 0.00060 mg/L 01116117 09:19

Chloromethane <0.00083 0.0010 0.00083 mg IL 01116117 09:19

cis· 1,2·Dichloroethene <0.00050 0.0010 0.00050 mg IL 01116117 09:19

Cis· 1, 3·Dich!oropropene <0.00050 0.0050 0.00050 mg IL 01116117 09:19

Dichlorobromomethane <0.00050 0.0010 0.00050 mg IL 01116/17 09:19

2-Butanone (MEK) <0.0026 0.025 0.0026 mgll 01116117 09:19

Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19

4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mgll 01116117 09:19

Methyl tert·butyl ether <0.00074 0.0010 0.00074 mg/L 01116117 09:19

Methylene Ch.loride <0.0030 0.0050 0.0030 mg/L 01116117 09:19

Styrene <0.0010 0.0010 0.0010 mgll 01116117 09:19

Tetrach!oroethene <0.00058 0.0010 0.00.058 mg IL 01116117 09:19

Toluene <0.00070 0.0010 0.00070 mg IL 01116117 09:19

trans· 1,2·Dichloroethene <0.00050 0.0010 0.00050 mg IL 01116117 09:19

trans· 1,3·Dfchloropropene <0.00050 0.0050 0.00050 mg IL 01116117 09:19

Trichtoroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:19

Trichlorofluoromethane <0.00052 0.0010 0.00052 mg IL 01116117 09:19

1,2,4·Trichtorobenzene <0.00082 0.0010 0.00082 mg/L 01116117 09:19

Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01116117 09:19

lsobutyl alcohol <0.010 0.025 0.010 mg/L 01116117 09:19

Xylenes, Total <0.0016 0 . .010 0.0016 mg IL 01116/17 09:19

MB MB Surroga.te %Recovery Qualifier Limits Prepared Analyzed Dll Fae 4·Bromofluorobehzene 98 78-118 01116117 09:19 1

Dibromoffuoromethane 104 81-121 01116117 09:19 1

Toluene-dB (SutT) gg 80-120 01116117 09:19


Page71 of140 2/1/2017


QC Sample Results TestAmerica Job ID: 400-132540-1

Method: 8260C ·Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: LCS 400·33852911002 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338529

Spike LCS LCS %1Rec.

Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0516 mg/L 103 67 -131

1, 1, 1 -Trichloroethane 0.0500 0.0505 mg/L 101 68-130

1, 1,2,2-Tetrachloroethane 0.0500 0.0511 mg/L 102 70-131

1, 1,2-Trichloroethane 0.0500 0.0482 mg IL 96 70-130

1, 1-Dichloroethane 0.0500 0.0521 mg/L 104 70-130 1, 1-Dich!oroethene 0.0500 0.0603 mg/L 121 63-134

1,2-Dlbromo-3-Chloropropane 0.0500 0.0589 mg/L 118 54-135

1,2-Dichlorobenzene 0.0500 0.0479 mg IL 96 67 -130 1,2-Dich!oroethane 0.0500 0.0492 mg/L 98 69-130

1,2-Dichloropropane 0.0500 0.0468 mglL 94 70-130

1,3-Dichlorobenzene 0.0500 0.0467 mg/L 93 70-130

1,4-Dich!orobenzene 0.0500 0.0469 mg/L 94 70-130

Acetone 0.200 0.251 mg/L 125 43-160

Benzene 0.0500 0.0491 mglL 98 70- 130

Bromofonn 0.0500 0.0713 mg/L 143 57 -140 Bromomethane 0.0500 0.0496 mg/L 99 10-160

Carbon disulfide 0.0500 0.0562 mg IL 112 61 - 137

Carbon tetrachloride 0.0500 0.0580 mg/L 116 61 - 137

Ch!orobenzene 0.0500 0.0479 mg/L 96 70-130

Chlorodibromomethane 0.0500 0.0564 mg IL 113 67 -135

Chloroethane 0.0500 0.0522 mg/L 104 55-141

Ch!orofonn 0.0500 0.0507 mglL 101 69-130

Chloromethane 0.0500 0.0500 mglL 100 58-137

cis-1,2-Dichloroethene 0.0500 0.0513 mg/L 103 68-130

cis-1,3-Dichloropropene 0.0500 0.0475 mg IL 95 69-132

Dichlorobromomethane 0.0500 0.0511 mglL 102 67-133

2·Butanone (MEK) 0.200 0.203 mg IL 102 61-145

Ethylbenzene 0.0500 0.0480 mg/L 96 70-130

4-Methyl-2-pentanone (MIBK) 0.200 0.202 mglL 101 69-138 Methyl tert-butyl ether 0.0500 0.0497 mg/L 99 66-130

Methylene Chloride 0.0500 0.0532 mg/L 106 66-135

Styrene 0.0500 0.0445 mg IL 89 70-130

Tetrachloroethene 0.0500 0.0544 mg IL 109 65-130

Toluene 0.0500 0.0469 mg/L 94 70-130

trans-1,2-Dichloroethene 0.0500 0.0544 mg/L 109 70-130

trans-1,3-Dich!oroprppene 0.0500 0.0458 mg/L 92 63-130 Trichloroethene 0.0500 0.0519 mg IL 104 70-130

Trichlorofluoromethane 0.0500 0.0546 mg IL 109 65-138

1,2,4~Trichlorobenzene 0.0500 0.0492 mg/L 98 60-140

Vinyl chloride 0.0500 0.0538 mg/L 108 59-136 Xylenes, Total 0.100 0.0940 mg/L 94 70-130

LCS LCS Surrogate %Recovery Qualifier Limits

4-Bromonuorobenzene 97 78-118

Dibromoftuoromethane 108 81" 121 Toluene-dB (Surr) 98 80-120


Page 72 of 140 2/1/2017

E1

QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol

Method: 8260C ·Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: MB 400-338771/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 338771

MS MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

1, 1, 1,2-Tetrach!oroethane <0.00052 0.0010 0.00052 mg/L 01/17/17 15:21 1 1, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

1, 1,2-Trichloroethane <0.00050 0.0050 0.00050 mg/L 01/17/1715:21

E 1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

1, 1-Dichloroethene <0.00050 0.0010 0.00050 rng/L 01/17/17 15:21

1,2-Dibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01/17/17 15:21

1,2-Dichlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

1,2-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

1,2-Dichloropropane <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

1,3-Dich!orobenzene <0.00054 0.0010 0.00054 mg/L 01/17/17 15:21

1,4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01/17/17 15:21

Acetone <0.010 0.025 0.010 mg/L 01/17/17 15:21

Benzene <0.00038 0.0010 0.00038 mg/L 01/17/17 15:21

Bromoform <0.00071 0.0050 0.00071 mg/L 01/17/17 15:21

Bromomethane <0.00098 0.0010 0.00098 mg/L 01/17/1715:21

Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

Chlorodibromon1ethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

Ch!oroethane <0.00076 0.0010 0.00076 mg/L 01/17/17 15:21

Chloroform <0.00060 0.0010 0.00060 mg/L 01/17/17 15:21

Chloromethane <0.00083 0.0010 0.00083 mg/L 01/17/17 15:21

cis-1 ,2-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21

cis-1,3-Dichloropropene <0.00050 0.0050 0,00050 mg/L 01/17/17 15:21

Dichlorobromomethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

2-Butanone (MEK) <0.0026 0.025 0.0026 mg/L 01/17/17 15:21

Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg/L 01/1711715:21

Methyl tert-butyl ether <0.00074 0.0010 0.00074 mg/L 01/17/17 15:21

Methylene Chloride <0.0030 0.0050 0.0030 mg/L 01/17/17 15:21

_Styrene <0.0010 0.0010 0.0010 mg/L 01/17/17 15:21 Tetrachloroethene <0.00058 0.0010 0.00058 mg/L 01/17/1715:21

Toluene <0.00070 0.0010 0.00070 mg/L 01/17/1715:21

trans-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01117/1715:21

trans-1,3-Dich loropropene <0.00050 0.0050 0.00050 mg/L 01/17/1715:21

Trichloroethene <0.00050 0.0010 0.00050 mg/L 01117/1715:21

Trichlorofluoro1nethane <0.00052 0.0010 0.00052 mg/L 01/17/1715:21

1,2,4-Trichlorobenzene <0.00082 0.0010 0.00082 mg/L 01/17/17 15:21

Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21

lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/17/1715:21

Xylenes, Total <0.0016 0.010 0.0016 mg/L 01/17/17 15:21

MB MB Surrogate %Recovery Qualifier Limits _Pre pa, red Analyzed DI/ Fae

4-Brotnofluorobenzene 99 78-118 0111711715:21 1

Dibromofluoro1nethane 103 81.121 0111711715:21

Toluene--d8 (Surr) 100 80-120 01117117 15:21


Page 73 of 140 2/1/2017



Method: S260C ·Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: LCS 400-338771/1002 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338771

Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0475 mg/L 95 67 -131 1, 1, 1-Trichloroethane 0.0500 0.0506 mg/L 101 68 -130

1, 1,2,2-Tetrach!oroethane 0.0500 0.0407 n1g/L 81 70-131 1, 1,2-Trichloroethane 0.0500 0.0445 mg/L 89 70 -130

1, 1-Dich!oroethane 0.0500 0.0526 mg/L 105 70-130

1, 1-Dichforoethene 0.0500 0.0598 mg/L 120 63-134

1,2-Dibromo-3-Ch!oropropane 0.0500 0.0458 mgll 92 54-135

1,2-Dich!orobenzene 0.0500 0.0427 mg/L 85 67 -130 1,2-Dichloroethane 0.0500 0.0472 mg IL 94 69 -130

1,2-Dichloropropane 0.0500 0.0470 mg IL 94 70-130

1,3-Dich!orobenzene 0.0500 0.0439 mg IL 88 70-130

1,4-Dichlorobenzene 0.0500 0.0422 mg/L 84 70-130 Acetone 0.200 0.215 mg/L 108 43-160

Benzene 0.0500 0.0500 mg/L 100 70 -130

Bromofonn 0.0500 0.0578 mg/L 116 57 .140

Bromomethane 0.0500 0.0433 mg/L 87 10-160

Carbon disulfide 0.0500 0.0575 mg/L 115 61-137

Carbon tetrachloride 0.0500 0.0583 mg/L 117 61 -137

Ch!orobenzene 0.0500 0.0470 mg IL 94 70-130

Chlorodibromon1ethane 0.0500 0.0508 mg IL 102 67 -135

Chloroethane 0.0500 0.0519 mg/L 104 55-141

Chloroform 0.0500 0.0505 n1g/l 101 69 -130

Chloromethane 0.0500 0.0484 1ng/l 97 58-137

cis-1,2-0ichloroethene 0.0500 0.0502 mg/L 100 68-130

cis-1,3-Dichloropropene 0.0500 0.0467 mg IL 93 69-132

Dichlorobromomethane 0.0500 0.0494 mg/L 99 67 -133

2-Butanone (MEK) 0.200 0.184 mg/L 92 61-145

Ethyfbenzene 0.0500 0.0482 mglL 96 70.130

4-Methyl-2-pentanone (MIBK) 0.200 0.184 mg/L 92 69-138

Methyl tert-butyl ether 0.0500 0.0465 mg/L 93 66-130

Methylene Chloride 0.0500 0.0585 mg IL 117 66 -135

Styrene 0.0500 0.0441 mg/L 88 70-130

T etrachloroethene 0.0500 0.0565 mglL 113 65 -130

Toluene 0.0500 0,0465 mg/L 93 70 -130

trans-1,2-Dichloroethene 0.0500 0.0548 mg IL 110 70.130

trans-1,3-Dich!oropropene 0.0500 0.0425 mg/L 85 63-130 Trichloroethene 0.0500 0.0544 mg IL 109 70 .130

Trichlorofluoromethane 0.0500 0.0515 mg IL 103 65-138

1,2,4-Trichlorobenzene 0.0500 0.0443 mg/L 89 60 -140

Vinyl chloride 0.0500 0.0525 mg/L 105 59-136

Xylenes, Total 0.100 0.0934 mg/L 93 70-130

LCS LCS Surrogate %Recoyery Qualifier Limits 4~Bromofluorobenie,ne 93 78-118 Dibromofluoromethane 104 81- 121 Toluene-dB (Surr) 95 80-120


Page 74 of 140 2/1/2017

E

QC Sample Results Client: C-K Associates ProjecUSite: Moffat & Nichol

Method: S260C ·Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: MB 400·339082114-A Matrix: Solid Analysis Batch: 339083

Analyte

1, 1, 1,2-T etrach!oroethane 1, 1, 1-Trichloroethane

1, 1,2,2-Tetrach!oroethane 1, 1,2-Trichloroethane

1, 1-Dichloroethane 1, 1-Dlchloroethene

1,2-Dibromo-3-Chforopropane

1,2-Dichlorobenzene 1,2-Dichloroethane

1,2-Dichloropropane 1,3-Dichlorobenzene

1,4-D!chlorobenzene Acetone Benzene Bromofonn Bromomethane Carbon disulfide



Chloroethane

Chloroform Ch!oromet11ane

cis-1,2-Dich!oroethene c!s-1,3-Dichloropropene

Dichforobromomethane 2-Butanone (MEK)

Ethyfbenzene



Methylene Chloride Styrene Tetrach!oroethene


trans-1,3-Dichloropropene Trichloroethene Trichtorofluoromethane

1,2,4-Trichtorobenzene Vinyl chloride lsobutyl alcohol Xylenes, Total

Surrogate 4-Bromofluorobenzene

Dibromofluoromethane Toluene-dB (Surr)

MB MB Result Qualifier

<0.0025 <0.0011

<0.0025 <0.0025

<0.00083 <0.0025

<0.0033

<0.00071 <0.00082

<0.0025 <0.00095

<0.0025 <0.0073

<0.00067

<0.0025 <0.0025 <0.0025

<0.0017 <0.00052 <0.0025

<0.0025 <0.0025 <0.0010

<0,00076

<0.0012 <0.0025 <0.0060

<0.00061

<0.0050 <0.0010

<0,010

<0.0010 <0.0025

<0.0010 <0.0025

<0,0025 <0.0010 <0.0025

<0.0020 <0.0025

<0.010

<0.0019

MB MB %Recovery Qualifier

95 100

105

RL 0.0050 0.0050 0.0050 0.0050

0.0050 0.0050 0.0050

0.0050 0.0050 0.0050

0.0050

0.0050 0.025

0.0050 0.0050 0.0050

0.0050 0.0050

0.0050 0.0050 0.0050

0.0050 0.0050 0.0050

0.0050 0.0050 0.025

0.0050

0.025 0.0050

0.015 0.0050 0.0050

0.0050 0.0050

0.0050 0.0050

0.0050

0.0050 0.0050

0.025

0.010

Limits 72 .122

79-123 BO- 120


0.0025 mg/Kg 0.0025 mg/Kg

0.00083 mg/Kg 0.0025 mg/Kg

0.0033 mg/Kg

0.00071 mg/Kg 0.00082 mg/Kg

0.0025 mg/Kg 0.00095 mg/Kg

0.0025 mg/Kg 0.0073 mg/Kg

0.00067 mg/Kg

0.0025 mg/Kg 0.0025 mg/Kg

0.0025 mg/Kg 0.0017 mg/Kg

0.00052 mg/Kg 0.0025 mg/Kg 0.0025 mg/Kg

0.0025 mg/Kg 0.0010 mg/Kg

0.00076 mg/Kg 0.0012 mg/Kg

0.0025 mg/Kg 0.0060 mg/Kg

0.00061 mg/Kg

0.0050 mg/Kg 0.0010 mg/Kg

0.010 mg/Kg

0.0010 mg/Kg 0.0025 mg/Kg

0.0010 mg/Kg

0.0025 mg/Kg

0.0025 mg/Kg 0.0010 mg/Kg

0.0025 mg/Kg 0.0020 mg/Kg 0.0025 mg/Kg

0.010 mg/Kg

0.0019 mg/Kg

Page 75 of 140


Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339082

D Prepared Analyzed 01/19/17 08:59 01/19/17 11:47 01/19/1708:59 01/19/1711:47

01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/17 11:47

01/19/17 08:59 01/19/17 11:47 01/19/17 08:59 01/19/1711:47

01/19/17 08:59 01/19/1711:47

01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47 01/19/1708:59 01119/1711:47

01/19/17 08:59 01/19/1711:47

01/19117 08:59 01/19/17 11:47 01/19/17 08:59 01/19/1711:47

01/19/1708:59 01/19/1711.:47 01/19117 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47

01/19/17 08:59 01/19/1711:47

01/19/17 08:59 01/19/1711:47 01/19/1708:59 01/19/1711:47

01/19/1708;59 01/19/1711:47

01/19/17 08:59 01/19/1711:47 01119117 08:59 01119/1711:47

01/19/17 08:59 01119/1711:47

01119/1708:59 01/19/1711:47 01119/17 08:59 01/1911711:47 01/19/17 08:59 01/19/1711:47 01/19/1708:59 01/19/1711:47

01/19/17 08:59 01/19/17 11:47 01/19/17 08:59 01/19/17 11:47

01/19117 08:59 01119/1711 :47

01/19/1708:59 01119/1711:47 01/19/17 08:59 01/1911711:47

01/19117.08:59 01119/1711:47 01/19/17 08:59 01119/1711:47

01/19117.08:59 01119/1711:47 01119117 08:59 01/1911711:47

01/19/1708:59 01/1911711:47 01/19117 08:59 01/19/1711:47

01/19/17 08:59 01/1911711:47 01/19/17 08:59 01119/17 11:47

01/19/1708;59 0111911711:47

Prepared Analyzed 0111911708.'59 0111911711:47

01119117 08:99 0111911711:47

01119117 08:59 0111911711:47

Oil Fae

1

DI! Fae 1 1

1


2/1/2017

Client: C-K Associates Project/Site Moffat & Nichol


Method: 8260C ·Volatile Organic Compounds by GC/MS {Continued)

Lab Sample ID: LCS 400·339082115-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339083 Prep Batch: 339082

Spike LCS LCS 0/oRec. Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0492 mg/Kg 96 65-130

1, 1, 1 -Tr!chloroethane 0.0500 0.0479 mg/Kg 96 63-130

1, 1,2,2-Tetrach!oroethane 0.0500 0.0500 mg/Kg 100 60-131

1, 1,2-Trichloroethane 0.0500 0.0489 mg/Kg 98 65-130

1, 1 -Dichloroethane 0.0500 0.0484 mg/Kg 97 59-130

1, 1 -Dich!oroethene 0.0500 0.0489 mg/Kg 98 55-137

1,2-Dibromo-3-Ch!oropropane 0.0500 0.0468 n1g/Kg 94 49 -130

1,2-Dichlorobenzene 0.0500 0.0495 mg/Kg 99 64 -130

1,2-Dichforoethane 0.0500 0.0472 mgl!<g 94 62-130

1,2-Dichloropropane 0.0500 0.0477 mg/Kg 95 64-130

1,3-Dichlorobenzene 0.0500 0.0467 mg/Kg 97 66-13.0

1,4-Dichlorobenzene 0.0500 0.0483 mg/Kg 97 65-130

Acetone 0.200 0.197 mg/Kg 98 46-160

Benzene 0.0500 0.0476 mg/Kg 95 65-130

Bromofonn 0.0500 0.0455 mg/Kg 91 52-136

Bromomethane 0.0500 0.0644 mg/Kg 129 12-160

Carbon disulfide 0.0500 0.0455 mg/Kg 91 46-141

Carbon tetrachloride 0.0500 0.0491 n1g/Kg 98 60-130

Ch!orobenzene 0.0500 0.0495 mg/Kg 99 70-130

Chlorodibromomethane 0.0500 0.0463 mg/Kg 97 58-132

Chloroethane 0.0500 0.0493 mg/Kg 99 55-134

Chforofonn 0.0500 0.0476 mg/Kg 95 62-130

Chloromethane 0.0500 0.0461 mg/Kg 92 49-136

cis-1,2-Dichloroethene 0.0500 0.0467 mg/Kg 93 53-135

cis· 1,3-Dich!oropropene 0.0500 0.0456 mg/Kg 91 61-130

Dichlorobromomethane 0.0500 0.0466 mg/Kg 93 61-130

2-Butanone (MEK) 0.200 0.200 mg/Kg 100 55-130

Ethylbenzene 0.0500 0.0494 mg/Kg 99 70-130

4-Methyl-2-pentanone (MIBK) 0.200 0.193 mg/Kg 96 56-130

Methyl tert-butyl ether 0.0500 0.0434 mg/Kg 87 63-130

Methylene Chloride 0.0500 0.0429 mg/Kg 86 57. 132

Styrene 0.0500 0.0490 mg/Kg 98 66-130

Tetrach!oroethene 0.0500 0.0461 mg/Kg 92 67 -130

Toluene 0.0500 0.0495 mg/Kg 99 70-130

trans-1,2-Dichloroethene 0.0500 0.0483 mg/Kg 97 58 .134

trans-1,3-Dichloropropene 0.0500 0.0452 mg/Kg 90 60-130

Trichloroethene 0.0500 0.0508 mg/Kg 102 65-130

TrichlorofJuoromethane 0.0500 0.0453 mg/Kg 91 61 -136

1,2,4-Trichlorobenzene 0.0500 0.0487 mg/Kg 97 56-138

Vlnyl chloride 0.0500 0.0472 mg/Kg 94 52-132

Xylenes, Total 0.100 0.0975 mg/Kg 97 70-130

LCS LCS Surrogate %Recovety Quallfler Limits 4-Bromonuorobenzene 97 72-122 Dibromonuoromethane 104 79-123 ToJuene-<.:18 (Surr) 104 80-120


Page 76 of 140 2/112017

E


QC Sample Results

Method: 8260C - Volatile OrganicCompounds byGC/MS (Continued)

Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 339083

Analyte

1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichloroethane

1, 1,2,2-Tetrachloroethane 1, 1 ,2-Trichloroethane

1, 1-Dich!oroethane 1, 1-Dlchloroethene 1,2-Dibromo-3-Chloropropane

1,2-Dich!orobenzene 1,2-Dichloroethane

- 1,2-Dichloropropane

1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene

Bromofonn Bromomet!iane Carbon disulfide Carbon tetrachloride

Chlorobenzene Ch!orodibromomethane

Chloroethane

Chloroform Ch!oromethane

_cis-1,2-Dichloroethene ds-1,3-Dichloropropene

Dichlorobron1omethane Ethylbenzene Methyl tert-butyl ether



Styrene Tetrachloroethene


trans-1,3-Dichforopropene Trich!oroethene

Trichlorofluoron1ethane Vinyl chloride

Xy!enes. Total 1,2,4-Trichlorobenzene

surrogate 4-c:Bromonuorobenzene Dibromonuoron;etbane To/uene-d8 (Surr)

Sample San1ple

Result Qualifier

<0.21 <0.093 <0.21

<0.21

<0.070 <0.21 <0.28

<0.060 <0.069

<0.21 <0.080

<0.21 <0.61

<0.056 <0.21

<0.21

<0.21

<0.14

<0.044 <0.21

<0.21

<0.21 <0.084

<0.064 <0,10 <D.21

<0.051 <0.084 <0.84

<0.50 <0.42

<0.084 <0.21

0.62 <0.21 <0.21

<0,084

<0.21 <0.21

<0.16

<0.17

MS MS %1(ecov_ety Qu_allfler

100

98 104

Spike

Added 4.21 4.21 4.21

4.21

4.21 4.21

4.21

4.21 4.21

4.21 4.21

4.21 16.8 4.21

4.21 4.21

4.21 4.21

4.21 4.21 4.21

4.21

4.21 4.21 4.21

4.21 4.21 4.21

4.21 16.8

16.8

4.21 4.21

4.21 4.21

4.21 4.21 4.21

4.21 8.42 4.21

Limits

72-122 79-123 80-120

MS MS Result Quallfler

4J4 3.88

4.75 4.34

3.75 3.88 4.21

5.00 3.98

4.04

4.88

4.88 16.1 4.07

4.04 4.52

3.45 3.95

4.34 4.06

2.53

4.12 3.85 3.94 3.75

3:91 4.29 3.61

3.82 16.1

15.4 4.37 4.28

4.88 4.06

3.87 4.31

4.25

3.75 8.60 4.71

Page 77 of 140

Unit

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

n1g/Kg mg/Kg

mg/Kg

mg/Kg

n1g/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg


D ,,

Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 339082 0/oRec. Limits

37 -130 92 41-130

113 10-149

103 37 -130 89 41-130 92 39-138

100 14 -132 119 20-130

95 37-130 g6 39-130

116 22-130

116 21-130 96 10-160

97 38-131 96 24-136

107 10-160

82 29-141 94 36-134

103 37-130 97 32-132 60 36-139

98 39-130 92 35-136 94 32-135

89 34-130 93 37-130

102 35-130

86 34-132 91 36-132 96 19-139

92 21-144 104 31 -130 102 27 -147

101 42-130

96 40-134 92 31-130

103 34-144

101 41-143

89 35-136 102 35-130 112 10-141


21112017

QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol

Method; 82GOC ·Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: 400-132588·6 MSD Matrix: Solid Analysis Batch: 339083

Analyte

1, 1, 1,2-T etrachloroethane 1, 1, 1 -Trichloroethane 1, 1,2,2-Tetrach!oroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dich!oroethene 1,2-Dibromo-3-Ch!oropropane

1,2-Dichlorobenzene 1,2-Dich!oroethane

1,2-Dlchloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene

Bromofonn Bromomethane


Chlorobenzene Ch!orodibromomethane Chloroethane

Chloroform Chloromethane cis-1,2-Dfchloroethene

cis-1,3-Dlchloropropene Dichlorobromomethane

Ethylbenzene Methyl tert-butyl ether Me1hylene Chloride 2-Butanone (MEK)


Styrene Tetrach1oroethene

Toluene trans-1,2-Dich loroethene

trans-1, 3-Dich loropropene Trichloroethene Trichtorofluoromethane

Vinyl chloride Xy!enes, Total 1,2,4-Trichlorobenzene

Su"Qgate 47Brom_ofluorobenzene Dibromofluoromethane To/uene.<f8 (Surr)

Sample San1ple Result Qualifier

<0.21 <0.093 <0.21 <0.21

<0.070 <0.21

<0.28

<0.060

<0.069 <0.21

<0.080 <0.21 <0.61

<0.056

<0.21 <0.21

<0.21

<0.14

<0.044 <0.21

<0.21

<0.21

<0.084

<0.064 <0.10

<0.21 <0.051

<0.084 <0.84 <0.50

<0.42

<0.084 <0.21

0.62 <0.21 <0.21

<0.084

<0.21

<0.21 <0.16

<0.17

MSD MSD %Recovery Qualifier

98 102 101

Spike Added

4.21 4.21

4.21 4.21

4.21 4.21

4.21 4.21 4.21 4.21

4.21 4.21 16.8

4.21 4.21 4.21

4.21 4.21

4.21 4.21 4.21

4.21 4.21

4.21

4.21 4.21 4.21

4.21 4.21 16.8 16.8

4.21 4.21

4.21 4.21

4.21 4.21

4.21

4.21 8.42 4.21

Limits

72-122 79.123 80.120

MSD MSD Result Qualifier Unit

4.30 mg/Kg

4.23

4.63 4.34

3.99 4.44

4.17

4.82 4.31

4.29 4.62

4.70 17.3 4.33

3.98 4.71

3.76 4.23

4.34 4.00 2.57

4,36 4.25 4.23

4.07

4.16 4.30 3.94

4.18 17.2

16.6

4.38 425 4.78

4.41 3.87 4.42

4.43 4.10 8.64

4.52

mg/Kg mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

1ng/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

Page 78 of 140


Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 339082 VoRec. RPO

D t'/oRec ~:t 102

Limits 37 .130

{I 100 41-130 ,, 110 10.149

;:r 103 37 .130

" 95 41-130 " 106 39.138 1:1 99 14-132

,, 115 20.130

l) 102 37.130

" 102 39-130 ,,, 110 22.130

,,, 112 21-130

" 103 10 .160 ,,, 103 38.131 ,,, 95 24 .136

" 112 10.160 a 89 29.141 1,1 100 36.134

1:r 103 37-130

" 95 32.132

" 61 36.139 ,, 104 39.130

" 101 35.136

" 101 32 .135

" 97 34.130 ,,, 99 37 .130

" 102 35.130 p 94 34.132

" 99 36.132 1) 102 19.139

" 99 21.144

" 104 31.130 ,,, 101 27 -147

" 99 42-130 " 105 40.134 ;) 92 31-130 ,, 105 34 .144

" 105 41-143

" 97 35.136

" 103 35-130 " 107 10 -141

RPO Limit 4 34 8 3

0 6

14

4

8

6 6

4

7 6

2 4

9 7

0 2

2

6 10

7

8 6 0

9

9 6

7 0

2 8

0 2 4

9 0 4

40

44

~! B 37

38

40 32

35

41

40 38 36

34 47 39

44

37 34

42 35 41

35 35

34

46 31

38 41

39

39 44 37

38

34 42

42 43 39 53


2/1/2017


QC Sample Results

Method: 8260C • Volatile Organic Compounds by GC/MS (Continued)

Lab Sample ID: MB 400·339330/1 ·A Matrix: Solid Analysis Batch: 339331

Analyte 1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichtoroethane

1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane

1, 1-Dichloroethane 1, 1-Dichloroethene 1,2-Dibromo-3-Chloropropane

1,2-Dichlorobenzene 1,2-Dichloroethane

1,2-Dich!oropropane

1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene

Brornoform Bromomethane Carbon disulfide


Chlorobenzene Chlorodfbromomethane

Chloroethane Chloroform Ch1oromethane .cis-1,2-Dtchloroethene cis-1,3-Dichloropropene

Dichlorobromomethane 2-Butanone (MEK)

Ethylbenzene 4-Methyl-2-pentanone (MIBK)


Methylene Chloride

Styrene Tetrachloroethene Toluene trans· 1,2 -Dich!oroethene

trans· 1,3-Dichloropropene Ttichloroethene Trich!orofluoromethane 1,2,4-Trichlorobenzene Vinyl chloride lsobutyl alcohol

Xylenes, To~al

surrogate 4-Bromonuorobenzene Dibromofluoromet/1ane Toluene-dB (Surr)


<0.0025 <0.0011

<0.0025 <0.0025

<0.00083 <0.0025

<0.0033

<0.00071 <0.00082

<0.0025 <0.00095

<0.0025 <0.0073

<0.00067

<0.0025 <0.0025 <0.0025 <0.0017

<0.00052 <0.0025

<0.0025 <0.0025 <0.0010

<0.00076 <0.0012

<0.0025 <0.0060

<0.00061

<0.0050 <0.0010

<0.010

<0.0010 <0.0025

<0.0010 <0.0025

<0.0025 <0.0010

<0.0025

<0.0020

<0.0025 <0.010

<0.0019


96

100 gJ

RL 0.0050 0.0050

0.0050

0.0050

0.0050 0.0050

0.0050

0.0050 0.0050

0.0050

0.0050

0.0050 0.025

0.0050 0.0050 0.0050 0.0050

0.0050

0.0050 0.0050 0.0050

0.0050 0.0050

0.0050 0.0050

0.0050 0.025

0.0050

0.025 0.0050

0.015

0.0050 0.0050 0,0050

0.0050

0.0050 0.0050

0.0050 0.0050 0.0050 0.025

0.010

Llmlts 72-122

7g_1z3

80-120


0.0025 mg/Kg 0.0025 mg/Kg

0.00083 mg/Kg 0.0025 mg/Kg 0.0033 mg/Kg

0.00071 mg/Kg 0.00082 mg/Kg

0.0025 mg/Kg

0.00095 mg/Kg

0.0025 mg/Kg 0.0073 mg/Kg

0.00067 mg/Kg

0.0025 mg/Kg 0.0025 mg/Kg

0.0025 mg/Kg 0.0017 mg/Kg

0.00052 mg/Kg 0.0025 mg/Kg 0.0025 mg/Kg

0.0025 mg/Kg 0.0010 mg/Kg

0.00076 mg/Kg

0.0012 mg/Kg 0.0025 mg/Kg 0.0060 mg/Kg

0.00061 mg/Kg

0.0050 mg/Kg 0.0010 mg/Kg

0.010 mg/Kg 0.00.10 mg/Kg 0.0025 mg/Kg

0.0010 mg/Kg 0.0025 mg/Kg

0.0025 mg/Kg 0,0010 mg/Kg

0.0025 mg/Kg

0.0020 mg/Kg 0.0025 mg/Kg 0.010 mg/Kg

0.0019 mg/Kg

Page 79 of 140



0 Prepared Analyzed Oil Fae 01122117 07:44 01122117 09;19 01122117 07:44 01/22117 09:19

01/22117 07:44 01122117 09:19 01/22117 07;44 01122/17 09:19

01/22117 07:44 01/22117 09;19 01122/17 07:44 01/22117 09:19

01122117 07:44 01/22/17 09:19

01122117 07:44 01122117 09:19 01/2211707:44 01/22117 09:19

01122117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19

01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22/17 09:19 01/22117 07:44 01/22/17 09:19

01122117 07:44 01/22/17 09:19 01122117 07:44 01/22/17 09:19

01122117 07:44 01/22117 09:19

01/22117 07:44 01122/17 09:19 01/22117 07:44 01122/17 09:19 01122117 07:44 01/22117 09:19

01122117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19

01122117 07:44 01/22117 09:19 01/22117 07:44 01/22/17 09:19

01/22117 07:44 01122/17 09:19 01/22117 07:44 01122117 09:19 01/22/17 07:44 01122117 09:19

01/22117 07:44 01/22/17 09:19 01/22117 07:44 01/22117 09:19

01122117 07:44 01/22117 09:19

01122117 07:44 01/22117 09:19 01122117 07:44 01122/17 09:19 01/22117 07:44 01122/1709:19

01/22117 07:44 01122117 09:19

01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19

01/22117 07:44 01/22117 09:19 01122117 07:44 01/22117 09:19

01122117 07:44 01/22/17 09:19 01122117 07:44 01/22/17 09:19

01/22117 07:44 01/22117 09:19

Prepared Analyzed 01122117 07:44 01122117 09;19

01122117 07:44 01/22117 09:19

01122117 07:44 01122117 09:19

1

1

DI/ Fae 1 1


2/1/2017

E



Method: 8260C "Volatile Organic Compounds by GCIMS (Continued)

Lab Sample ID: LCS 400-33933012-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339331 Prep Batch: 339330

Spike LCS LCS O/oRec.

Analyte Added Result Qualifier Unit D 0/oRec Limits

1, 1, 1,2-T etrachloroethane 0.0500 0.0495 mg/Kg 99 65 .130

1, 1, 1-Trichloroethane 0.0500 0.0496 mg/Kg 99 63-130

1, 1,2,2-Tetrachloroethane 0.0500 0.0481 mg/Kg 96 60-131

1, 1,2-Trichloroethane 0.0500 0.0470 mg/Kg 94 65-130

1, 1-Dichforoethane 0.0500 0.0502 mg/Kg 100 59-130

1, 1-Dichloroethene 0.0500 0.0509 n1g/Kg 102 55-137

1,2-Dibromo-3-Ch!oropropane 0.0500 0.0501 mg/Kg 100 49- 130

1,2-Dichlorobenzene 0.0500 0.0479 mg/Kg 96 64-130

1,2-0ichloroethane 0.0500 0.0503 mg/Kg 101 62-130

1,2-Dich!oropropane 0.0500 0.0487 mg/Kg 97 64.130

1,3-DichJorobenzene 0.0500 0.0488 mg/Kg 98 66-130

1,4-0lchlorobenzene 0.0500 0.0487 mg/Kg 97 65-130

Acetone 0.200 0.201 mg/Kg 100 48-160

Benzene 0.0500 0.0494 mg/Kg 99 65. 130

Bromofonn 0.0500 0.0493 mg/Kg 99 52-136

Bromomethane 0.0500 0.0587 mg/Kg 117 12 .160

Carbon disulfide 0,0500 0.0488 mg/Kg 98 46-141

Carbon tetrachloride 0.0500 0.0510 019/Kg 102 60-130

Chlorobenzene 0.0500 0.0489 mg/Kg 98 70-130

Chforodibromome~h~ne 0.0500 0.0504 mg/Kg 101 58-132

Chloroethane 0.0500 0.0533 mg/Kg 107 55 -134

Chloroform 0.0500 0.0497 mg/Kg 99 62-130

Chlorornethane 0.0500 0.0517 mg/Kg 103 49-136

cis-1,2-Dichloroethene 0.0500 0.0484 mg/Kg 97 53-135

cis-1,3-Dichf oropropene 0.0500 0.0490 mg/Kg 98 61 - 130

Oichlorobromomethane 0.0500 0.0505 mg/Kg 101 61-130

2-Butanone (MEK) 0.200 0.233 mg/Kg 116 55 .130

Ethylbenzene 0.0500 0.0484 mg/Kg 97 70-130

4-Methyl-2-pentanone (MIBK) 0.200 0.215 mg/Kg 107 58-130

Methyl tert-butyl ether 0.0500 0.0506 mg/Kg 101 63 .130

Methylene Chloride 0.0500 0.0537 mg/Kg 107 57 -132

Styrene 0.0500 0.0471 mg/Kg 94 68-130

Tetrachloroethene 0.0500 0.0524 mg/Kg 105 67 -130

Toluene 0.0500 0.0474 mg/Kg 95 70 .130

trans-1,2-Dichloroethene 0.0500 0.0533 mg/Kg 107 58-134

trans-1,3-Dichloropropene 0.0500 0.0476 mg/Kg 95 60-130

Trichloroethene 0.0500 0.0525 mg/Kg 105 65-130

Trichlorofluoromethane 0.0500 0.0506 mg/Kg 101 61-136

1,2,4-T richlorobenzene 0,0500 0.0528 mg/Kg 106 56-138

Vinyl chloride 0.0500 0.0529 mg/Kg 106 52-132

Xylenes, Total 0.100 0.0946 mg/Kg 95 70 .130

LCS LCS surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene 93 72-122 Dibromofluoromethane 105 79-123

Toluene-dB (Surr) 97 80-120


Page 80 of 140 2/1/2017

E


QC Sample Results

Method: 82700 • Semivo!atile Organic Compounds (GC/MS)

Lab.Sample ID: MB 400-338284/1 ·A Matrix: Water Analysis Batch: 338574

Analyte

An Hine 1, 1 '-Bipheny! Bis(2-chloroethyl)ether bis (2~chloroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chtoroani!ine 2-Chloronaphthalene 2-Ch!orophenol Dlbenzofuran 3,3'-Dich!orobenzidine 2,4-Dichlorophenol Diethyl phthafate 2,4-Dimethylphenof Dimethyl phthalate 1,3~Dinitrobenzene

-2,4-Dinitropheno! 2,4-Dinitroto!uene 2,6-Dinllrotoluene Di-n-octyl phthalate Hexach!orobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lsophorone 2-Nitroaniline ,3-Nitroanmne 4-Nitroanillne Nitrobenzene 4-Nitrophenol N-Nitrosodi.n-propylamine N~Nitrosodiphenylamine

PentilQhlorophenol

Phenol 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2.4,6· Trichloropheno!

Surrogate 2-Fluoroblphenyl

2-Fluorophenol Nitrobenzene·df5 P/Jehol-d5 Terpheny/-d14



<0.0038 <0.00017 <0.0027

<0.00016 0.00598 J

<0.00019 <0.0034

<0.00014 <0.0022

<0.00017

<0.0026

<0.0030 0.000429 J <0.0035

<0.00017 <0.0010

<0.0034 <0.0019

<0.0019 0.000230 J <0.00017 <0.00055

<0.0026

<0.0042 <0.00014

<0.0022 <0.0018

<0.0015 <0.00013

<0.0021

<0.0033 <0.00018 <0.0014

<0.0026 <0.00018

<0.0016 <0.00018

<0.0037

<0.0035


76 61

76

73

104

78

RL 0.010 0.010

0.010 0.010

0.010 0.010

0.010

0.010 0.010

0.010

0.010

0.010 0.010 0.010

0.010 0.010 0.030

0.010 0.010 0.010

0.010 0.010 0.020

0.010 0.010

0.010 0.010 0.010

0.010 0.010

0.010

0.010 0.020 0.010

0.010

0.010 0.010

0.010 0.010

Limits 46-124

13-113 36-126

17 -127

44-149

26-150


0.00017 mg/L 0.0027 mg/L

0.00016 mg/L

0.0020 mg/L 0.00019 mg/L 0.0034 mg/L

0.00014 mg/L 0.0022 mg/L

0.00017 mgil

0.0026 mg/L

0.0030 mg/L 0.00024 mg/L

0.0035 mg/L 0.00017 mg/L

0.0010 mg/L

0.0034 mg/L 0.0019 mg/L

0.0019 mg/L 0.00017 mg/L 0.00017 mg/L

0.00055 mg/L 0.0026 mg/L

0.0042 mg/L 0.00014 rngil

0.0022 mg/L 0.0018 mg/L 0.0015 mg/L

0.00013 mg/L 0.0021 mg/L

0.0033 mg/L 0.00018 mg/L 0.0014 mg/L

0.0026 mg/L 0.00018 mg/L

0.0016 mg/L 0.00018 mg/L

0.0037 mg/L

0.0035 mg/L

Page 81 of 140



O Pr_epared Analyzed 01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51

01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51

01/12117 16:23 01/16/17 19:51 01/1211716:23 01/16/1719:51

01/12117 16:23 01/16/1719:51

01/12117 16:23 01/16/1719:51 01/12/1716:23 01/16117 19:51

01/1211716:23 01/16/1719:51 01/1211716:23 01/16/17 19:51

01/1211716:23 01/16/1719:51 0111211716:23 01/16/17 19:51 01/1211716:23 01/16/1719:51

01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51

01/1211716:23 01/16/17 19:51 01/12117 16:23 01/16/17 19:51

01/12117 16:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51

01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51

01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51

01/1211716:23 01/16/17 19:51 .01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51

01/1211716:23 01116117 19:51 0111211716:23 01116117 19:51

0111Z/1716:23 01116/1719:51

0111211716:23 01/1611719:51 01/1211716:23 01116/17 19:51 0111211716:23 01116117 19:51

0111211716:23 01116/17 19:51 0111211716:23 01116117 19:51 0111211716:23 01116117 19:51 .0111211716:23 01116117 19:51

0111211716:23 01116117 19:51

Prepared Analyzed 0111211716:23 0111611719:51

0111211716:23 01116117 19:51

0111211716:23 0111611719:51

0111211716:23 01116117 19:51

0111211716:23 0111611719:51

0111211716:23 01116117 19:51

Oil Fae 1

1

Dif Fae 1


2/1/2017

B



Method: 82700 • Semivolatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 400·338284/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338574 Prep Batch: 338284

Spike LCS LCS il/nRec. Analyte Added Result Qualifier Unit D 0/oRec Limits

Aniline 0.120 0.0908 mg/L 76 10-150 Bis(2-chloroethyl)ether 0.120 0.0988 mg/L 82 55-130 bis (2-ch!oroisopropyl) ether 0.120 0.0961 mg IL 80 39-136 Bis(2-ethythexyl) phthalate 0.120 0.145 mg/L 121 62-139 Butyl benzyl phthatate 0.120 0.133 mg/L 111 59-145 4-Chloroaniline 0.120 0.0828 rng/L 69 10 -150 2-Chloronaphtha!ene 0.120 0.0989 mg/L 82 62-130 2-Chlorophenol 0.120 0.0894 mg/L 74 60-130 Dlbenzofuran 0.120 0.104 rng/L 87 69-130 2,4-Dich!orophenol 0.120 0.100 mg/L 84 50-130 Diethyl phthalate 0.120 0.109 rng/L 91 60-133 2,4-0imethylphenol 0.120 0.0845 rng/L 70 52-132 Dimethyl phthalate 0.120 0.104 rng/L 87 69-130 2,4-Dinitropheno! 0.240 0.0607 mg/L 25 15-150 2,4-Dinitrotoluene 0.120 0.110 mg/L 92 66-140 2,6-Dinltroto!uene 0.120 0.107 rng/L 89 70-130 Di-n-octyl phthalate 0.120 0.129 rng/L 108 57 -148 Hexach!orobenzene 0.120 0.104 mg/L 87 67-132

Hexachlorobutadiene 0.120 0.0943 mg/L 79 34 -150 Hexachlorocyclopentadiene 0.120 0.0447 rng/L 37 1 -150 Hexachloroethane 0.120 0.0937 rng/L 78 34-133 lsophorone 0.120 0.101 mg/L 84 60-130 2-Nitroani!ine 0.120 0.106 mg/L 88 30-130 3-Nitroaniline 0.120 0.0943 rng/L 79 10-150 4-Nitroaniline 0.120 0.107 rng/L 89 10-150 Nitrobenzene 0.120 0.0966 mg/L 81 55-130 4-Nitrophenol 0.240 0.148 mg/L 62 31-150 N-Nitrosodi-n-propylamine 0.120 0.100 rng/L 83 55-130 N-Nitrosodiphenylamine 0.119 0.0990 mg/L 83 36-150 Pentachlorophenol 0.240 0.143 mg/L 60 46-136 Phenol 0.120 0.0930 rng/L 77 34-137 1,2,4-Trichlorobenzene 0.120 0.0979 rng/L 82 57 -130 2,4 ,5-Trichlorophenol 0.120 0.101 mg/L 84 67 -130

2,4,6-Trichlorophenol 0.120 0.0997 mg/L 83 67 -130


2-FJuorobipheny/ 69 46-124 2-Fluorophenol 48 13-113 Nifrobenzene-d5 70 36-126 Phenol-d5 67 17 -127 Terphenyl-d14 92 44-149 2,4,6-Tribromophenol 80 26-150


Page 82of140 2/1/2017

a


Method: 82700 - Semivolatile Organic Compotmds (GC/MS) (Continued)

Lab Sample ID: LCSD 400-338284/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 338574 Prep Batch: 338284

Spike LCSO LCSO 0/oRec. RPO Analyte Added Result Qualifier Unit 0 0/oRec Limits RPO Limit Aniline 0.120 0.102 mg/l 85 10-150 11 30 Bis(2-chloroethyl)ether 0.120 0.104 mg/L 87 55-130 5 30 bis (2-chloroisopropyl) ether 0.120 0.101 mg IL 84 39-136 5 30 Bis(2-ethylhexyl) phthalate 0.120 0.143 mg/L 119 62-139 30

E Butyl benzyl phthalate 0.120 0.146 mg IL 122 59-145 9 30 4-Chloroaniline 0.120 0.105 rng/l 87 10-150 23 30 2-Chloronaphtha!ene 0.120 0.108 mg/L 90 62-130 9 30 2-Chlorophenol 0.120 0.0970 mg/L 81 60-130 8 30 DibenzofUran 0.120 0.112 mgll 94 69-130 8 30 2,4-Dich!orophenol 0.120 0.108 mg/L 90 50-130 7 30 Diethyl phtha!ate 0.120 0.119 mg/L 99 60-133 9 30

2,4-0lmethylphenol 0.120 0.0900 rng/L 75 52-132 6 30 Dimethyl phtha!ate 0.120 0.114 mglL 95 69-130 9 30 2,4-Dinitrophenol 0.240 0.113 rng/L 47 15-150 60 30

2,4-Dinitroto!uene 0.120 0.122 mg/l 101 66-140 10 30 2,6-Dinitrotoluene 0.120 0.117 mg IL 97 70-130 9 30 Di-n-octyl phthalate 0.120 0.144 rng/L 120 57 -148 11 30

Hexachlorobenzene 0.120 0.112 n1g/L 93 67 -132 7 30

Hexachtorobutadiene 0.120 0.102 rng/L 85 34' 150 8 30 Hexachlorocyclopentadiene .0.120 0.0489 mg/L 41 1-150 9 30

Hexachloroethane 0.120 0.101 mgll 84 34-133 7 30 lsophorone 0.120 0.109 mg/L 91 60-130 8 30 2-Nitroaniline 0.120 0.115 mg/L 96 30-130 9 30

3-Nitroaniline 0.120 0.106 mg/L 89 10-150 12 30 4-Nitroaniline 0.120 0.115 mg IL 96 10-150 8 30 Nitrobenzene 0.120 0.103 mg/L 86 55-130 7 30 4-Nitrophenol 0.240 0.177 mg IL 74 31 -150 18 30 N-Nitrosodi-n-propylamine 0.120 0.105 mg/L 88 55-130 5 30 N-Nitrosodiphenylamine 0.119 0.108 mg IL 91 36-150 8 30 Pentachloropheno1 0.240 0.217 mg/L 90 46-136 41 30 Phenol 0.120 0.0994 mg/L 83 34-137 7 30

1,2,4-Trichlorobenzene 0.120 0.103 mg IL 86 57-130 5 30 2,4,5-Trichlorophenol 0.120 0.115 mg IL 96 67 -130 13 30

2.4 ,6-Trichloropheno! 0.120 0.108 mg IL 90 67" 130 8 30

LCSD LCSD Surrogate %Recovery Quallfler Llrnlrs 2-Ffuorobiphenyl 74 46-124 2-Ffuorophenol 60 13-113 Nitrobenzene-d5 75 36-126 Phenol-d5 74 17 -127 Terpl1enyf·d14 101 44-149 2,4,6-Tribromophenol 88 26-150


Page 83 of 140 2/1/2017



Method: 8270D - Semivolatile Organic Compotmds (GC/MS) (Continued)

Lab Sample ID: MB 400·338556110-A Matrix: Solid Analysis Batch: 338741

A_nalyte Acenaphthene Acenaphthylene

Aniline Anthracene Benzo[a]anthracene Benzo[a]pyrene

Benzo[b]f!uoranthene

Benzo[g,h.iJperylene Benzofk]fluoranthene

1,1'-Biphenyl

Bis(2-chloroethyl)ether

bis (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate


4-Chloroaniline 2-Chloronaphthalene

2-Ch!orophenof

Chrysene Dibenz(a.h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine

2.4-Dichlorophenol Diethyl phthalate

2,4-Dimethylpheno! Dimethyl phthalate 1,3-0lnitrobenzene

2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitroto!uene Di-n-octyl phthalate

Fluoranthene


Hexachlorobutadiene Hexachlorocyclopentadiene

Hexachloroethane lndeno[1,2,3-cdJpyrene

lsophorone 2~Methylnaphthalene

Naphthalene 2~Nitroanmne

3-Nitroaniline 4-Njtroanifine Nitrobenzene 4-Nitrophenol

N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine

Pentachlorophenol

MB MB Result Qualifier <0.033 <0.033 <0.043

<0.033

<0.033 <0.033

<0.033

<0.033 <0.033

<0.033 <0.033

<0.033 <0.033

<0.033

<0.033 <0.033

<0.033 <0.033

<0.033 <0.033

<0.033

<0.033 <0.033

<0.033

<0.033

<0.033 <0.29

<0.033

<0.033 <0.033

<0.033 <0.033

<0.10

<0.033 <0.066

<0.10 <0.033

<0.033

<0.033 <0.033

<0.033 <0.033

<0.033 <0.033

<0.11

<0.11 <0.033 <0.066

RL 0.33 0.33 0.33 0.33

0.33 0.33 0.33

0.33 0.33 0.33

0.33

0.33 0.33 0.33 0.33 0.33

0.33 0.33

0.33 0.33 0.33

0.33 0.33 0.33

0.33 0.33 0.99

0.33 0.33 0.33

0.33 0.33 0.33

0.33 0.33

0.33 0.33

0.33

0.33 0.33 0.33

0.33 0.33 0.33

0.33 0.33 0.33 0.66

Page 84 of 140

MDL Unit 0.033 mg/Kg 0.033 mg/Kg 0.043 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg


0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.29 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.10 mg/Kg

0.033 mg/Kg 0.066 mg/Kg

0.10 mg/Kg 0.033 mg/Kg

0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg

0.033 mg/Kg

0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg

0.11 mg/Kg 0.11 mg/Kg

0.033 mg/Kg 0.066 mg/Kg


D Prepared Analyzed 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/1711712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 0111711712:42 01/16/17 09:16 01/17/17 12:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42

01/16/17 og:16 01/17/1712:42

01116/17 09:16 01/17/1712:42 01/.16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/17 12:42

01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01117/1712.:42 01/16/17 09:16 01/1711712:42

01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/1709:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42

Dllfac 1

1

1


2/112017



Method: S270D • Semivolatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: MB 400-338556/10-A Matrix: Solid Analysis Batch: 338741

MB MB

Analyte Result Qualifier

Ptienanthrene <0.033 Phenol <0.033 Pyrene <0.033 1,2,4, 5~ T etrachlorobenzene <0.033

2, 3 ,4, 6-T etrach1orophenol <0.033 1,2,4-Trichlorobenzene <0.033 2,4,5-Trichlorophenol <0.033 2,4,6-Trichlorophenol <0.033

MB MB Surrogate %Recovery 2-FluOiobipheny/ 2-FluorophenoJ Nitrobenzene-d5 Phenol-d5 Terphenyl-d14


Lab Sample ID: LCS 400-338556/9-A Matrix: Solid Analysis Batch: 338741

Anatyte Acenaphthene Acenaphthylene Aniline

Anthracene Benzo[a]anthracene Benzofa]pyrene Benzo[b]fluoranthene Benz'o[g,h,i]perylene Benzo[k]fluoranthene Bi_s(2-chloroethyl_)ether bls (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanlline 2-Chloronaphthalene 2-Chlorophenol Chrysene Oibenz(a,h)anthracene

Dibenzofuran 2,4-Dlch!orophenol Diethyl phthalate 2.4-Dimethylphenol Dimethyl phthalate 2,4-Dlnitrophenol 2,4-Dinitrotoluene 2,6-Dinitroto!uene

91

88

78

89

118

104

Qualifier

Client Sample ID: Method Blanf{ Prep Type: Total/NA Prep Batch: 338556

RL MDL Unit D Prepared Analyzed Oil Fae 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/1712:42 1 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/1712:42

0.33 0.033 mg/Kg 01116/17 09:16 01/17/17 12:42

0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42

0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42

0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42

Limits Prepared Analyzed Dlf Fae

27-127 01/16117 09:16 0111711712:42 1

25-128 01116117 og:16 0111711712:42 1

15-136 01116117 09:16 0111711712:42

29 •. 130 0111611709:16 0111711712:42 1 24.146 01116117 09:16 0111711712:42 1

10-150 01116117 09:16 0111711712:42 1

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338556

Spike LCS LCS o/oRec. Added Result Qualifier Unit D o/oRec Limits

1.99 1.54 mg/Kg 78 50-130

1.99 1.56 mg/Kg 78 50-130 1.99 1.22 mg/Kg 61 34.130

1.99 1.62 mg/Kg 81 50 .130

1.99 1.75 mg/Kg BB 50-130 1.99 1.60 mg/Kg 81 50-130 1.99 1.60 mg/Kg 81 50-130

1.99 1.84 mg/Kg 92 50 .132

1.99 1.57 mg/Kg 79 50 .130

1.99 1.36 mg/Kg 68 37 -130 .1.99 1.28 mg/Kg 64 14-149

1.99 1.86 mg/Kg 93 62-140 1.9.9 1.73 mg/Kg 87 57 .139

1.99 1.28 mg/Kg 64 29-130 1.99 1.47 mg/Kg 74 60-130

1.99 1.37 mg/Kg 69 57-130 1.99 1.74 mg/Kg 88 50-130 1.99 1.72 mg/Kg 87 43-133

1.99 1.56 mg/Kg 78 37 .137

1.99 1.61 mg/Kg 81 56-130 1.99 1.32 mg/Kg 66 63.130

1.99 1.44 mg/Kg 72 43-130

1.99 1.58 mg/Kg 79 65.130

3.98 1.84 mg/Kg 46 10.130

1.99 1.65 n1g/Kg 83 56.130

1.99 1.56 mg/Kg 79 65-130


Page 85 of 140 2/112017

El

QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol

Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 400-338556/9-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 338741 Prep Batch: 338556

Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits bi-n-ociyl phthalate 1.99 1.81 mg/Kg 91 57 -140 Fluoranthene 1.99 1.70 mg/Kg 85 50-130 Fluorene 1.99 1.62 mg/Kg 82 50-130 Hexachlorobenzene 1.99 1.71 mg/Kg 86 44-136 a Hexachlorobutadiene 1.99 1.49 mg/Kg 75 44-130 Hexachlorocyclopentadiene 1.99 1.50 mg/Kg 76 1-150

Hexachloroethane 1.99 1.22 mg/Kg 61 44-130

lndeno[1,.213-cd]pyrene 1.99 1.75 mg/Kg 88 43-131 lsophorone 1.99 1.41 mg/Kg 71 48-130 '2-Methylnaphtha1ene 1.99 1.58 mg/Kg 79 50-130

Naphtha.Jene 1.99 1.39 mg/Kg 70 45-130

2-NitroaniUne 1.99 1.43 mg/Kg 72 46-133 3-Nitroanmne 1.99 1:29 mg/Kg 65 10-150 4-Nitroanillne 1.99 1.29 mg/Kg 65 10-150 Nitrobenzene 1.99 1.31 mg/Kg 66 49-130 4-Nitrophenaf 3.98 2.78 mg/Kg 70 10-150 N-Nitrosodi-n-propylam!ne 1.99 1.28 mg/Kg 64 44-130 N-Nitrosodiphenylamine 1.97 1.48 mg/Kg 75 49-148

Pentachlorophenol 3.98 2.90 mg/Kg 73 10-150 Phenanthrene 1.99 1.60 mg/Kg 80 5-130

Phenol 1.99 1.36 n1g/Kg 68 43-130 Pyrene 1.99 1.84 mg/Kg 92 47 -135

1,2,4M T rlchlor_obenzene 1.99 1..47 mg/Kg 74 50-112 2,4,5-TrichlorophenoJ 1.99 1.7.6 mg/Kg 88 51 -130 2,4 ,6~ Trichlorophenol 1.99 1.78 mg/Kg 90 57 -130

LCS LCS

Surrogate %Recovery Qua/If/er Limits 2MF1Uoroblphenyl 78 27-127 2-Fluorophenol 74 25-128 Nitrobenzene-d5 67 15-136 ·Phenol-<15 75 29-130 Terpheny/,d14 100 24-146 2,4;6-Tribromopheno/ 99 10-150

Lab Sample ID: 400-132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA

· Analysis Batch: 338741 Prep Batch: 338556 Sample sample Spike MS MS 0/oRec.

Analyte Result Qualifier Added Result Qualifier Unit D o/aRec Limits

Acenaphthene <0.066 3.99 3.16 mg/Kg ·l:f- 79 40-140

Acenaphthylene <0.066 3.99 3.19 mg/Kg i) 80 40-140 Aniline <0.086 3.99 2.51 mg/Kg " 63 40-140

Anthracene <0.066 3.99 3.21 n1g/Kg 1:( 81 40-140

Benzo[a]anthracene 0.084 J 3.99 3.40 mg/Kg ·i:i 83 40-140

Benzo[a)pyrene 0.11 J 3.99 3.20 mg/Kg " 77 40-140 Ben.io[b]fluoranthene 0.26 J 3.99 3.45 mg/Kg " 80 40-140 Benzo[g,h,iJperylene <0.066 3.99 2.28 mg/Kg ·>:i 57 40-140 Benzo[k]fluoranthene <0,066 3.99 3.50 mg/Kg i) 88 40-140


Page 86of140 2/1/2017



Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued)


Analyte Bis(2°-Chf6'i6.ettiyl)'e.tlier bls (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Ch!oroanlline 2-Chloronaphtha!ene 2-Chloropheno! Chrysene Dibenz_(a,h)anthracene Dibenzofuran 2,4-Pichlorophenol Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 2,4-Dinitropheno! 2,4-Dinitroto/uene 2,6-Dinitrotoluene Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene HexaChlorobutS:diene Hexi;ichlo_ro<;yclopentadiene Hexachloroethane lndenof1 ,2,3.-cd}pyrene

Jsophorone 2-Methylnaphthalene Naphthalene 2-Nitroaniline 3-Nitroanmne 4-N!troaniline Nitrobenzene 4-Nitrophen·ol N-Nitrosodi-n-propylamlne N-Nit~osodiphenylamine

Pentachloropheno.1 Phenanthrene Phenol Pyrene 112,4-Trichlorobenzene 2,4 ,5· Trlchlorophenol 2,4,6-Trichlorophenol

Surrogate ·2~FiiiO'TObtP6eny1

2-Fluo'rophe.hol NitroQenzene-dS Phenol-d5

Sample Sample Result Qualifier <0.066

<0.066 <0.066

<0.066

<0.066

<0.066

<0.066

0.13 J

<0.066 <0.066

<0.066

<0.066 <0.066

<0.066

<0.58 F2 F1

<0.066

<0.066

<0.066

0.27 J

<0.066

<0.20

<0.066

<0.13 F1

<0.20

<0.066

<0.066 <0.066

<0.066

<0.066

<0.066 <0.066

<0.066

<0.22 <0.22

<0.066

<0.13 <0.066

<0.066

0.23 J

<0.066

<0.066

<0.066

MS MS %Recovery Qualifier

77 78 68

78

Spike Added

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3 .. 99

7.97

3.99 3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3.99

3,99

7.97 3,99

3.95 7,97

3.99 3.99

3.99

3.99 3.99

3.99

Li mils 27.127 25.128

15.136

29-130

MS MS Result Qualifier Unit

2.99 mg/Kg

2.75

3.77

3.52

2.59

3.03

3.02

3.45

2.54

3.13

3.47

2.71

3.17

3.35

2.92 F1

3.32 3.19

3.56

3.37

3.27

3.31

2.99

0.741 F1 2.10

2.46

3.05

3.28

2.90

3.10

2.68

2.59

2.82 5.89

2.79

2.99

6.02

3.20 3.04

3.74

3.00 3.65

3.83

mg/Kg mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg

mg/Kg

mg/Kg n1g/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg mg/Kg

nig/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg

Page 87 of 140

Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556

D o/oRec 1::i 75

O/oRec.

Limits

40-140

69 40-140

95 40-140

88 40.140

65 40-140 76 40.140

76 40-140

83 40-140

64 40-140

79 40-140

87 40-140

68 40-140

79 40-140

84 40.140

37 40-140

83 40-140 80 40.140

89 40.140

78 40-140 82 40.140

83 40-140

75 40-140

19 40-140

53 40-140 62 40.140

76 40.140

82 40-140 73 40.140

78 40.140

67 40-140

65 40-140

71 40.140

74 40-140

70 40-140

76 40.140

76 40-140

80 40-140 76 40.140

88 40.140

75 40-140 92 40.140

96 40-140


2/1/2017



Method: 82700 • Semivolatile Organic Compounds (GCIMS) (Continued)


Surrogate Terphenyl-d14 2,4,6-Tribromophenol

MS MS %Recovery Qualifier

g5

g8

Lab Sample ID: 40.0-132588-6 MSD Matrix: So.lid Analysis Batch: 338741

Analyte Acenaphthene

Acenaphthy/ene Aniline Anthracene Benzo[a]anthracene

Benzo[a]pyrene Benzo[b]fluoranthene. Benzo[g,h,i]perylene

Benzo[k]fluoranthene Bis(2-chloroethyl)ether

bis (2-chlorolsopropyl) ether Bis(2-ethylhexyl) phthalate

Butyl benzyl Pht.ha!ate 4-Chloroaniline

2-Chio'ronaphthalene 2-Ch!oropheno!

Chrysene Dibenz(a,h)anthracene Dibenzofuran 2,4-Dlchtorophenol Diethyl phthalate 2,4-Dimethylphenol

Dimethyl phthalate 2,4-0initrophenol 2,4-0initrotoluene

2,6-0initroto!uene Di-n-octyl phthalate Fluoranthene Fluorene

Hexachlorobenzene

Hexachlorobutadiene Hexachlorocyclopentadiene Hexach!oroethane

lndeno[1,2,3·cd]pyrene

lsophorone 2-Methylnaphthalene'

Naphthalene

2-Nitroaniline 3-Nitroanillne 4-NitroanHine

sample sample

Result Qualifier

<0.066 <0.066

<0.086 <0.066 0.084 J

0.11 J

0.26 J <0.066

<0.066 <0.066 <0.066 <0.066

<0.066 <0.066

<0.066 <0.066

0.13 J <0.066

<0.066 <0.066 <0.066

<0.066

<0.066 <0.58 F2 F1

<0.066

<0.066 <0,066

0.27 J <0.066

<0.20

<0.066 <0.13 F1

<0.20 <0.066 <0.066 <0.066

<0.066 <0.066 <0.066 <0.066

Lf1nits 24-146

10-150

Spike

Added 4.08

4.08 4.0.8 4.08 4.08

4.08

4.08 4.08

4.08 4.08 4.08

4.08

4.08 4.08

4.08

4.08

4.08 4.08

4.08 4.08 4.08

4.08

4.08

8.16 4.08 4.08 4.08

4.08 4.08

4.08

4.08 4.08

4.08

4.08 4.08

4.08

4.08

4.08 4.08 4.08

MSD MSD

Result 3.33

3.36 2.47

3.42 3.75 3.54

3.71 2.71 3.83

2.94

2.77 3.96

3.68 2.64 3.17

3.00 3.74 2.93

3.31

3.53

2.78 3.17

3.43

Qualifier Unit

4.14 F2 3.47

3.31

3.73 3.77

3.45 3:53

3.14 0.823 F1

2.07

2.86 3.04

3.41

2.9g 3.13 2.73

2.66

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

n1g/Kg mg/Kg

mg/Kg

mg/Kg

mg/l<;g

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

n1g/Kg mg/Kg

Page 88 of 140

Client Sample JD: CK-5 Prep Type: Total/NA Prep Batch: 338556

Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556 °lo Rec. RPO

D %Rec

" 82

" 82

Limits 40-140

40 -140 60 40-140 84 40-140

90 40-140 84 40-140

85 40-140 66 40.140

94 40-140 72 40-140 68 40-140

97 40-140

90 40-140 65 40-140

78 40-140

74 40-140 3g 40-140

72 40-140

81 40-140 86 40-140 68 40-140 78 40-140

84 40-140

51 40-140 85 40-140

81 40-140 91 40.140 86 40-140 85 40.140

86 40-140

77 40-140 20 40-140 51 40 .140

70 40-140 75 40-140 84 40.140

73 40.140

77 40-140 67 40-140 65 40.140

RPO 5

5 2 6

10 10

7

17 g

2

1

5

5 2

5

8

14 5

2

3

0

2

35 4

4

5 11

5

6 5

10

1

15 0 4

3

2

3

Limit 30

30

30 30 30

30 30 30 30

30 30

30 30 30 30

30 30 30

30 30 30 30

30

30 30 30

30 30

30

30

30 30 30

30 30 30 30

30 30

30


21112017

Client: C-K Associates Projecl/Site: Moffat & Nichol


Method: ll270D - Semivo!atile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: 400-132588-6 MSD Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556

Matrix: Solid Analysis Batch: 338741

Analyte Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine

N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene

Phenol

Pyrene 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4 ,6-Trichlorophenol

Surrogate 2-Fluorobiphenyl 2-Fluorophenof Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 2, 4,6-Tribromophenol

sample Sample

Result Qualifier

<0.066 <0.22

<0.22

<0.066 <0.13

<0.066

<0.066

0.23 J <0.066 <0.066

<0.066

MSD MSD

%Recovery Qualifier 90 86 77

87 113

112

Lab Sample ID: MB 400-339125/1-A Matrix: Water Analysis Batch: 339188

Analyte Aniline 1, 1'-Siphenyl Bis(2-chloroethyl)ether bis (2-ch!oroisopropyl) ether

Bis(2-ethylhexyl) phthalate _Butyl benzyl phthalate 4-Chlqroanl!ine

2-Ch!oronaphthalene

2-Chlorophenol Dibenzofuran 3,3'-Dich!orobenzidlne 2,4-Dich1orophenol

Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dinitrophenol

2.4-Dinitrotoluene 2,6-Dinltroto!uene

Di-n-octyl phthalate Hexachloroi;>enzene

Hexachlorobutadiene Hexachlorocyclopentadiene


<0.00095 <0.000043 <0.00068

<0.000040

0.0123 <0.000048

<0.00085

<0.000035

<0.00055 <0.000043 <0.00065 <0.00075

0.00009.32 J <0.00088

<0.000043

<0.00025 <D.00085

<0.00048

<0.00048

0.000574 J <0.000043

<0.00014 <0.00065

Spike

Added

4.08 8.16 4.08

4.05

8.16 4.08

4.08 4.08

4.08 4.08 4.08

Limits

27 .127

25-128 15-136 2g.130

24-146 10-150

RL 0.0025

0.0025 0.0025 0.0025

0.0025

0.0025 0.0025

0.0025

0.0025 0.0025 0.0025 0.0025

0.0025 0.0025 0.0025 0.0025 0.0075

0.0025 0.0025

0.0025 0.0025

0.0025 0.0050

MSD MSD

Result Qualifier Unit 2.86 mg/Kg 6.11

2.78 3.12 6.38 3.42 3.01

4.22 3.13 3.75 3.90

MDL Unit

0.00095 mg/L

0.000043 mg/L 0.00068 mg/L

0.000040 mg/L

0.00050 mg/L

0.000048 fl1QIL 0.00085 mg/L

0.000035 mg/L

0.00055 mg/L

0.000043 mg/L 0.00065 mgll

0.00075 mg/L

0.000060 mg/L 0.00088 mg/L

0.000043 mg/L

0.00025 mg/L 0.00085 mg/L 0.00048 mg/L 0.00048 mg/L

0.000043 mg/L 0.000043 mglL 0.00014 mg/L

0.00065 mg/L

mg/Kg mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg mg/Kg

mg/Kg mg/Kg

mg/Kg

Page 89 of 140

%Rec. RPO

D %Rec

" 7o Limits RPO Linllt 40-140 1 30

75 40.140 4 30 68 40-140

77 40-140

78 40-140 84 40.140

74 40-140

98 40-140 77 40-140 92 40-140 96 40.140

0

4

6 7

12

4

3

2

30 30

30 ~ 30 ll;Jll 30 30

30 30 30


O Prepared Analyzed 01119/17 15:31 01120117 15:57

0111911715:31 0112011715:57 01/19/17 15:31 01120117 15:57

0111911715:31 01120117 15:57 01119/17 15:31 0112011715:57

01/1911715:31 01/2011715:57 01/19117 15:31 0112011715:57

011.1911715:31 0112011715:57 01/19/1715:31 01120/17 15:57

01119/1715:31 01/20/1715:57 0111911715:31 01/20117 15:57

01/1911715:31 01/20117 15:57 0111911715:31 01120117 15:57 01/19/17 15:31 01120/17 15:57 01/19/1715:31 0112011715:57

01/19/1715:31 01120117 15:57 01119/1715:31 01120117 15:57 01/1911715:31 01/2011715:57

01/1911715:31 01120117 15:57 01/19/17 15:31 01120117 15:57 0111911715:31 0112011715:57 01/19/1715:31 01120/1715:57

0111911715:31 01120117 15:57

011 Fae 1


2/112017



Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued)

Lab Sample ID: MB 400-339125/1-A Client Sample ID; Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339188 Prep Batch: 339125

MB MB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae

Hexachloroethane <0.0011 0.0025 0.0011 mg IL 01/19/1715:31 0112011715:57 1

lsophorone <0.000035 0.0025 0.000035 mg IL 01119/1715:31 0112011715:57

2-N!troaniline <0.00055 0.0025 0.00055 mg/L 01/19/1715:31 01120/17 15:57

3-Nitroanmne <0.00045 0.0025 0.00045 mglL 01/19/1715:31 01120117 15:57

4-Nltroanfline <0.00038 0.0025 0.00038 mg IL 01/19/1715:31 01120/1715:57

Nitrobenzene <0.000033 0.0025 0.000033 mg IL 01/19/1715:31 01120/1715:57

4-Nitrophenol <0.00053 0.0025 0.00053 mg IL 01/1911715:31 01120/17 15:57

N-Nitrosodi-n-propylamine <0.00083 0.0025 0.00083 mg IL 0111911715:31 01120117 15:57

N-Nitrosodiphenylamine <0.000045 0.0025 0.000045 mg IL 0111911715:31 01120117 15:57

Pentachforophenol <0.00035 0.0050 0.00035 mg IL 01119/1715:31 01120/17 15:57

Phenol <0.00065 0.0025 0.00065 mg IL 01119/1715:31 01120/17 15:57

1.2,4, 5-Tetrachlorobenzene <0.000045 0.0025 0.000045 mg IL 01119/1715:31 01120117 15:57

2,3 ,4, 6-T etrachlorophenol <0.00040 0.0025 0.00040 mg IL 01/19/1715:31 01120117 15:57

1,2,4· Trichlorobenzene <0.000045 0.0025 0.000045 mg IL 01/19/1715:31 0112011715:57

2,4,5-Trichlorophenol <0.00093 0.0025 0.00093 mg IL 01/19/1715:31 0112011715:57

2,4,6-Trichloropheno! <0.00088 0.0025 0.00088 mg IL 01/19/1715:31 0112011715:57

MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae

2-Fluorobiphenyl 91 46 .124 0111911715:31 0112011715:57 1

2-Fluorophenol 42 13.113 0111911715:31 0112011715:57

Nitrobenzene-d5 BB 36-126 0111911715:31 01/2011715:57

Phenol-dS 54 17 -127 0111911715;31 01120117 15:57 1

Terphenyl..<J14 112 44-149 0111911715:31 01120117 15:57

2,4,6-Tribromophenol 6.1 26-150 0.111911715:31 0112011715:57

Lab Sample ID: LCS 400-3.39125/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis .Batch; 339188 Prep Batch: 339125

Spike LCS LCS o/aRec. Analyte Added Result Qualifier Unit D o/oftec Limits

Aniline 0.120 0.0882 m9IL 74 21.120

Bis(2-chloroethyl)et11er 0.120 0.0872 mg IL 73 44 -120

bis (2-chloroisopropyl) ether 0.120 0.0928 mg IL 77 33-121

Bis(2-ethylhexyl) phthalate 0.120 0.137 mg IL 114 52, 147

Butyl benzyl phthalate 0.120 0.110 mg IL 91 54-133

4-Chloroaniline 0.120 0.0918 mg IL 76 26-120

2-Ch!oronaphthalene 0.120 0.0944 mg/L 79 52.121

2-Chlorophenol 0.120 0.0753 mg IL 63 40-120

Oibenzofuran 0.120 0.0993 mg/L 83 56-122

2,4-Dichlorophenot 0.120 0.0945 mg IL 79 49-120

Diethyf phthalate 0.120 0.109 mg IL 91 50 .137

2,4-Dimethylphenol 0.120 0.0811 mg IL 68 48-120

Dimethyl phthalate 0.120 0.0981 mg IL 82 57 -124

2,4-Dinitropheno! 0.240 0.0392 mg IL 16 10-150

2,4-Dinitrotoluene 0.120 0.107 mg IL 89 54-142

2,6-Dinitroto!uene 0.120 0.0996 mg IL 83 55-130

Di-n-octyl phthalate 0.120 0.117 mg/L 97 57 .138

Hexachlorobenzene 0.120 0.0999 mg/L 83 52-129


Page 90 of 140 2/1/2017

E


QC Sample Results Tes!America Job ID: 400-132540-1

Method: 82700 - Semivo!atile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 400-33912512-A Client sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339188 Prep Batch: 339125

Spike LCS LCS 0/oRec.

Analyte Added Result Qualifier Unit 0 0/oR~c Limits Hexach!orobutadiene .0.120 0.0835 mg/L 70 45-120 Hexachlorocyclopentadlene 0.120 0.0553 mg/L 46 10-134 Hexachloroethane 0.120 0.0772 mg/L 64 41-120 lsophorone 0.120 0.0931 mg/L 78 48.120 2-Nitroaniline 0.120 0.101 mg/L 84 51-145 3-Nitroan!line 0.120 0.0995 n1g/L 83 37 .127 4-Nitroani!ine 0.120 0.101 mg/L 84 36-137 Nitrobenzene 0.120 0.0904 mg/L 75 45-120 4-Nitropheno! 0.240 0.106 mg/L 44 23-146 N-Nitrosodi-n-propylamine 0.120 0.0934 mg/L 78 45-120 N-Nitrosodiphenylamine 0.119 0.0959 mg/L 81 54-120 Pentachlorophenof 0.240 0.0916 mg/L 38 31-130 Phenol 0.120 0.0614 mg/L 51 40-120 1,2,4-Trichlorobenzene 0.120 0.0855 mg/L 71 47 -120 2,4,5-Trichlorophenol 0.120 0.103 mg/l 86 51 -136 2,4,6-Trichloropheno! 0.120 0.0918 mg/L 77 50-127

LOS LOS

Surrogate %Recovery Qualifier Limits 2-Fluorobiphenyl 85 46-124 2-Fluorophenol 66 13-113 Nitrobenzene-d5 81 36-126 Phenoi-d5 57 17 -127

Terphenyl-d14 95 44-149 2,4,6-Tribromophenol 95 26-150


Spike LCSO LCSO o/oRec. RPO Analyte Added Result Qualifier Unit 0 %Rec Limits RPO Limit Aniline 0.120 0.0929 mg/L 77 21-120 5 30 Bis(2-chloroethyl}ether 0.120 0.0906 mg/L 76 44 - 120 4 30 bis {2-chloroisopropyl) ether 0.120 0.0971 mg/L 81 33-121 5 30 Bis(2-ethylhexyl) phthalate 0.120 0.129 mg/L 107 52-147 6 30 Butyl benzyl phthatate 0.120 0.121 mg/L 101 54-133 10 30 4-Ch!oroaniline 0.120 0.0964 mg/L 80 26-120 5 30 2-Chloronaphthalene 0.120 0.0996 n1g/L 83 52-121 5 30 2-Chloropheno! 0.120 0.0593 1119/L 49 40-120 24 30 Dfbenzofuran 0.120 0.106 mg/L 88 56-122 6 30 2,4-Dichlorophenol 0.120 0.0502 mg/L 42 49-120 61 30 Diethyl phtha!ate 0.120 0.114 mg/L 95 50-137 4 30 2,4-Dimetliylphenol 0.120 0.0817 mg/L 68 48-120 30 Dimethyl phthalate 0.120 0.102 mg/L 85 57 -124 4 30 2,4-Dinltrophenol 0.240 <0.0034 mg/L 0 10-150 200 30 2,4-Dinitrotoluene 0.120 0.107 mg/L 89 54-142 0 30 2,6-Dfnitrotoluene 0.120 0.103 mg/L 86 55-130 4 30 01-n-octyl phthalate 0.120 0.122 mg/L 101 57 .138 4 30 Hexachlorobenzene 0.120 0.112 mg/L 94 52-129 12 30


Page 91 of 140 2/1/2017

E

QC Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol


Dup al/NA 9125

RPO Llnlit

30

30 30 30

30

30 30

30 30 30 30

30 30

30 30

30

E


Lab Sample ID: LCSD 400-339125/3-A Matrix: Water Analysis Batch: 339188

Analyte Hexachlorobu!adiene Hexachlorocyclopentadiene Hexachloroethane lsophorone 2-Nltroaniline 3-Nitroaniline

4-Nitroani!ine

Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine

Pentachlorophenor Phenol 1,2,4-Trichlorobenzene

2,4 ,5-Trichlorophenol 2,4,6-Trichloropheno!

Surrogate

2-Fluorobiphenyl 2-Fluorophenol Nitrof)eniene-d5 Pl1enol-d5 Terphenyl-d14 2,4,6-Tribromophenol

LCSD LCSD

%Recovety Qualifier 91

35 85 42

107

53

Lab Sample ID: MB 400-34007911-A Matrix: Water Analysis Batch: 340421

Analyte

Aniline 1, 1'-Biphenyl Bis(2-chloroethyl)ether

bis (2-chloroisopropyl} ether Bis(2-ethylhexyl) phthalate


4-Chloroaniline

2-Chloronaphthalene 2-Chlorophenol

Dibenzofuran

3,3'-Dichlorobenzldlne 2,4-Dich!orophenol Diethyl phthalate

2,4-Dimethylphenol Dimethyl phthalate

1,3-0initrobenzene

2,4-Dinitrophenol 2,4-Dinitrotoluene

MB MB

Result auallfler

<0.00095

<0.000043 <0.00068

<0.000040 <0.00050

<0.000048 <0.00085

<0.000035 <0.00055

<0.000043 <0.00065

<0.00075

<0.000060

<0.00088

<0.000043 <0.00025 <0.00085

<0.00048

Client Sample ID: Lab Control SamplePrep Type: TotPrep Batch: 33

LCSD LCSD Spike

Added

0.120 0.120 0.120

0.120

0.120 0.120

0.120 0.120

0.240 0.120 0.119

0.240 0.120

0.120

0.120 0.120

Result Qualifier Unit

0.0880 mg/L

Limits

46-124

13-113 36-126

17 - 127 44-149 26 • .150

RL 0.0025

0.0025 0.0025

0.0607 0.0810

0.0963 0.111 0.113 0.106

0.0943

0.0196 0.0974

0.114

0.0709 0.0450

0.0899 0.0420

0.0500

MDL Unit

0.00095 mg/L

0.000043 mg/L

0.00068 mg/L

0.0025 0.000040 mg/L

0.0025 0.00050 mg/L

0.0025 0.000048 mg/L

0.0025 0.00085 mglL

0.0025 0.000035 mg/L

0.0025 0.00055 mg/L

0.0025 0.000043 mg/L

0.0025 0.00065 mg/L

0.0025 0.00075 mg/L

0.0025 0.000060 mg/L

0.0025 0.00088 mg/L

0.0025 0.000043 mg/L

0.0025 0.00025 m9/L

0.0075 0.00085 mg/L

0.0025 0.00048 mg/L

Page 92 of 140

mg IL

mg/L

mg IL

mg IL

mg/L

mg/L

mg/L

mg/L mg/L

mg/L

mglL

mg/L

mglL

mgll

m9/L

%1Rec. D o/oRec Limits RPO

73

51 45.120 5

10-134 9 68 41-120 5

80 48.120 3

92 51 -145 9 94

88

79

37 -127 36.137

45-120 8 23-146

81 45.120

95 54-120

30 31-130 38 40-120

75 47 -120 35 51-136

42 50-127

13

5

4

138 4

17

25

31 5

84

59

Client Sample ID: M.ethod Blank Prep Type: Total/NA Prep Batch: 340079

D Prepared Analyzed 01127/1711:20 01/31/1718:31 01/27/1711:20 01/31/1718:31 01/27/1711:20 01131/1718:31

01/27/1711:20 01/31/1718:31 01/27/1711:20 01/31/1718:31 01/27/1711;20 01131/1718:31 01/27/1711:20 01/31/1718:31

01/27/1711:20 01/31/1718:31 01/27/1711:20 01/31/17 .18:31 01/27/1711:20 01131/1718:31

01127/1711:20 0113111718:31

01127/1711:20 01/31/1718:31 01127/1711:20 01/31/1718:31 01/2711711:20 01/31/17 .18:31

01/27/1711:20 01131117 18:31

01127/1711:20 01/:l1/1718:31 0112711711:20 01131/1718:31 01/27/1711:20 0113111718:31

011 Fae 1


211/2017





MB MB

Anatyte Result Qualifier 2,6-Din!troto!uene <0.00048 Di-n-octyl phthalate 0.000602 J Hexachlorobenzene <0.000043

Hexachforobutadiene <0.00014

Hexachlorocyclopentadiene <0.00065 Hexach1oroethane <0.0011

lsophorone <0.000035 2-NltroaniHne <0.00055

3-Nitroani!ine <0.00045 4-Nitroaniline <0.00038

Nitrobenzene <0.0Q0033 4-Nitrophenol <0.00053 N-Nitrosodi-n-propylamine <0.00083

N~Nitrosodiphenylamine <0.Q00045

Pentachlorophenol <0.00035 Phenol <0.00065 1,2,4,5-T etrachlorobenzene <0.000045

2,3,4,6-Tetrachlorophenol <0.00040 1,2,4-Trichlorobenzene <0.000045 2,4,5-Trlchforophenol <0.00093

2,4,6-Trichlorophenol <0.00088

MB MB Surrogate %Recovery Qualifier 2-Fluorobiphenyl 66

2-Fluorophenol 38

Nitrobenzene-d5 69

Pheno!-d5 57 Terpheny/-d14 88

2,4,6-Tribromopheno! 28

Lab Sample ID: LCS 400-340079/2·A Matrix: Water Analysis Batch: 340421

Analyte Aniline 8is(2-chloroethyl)ether

bis (2-chlorolsopropyl} ether Bis(2-ethythexyl) phthalale

Butyl benzyl phthatate 4-Chloroaniline

2-Chloronaphthalene 2-Ch!orophenol

Dlbenzofuran 2,4-Dich!orophenol Diethyl phthalate

2,4-Dimethylphenol

Dimethyl phthalate

RL MDL Unit 0.0025 0.00048 mg/L

0.0025 0.000043 mg/L

0.0025 .0.000043 rng/L

0.0025 0.00014 rng/L

0.0050 0.00065 rng/L

0.0025 0.0011 rng/L

0.0025 0.000035 mg/l

0.0025 0.00055 mg/L

0.0025 0.00045 rng/L

0.0025 0.00038 mg/L

0.0025 0.000033 mg/L

0.0025 0.00053 mg/L

0.0025 0.00083 mg/L

0.0025 0.000045 mg/L

0.0050 0.00035 mg/L

0.0025 0.00065 mg/L

0.0025 0.000045 mg/L

0.0025 0.00040 mg/L

0.0025 0.000045 mg/L

0.0025 0.00093 mg/L

0:0025 0.00088 mg/L

Limits 46" 124

13-113

36-126

17 -127

44.149

26-150

Spike LCS LCS

Added Result Qualifier

0.0300 0.0181

0.0300 0.0206

0.0300 0.0251 0.0300 0.0261

0.0300 0.0259 0.0300 0.0159

0.0300 0.0197

0.0300 0.0157 0.0300 0.0206

0.0300 0.0196 0.0300 0.0227

0.0300 0.0177

0.0300 0.0201

Page 93 of 140

D


Prepared 01127/1711:20

0112711711:20 01127/1711:20

01/27/1711:20 0112711711:20 01127/1711:20 0112711711:20

0112711711:20 0112711711:20

01/27/17 11:20

01127/1711:20

01/27/1711:20 01/2711711:20

01/27/1711:20

01/27/1711:20

01/2711711:20 01/27/1711:20

01/27/1711:20

01/27/1711:20 01/27/1711:20

01127/1711:20

Prepared 0112711711:20

0112711711:20

0112711711:20

0112711711:20

01127117 11 :20

0112711711:20

Analyzed 01131117 18:31

01131117 18:31 0113111718:31

01131117 18:31

0113111718:31 01131117 18:31

01131117 18:31

0113111718:31

01131/17 18:31 0113111718:31

01131/17 18:31

01131/17 18:31 01131/17 18:31

01131/17 18:.31

01131117 18:31

01131/1718:31 01131/17 18:31

01131/17 18:31

01131/17 18:31 01131/1718:31

01131/1718:31

Analyzed

01131117.18:31

0113111718:31

0113111718:31

0113111718:31

0113111718:31

0113111718:31

OJI Fae 1

DJ/Fae

1

1 1

1

1

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 340079 '%Rec.

Unit mgll

mg/L

mg/L

mg/L

rng/L

mg/L

mg/L

mg/L

mg/L

mg IL

rng/L

mg/L

mg/L

D o/oRec 60

69

84 87 86

53

66 52

69

65 76

59

67

Limits 21-120

44-120

33-121 52-147

54-133 26-120

52-121

40-120 56-122

49.120 50-137

48-120

57 -124


2/1/2017



Method: 82700 - Semivo!ati!e Organic Compounds {GC/MS) (Continued)

Lab Sample ID: LCS 400-340079/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 340421 Prep Batch: 340079

Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit 0 %Rec Limits 2,4-Dinltrophenol 0.0600 0.0121 mg IL 20 10-150 2.4-Dinitrotoluene 0.0300 0.0210 n1g/l 70 54-142 2,6-Dinitroto!uene 0.0300 0.0194 mg/L 65 55-130 Pi-n-octyl phthalate 0.0300 0.0249 mg/L 83 57 -138 Hexachlorobenzene 0.0300 0.0198 mg IL 66 52-129 Hexachlorobutadiene 0.0300 0.0188 mg/L 63 45-120 Hexach!orocyclopentadiene 0.0300 0.00416 J mg/L 14 10-134 Hexachloroethane 0.0300 0.0209 mg/L 70 41-120

lsophorone 0.0300 0.0208 mg/L 69 48-120 2-Nitroaniline 0.0300 0.0234 mg IL 78 51.145

3-Nitroaniline 0.0300 0.0200 mg IL 67 37 -127

4-Nltroaniline 0.0300 0.0198 mg IL 66 36-137 Nitrobenzene 0.0300 0.0207 mg/L 69 45-120 4-Nitrophenol 0.0600 0.0411 mg IL 69 23 .146

N-Nitrosodi-n-propylamine 0.0300 0.0240 mg IL 80 45-120 N-Nitrosodiphenylamine 0.0298 0.0199 mg/L 67 54-120

Pentachlorophenol 0.0600 0.0239 mg IL 40 31-130 Phenol 0.0300 0.0176 mglL 59 40 .120 1,2,4-Trichlorobenzene 0.0300 0.0187 mg/L 62 47 -120 2,4,5· Trichlorophenol 0.0300 0.0201 mg/L 67 51-136 2,4,6-Trich!orophenol 0.0300 0.020:) mg IL 68 50-127

LCS LCS :surrogate %Recovery Qua/Iner Limits 2-Fluorobipl1eny/ 64 46-124

2-Fluorophenol 30 13-113 Nitrobenzene-d5 66 36.126

Phenol-d5 58 17 -127 Tel)Jhenyl-d14 76 44-149 2,4,6-Tribromophenof 68 26-150


Spike LCSO LCSO 0/oRec. RPO Analyte Added Result Qualifier Unit 0 o/oRec Limits RPO Limit Aniline 0.0300 0.0201 mg/L 67 21-120 11 30 Bis(2-chloroethyl)ether 0.0300 0,0233 mg IL 78 44-120 12 30

bis (2-chloroisopropyl) ether 0.0300 0.0285 mg/L 95 33-121 12 30 Bis(2-ethylhexyl) phthalate 0.0300 0.0288 mg IL 96 52-147 10 30 Butyl benzyl phthalate 0.0300 0.0282 mg/L 94 54 .133 9 30 4-Chloroaniline 0.0300 0.0178 mg IL 59 26.120 11 30 2-Chloronaphthalene 0.0300 0.0220 mglL 73 52-121 11 30 2-Chlorophenol 0.0300 0.0208 mg/L 69 40-120 28 30 Dlbenzofuran 0.0300 0.02:)3 mglL 78 56-122 12 30 2,4-Dichlorophenol 0.0300 0.0232 mg IL 77 49-120 17 30 Diethyl phthalate 0.0300 0.0265 mg/L 88 50-137 15 30 2,4-0imethylphenol 0.0300 0.0193 mg IL 64 48-120 9 30 Dimethyl phthalate 0.0300 0.0227 mg/L 76 57 -124 ·12 30


Page 94 of 140 2/1/2017

II

QC Sample Results Client: C-K Associates Project/Site; Moffat & Nichol

TestArnerica Job ID: 400-132540-1

Method: 82700 - Semivolatile Organic Compounds (GCIMS).(Continued)


Spike LCSD LCSD o/oRec. RPO Analyte Added Result Qualifier Unit D 0/C)Rec Limits RPO Limit

2,4-Dinitrophenol 0.0600 0.0250 mg/L 42 10-150 70 30 2,4-Dinitrotoluene 0.0300 0.0239 mg/L 80 54 .142 13 30 2,6-Dinitrotpluene 0.0300 0.0218 mg/L 73 55-130 12 30

Di-n-octyl phthalate 0.0300 0.0283 mg/L 94 57 -138 13 30

Hexachlorobenzene 0.0300 0.0218 mg/L 73 52-129 10 30 Hexach!orobutadiene 0.0300 0.0211 mg/L 70 45-120 12 30

Hexachlorocyclopentadiene 0.0300 0.00510 mg/L 17 10-134 20 30

Hexachloroethane 0.0300 0.0233 mg/L 78 41 -120 11 30 lsophorone 0.0300 0.0238 mg/L 79 48-120 14 30 2-Nitroanlline 0.0300 0.0264 mg/L 88 51 -145 12 30

3-Nltroanifin'e 0.0300 0.0223 mg/L 74 37 .127 11 30

4-Nitroaniline 0.0300 0.0228 mg/L 76 36 .137 14 30 Nitrobenzene 0.0300 0.0233 mg/L 78 45-120 12 30

4-Nitrophenol 0.0600 0.0474 mg/L 79 23 .146 14 30

N-NitrosodJ-n-propylamine 0.0300 0.0269 mg/L 90 45-120 11 30

N-Nitrosodiphenylamine 0.0298 0.0222 mg/L 75 54-120 11 30

Pentachlorophenol 0.0600 0.0321 mg/L 54 31 -130 29 30 Phenol 0.0300 0.0216 mg/L 72 40-120 21 30

1,2.4-Trichlorobenzene 0.0300 0.0210 mg/L 70 47 -120 12 30 2,4,5-Trichlorophenol 0.0300 0.0231 mg/L 77 51 -136 14 30 2,4,6-Trichlorophenol 0.0300 0,0234 mg/L 78 50-127 14 30

LCSD LCSD Surrogate %Recovery Qualifier Limits 2~Fluorobfphenyl 74 46-124 2-Fluorophenol 58 13.113

Nitrobenzene-d5 78 36-126

Phenof-d5 76 17 -127 Terphenyl-d14 90 44-149 2, 4,6-Tribromophenol 79 26-150

Method: .82700 LL - Semivolatile Organic Compounds by GC/MS - Low Level

Lab Sample ID: MB 400·338284/1-A Client Sample ID: Methoc;I Blank Matrix: Water Prep Type; Total/NA Analysis Batch: 338569 Prep Batch: 338284

MB MB

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae Acenaphthene <0.000032 0.00020 0.000032 mg/L 01/1211716:23 01/16/1717'40

Acenaphthylene <0.000045 0.00020 0.000045 mg/L 01/12117 16:23 01/16/1717:40

Anthracene <0.000032 0.00020 0.000032 mg/L 01/1211716:23 01/16/1717:40

Benzq[a]anthracene <0.000046 0.00020 0.000046 mg/L 01/12117 16:23 01/16/1717:40

Benzo[a]pyrene <0,000042 0.00020 0.000042 mg/L 01/1211716:23 01/16/1717:40

Benzo[b]fluoranthene <0.000034 0.00020 0.000034 mg/L 01/12117 16:23 01/16/1717:40

Benzo[k}fluoranthene <0.00010 0.00020 0.000.10 mg/L 01/1211716:23 01/16/1717:40

Chrysene <0.000074 0.00020 0.000074 mg/L 01/1211716:23 01/16/1717:40

Dibenz(a,h)anthracene <0.000050 0,00020 0.000050 mg/L 01/1211716:23 01/16/1717:40

Fluoranthene <0.000068 0,00020 0.000068 mg/L 01/1211716:23 01/16/1717:40

Fluorene <0.00011 0.00020 0.00011 mg/L 01/1211716:23 01/16/1717:40

TestArnerica Pensacola

Page 95 of 140 2/1/2017

E



Method: 82700 LL - Semivolati!e Organic Compounds by GC/MS - Low Level {Continued)


MB MB


lnden6(1 ,2,3-cd]pyrene <0.000043

2·Methylnaphthalene <0.000060 Naphthalene <0.000094

Phenanthrene <0.000036

Pyrene <0.000040

MB MB Surrogate %Recovery Qualifier

2·Fluorobiphenyl 108

Nitrobenzene-d5 100

Terphenyl-d14 140 x

Lab Sample ID: LCS 400·33828412-A Matrix: Water Analysis Batch:_ 3.3.8569


Acenaphthylene

Anttiracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzofk]fiuoranthene

Chrysene Dibenz{a,h)anthrace_ne Fluoranthene

Fluorene

lndeno[ 1,2,3·cd]pyrene 2·Methylnaphthatene

Naphthalene

Phenanthrene

Pyrene

Surrogate 2~Fluorobiphenyl

Nitrobenzene-dS

Terp/1eny/-d14

LCS LCS

%Recovety Qua/If/er 80

91

89

Lab .Sample ID: LCSD 400-33828413-A Matrix: Wa_ter Analysis Balch: 338569


Acenaphthylene

Anthracene

Benzo[a]anthracene Benzo[a]pyrene


RL MDL Unit D Prepared Analyzed Oil Fae

0.00020 0.000043 mg/L 01/1211716:23 01116117 17:40 1 0.00020 0.000060 mg/L 0111211716:23 01116117 17:40 0.00020 0.000094 mg/L 0111211716:23 0111611717:40

0.00020 0.000036 mg/L 01/1211716:23 01116117 17:40

0.00020 0.000040 mg IL 0111211716:23 01116117 17:40

Ll1nlts Prepared Analyzed Dll Fae

15-122 0111211716:23 01116117 17:40 1

19-130 0111211716:23 0111611717:40 1

33 -138 0111211716:23 01116117 17:40


Spike LCS LCS 0/oRec.

Added Result Qualifier Unit D 0/oRec Limits

0.120 0.116 mg/L 96 41-120

0.120 0.124 mg/L 103 44 -120 0.120 0.122 mg/L 102 49 -120

0.120 0.124 mg/L 103 61-135

0.120 0.125 mg/L 104 52-120

0.120 0.126 mg/L 105 53-134

0.120 0.123 mg/L 102 57 -134

0.120 0.120 mg/L 100 55 -122

0.120 0.122 mg IL 102 48. 146

0.120 0.125 mg IL 104 54-128

0.120 0.116 mg IL 97 45-125

0.120 0.120 mg/L 100 43-142

0.120 0.120 mg/L 100 32-124

0.120 0.112 mg IL 93 39.125

0.120 0.120 mg/L 100 48-120

0.120 0.130 mg/L 108 48-132

Limits 15-122

19-130

33-138

Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 338284

Spike LCSD LCSD o/oRec. RPO Added Result Qualifier Unit D o/ciRec Limits RPO Limit

0.120 0.120 mg IL 100 41-120 4 56 0.120 0.130 mg IL 108 44-120 5 56

0.120 0.134 mglL 112 49-120 9 51

0.120 0.127 n1g/L 106 61-135 3 49 0.120 0.131 mg/L 109 52.120 5 50


Page 96 of 140 2/112017

B



Method: 8270D LL. Semivolatile Organic Compounds by GC/MS ·Low Level (Continued)


Spike LCSO LCSO o/oRec, RPO Analyte Added Result Qualifier Unit 0 o/oRec Limits RPO Limit Benz6[b]fiuoranthene 0.120 0.133 mg IL 111 53-134 6 54

Benzo[kJfluoranthene 0.120 0.134 mg IL 111 57-134 8 52 Chrysene 0.120 0.129 mg IL 107 55-122 7 50 Oibenz(a,h)anthracene 0.120 0.131 mgll 109 48-146 6 50 Fluoranthene 0.120 0.136 mg/L 113 54-128 8 52 Fluorene 0.120 0.126 mglL 105 45-125 8 56 lndeno[1 ,2,3-cd]pyrene 0.120 0.128 mg/L 107 43-142 7 51 2-Methylnaphthalene 0.120 0.124 mg IL 104 32-124 3 57 Naphthalene 0.120 0.119 mg IL 100 39-125 6 56 Phenanlhrene 0.120 0.129 mg/L 107 48-120 7 56 Pyrene 0.120 0.141 mg IL 117 48-132 8 52

LCSD LCSD Surrogate %Recovery Quaflfler Limits 2-Fluorobipl1enyl 86 15-122

Nifrobenzene-d5 92 19-130

Terphenyl-d14 92 33-138

Lab Sample ID: MB 400-33912511-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125

MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae Ac~naphthene <0.000032 0.00020 0.000032 mg IL 0111911715:31 01124117 15:18 1 Acenaphthylene <0.000045 0.00020 0.000045 mg/L 01119/1715:31 01/24/17 15:18 Anthracene <0.000032 0.00020 0.000032 mg/L 0111911715:31 01/24/17 15:18

Benzo[a]anthracene <0.000046 0.00020 0.000046 mg/L 01/1911715:31 01124/17 15:18

Benzo[a]pyrene <0.000042 0.00020 0.000042 mg/L 01119/1715:31 01/24/17 15:18

Benzo{b]fluoranthene <0.000034 0.00020 0.000034 mg/L 01119/1715:31 01/24117 15:18 Benzo[k]fluoranthene <0.00010 0.00020 0.00010 mg/L 01/19/1715:31 01124117 15:18

Chrysene <0.000074 0.00020 0.000074 mg/L 0111911715:31 0112411715:18

Dibenz(a,h)anthracene <0.000050 0.00020 0.000050 mg IL 01/19/1715:31 01/2411715:18

Fluoranthene <0.000068 0.00020 0.000068 mg/L 01/1911715:31 0112411715:18 Fluorene <0.00011 0.00020 0.00011 mg/L 01/19/1715:31 01124/17 15:18

lndeno[1,2,3-cdJpyrene <0.000043 0.00020 0.000043 mg/L 0111911715:31 01124/17 15:18 2-Methylnaphthalene <0.000060 0.00020 0.000060 mg/L 01/1911715:31 01/24/1715:18 Naphthalene <0.000094 0.00020 0.000094 mg/L 01/19/1715:31 01/24/1715:18

Phenanthrene <0.000036 0.00020 0.000036 mg/L 01/19/1715:31 01124117 15:18

Pyrene <0.000040 0.00020 0.000040 mg/L 01119/1715:31 01124117 15:18

MB MB Surrogate %Recovery Qua/If/er Limits Prepared Analyzed Dlf Fae

2-Ffuorobiplienyl 116 15-122 01119117 15:31 01124117 15:18 1

Nitrobenzene-dS 101 19-130 01119117 15:31 0112411715:18 1 Terphenyl-d14 135 33-138 0111911715:31 01124117 15:18


Page 97 of 140 2/1/2017

B

Client: C-K Associates Projecl/Site: Moffat & Nichol


Method: 82700 LL - Semivolatite Organic Compounds by GC/MS - low Level (Continued)

Lab Sample ID: LCS 400-33912512-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125

Spike LCS LCS 0/oRec. Analyte Added Result Qualifier Unit 0 0/oRec Limits Acenaphthene 0.120 0.127 mg/L 106 41-120 Acenaphthylene 0.120 0.126 mg/L 105 44-120

Anthracene 0.120 0.125 n1g/L 104 49-120 Benzo[a]anthracene 0.120 0.129 mgfL 108 61 .135

Benzo[aJpyrene 0.120 0.120 mg/L 100 52-120 Benzo{b}fluoranthene 0.120 0.124 mg/L 103 53 .134

Benzo[k]fluoranthene 0.120 0.116 mg/L 97 57-134

Chrysene 0.120 0.116 mg/L 97 55 - 122 Dibenz(a,h)a_nthracene 0.120 0.132 mg/L 110 48-146

Fluoranthene 0.120 0.130 mg/L 109 54 .128

Fluorene 0.120 0.129 mg/L 107 45-125

lndeno[1,2,3·cd]pyrene 0.120 0.127 mg/L 106 43-142 2~Methylnaphthalene 0.120 0.121 mg/L 101 32-124 Naphthalene 0.120 0.111 mg/L 92 39-125

Phenanthrene 0.120 0.131 mg/L 109 48-120 Pyrene 0.120 0.135 mg/L 113 48-132

LCS LCS

Surrogate %Recovety Quallfler Limits 2-Fluoro!Jiphenyl 114 15-122 Nitrobenzene-05 100 19-130

Terpllenyl·d-14 132 33-138

Lab Sample ID: LCSD 400-33912513-A Client Sample ID: Lab Control Sample Dup Matrix; Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125

Spike LCSO LCSO o/oRec. RPO Analyte Added Result Qualifier Unit 0 o/aRec Limits RPO Limit Acenaphthene 0.120 0.115 mg/L 96 41-120 10 56 Acenaphthylene 0.120 0.115 mg/L 96 44-120 9 56 Anthracene 0.120 0.111 mg/L 92 49-120 12 51 Benzofa]anthracene 0.120 0.116 mg/L 97 61-135 11 49 Benzo{a]pyrene 0.120 0.109 mg/L 91 52-120 10 50 Benzo[b)fiµoranthene 0.120 0.112 mg/L 94 53-134 10 54 Benzo[k]fluoranthene 0.120 0.104 mg/L 87 57 -134 11 52 Chrysene 0.120 0.103 mg/L 86 55-122 12 50 Dlbenz(a,h)anthracene 0.120 0.114 mg/L 95 48-146 15 50 Fluoranthene 0.120 0.118 mg/L 98 54-128 10 52 Fluorene 0.120 0.116 mg/L 96 45-125 11 56 lndeno[ 1,2,3-cd]pyrene 0.120 0.110 mg/L 92 43-142 14 51 2~Methy1naphthalene 0.120 0.112 mg/L 93 32-124 8 57 Naphthalene 0.120 0.103 mg/L 86 39-125 7 56 Phenanthrene 0.120 0.118 mg/L 99 48-120 10 56 Pyrene 0.120 0.121 mg/L 101 48-132 11 52

LCSD LCSD Surrogate %Recovery Quallfler Lfmlts 2-Fiuorohiphenyl 105 15-122 Nitrobenze11e-d5 91 19-130


Page 98 of 140 21112017

E

QC Sample Results Client: C-K Associates Project/Site: Moffat & Nicllol


Method: 82700 LL - Semivolatile Organic Compounds by GCIMS. Low Level (Continued)

Lab Sample ID: LCSD 400-339125/3-A Matrix: Water Analysis Batch: 339599

Surrogate Terphenyl-d14

LCSD LCSD %Recovery Qualifier

117

Lirnits

33-138

Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 339125

Method: MAVPH - Massachusetts • Volatile Petroleum Hydrocarbons (GC)

Lab Sample ID: Ms 400-338604/1-A Matrix: Solid Analysis Batch: 338571

MB MB Analyte Result Qualifier C6-C8 Aliphatics <1.5

C8-C10 Aliphatics <2.5 C8-C 10 Aromatics <t3,

MB MB Surrogate %Recovery Qualifier a,a,a-Trifluorotoluene (fid) 75 a,a,a-Trifluorotoluene (pid) 76

Lab Sample ID: LC.S 400-338604/2-A Matrix: Solid Analysis Batch: 338571

Analyte CB-C 1 O Aromatics

C5-C8 Aliphatics

C9-C12 AllphaUcs

Surrogate a,a,a-Trifluorotoluene (fid)

a,a,a-Trifluorotoluene (pid)

LCS LC$ %Recovery Qualifier

107

.109

Lab Sample IP: LCSD 400-338604/3-A Matrix: Solid Analysis Batch: 338571

Analyte CB-C 1 O Aromatics

C5-C8 Aliphatics

C9-C12 Allphatics

Surrogate a,a,a-Trifluorotoluene (fid)

a,a,a-TrifluorotoJuene (pid)

LCSD LC.SD %Recov~ry 'Qualifier

100

101

RL 1.5 2.5

1.3

Lltnlts

70-130

70. 130

Spike LCS

Added Result

2.50 2.57 15.0 13.0

17.5 16.8

Limits 70-130

70-130

Spike LCSD Added Result

2.50 2.39

15.0 12.4

17.5 15.2

Limits 70-130

70-130

Page 99 of 140

MDL Unit 1.5 mg/Kg

2.5 mg/Kg

1.3 mg/Kg

LCS Qualifier


D Prepared Analyzed OJI Fae 0111611710:30 0111611.712:45 50 01/16117 10:30 01/16117 12:45 50 0111611710:30 01/16117 12:45 50

Prepared Analyzed Dll Fae 01111!/1710'30 01116117 12:45 50

0111611710:30 01116117 12:45 50

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338604 o/oRec.

Unit

mg/Kg

mg/Kg

mg/Kg

D %Rec Limits

10:3 70-130 87 70-130

96 70-130

Client Sample ID: Lab Contro.I Sample Pup Prep Type: Total/NA Prep B.atch: 338604

LCSD Qualifier Unit

mg/Kg

mg/Kg

mg/Kg

o/oRec. RPO 0 %Rec Limits RPO Limit

96 70-130 7 25

83 70-130 87 70.130

5 10

25

25


2/1/2017



Method: MAVPH. Massachusetts. Volatile Petroleum Hydrocarbons (GC) (Continued)

Lab Sample ID: 400-132588·6 MS Matrix: Solid Analysis Batch: 338571

Sample San1ple

Analyte Result Qualifier C8-C10 Aromatics <6.1

C5-C8 Aliphatics <13

C9-C12 A!iphatics <6_9

MS MS Surrogate %Recovery QuallfJer a,a,a-Ttifluorotoluene (fid) 79 a,a,a-Trifluorototuene (pid) 79

Lab Sample ID: 400-132588-6 MSD Matrix: Solid Analysis Batch: 338571

Sample Sample

Analyte Result Quallfler C8-C10 Aromatics <6.1

C5-C8 Aliphatics <13

C9-C12 Alfphatics <6.9

MSD MSD

Surrogate %Recovery Qualifier

8,a,a-Trifluorotoluene (fid) 94 fJ,a,a-Trifluorotoluene (pid) 93

La.b Sample ID: MB 400-339057/2 Matrix: Water Analysis Batch: 339057

MB MB


C6-C8 Aliphatics <0.030

C8-C10 Aliphatics <0.050

C8-C10 Aromatics <0.025

MB MB Surrogate %Recovery Qualifier

a,a,a-Trifluoroto/uene (fid) 106. a,a,a-Trifluorotoluene (pid) 106

Lab Sample ID: LCS 400-3390.57/3 Matrix: Waler Analysis Batch: 339057

Analyte

C8-C10 Aromatics

C5-C8 AHphatics _C9-C12 Aliphatics

Surrogate

a,a,a-Trifluorotoluene (fid)

a,a,a-Trifluorotoluene (pid)

LCS LCS

%Recovery Qualifier

107 108

Spike

Added

12.2

73.4

85.7

Limits 70-130

70-130

Spike

Added

.12.2

73.4

85.7

Limits 70-130 70-130

RL

0.030

0.050

0.025

Limits to: 130

70-130

Spike

Added

o.o5oo 0.300

0.350

Limits 70-130 70-130

MS MS

Result Qualifier

11.6

56.3

68.2

MSD MSD

Result Quallfler

13.2

66.6

76.4

MDL Unit

0.030 mg/L

0.050 mg/L

0.025 mg/L

LCS LCS

Result Qualifier

0.0474

0.259

0.319

Page 100 of 140

Unit mg/Kg

mg/Kg

nig/Kg

Unit

mg/Kg

mg/Kg

mg/Kg

D

Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338604 0/oRec.

0 o/oRec Limits i;1 94 70-130 0 77 70-130 ·l:l 80 70-130

Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 338604 o/oRec. RPO

0 o/oRec Limits RPO Limit n 108 70-130 13 25 .1;1 91 70-130 17 25 n 89 70-130 11 25

Client Sample ID: Meth<>d Blank Prep Type: T<>tal/NA

Prepared Analyzed Oil Fae

0111911713:26 1

01/19/17 13:26

01/19/1713:26

Prepared Analyzed DI/ Fae 0171911113.'26 1 0111911713:26

Client Sample ID: Lab C<>ntrol Sample Prep Type: Total/NA

%Rec. Unit 0 ~%Rec j..lmlts

mg/L 95 70-130

mg/L 86 70-130

mg/L 91 70-130


2/1/2017

E



Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)

Lab Sample ID: LCSO 400-339057/4 Matrix: Water Analysis Batch: 339057

Analyte CB-C1 O Aromatics

C5-C8 A!iphatics

C9-C12 Aliphatics

Surrogate a,a,a-Trif/uorotoluene (fid)

8,a,a-Trifluorotoluene (pid)


105

107

Spike

Added

0.0500 0.300

0.350

Lltnlts

70-130

70-130

Method: 8011 - EDS, DBCP, and 1.,2,3-TCP (GC)


MB MB

LCSD

Result

0.0488 0.260

0.327

LCSD

Qualifier

Client Sample ID: Lab Control Sample Oup Prep Type: Total/NA

Unit mg/L

mg/L

n1g/L

o/oRec. RPO 0 0/oRec Limits RPO Limit

98 70-130 3 25 87 70-130 1 25 93 70-130 3 25

Client sample ID: Method Blank Prep Type: T.otal/NA Prep Batch: 339493

-Analyte

1,2-Dibromo-3-Chloropropane

Result Qualifier <0.0000055

RL MOL Unit O Prepared Analyzed DU Fae 0.000030 0.0000055 mg/L 0112311716:25 01126117 21:11 1

Surrogate 4-Bromof/uorobenzene

MB MB

%Recovery Qua/If/er 109

Limits

51-149

Lab Sample ID: LCS 400-339493/2-A Matrix: Water Analysis Batch: 339878

'Analyte

1,;2-Dibromo-3-Ch!oropropane

Surrogate -4-Bromofluorobenzene

LCS LCS %Recovery Qualifier

97

Lab Sample JO: LCSO 400-33949313-A Matrix: Water Analysis Batch: 339878

Analyte 1,2-Dibromo-3-Chloropropane

Surrogate

4·Bromof/uorobenzene

LCSD LCSD %Recovety Qualifier

108

Spike Added

0.000100

Limit~

51-149

Spike Added

0.000100

Limits

51-149

LCS LCS

Prepared Analyzed Dlf Fae 01123/1716:25 01126117 21:11 1

Client Sample 10: Lab Control Sample Prep Type: Total/NA Prep Batch; 339493 o/oRec.

Result Qualifier Unit 0 o/oRec Limits

0.000111 mg/L 111 60-140

Client Sample lO: Lab ControJ Sample Oup Prep Type: TotaJ/JllA Prep Batch: 33.9493

LCSD LCSO

Result Qualifier Unit 0.000117 mg/L

0 %Rec 117

0/oRec. RPO Limits RPO Limit 60-140 5 30


Page 101 of 140 2/1/2017

E


Method: 80818 • Orga11ochlori11e Pesticides (GC)

Lab Sample JD: MB 400-338239/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239

MB MB

Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed DH Fae Aldrin <0.00000030 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25 1

0 alpha-BHC 0.00000102 J 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25

6

E beta-BHC <0.00000030 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/1712:25

0 delta-BHC 0.00000176 J 0.0000050 0.0000002 mg/L 01/12/1713:08 01/19/1712:25

1 gamma-BHC (Undane) <0.0000025 0.0000050 0.0000025 mg/L 01 /12/17 13:08 01/19/1712:25 -atpt}a-Chlordane <0.00000042 0.0000050 0.0000004 mg/L 01/12/1713:08 01119/1712:25

2 gamma-Chlordane <0.00000032 0.0000050 0.0000003 mg IL 01/12/1713:08 0111911712:25

2 4,4'-DDE <0.00000022 0.0000050 0.0000002 mg IL 01112/1713:08 01/19117 12:25

2 Dieldrin 0.000000678 J 0.0000050 0.0000003 mg/L 01 /12/17 13:08 01/19/17 12:25

0 Endosulfan I <0.00000030 0.0000050 0.0000003 mg/L 01112/17 13:08 01/19/17 12:25

0 Endosulfan l I <0.00000074 0.0000050 0.0000007 mg/L 01/12/1713:08 01/19/17 12:25

4 Endosu!fan sulfate <0.00000021 0.0000050 0.0000002 mg/L 01/12/1713:08 01/19/17 12:25

1 Endrin <0.00000030 0.0000050 0.0000003 mg/L 01/1211713:08 01/19/1712:25

0 Endrin aldehyde <0.00000028 0.0000050 0.0000002 mg/L 01/12/1713:08 01119/17 12:25

8 Endrin ketone <0.00000038 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25

8 Heptachlor <0.00000031 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/1712:25

1 Heptachlor epoxide <0.00000032 0.0000050 0.0000003 mg/L 01/12117 13:08 01/19/1712:25

2 Methoxychlor <0.00000041 0.0000050 0.0000004 mg/L 01/12/1713:08 01/19/17 12:25

1 Toxapheoe <0.000030 0.00030 0,000030 mg/L 0111211713:08 01/19/17 12:25

MS MS $urrogate %Recove_ty Qua/If/er Limits Prepared Analyzed Dll Fae DCB Decachlorobipheny/ 56 10-130 0111211713:08 0111911712:25 1

Tetrachloro-m-xyJene gg 43-130 0111211713:08 0111911712:25 1

. Lab Sample ID: LCS 400-338239/2-A Client Sample ID: Lab Control Sampl!! Matrix: Water Prep Type: Total/NA Analysis Saleh: 339079 Prep Batch: 338239

Spike LCS LCS o/GRec. Analyte Mded Result Qualifier Unit 0 %Rec Limits

Aldrin 0.000500 0.000445 mg/L 89 52-150 alpila-BHC 0.000500 0.000403 mg/L 81 50 -150 beta-BHC 0.000500 0.000409 mg/L 82 58-150 delta-BHC 0.000500 0.000377 mg/L 75 42 .150 gamma~BHC {Lindane) 0.000500 0.000389 n1g/L 78 53-150 alpha-Chlordane 0.000500 0.000416 mg/L 83 63 .150


Page 102of140 2/1/2017


Method: 80818 • Organochlorine Pesticides (GCJ (Continued)

Lab Sample ID: LCS 400-338239/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239

Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit D o/oRec Limits gamm·~-·ch10fd8rie 0.000500 0.000362 mg/L 72 62-150

4.4'·DDE 0.000500 0.000408 mg IL 82 65-150 Die!drln 0.000500 0.000373 mg IL 75 64-150

Endosulfan l 0.000500 0.000367 mg IL 73 40-127

B Endosulfan II 0.000500 0.000415 mg IL 83 40-135

Endosurran sulfate 0.000500 0.000400 n1g/L 80 50-150 Endrin 0.000500 0.000402 mg IL 80 63-150

Endrin aldehyde 0.000500 0.000424 mg/L 85 40-150 Endrln ketone 0.000500 0.000392 mg/L 78 52-150 Heptachlor 0.000500 0.000402 mg/L 80 59-150

Heptachlor epoxid€? 0.000500 0.000386 mg/L 77 63 .150

Methoxychlor 0.000500 0.000424 mg IL 85 57 -150


bcB Decachlorobiphenyl 67 10-130 Tetrachforo-m-xylene 88 43-130

Lab Sample ID: LCSD 400-33823913-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239

Spike LCSD lCSD o/oRec. RPO Analyte Added Result auaHfler Unit D o/oRec Limits RPO Limit Aldrin 0.000500 0,000462 mg/L 92 52-150 4 40 alpha-BHC 0.000500 0.000407 mg/L 81 50-150 40 bela·BHC 0.000500 0.000404 mg IL 81 58-150 1 40 delta-BHC 0.000500 0.000370 mg IL 74 42-150 2 40 gamma-BHC (Lindane) 0.000500 0.000383 mg IL 77 53-150 2 40 alpha-Chlordane 0.000500 0.000412 mg/L 82 63-150 40 gamma-Chlordane 0.000500 0.000355 mg/L 71 62-150 2 40 4.4'-DDE 0.000500 0.000399 mg IL 80 65-150 2 40

Dieldrin 0.000500 0.000360 mg/L 72 64-150 4 40 Endosulfan J 0.000500 0.000356 mg/L 71 40-127 3 40 Endosulfan II 0.000500 0.000386 mg IL 77 40-135 7 40

Enqosu!fan sulfate O.OOQ500 0.000362 mg IL 72 50-150 10 40

Endrin 0.000500 0.000380 mg/L 76 63-150 6 40 'Endrin a)dehyde 0.000500 0.000391 mg/L 78 40-150 8 40

Endrin ketqne 0,000500 0.000347 mg/L 69 52-150 12 40 Heptach!or 0.000500 0.000389 mg IL 78 59-150 3 40 Heptachtor-epoxlde 0.000500 0.000382 mg/L 76 63-150 40 Methoxychlor 0.000500 0.000368 mg/L 74 57 -150 14 40

LCSD LCSD Surrogate %Recovery Qualifier Limits

DCB Decacf11orobipheny/ 52 10-130 TetraCh/oro-m-xylene 91 43-130


Page 103of140 2/1/2017


QC Sample Results

Method: 808113 • Organoch!orine Pesticides (GC) (Continued)

Lab Sample ID: MB 400·338557/10-A Matrix: Solid Analysis Batch:.338801

MB MB Analyte Result Qualifier

Aldrin <0.00061

alpha-BHC <0.00024

beta-BHC <0.00050

delta-BHC <0.00032

gamma-BHC (Undane) <0.00022

alpha-Chlordane <0.00028

gamma-Chlordane <0.00027

4,4'-DDD <0.00019

4,4'-DDE <0.00027

4,4'-DDT <0.00077

Dietdrin <0.00036

Endosulfan I <0.00021

Endosulfan II <0.00023

Endosulfan .sulfate <0.00021

Endrin <0.00019

Endrin aldehyde <0.00029

Endrln ketone <0.00035

Heptachlor <0.00024

Heptachlor epoxide <0.00045

Methoxychlor <0.00033

Toxaphene <0.029

MB MB Surrogate %Recovery Qualifier ·ocB DecaCh!orobiphenyJ

Tetrachlorcrm-xy!_ene

Lab Sample ID; LCS 4!l0·338557/9·A Matrix; S.olid Analysis £latch: 338801

g9

95

RL MDL 0.0017 0.00061

0.0017 0.00024

0.0017 0.00050

0.0017 0.00032

0.0017 0.00022

0.0017 0.00028

0.0017 0.00027

0.0017 0.00019

0.0017 0.00027

0.0017 0.00077

0.0017 0.00036

0.0017 0.00021

0.0017 0.00023

0.0017 0,00021

0.0017 o.0001g

0.0017 0.00029

0.0017 0.00035

0.0017 0.00024

0.0017 0.00045

0.0017 0.00033

0.10 0.029

Limits 26-129 31-122

Spike LCS LCS

Unit mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

D



Prepared

01/16/17 09:24

01/16117 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01116/17 09:24

01 /16/17 09:24

01 /16/17 09:24

01/16/17 09:24

.01116/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

01/16/17 09:24

Analyzed

01/17/17 19:18

01/17/17 19:18

01/17/17 19:18

01/17/1719:18

01117117 19:18

01/17/17 19:18

01/17/1719:18

01/17/1719:18

01/17/17 19:18

01/17/1719:18

01/17/1719:18

01/17/1719:18

01/17/17 19:18

01/17/17 19:18

01/17/17 19:18

01/17/17 19:18

01/17/17 19:18

01/17/1719:18

01/17/1719:18

01/17/17 19:18

01/17/1719:18

Oil Fae

1

1

Prepared Analyzed DI/ Fae

01116117 09:24 0111711719:18 1 011161.17 09:24 0111711719:18 1

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep flatch: 338557 %Rec.

An~lyte Added Result Qualifier Unit D 1%Rec Limits Aldrin

alpha-BHC beta-BHC delta-BHC gamma-BHC (lindane)

alpha-Chlordane

gamma·Chtordane

4,4'-DDD

4,4'-DDE

4,4'-DDT

Die!drin

Endosulfan I

Endosulfan II Endosulfan sulfate

Endrin

Endrfn aldehyde

Endrfn ketone

0.0333 0.0452

0.0333 0.0291

0.0333 0.0325

0.0333 0.0328

0.0333 0.0288

0.0333 0.0327

0.0333 0.0330

0.0333 0.0343

0.0333 0.0392

0.0333 0.0353

0.0333 0.0398

0.0333 0.0324

0.0333 0.0353

0.0333 0.0303

0.0333 0.0335

0.0333 0.0345

0.0333 0.0313

Page 104of140

mg/Kg 136 47 -137

mg/Kg 87 50-148

mg/Kg 98 46-133

mg/Kg 98 10-162

mg/Kg 86 50-148

mg/Kg 98 35.134

mg/Kg 99 39-146 mg/Kg 103 46.152

n1g/Kg 118 49-148

mg/Kg 106 44 -168 mg/Kg 119 41-164

mg/Kg 97 50-141

mg/Kg 106 47 -148

mg/Kg 91 50 -145

mg/Kg 100 45-159

mg/Kg 103 10.190

mg/Kg 94 48-159


2/112017


Method: 8081 B • Organochlorine Pesticides (GC) (Continued)

Lab Sample ID: LCS 400.338557/9-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 338801 Prep Batch: 338557

Spike LCS LCS %Rec. ·Analyte Added Result Qualifier Unit D o/oRec Limits HePt8ch.lor 0.0333 0.0292 mg/Kg 87 46-158 Heptachlor epoxide 0.0333 0.0330 mg/Kg 99 49-148 Methoxych!or 0.0333 0.0329 mg/Kg 99 40.164

LCS LCS B Surrogate %Recovery Quafifier Limits

DCB Decachlorobiphenyl 86 26-129 Tetrachforo-1n-xylene 85 31-122

Lab.Sample ID: 400.132588.6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338801 Prep Batch: 338557

Sample Sample Spike MS MS 0/oRec. Analyte Result Qualifier Added Result Qualifier Unit D 0/oRec Limits Aldrin <0.0024 0.0681 0.0735 mg/Kg

,, 1b8 10-154 alpha-BHC <0.00096 0.0681 0.0548 mg/Kg " 80 15-152 beta-BHC <0.0020 0.0681 0.0625 mg/Kg " 92 10.160 della-BHC <0.0013 0.0681 0.0612 mg/Kg " 90 10-160 gamma-BHC (Lindane) <0.00088 0.0681 0.0521 mg/Kg i) 77 26-142 alpha-Chlordane 0.0014 J 0.0681 0.0714 mg/Kg " 103 10-160 gamma-Chlordane 0.0025 J 0.0681 0.0718 mg/Kg " 102 10-160 4,4'-DDD <0.00076 0.0681 0.0694 mg/Kg :l;l 102 13-146 4,4'-DDE <0.0011 0.0681 0.0799 mg/Kg " 117 23-143

4,4'-DDT <0.0031 0.0681 0.0685 mg/Kg " 101 10-160

Die!drln <0.0014 0.0681 0.0649 mg/Kg " 95 10-160 Endosulfan I <0.00084 0.0681 0.0593 mg/Kg ·.t;t 87 10.160

Endosu!fan II <0.00092 0.0681 0.0736 mg/Kg ,, 108 10-160 Endosulfan sulfate <0.00084 0.0681 0.0591 mg/Kg " 87 27 -143 Endrln <0.00076 0.0681 0.0659 mg/Kg " 97 20-156 Endrln aldehyde <0.0012 0.0681 0.0611 mg/Kg i) 90 14-160 Endrin ketone <0.0014 0.0681 0.0618 mg/Kg " 91 31.155

Heptachlor <0.00096 0.0681 0.0539 mg/Kg " 79 10-160 ,Hept~chlor epoxide <0.0018 0.0681 0.0655 mg/Kg " 96 10-160 Methoxychtor <0.0013 0.0681 0.0610 mg/Kg ~;; 90 10-160

MS MS Surrogate %Recovery Quaflfler Limits DCB Decachlorobiphenyl 81 26-129 Tetrachloro~tn-xylene 83 31-122

Lab Sample ID: 400'132586·6 MSD Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 336801 Prep Batch: 338557

Sample Sarnple Spike MSD MSD 0/oRec. RPO Analyte Result Qualifier Added Result Qualifier Unit D o/oRec Limits RPO Limit

Aldrin <0.0024 0.0681 0.0665 mg/Kg -l~ 98 10 .154 10 60 alpha-BHC <0.00096 0.0681 0.0539 mg/Kg " 79 15-152 2 60 bela-BHC <0.0020 0.0681 0.0552 mg/Kg " 81 10-160 12 60 delta-BHC <0.0013 0.0681 0.0530 mg/Kg " 78 10-160 14 60 gamrna-BHC (Undane) <0.00088 0.0681 0.0489 mg/Kg " 72 26-142 6 60


Page 105 of 140 2/1/2017


QC Sample Results

Method: SOS1B - Organochlorine Pesticides (GC) (Continued)


MSD MSD Analyte alpha-Chlordane gamma-Chlordane 4,4'-DDD

4,4'-DDE 4,4'-DDT

Sample Result 0.0014

Sample

Qualifier J

Spike

Added

0.0681 0.0681 0.0681 0.0681

0.0681 0.0681

0.0681

0.0681 0.0681 0.0681 0.0681

0.0681 0.0681 0.0681

0.0681


Die!drin Endosulfan I

Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde

Endrin ke~qne Heptachlor Heptachlor _epoxfde Methoxychlor

Surrogate

DCB Decachlorobiphenyl Tetrachloro-m-xylene

0.0025 J <0.00076

<O.Q011

<0.0031 <0.0014

<0.00084

<0.00092 <0.00084 <0.00076

<0.0012

<0.0014 <0.000.96

<0.00.18 <0.0013

MSO MSO

%Recovery Qualifier 61 68

Lab Sample ID: MB 400-33905411-A Matrix: Water Analysis .Batch: 339554

Analyte Aldrin

alpha-BHC

beta-BHC

df;llta-BHC

gamma-BHC (Undane) alpha~Chlordane

gamma~Ch!ordane

4,4'-DDD

4,4'-DDE

4,4'-DDT

Dieldrin

Endosulfan I

Endosulfan II


<0.00000030

<0.00000036

<0.00000030

<0.00000021

<0.0000025

<0.00000042

<0,00000032

<0.00000030

<0.00000022

<0.00000039

<0.00000030

<0.00000030

<0.00000074

0.0597 mg/Kg

Limits

26-129

31-122

0.0589 0.0617

0.0622 0.0528 0.0599

0.0525 0.0560

0.0481 0.0594 0.0518

0.0513 0.0486 0.0596

0.0480

RL MDL Unit

0.0000050 0.0000003 mg/L 0

0.0000050 0.0000003 mg/L 6

0.0000050 0.0000003 mg/L 0

0.0000050 0.0000002 mg/L 1

0.0000050 0.0000025 mg/L

0.0000050 0.0000004 mgll 2

0.0000050 0.0000003 mg/L 2

0.0000050 0.0000003 mg/L 0

0.0000050 0.0000002 mg/L 2

0.0000050 0.0000003 mg/L 9

0.0000050 0.0000003 mg/L 0

0.0000050 0.0000003 mg/L 0

0.0000050 0.0000007 mg/L 4

Page 106of140

mg/Kg mg/Kg

mg/Kg

mg/Kg n1g/Kg

mg/Kg mg/Kg

mg/Kg mg/Kg mg/Kg

mg/Kg mg/Kg

mg/Kg

mg/Kg


Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338557 %Rec. RPO

D o/cRec Limits RPO Limit

" 86 10-160 16 60 83 10-160 91 13-146

91 23-143 78 10.160 88 10-160 77 10.160 82 10.160

71 27-143 87 20-156

76 14-160

75 31-155 71 10.160

87 10-160 70 10.160

20 12

25 26 8

12

27 20 10 17

19 10 9

24

60 88

86

43 E 60 60

49 60 60 37

60 60 60

47


0 Prepared Analyzed 011 Fae b1ii9i1i10:03 01124117 11:48 1

0111911710:03 01/24/1711:48

0111911710:03 01124/1711:48

01119/1710:03 01124/17 11:48

01/1911710:03 01/24/1711:48

01/1911710:03 01124/17 11:48

01/19/1710:03 01/24/1711:48

01/19/1710:03 01124/1711:48

01/19/1710:03 01/24117 11:48

01/19/1710:03 01124/1711:48

01/19/1710:03 0112411711:48

01119/1710:03 0112411711:48

01119/1710:03 0112411711:48


2/1/2017


QC Sample Results

Method: 80818 • Organochlorine Pesticides (GC) (Continued)


MB MB

Analyte Result Qualifier RL MDL

Endosulfan sulfate <0.00000021 0.0000050 0.0000002 1

Endrin <0.00000030 0.0000050 0.0000003 0

Endrin aldehyde <0.00000028 0.0000050 0.0000002 8

Endrin ketone <0.00000038 0.0000050 0.0000003 8

Heptachlor <0.00000031 0.0000050 0.0000003 1

Heptachlor epoxlde <0.00000032 0.0000050 0.0000003 2

Methoxychlor <0.00000041 0.0000050 0.0000004 1

Toxaphene <0.000030 0.00030 0.000030

MB MB Surrogate %Recovery Qua/Iller Limits

DCB Decachlorobiphenyl 93 10. 130

Tetrachloro-m-xylene 69 43-130


Spike LCS LCS

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

Analyte Added Result Qualifier

Aldrln 0.000500 0.000398 alpha-BHC 0.000500 0.000408 beta-BHC 0.000500 0.000367 delta-BHC 0.000500 0.000446 gamma-BHC (Undane) 0.000500 0.000394 alpha-Chlordane 0.000500 0.000391 gamma-Chlordane 0.000500 0.000422 4,4'-DDD 0.000500 0.000421 4,4'-DDE 0.000500 0.000505 4,4'-DDT 0.000500 0.000387 Dieldrin 0.000500 0.000440 Endosulfan I 0.000500 0.000422 Endosu!fan IJ 0.000500 0.000396 Endosulfan sulfate 0.000500 0.000368 Endrln 0.000500 0.000418 Endr!n aldehyde 0.000500 0.000353 Endrin ketone 0.000500 0.000363

Heptachlor 0.000500 0.000348 Heptachlor epoxide 0.000500 0.000418 Methoxychlor 0.000500 0.000373

LOS LOS Surrogate %Recovery Quill/tier Limits

DCB Decac/1/orobiphenyl 53 10-130 Tetrac/1/oro·m·xylene 77 43.130

Page 107of140



D Prepared Analyzed Dll Fae

01119117 10:03 01124117 11:48 1

01119/1710:03 01/24/1711:48

01/1911710:03 01/2411711:48 1 E 01119/1710:03 01/24/1711:48

01/19/17 10:03 01/2411711:48

0111911710:03 01/2411711:48

0111911710:03 0112411711:48

01119/17 10:03 0112411711:48

Prepared Analyzed DI/ Fae 0111911710:03 0112411711:48 1 0111911710:03 0112411711:48

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339054 D/oRec.

Unit D 0/oRac Limits

mg/L 80 52 -150 mg/L 82 50.150

mg/L 73 58.-150

mg/L 89 42-150 mg/L 79 53-150 mg/L 78 63 -150

mg/L 84 62 -150 mg/L 84 58 -150 mg/L 101 65 -150

mg/L 77 59 -150 mg/L 88 64 -150 mg/L 84 40.127

mg/L 79 40.135

mg/L 74 50 -150

mg/L 84 63-150 mg/L 71 40 -150 mg/L 73 52 .150

mg/L 70 59.150

mg/L 84 63 .150 mg/L 75 57 -150


2/1/2017


QC Sample Results

Method: 808113 - Organochlorine Pesticides (GC) (Continued)


Lab Sample ID: LCSD 400·339054/3·A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 339554 Prep Batch: 339054

Spike LCSD LCSD 0/oRec. RPO

Analyte Added Result Qualifier Unit D o/oRec Limits RPO Lirnlt Aldrin 0.000500 0.000403 mg/L 81 52-150 40 alpha-BHC 0.000500 0.000412 mg IL 82 50-150 40 beta-BHC 0.000500 0.000402 mg IL 80 58-150 9 40 delta-BHC 0.000500 0.000457 mg IL 91 42-150 3 40 gamma-BHC (Lindane) 0.000500 0.000412 mg/L 82 53-150 4 40 alpha-Chlordane 0.000500 0.000414 mg IL 83 63-150 6 40 gamma-Chlordane 0.000500 0.000450 n1g/L 90 62-150 6 40

4.4'-DDD 0.000500 0.000454 mg/L 91 58-150 8 40 4.4'-DDE 0.000500 0.000500 mg IL 100 65-150 40

4,4'.DDT 0.000500 0.000417 mg IL 83 59-150 7 40

Dieldrin 0.000500 0.000472 mgll 94 64-150 7 40

Endosulfan l 0.000500 0.000447 mglL 89 40-127 6 40 Endosulfan II 0.000500 0.000429 mg/L 86 40-135 8 40 Endosu!fan sulfate 0.000500 0.000395 mg IL 79 50-150 7 40

Endrin 0.000500 0.000453 mg/L 91 63 .150 8 40

Endrin aldehyde 0.000500 0.000387 mg/L 77 40-150 9 40

Endrin ketone 0.000500 0.000386 mglL 77 52.150 6 40

Heptach!or 0.000500 0.000373 mgll 75 59-150 7 40

Heptachlor epoxide 0.000500 0.000440 mglL 88 63-150 5 40 Methoxychlor 0.000500 0.000385 mg/L 77 57 .150 3 40

LCSD LCSD Surrogate %Recovery Qualifier' Limits DCB lJecachforobiphenyi 106 10·~ 130

Tetrachloro-m-xylene 68 43-130

Method: MA-EPH - Massachusetts • Extractable Petroleum Hydrocarbons (GC)

Lab Sample ID: MB.400·339010/16-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010

MB MB Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed 011 Fae C10-C12 Aliphatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 01/2411717:14 1 C12~C16 Aliphatics <1.6 1.6 1.6 mg/Kg 01119/17 07:20 0112411717:14

C16-C35 Aliphatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 0112411717:14

MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae 1-Cl1forooctadecane 95 40-140 01119117 07:20 0112411717:14 1

Lab Sample ID: MB 400-339010/16-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010

MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae c10-c12 Aromatics <1.6 1.6 1.6 mg/Kg 01119/17 07:20 01124117 21:26 1 C12-C16 Aromatics <1.6 1.6 1.6 mg/Kg 01/19117 07:20 01124117 21:26

C21-C35 Aromatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 01124117 21:26


Page 108of140 2/112017

m



Method: MA-EPH - Massachw:;etts - Extractable Petroleum Hyctrncarbons {GC) (Continued)


MB MB


C16-C21 Aromatics <1.6

MB MB Surrogate %Recovery Qualifier o-Terphenyl 83


Analyte

C9-C18 Aliphatics

C19-C36 A!lphatics

'Surrogate 1-Chlorooctadecane

LCS LCS %Recovery Quallfler

98


Analyte C11-C22 Aromatics

Surrogate o-Terphenyl


123

Lab Sample ID: LCSD 400-339010/15.-A Matrix: Solid Analysis Batch: 339632

Analyte C9-C18 Aliphatics

C19·C36 Aliphatics

Surrogate 1-Ch!orooctadecane


106

Lab Sample ID: LCSD 400-339010/15-A Matrix: Solid Analysis Batch: 339633

Analyte C11-C22 Aromatics

surrogate

O:.ierriHenYl


118

RL 1.6

Limits 40-140

Spike

Add.ed

20.0 26.6

Llrnlts

40 • .140

Spike

Added 56.6

Limits 40-140

Spike

Added 19.9

26.5

Limits 40 -1.40

Spike

Added 56.4

Ll1nlts

4o:T46

MDL Unit 1.6 mg/Kg


0 Prepared Analyzed OJI Fae 01119/17 07:20 01/24/17 21:26 . 1

Prepared Analyzed

01119117 07:20 01124117 21:26 Dlf Fae

1


LCS LCS 0/oRec.

Result Qualifier Unit D 0;11Rec Lilnlts 10.5 mg/Kg 53 40-140 24.4 mg/Kg 92 40-140

Client Sample ID: Lab Control Sample

LCS

Result 65.0

LCSO

Result 11.4 26]

Prep Type: Total/NA Prep Batch: 339010

LCS 0/oRec. Qualifier Unit D o/oRec Limits

mg/Kg 115 40-140

Client Sample ID: Lab Control Sample Oup Prep Type: To.tal/NA Prep Batch: 339010

LCSD o/oRec. RPO Qualifier Unit D 11/oRec Lhnlts RPO Limit

mg/Kg 57 40.140 9 50 mg/Kg 100 40-140 9 50

Client Sample ID: Lab Control Sample Dup Prep Type: Total/N.A Prep Batch: 339010

LCSD LCSD %1Rec. RPO

Res_ult Qualifier Unit D 0/oRec Limits RPO Limit 62.8 mg/Kg 111 40-140 4 50


Page 109of140 2/1/2017

Client: C-K Associates Project/Site: Moffat & Nicl1ol


Method: MA-EPH • Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)

Lab Sample ID: 400·132588·6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010

Sample Sample Spike MS MS OfoRec. Aoalyte Result Qualifier Added Result Qualifier Unit 0 0/aRec Limits C19-C36 Aliphatics 12 54.7 70.5 mg/Kg ;:;; 108 40-140

C9-C18 Al!phatics <3.3 41.0 20.2 mg/Kg ;;r 49 40-140

MS MS

Surrogate %Recovery Qualifier Limits 1-Chlorooctadecane 88 40-140

Lab Sample ID: 400·132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010

Sample Sample Spike MS MS 0/oRec.

Analyte Result Qualifier Added Result Qualifier Unit 0 o/oRec Limits

C11-C22 Aromatics <6.1 116 142 mg/Kg n 123 40-140

MS MS

Surrogate %Recovery Qualifier Limits o-Ter{>h'eriyl 86 40-140

Lab Sample JD: 400·.132588·6 MSD Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010

Sample Sample Spike MSO MSD 0/nRec. RPO

Analyte Result Qualifier Added Result Qualifier Unit D 'Yo Rec Limits RPO Limit

C19-C36 Aliphatics 12 54.1 61.4 mg!Kg {( 92 40-140 14 50

C9-C18 Aliphatics <3.3 40.6 20.0 mg/Kg ·t:I 49 40-140 50

MSD MSD

Surrogate %Recovery Qualifier Limits

1-Chlorooctadecane 82 40.140

Lab Sample ID: 400·132588·6 MSD Client Sample 10: CK·5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010

Sample Sample Spike MSO MSD o/oRec. RPO

Analyte Result Qualifier Added Result Qualifier Unit D o/oRec 1-lmlts RPO Limit

C11-C22 Aromatics <6.1 115 119 mg/Kg ~:i 103 40-140 18 so MSD MSD

Surrogate %Recovery Qualifier Limits o-Terpheny/ 9g 40-140

Lab Sample ID: MB 400-339262/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339948 Prep Batch: 339262

MB MB


C10-C12Aliphatics <0.050 0.050 0.050 mg/L 0112011715:54 0112611716:56 1

C12-C16 Aliphallcs <0.050 0.050 0.050 mg/L 01120/1715:54 01126117 16:56

C16-C35 Allphatics <0.050 0.050 0.050 mg/L 0112011715:54 0112611716:56


Page 110 of 140 2/1/2017

B



Method: MA-EPH ~Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)

Lab Sample ID: MB 400-33926211 ·A Matrix: Water Analysis Batch: 339948

Surrogate

1-ChlorOoctadecane


79


MB

Analyte Result

C10-C12 Aromatics <0.050 C12-C16 Aromatics <D.050

C21-C35 Aromatics <0.050 C16-C21 Aromatics <0.050

MB Surrogate %Recovery o-Terphenyi 73 2-Bromonaphthalene 57

2-Fluorobiphenyl 119

Lab Sample ID: LCS 400-33926212-A Matrix: Water Analysis Batch: 339948

Analyte

C9-C18 Allphatics

C19-C36 Aliphatics

MB

Qualifier

MB Qualifier

Surrogate f.·Chloroociadecane

LCS LCS



Analyte C11-C22_Aromatics

Surrogate

o-Terpheny/ 2-Bromonaphthalene 2-Fluorobiphenyl


85 50

121

Lab Sample ID: LCSD 400·339262/3-A Matrix: Water Analysis Batch: 339948

Aoalyte C9'C18 Aliphatics

C19·C36 Aliphatics

Limits 40.140

RL

0.050 0.050

0.050 0.050

Limits 40.140

40 •. 140

40.140

Spike

Added

0.300 0.400

Limits 40.140

Spike

Added 0.850

Limits 40-140

40-140

40.140

MDL Unit 0.050 mg/L 0.050 mg/L

0.050 mg/L

0.050 mg/L

LCS LCS

Result Qualifier 0.199

0.317

LCS LCS

Result Qualifier 0.701


Prepared Analyzed Dll Fae 01120117 15:54 0112611716:56 1


D Prepared Analyzed Dll Fae 01/20/17 15:54 01/26/17 19:30 01/20/1715:54 01126/17 19:30

01/20/17 15:54 01/26/1719:30 01/20/17 15:54 01/26/1719:30

Prepared Analyzed Dll Fae 0112011715:54 0112611719:30 1

0112011715:54 01126117 19:30

01120117 15:54 0112611719:30


Unit D 0/oRec Lhnlts mg/L 66 40 .140

mg/L 79 40 -140

Client Sample ID: Lab Control Sample Prep Type; Total/NA Prep Batch: 339262 o/oRec.

Unit D 0/oRec Limits

mg/L 82 40.140

Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Bati;h:. 339262

Spike LCSD LCSD 0/oRec. RPO Added Result Ouallfler Unit D %Rec Limits RPO Limit

0.300 0.274 mg/L 91 40.140 32 50 0.400 0.331 mg/L 83 40.140 4 50


Page 111 of140 2/1/2017

B


Method: 6010C - Metals (ICP) (Continued)


-Analyte

Lead

Selenium Thallium Vanadium

· Zinc

Lab Sample ID: MB 400·338440/1 ·A Matrix: Solid Analysis Balch: 338689


<0.20

<D.40

<0.20

Spike

Added

1.00

1.00 1.00

1.00 1.00

LCS

Result 1.01

0.986 0.995

1.04 1.04

LCS

Qualifier

MDL Unit

0.20 mg/Kg

0.40 mg/Kg

0.20 mg/Kg



Unit D o/eRec Limits mg/L 101 80-120

mg/L 99 80-120 mg/L 99 80.120

mg/L 104 80.120

mg/L 104 80-120


D Prepared Analyzed DU Fae 01115/1711:30 01/16/1715:32 1 01/15/1711:30 01/16/17 15:32

01/15/1711:30 01116/17 15:32

Analyte Silver -Arsenic

Barium Beryllium Cobalt

Chromium Copper

Nickel Lead

Selenium Thallium Vanadium Zinc

<0.099

RL 0.50

0.99 0.99 0.30 0.99

0.99 2.0

0.099 mg/Kg 01/15/1711:30 01/16/1715:32 <0.30

<0.20 <0.20

<0.30

<0.20

<0.40 <0.40

<0.30

<D.79


Analyt_e Silver

Arsenic Barium Berymum Cobalt

Chromium Copper Nickel

Lead

Selenium Thallium

Vanadium Zinc

Spike

Added

49.7

99.4 99.4 49.7

99.4 99.4 99.4 99.4

99.4

99.4 99.4

99.4

99.4

0.50

0.99

2.0 0.99

2.0

2.0

LCS

Result

51.5

104

107 53.4

101

107 105

103 101

99.4 99.6

107 105

of 140

0.30 mg/Kg 01/15/1711:30 01/16/17 15:32

0.20 mg/Kg 01/15/1711:30 01/16/17 15:32 0.20 mg/Kg 01/15/1711:30 01/16/1715:32

0.30 mg/Kg 01/15/1711:30 01/16/17 15:32

0.20 mg/Kg 01/15/1711:30 01/16/17 15:32

0.40 mg/Kg 01/15/1711:30 01/16/17 15:32

0.40 mg/Kg 01115/17 11 :30 01/16/1715:32

0.30 mg/Kg 01/15/1711:30 01/16/17 15:32

0.79 mg/Kg 01/15/1711:30 01/16/17 15:32


LCS o/oRec. Qualifier_ Unit D 0/oRec Limits

mg/Kg 104 80-120 mg/Kg 105 80-120 mg/Kg 108 80-120 mg/Kg 107 80-120 mg/Kg 102 80-120 mg/Kg 107 80-120 mg/Kg 106 80-120 mg/Kg 104 80-120 mg/Kg 102 80.120 mg/Kg 100 80-120 mg/Kg 100 80-120

mg/Kg 107 80-120 mg/Kg 106 80-120


2/1/2017

E

QC Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol

Method: 6010C. Metals (ICP) {Continued)


Analyte

Silver Arsenic Barium Beryllium Cobalt Chromium Copper

Nickel Lead Selenium

Thamum Vanadium Zinc

Sample Sample

Result Qualifier

<0.37 12

120 0.33 J

4.8 26

44

12 64

1.3 J <0.74

14 150

Lab Sample ID: 400-132588-6.MSD Matrix: Solid Analysis Batch: 338689

Analyte Silver Arsenic Barium Beryllium Cobalt Chromium Copper

Nickel Lead

Selenium Tham um Vanadium Zinc

Sample Sample

Result Qualifier <0.-37

12

120 0.33 J

4.8 26 44

12 64 1.3 J

<0.74

14 150

Lab Sample ID; MB 400-338528/1-A Matrix: Solid Analysis Batch: 338847

Analyte

Silver Arsenic

Barium Beryllium Cobalt Chromium Copper

Nickel Lead

Selenium


<0.19

<0.39 <0.19

<0.097

<0.29

<0.19

<0.19

<0.29 <0,19

<0.39

Spike

Added 93.6 187

187 93.6

187 187

187

187 187

187 187

187 187

Spike

Added 93.5 187

187 93.5

187 187 187

187 187 187

187 187 187

RL 0.49 0.97 0.97

0.29

0.97 0.97

1.9 0.49 0.97

1.9

MS MS

Result Qualifier

94.4 202

304 96.9

198 217 243

208 253

184

186

210 325

MSD MSD

Unit mg/Kg

mg/Kg

mg/Kg mg/Kg

mg/Kg mg/Kg mg/Kg

mg/Kg mg/Kg

mg/Kg mg/Kg

n1g/Kg mg/Kg

Result Qualifier Unit 93.4 mg/Kg 198 mg/Kg

299 mg/Kg

95.9 mg/Kg

195 mg/Kg 212 mg/Kg

234 mg/Kg

205 mg/Kg 244 mg/Kg 180 mg/Kg

185 mg/Kg

208 mg/Kg 343 mg/Kg


0.19 mg/Kg 0.097 mg/Kg

0.29 mg/Kg 0.19 mg/Kg


of 140


Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338440 o/oRec.

0 o/oRec Llrnits l.\ 101 75-125

" 101 75-125 l) 101 75-125 l) 103 75 .125 ,, 103 75-125

" 102 75-125 ;;1 106 75-125

l) 105 75-125

" 101 75-125

" 97 75-125 l) 99 75-125

'~ 105 75-125

" 92 75-125

Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338440 O/oRec. RPO

D 0/oRec Llrnits <1 100 75-125

RPO Limit

20 " 100 75-125 2 20

" 98 75-125 2 20 i:1 102 75-125 20 ;;1 102 75-125 1 20 u 99 75-125 2 20

" 102 75-125 4 20 1:1 103 75-125 1 20 " 96 75-125 4 20 l) 95 75-125 2 20 l) 99 75-125 20 ,, 104 75-125 1 20 " 101 75-125 5 20


0 Prepared Analyzed Oil Fae

01116/17 08:55 01/17/1712:45 1 01/16/17 08:55 01/17/1712:45

01/W17 08:55 01/17117 12:45

01/16/17 08:55 01/17/17 12:45 01/16/17 08:55 01/17/1712:45 01/16/17 08:55 01/17/17 12:45

01/16/17 08:55 01/17/17 12:45

01/16/17 08:55 01/17/17 12:45 01/16/17 08:55 01/17/17 12:45 01/16117 08;55 01117/1712:45


2/1/2017

QC Sample Results Client: C-K Associates TestAmerica Job JD: 400-132540-1 Project/Site: Moffat & Nichol

Method: 6010C - Metals (ICP) (Continued)

Lab Sample ID: MB 400-338528/1-A Client Sample JD: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528

MB MB


Thallium <0.39 0.97 0.39 mg/Kg 01/16/17 08:55 01/17/17 12:45 1 Vanadium <0.2~ 1.9 0.29 mg/Kg 01/16/17 08:55 01/17/1712:45

Zinc <0.78 1.9 0.78 mg/Kg 01/16/17 08:55 01/17/17 12:45

Lab Sample ID: LCS 400·338528i2·A Client Sample ID: Lab Control Sample E Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528

Spike LCS LCS o/oRec.

Analyte Added Result Qualifier Unit D 0/oRec Limits

Silver 48.4 50.5 mg/Kg 104 80 -120 Arsenic 96.8 102 mg/Kg 105 80.120

Barium 96.8 105 mg/Kg 108 80.120

Beryllium 48.4 52.4 mg/Kg 108 80.120

Cobalt 96.8 99.7 mg/Kg 103. 80-120 Chromium 96.8 104 mg/Kg 107 80.120

Copper 96.8 103 mg/Kg 107 80.120

Nickel 96.8 101 mg/Kg 104 80.120 Lead 96.8 99.8 mg/Kg 103 80.120

Selenium 96.8 97.8 mg/Kg 101 80 .120

Thallium 96.8 99.4 mg/Kg 103 80.120

Vanadium 96.8 104 mg/Kg 108 80.120

Zinc 96.8 103 mg/Kg 106 80.120

Lab Sample ID: 400·132650·1 MS Client Sample ID: CK-6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528

Sample Sample Spike MS MS o/11Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits

Silver <0.35 88.3 88.9 mg/Kg " 101 75.125

Arsenic 7.1 177 180 mg/Kg ,,

98 75 .125

Bariwn 87 F1 177 313 F1 mg/Kg J~ 128 75.125

Beryllium 0.37 J 88.3 89.9 mg/Kg " 101 75 .125

Cobalt 4.1 177 187 mg/Kg i'.l 104 75-125

Chromium 11 177 190 mg/Kg ~:1 101 75 .125

Copper 37 177 207 mg/Kg i;i 96 75.125

Nickel 12 177 195 mg/Kg ,, 104 75 .125

Lead 42 177 242 mg/Kg " 113 75.125

Selenium 0.87 J 177 169 mg/Kg ·1:1 95 75 .125

Thallium <0.71 177 178 mg/Kg 1~ 101 75.125

Vanadium 11 177 197 mg/Kg " 105 75 .125

Zinc 130 177 267 mg/Kg " 80 75.125

Lab Sample ID: 400·132650·1 MSD Client Sample ID: CK·6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528

Sarnple Sample Spike MSD MSD o/aRec. RPO

Analyte Result Qualifier Added Result Qualifier Unit D (l/oRec Limits RPO Limit

Silver <0.35 88.9 89.3 mg/Kg j) 100 75 .125 0 20 Arsenic 7.1 178 183 mg/Kg ,, 99 75 .125 2 20


of140 2/1/2017


Method: 6010C ·Metals (ICP) (Continued)


Analyte Barium Beryllium

Cobalt

Chroinium

Copper

Nickel

Lead

Selenium Thallium

Vanadiun1 Zinc

Sample Sample

Result Qualifier 87 F1

0.37 J 4.1

11

37 12

42 0.87 J

<0.71

11

130


Analyte

Silver

Arsenic

Barium

Beryllium

Cobalt

Chromium

Copper

Nickel

Lead

Selenium

Thallium

Vanadium

Zinc


<0.0020

<0.0040

<0.0020

<0.0010 <0.0030 <0.0020

<0.0020 <0.0030

<0.0020 <0.0040

<0.0040 <0.0030

<0.0080


Analyte Silver

Arsenic

Barium Beryllium Cobalt

Chromium

Copper

Nickel

Lead

Se!enlum

ThatHum Vanadiurn

Zinc

Spike

Added

178

88.9 178

178

178 178 178

178

178 178

178

RL 0.0050

0.010 0.010

0.0030 0.010 0.010

0.020 0.0050

0.010 0.020

0.010 0.020

0.020

Spike

Added a.sod

1.00

1.00 0.500

1.00

1.00

1.00 1.00

1.00 1.00

1.00 1.00

1.00

MSD MSD

Result Qualifier Unit 316 F1 mg/kg

91.1 mg/Kg

189 mg/Kg

192

249 197

219

174 179 198 264


0.0040 mg/L

0.0020 mg/L

0.0010 mg/L

0.0030 mg/l

0.0020 mg/L

0.0020 mg/L

0.0030 mg/L

0.0020 mg/L

0.0040 mg/L

0.0040 mg/L

0.0030 mg/L

0.0080 mg/l

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg


Client Sample ID: CK-6 Prep Type; Total/NA Prep Batch: 338528 %Rec. RPO

D 0/oRec Limits RPO Limit

" 129 75-125 20 " 102 75-125 ;/ 104 75-125 ,, 102 75-125

" 119 75-125 ::i 104 75-125

"' 99 75-125

" 97 75-125 !;1: 101 75-125 l) 105 75-125

78 75-125

19

10

3

20 20

20

20 E 20 20

20

20 20

20


O Prepared Analyzed Oil Fae 01/18/1710:09 01/19/1715:39 1 01118/1710:09 01/19/17 15:39

01118/1710:09 01/19/1715:39

01118/1710:09 01/19/1715:39 01/18/1710:09 01/19/1715:39

01118/1710:09 01/19/1715:39

01118/1710:09 01/19/1715:39 01/18/1710:09 01/19/1715:39

01118/17 10:09 01/19/1715:39

01118/1710:09 01/19/1715:39

01118/1710:09 01/19/1715:39 01/18/17 10:09 01/19/17 15:39 01/18/1710:09 01/19/1715:39

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep B:itch: 338893

LCS LCS


1.03

1.05 0.526 0.999

1.04 1.03 1.03 1.01

0.988 1.00 1.04 1.03

mg/l

mg/L

mg/l

mg/L

mg/L

mg/L

mg IL

mg/L

mg/L

mg IL mg/L

mg/L

0 °/oRec 100

0/oRec.

Limits

80-120 103 80-120 105 80-120

105 80-120 100 80-120

104 80-120

103 80-120 103 80-120

101 80-120

99 80-120 100 80-120 104 80-120

103 80-120


of140 21112017


Method: 7470A ·Mercury (CVAA)


MB MB Analyte

Mercury Result Qualifier

<0.000070

Lab Sample ID: LCS 400-337923/15-A Matrix: Waler Analysis Balch: 338420

Analyte Mercury


MB MB Analyte

Mercury Result Qualifier

<0.000070


Analyte

Mercury

Method: 7471A ·Mercury (CVAA)

Lab Sample ID: MB 400·337950/14-A Matrix: Solid Analysis Balch: 338612

A_nalyte

Mercury

MB Mil Result _Quallfi_er

<0.0075

Lab sample ID: LCS 400-337950/15-A Matrix: Solid Analysis Batch: 3386.12

Analyte Mercury

Lab Sample ID: 400-132588'6 MS Matrix: Solid Analysis Batch: 338612

Analyte

Mercury

Sample Sample Result Qualifier 0.052

RL MDL Unit



D Prepared Analyzed Oil Fae 0.00020 0.000070 mg/L 01/13/17 08:15 01/13/1712:31 1

Spike

Added 0.00101

Client Sample ID: Lab Control Sample

LCS LCS


RL MOL Unit

Prep Type: Total/NA 11!!1 Prep Batch: 337923 El o/oRec.

D 0/oRec Limits

87 80-120


D Prepared Analyzed 011.Fac 0.00020 . 0.000070 mg/L b1116i1116:11 01/1811712:35 1

Spike

Added

0.00101

Spike

Added

0.0631

Spike

Added 0.131

RL Q.012

LCS LCS

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338653 %1Rec.

Result Qualifier Unit D %Rec Limits

0.()0110 mg/L

MOL Unit 0.0075 mg/Kg

109 80-120


O Prepared Analyzed DH Fae 01/15/17 12:43 01116/17 09:21 1

LCS LCS

Client Sample ID: Lab C~mtrol sample Prep Type: Total/NA Prep Batch: 337950 0/oRec.

Result Qualifler Unit 0.0618 mg/Kg

MS MS Result Qualifier Unit 0.200 mg/Kg

D %Rec _Llo:iits 98 80-120

Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 337950 0/oRec.

O 0;0Rec Lltnlts

113 80-120


of 140 2/1/2017



Method: 7471A. Mercury (CVAA) (Continued)


Analyte

Mercury

Sa1nple Sample

Result Qualifier

0.052


MB MB Analyte Mercury

Result Qualifier

<0.0085

Lab Sample ID: LCS 400-338513/1 S·A Matrix: Solid Analysis Batch: 338612

Analyte tvfercury

Method: 335.2. Cyanide, Total

Lab Sample ID: MB 400-338793/1 ·A Matrix: Water Analysis Batch: 338792

MB MB Analyte Cyanide, Total


Lab Sample ID: LCS 400-338793/2-A Matrix: Water Analysis Balch: 338792

Anatyte Cyanide, Total

Method: 353.2 - Nitrogen, Nitrate-Nitrite

Lab Sample ID: MB 400-338427/7 Matrix: Water Analysis Batch: 338427

Analyte Nitrate Nitrite as N

Lab Sample ID: LCS 400·338427/23 Matrix: Water Analysis Batch: 338427

Analyte Nitrate Nitrite as N

MB MB Result Qualifier .:::Q.018

Spike

Added 0.132

RL 0.014

Spike

Added 0.0709 .

RL 0.0050

Spike

Added 0.274

Spike

Added 0.500

RL o.oso

MSD MSD

Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 337950 WaRec. RPO

Result Qualifier Unit D o/aRec Limits RPO Limit 0.168 mg/Kg 89 80.120 17 20


Client Sample ID: Method Blank Prep Type: Total/NA 11!1 Prep Batch: 338513 U

O Prepared Analyzed Oil Fae

01115/1712:43 01/16/1710:03 1


LCS LCS o/oRec.

Result Qualifier Unit D o/oRec Limits

0~0688 mg/Kg 97 80-120


LCS LCS

Client.Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338793

D Prepared Analyzed Oil Fae 01117/17 09:30 Oi/17117 14:18 1

Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338793 °!oRec.


0.306 mg/L

D 0/ 0Rec Limits

112 1s-12s

MOL Unit 0.018 mg/L

Client Sample ID: Method Blank Prep Type: Total/NA

0 Prepared Analyzed Oil Fae 01/13/1713:24 1

Client Sample ID: Lab Control Sample Prep Type: Total/NA

LCS LCS


0/GRec. D %Rec Limits

100 90-110


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Method: 353.2 • Nitrogen, Nitrate-Nitrite (Continued)

Lab Sample ID: MRL 400-33842716 Matrix: Water Analysis Batch: 338427

Analyte

Nitrate Nitrite as N

Lab Sample ID: MB 400-338579/14 Matrix: water Analysis Batch: 338579

Analyte


Lab Sample ID: LCS 400-338579115 Matrix: Water Analysis Batch: 338579

Analyte NJfrafe-NHrne-as N

Lab .Sample ID: MRL 400·338579/13 Matrix: Water Analysis Batch: 338579

Analyte


Lab Sample ID: MRL 400-338609/6 Matrix: Solid Analysis Batch: 338609

Analyle



Analyte


MB MB


MB MB

Result Qualifier

<0.36

Lab. Sample.ID: LCS 400-338576/2-A Matrix: Solid Analysis Batch: 338609

Analyte Nltraie -Nitrite as N

Lab Sample ID: 400-132588-1 MS Matrix: S.olid Analysis Batch: 338609

Analyte


Sample Sample

Result Qualifier

9.6 F1 F2

Spike

Added

0.0500

Spike

Added

0.500

Spike

Added 0.0500

Spike Ad.de.ct

0.0500

Spike Added

100

Spike

Added 62.9

RL

0.050

RL 1.0



MRL MRL


MDL Unit 0.018 mg/L

~%Rec.

o 1%Rec Limits

108 50.150

Client Sample ID: Method Blank Prep Type: Total/NA

D Prepared Analyzed Oil Fae

01116117 09:23 1

Client Sample ID: Lab Control $ample Prep Type: _Total/NA

LCS LCS


0.49'.l mg/L

%Rec.

D o/oRec Limits

99 90:110


MRL MRL


0.0370 J mg/L

0/oRec.

D %Rec Llrnlts

74 50-150


MRL MRL Result Qualifier Unit

0.0360 J mg/Kg

MDL Unit 0.36 mg/Kg

0/oRec.

0 o/oRec Limits

72 50-150

Client Sample ID: Method Blank Prep Type: Soluble

0 Prepared Analyzed Oil Fae

0111611712:14 1

Client Sample ID: Lab Control Sample Prep Type: SoJuble

LCS LCS Result Qualifier Unit

9.96 mg/Kg

MS MS


5.22 F1 mg/Kg

%Rec.

D 0/oRec Limits 100 90-110.

Client Sample I[): CK-1 Prep Type: Soluble

o/oRec. O 0/ 0 Rec Limits ~ -7 90-110


of 140 2/1/2017


Lab Sample ID: 400-132588-1 MSD Client Sample ID: CK.1 Matrix: S.olid Prep Type: Soluble Analysis Batch: 338609

Sample Sample Spike MS.O MSO 1>/oRec. RPO Analyte Result Qualifier Added Result Ouallfler Unit 0 %Rec Limits RPO Limit Nitrate Nitrite as N 9.6 F1 F2 62.9 7.05 F1 F2 mg/Kg " -4 90" 110 30 6

Lab Sample ID: 400-132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Soluble Analysis Batch:.338609

Sample sample Spike MS MS %1Rec.

Analyte Result Qualifier Added Result Qualifier Unit 0 0/oRec Limits D Nitrate Nitrite as N <0.74 F1 F2 41.0 33.2 F1 mg/Kg " 81 90" 110

Lab Sample ID; 400-132588-6 MSD Client Sample ID: .CK-5 Matrix: Solid Prep Type: Soluble Analysis Batch: 338609

Sample Sample Spike MSD MSO 0/oRec. RPO

Anaiyte Result Qualifier Added Result Qualifier Unit 0 °A> Rec Limits RPD Limit Nitrate Nitrite_as N <0.74 F1 F2 41.0 35.8 Ff F2 mg/Kg ~ 87 90-110 8 6

Lab Sample ID: 400-132650-5 MS Client Sample ID: CK-10 Matri)(: Solid Prep Type: Soluble Analysis Batch: 338609

Sample Sample Spike MS MS o/nRec.

Analyte Result Qualifier Added Result Qualifier Unit 0 %Rec Limits

Nitrate Nitrite as N <0.48 F1 26.6 2.42 F1 mg/Kg " 9 90 -110

Lab Sample ID: 400-132650-5 MSD Client Sample ID: CK-10 Matrix: Solid Prep Type: Soluble Analysis Batch: 338609

Sample Sample Spike MSO MSO 0/oRec. RPO Analyte Result Qualifier Added Result Qualifier Unit 0 0/oRec Limits RPO Limit Nitrate Nitrite as N <0.48 F1 26.6 2.34 F1 mg/Kg ·)~ 9 90" 110 3 6

Method: 7196A ·Chromium, Hexavalent

Lab Sample ID: MB 400-339244/6-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339470 Prep Batch: 339244

MB MB

Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae

Chromium, .hexavalent <3.3 4.7 3.3 mg/Kg 01/20/17 17:00 01/23/1712:03 1

Lab Sample.ID: LCS 400-339244/7-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339470 Prep Batch: 339244

Spike LCS LCS o/oRec.

Analyte Added Result Qualifier Unit 0 0/oRec Limits

Chromium, hexava!ent 94.6 so:3 mg/Kg 85 80-120


of140 2/1)2017


Method: 7196A - Chromium, Hexavalent (Continued)

Lab Sample ID: MRL 400-33924415-A Matrix: Solid Analysis Batch: 339470

Spike MRL MRL


Chromium, hexavalent 0.0500 0.0434

Lab Sample ID: 400-132588·.6 MS Matrix: Solid Analysis Batch: 339470

Sample Sample Spike MS MS

Analyte Result Qualifier Added Result Qualifier

Ghromium, hexavalent <5.8 F1 151 <5.3 F1

• Lab Sample ID: 400.132588·6 MSD Matrix: Solid Analysis Batch: 339470

Sa1nple Sample Spike MSO MSO

Analyte Result Qualifier Added Result Qualifier Chi-onii.Um, 'tlexav81e·nt <5.8 F1 178 <6.2 F1

Lab Sample ID: 400-132650·5 MS Matrix: Solid Analysis Batch: 339470

Sa1nple Sample Spike MS MS

A.nalyte Result Quallfier Added Result Qualifier

Chromium, hexavalent <3.4 F1 113 <4.0 F1

Lab Sample ID: 400-132650·5 MSD Matrix: Solid Analysis Batch: 339470

Sample Sample Spike MSO MSD

Analyte Result Qualifier Added Result Ql!alifle,t

thfofnlum, h~xavalerlt <3.4 F1 105 <'3.7 F1

Lab Sample 1.D: MB 400-339253/6 Matrix: Water Analysis Batch: 339253

MB MB

Analyte Result Qualifier RL MDL Unit

Chromium, hexavalent <0.0065 0.010 0.0065 mg IL

Lab Sample ID: LCS 400-339253/7 Matrix: Water Analysis Batch: 339253

Spike LCS LCS


Chromium, hexavalent 0.200 0.217

Lab Sample ID: 400-132650·6 MS Matrix: Water Analysis Batch: 339253

Sarnple Sample Spike MS MS

Analyte Result Qualifier Added Result aualltier Chromium, hexavalerlt <0.0065 0.200 0.208

of 140


Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339244 O/oRec.

Unit D 0/oRec Limits mg/L 87 50-150

Client Sample ID: CK-5 Prep Type: Total/NA m Prep Batch: 339244 o/oRec.

Unit D 0/oRec Limits

mg/Kg i) 0 75-125

Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 339244 o/oRec. RPO

Unit D 0/oRec Limits RPO Limit

mg/Kg " 0 75-125 NC 25

Client Sample ID: CK-10 Prep Type: Total/NA Prep Batch: 339244 0/oRec.

Unit D o/oRec Limits mg/Kg 1) 0 75-125

Client Sample ID: CK·10 Prep Type: Total/NA Prep Batch: 339244 0/oRec. RPO

Unit D 0/oRec Limits RPO Limit

mg/Kg p 0 75-125 NC 25

Client Sample ID; Method Blank Prep Type: Total/NA

D Prepared Analyzed DU Fae 01114117 09:18 1


%Rec. Unit D %Rec Limits

mg/L 109 90-110

Client Sample ID: RB-2 Prep Type: Total/NA

%Rec.

Unit 0 %Rec Limits

mglL 104 85-115


21112017


Lab Sample ID: 400-132650-6 MSD Matrix: Water Analysis Batch: 339253

Analyte Chromium, hexavalent

Sample Sample

Result Qualifier

<0.0065

Lab Sample ID: MB 400-339274/6 Matrix: Water Analysis Batch: 339274

Analyte

Chromium, hexava!ent

MB MB

Result Qualifier

<0.0065

Lab Sample ID: LCS 400.33927 4/7 Matrix: Water Analysis Batch: 339274

Analyte Chromium, hexava!ent

Lab Sample ID: MRL 400-339274/3 Matrix: Water Analysis .Batch: 339274

Analyte Chromium, hexavalent

Lap Sample ID: 400·132540·1 MS Matrix: Water Analysis Batch: 339274

Sample Sample Analyte Result Qualifier Chromium, hexavalent <0.0065

Lab Sample ID: 400-132540·1 MSD Matrix: Water Analysis Batch: 339274

S'ample Sample

Analyte Result Qualifier Chromi'um, hexava!ent <0.6065

Spike

Added 0.200

Spike

Added 0.200

Spike

Added

0.0100

Spike

Added

0.200

Spike

Added

0.200

Me_thod: 90128 • Cyanide,Total andor Amenable

Lab Sample ID: MB 400'339098/1-A Matrix: Solid Analysis Batch: 339005

Analyte Cyanide, Total

MB MB Result Qualifier <0.12

RL

0.010

RL 0.24

MSD MSD



D


Client Sample ID: RB-2 Prep Type: Total/NA

0/oRec. O 0/oRec Limits

103 85-115

RPO

RPO Limit 1 9

Clie.nt Sample ID: Method Blank Prep Type: Total/NA

Prepared Analyzed 01/12117 10:22

OJI Fae


LCS LCS


o/oRec.

0 %Rec Limits 105 90-110


MRL MRL


0.0132 mgiL

MS

Result

0.210

MSD

Result 0.220

MS

Qualifier

MSD

Qualifier

MDL Unit 0.12 mg/Kg

Unit

mg/L

Unit

niiJ/l.

0/oRec.

D 0/oRec Limits

132 50-150

Client Sample ID: RINSATE 1 Prep Type: Total/NA

0/oRec.

D 0/oRec Limits 105 85-115

Client Sample ID: RINSATE 1 Prep Type: Total/NA

0/oRec. RPO

D o/oRec Limits RPO Limit 110 85-115 5 9


0 Prepared Analyzed 011 Fae 01/18/1710:53 01/18/17 17:30 1


of140 2/1/2017

QC Sample Results Client: C-K Associates ProjecUSite: Moffat & Nichol

Method: 90128. Cyanide, Total andor Amenable (Continued)


Spike LCS LCS


Cyanide, Total 13.6 14.7


Sample Sample Spike MS MS

Analyte Result Qualifier Added Result Qualifier

Cyanide, Total <0.27 F1 20.1 12.3

Lab Sample 1.D: 400°132588·6 MSD Matrix: Solid Analysis Batch: 339005

Sa1nple Sample Spike MSO MSO

Analyte Result Qualifier Added Result Qualifier Cyanide, Total <!>:it F1 19.5 10.9 Fi

Lab Sample ID: 400°132650-5 DU Matrix: Solid Analysis Batch: 339005

S_ample Sample DU DU Analyte Result Qualifier Result Qualifier Cyanide, Total <0.17 <0.17

of140


Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339068 %1Rec.

Unit D o/e1Rec Limits mg/Kg 108 75-125

Client Sample ID: CK-5 Prep Type: Total/NA

E Prep Batch: 339068 o/oRec.

Unit D o/oRec Limits mg/Kg -(! 61 57 -136

Client Sample ID: CK·5 Prep Type; Total/NA Prep Batch: 339068 1%Rec. RPO

Unit D O/GRec Limits RPO Limit

mg/Kg " 56 57 .136 12 20

Client Sample ID: CK-10 Prep Type: Total/NA Prep Batch: 339068

RPO

Unit 0 RPO Limit

mg/Kg -!;! NC


2/1/2017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Client Sample ID: RINSATE 1 Lab Sample ID: 400-132540-1 Date Collected: 01111/1713:20 Matrix: Water Date Received: 01112/17 09:21

Batch Batch Diiution Batch Prepared

Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Analysis 8260C 338529 01/16/17 09:43 CLN TALPEN

Total/NA Prep 3520C 338284 01/12/1716:23 KLR TAL PEN

Total/NA Analysis 82700 338574 01/16/17 21:32 MAM TAL PEN

Total/NA Prep 3520C 338284 01/12/1716:23 KLR TAL PEN

Total/NA Analysis 82700 LL 338569 01/16/1718:58 S1S TAL PEN

Total/NA Analysis MAVPH 339057 01/19/17 22:24 MKA TAL PEN

E Total/NA Prep 8011 339493 01 /23/17 16:25 KH1 TAL PEN

Total/NA Analysis 8011 339878 01/27/17 00:09 KH1 TAL PEN

Total/NA Prep 3520C 338239 01/12/1716:15 KLR TALPEN

Total/NA Analysis 8081B 339079 0111911713:41 MAM TAL PEN

Total/NA Prep 3520C 339262 01 /20/17 15:54 KLR TAL PEN

Total/NA Analysis MA-EPH 339948 01126/17 17:25 RM TALPEN

Total/NA Prep 3520C 339262 01/20/1715:54 KLR TALPEN

Total/NA Analysis MA,EPH 339950 0112611719:59 RM TALPEN

Total/NA Prep 3010A 338333 01 /13/17 08:50 RJB TALPEN

Total/NA Analysis 6010C 338689 01/16/17 17:16 RJB TAL PEN

Total/NA Prep 7470A 337923 01/1311708:15 JAP TALPEN

Total/NA Analysis 7470A 338420 01/13/1712:58 JAP TALPEN

Total/NA Prep Oistill/CN 338793 01/17/17 09:30 BAB TAL PEN

Total/NA Analysis 335.2 338792 01/17117 14:18 BAB TALPEN

Total/NA Analysis 353.2 338427 01/13/1713:30 KJR TALPEN

Total/NA Analysis 7196A 339274 01/12/1710:56 JLB TALPEN

Client Sample ID: CK-1 Lab Sample ID: 400~132588-1 Date Collected: 0111111711:10 Matrix: Solid Date Received: 01/12117 16:57

Batch Batch Dllutlon Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 7471A 337950 01/15/17 12:43 JAP TALPEN

Total/NA Analysis 7471A 338612 01/16/17 09:31 JAP TALPEN

Total/NA Analysis Moisture 338696 01/17/1710:20 JNJ TALPEN

Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 Date Collected: 01/11/1711:10 Matrix: Solid Date Received: 01/1211716:57 Percent Solids: 31.8

Batch Batch Diiution Batch Prepared


Total/NA Prep 5035 339330 01/22117 07:44 RS TAL PEN

Total/NA Analysis 8260C 339331 01/22/1711:25 RS TALPEN

Total/NA Prep 3546 338556 01/16/17 09:16 RDT TAL PEN

Total/NA Analysis 82700 338849 01/18/1716:05 KJA TALPEN

Total/NA Prep 5035 338604 01/16/1711:00 MKA TAL PEN

Total/NA Ana'lysis MAVPH 50 338571 01/16/1718:19 MKA TALPEN


of140 2/1/2017


Batch Batch

Method

3546

8081B

Prep Type

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Soluble Soluble

Total/NA

Total/NA

Total/NA

Total/NA

Type

Prep Analysis

Prep

Analysis

Prep Analysis

Prep Analysis

Leach

Analysis

Prep

Analysis

Prep

Analysis

3546

MA-EPH

3546

MA-EPH

3050B

6010C

DJ Leach 353.2

3060A

7196A

90128

9012B

Client Sample ID: CK-2 Date Collected: 01111117 11 :40 Date Received: 01/1211716:57

Prep Type

Total/NA Total/NA

Total!NA

Batch Type

Prep Analysis

Analysis

Batch

Method

7471A

7471A

Moisture

Client Sample ID: CK-2 Date Collected: 0111111711:40 Date Received: 0111211716:57

Prep Type

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Soluble Soluble

Total/NA

Total/NA

Batch

Type

Prep Analysis

Prep Analysis

Prep Analysis

Prep Analysis

Batch Method

5035

8260C

3546

82700

5035 MAVPH

3546

8081B

Prep 3546

Analysis MA~EPH

Prep 3546

Analysis MA-EPH

Prep 3050B

Analysis 6010C

Leach DI Leach Analysis 353.2

Prep 3060A

Analysis 7196A

Run

Run

Run

Lab Chronicle

Dilution Factor

5

Dilution Factor

Dllutlpn Factor

so

5


Batch Prepared Number or Analyzed Analyst Lab 338557 01116117 09:24 RDT TAL PEN

338706 0111711718:11 TD

339010 01/19117 07:20 RDT

339632 0112411718:11 RM

339010 01119/17 07:20 RDT

339633 01124/17 22:24 RM

338440 0111511711:30 DN1

338689 01116/17 15:45 RJB

338576 01116117 09:57 KJR

338609 01/1611712:16 KJR

339244 0112011717:00 CLM

339470 01123/1712:03 CLM

339068 01/1811710:53 BAB

339005 0111811717:31 BAB

TAL PEN

TAL PEN

TAL PEN

TALPEN

TAL PEN

TAL PEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

L11b Sample ID: 400-132588•2 Matrix: Solid

Batch Prepared Number or Analyzed Analyst 337950 0111511712:43 JAP

338612 01116117 09:33 JAP

338607 0111611712:37 CJP

Lab

TAL PEN

TALPEN

TALPEN

Lab Sample ID: 400-132588•2 Matrix:. s.oli<J

Percent Solids.: 23.2

Batch Prepared Number or Analyzed Analy$t Lab 339330 01/22117 07:44 RS TAL PEN

339331 01/22/1711:50 RS

338556 01116117 09:16 RDT

338849 0111811716:38 KJA

338604 01/1611711:00 MKA

338571 01/1611719:18 MKA

338557 01/16117 09:24 RDT

338706 0111711718:41 TD

339010 01/19117 07:20 RDT

339632 01/2411718:21 RM

339010 01119117 07:20 RDT

339633 01/24/17 22:33 RM

338440 01/15/1711:30 DN1

338689 01116/17 15:48 RJB

338576 01116117 09:57 KJR

338609 01/16/1712:18 KJR

339244 01120117 17:00 CLM

339470 01/2311712:03 CLM

TALPEN

TAL PEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN

TALPEN


of140 2/1/2017

Lab Chronicle Client: C-K Associates Tes!America Job ID: 400-132540-1 Project/Site: Moffat & Nichol

Client Sample ID: CK-2 Lab Sample ID: 400-132588-2 Date Collected: 01/11/1711:40 Matrix: Solid Date Received: 01/12/17 16:57 Percent Solids: 23.2

Batch Batch Dllutlon Batch Prepared


'rotellNA Prep 9012B 339068 01/18/17 10:53 BAB TALPEN

Total/NA Analysis 9012B 339005 01/18/1717:31 BAB TALPEN

Client Sample ID: Duplicate Lab Sample ID: 400-13258$-3 Date Collected: 01/11/1712:00 Matrix: Solid Date Received: 01/12/1716:57

Batch Batch Dilution Batch Prepared B Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

TotallNA Prep 7471A 337950 01/1511712:43 JAP TALPEN


TotallNA Analysis Moisture 338607 01/16/1712:37 CJP TALPEN

Client Sample ID: Duplicate Lab Sample ID: 400-132588-3 Date Collected: 01/11/1712:00 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 32. 7

Batch Batch Dilution Batch Prepared


TotallNA Prep 5035 339330 01122/17 07:44 RS TAL PEN

TotallNA Analysis 8260C 339331 01/22/1712:15 RS TALPEN

Total/NA Prep 3546 338556 01/16117 09:16 ROT TAL PEN

Tota!INA Analysis 82700 338849 01118/1717:12 KJA TAL PEN

TotallNA Prep 5035 338604 01/16/17 11:00 MKA TALPEN

Total/NA Analysis MAVPH 50 338571 01116117 20:18 MKA TALPEN

Total/NA Prep 3546 338557 01/16117 09:24 ROT TALPEN

TotallNA Analysis 8081B 5 338706 01/17/1719:11 TD TAL PEN

. TotallNA Prep 3546 339010 01119117 07:20 ROT TALPEN

Total/NA Analysis MA·EPH 339632 01/24/1718:31 RM TAL PEN

Total/NA Prep 3546 33.9010 01/19/17 07:20 ROT TALPEN

TotallNA Analysis MA-EPH 339633 01/24/17 22:43 RM TALPEN

TotallNA Prep 3050B 338440 01/15/1711:30 ON1 TALPEN

Total/NA Analysis 6010C 338689 01/16/1715:51 RJB TAL PEN

Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TALPEN

Soluble Analysis 353.2 338609 01/16/17 12:19 KJR TALPEN

TotallNA Prep 3060A 339244 01/20/1717:00 CLM TALPEN

Tota!INA Analysis 7196A 339470 01/23/1712:03 CLM TALPEN

Total/NA Prep 9012B 339068 01/18/1710:53 BAB TALPEN

TotallNA Analysis 9012B 339005 01/18/1717:31 BAB TALPEN


of 140 2/1/2017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol

Client Sample ID: CK-3 Lab Sample ID: 400-132588-4 Date Collected: 01/11/1712:15 Matrix: Solid Date Received: Oi/12/1716:57

Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab tofoiiNii. Prep 7471A 337950 0111511712:43 JAP TAL PEN

Total/NA Analysis 7471A 338612 01116117 09:54 JAP TAL PEN

Total/NA Analysis Moisture 338607 0111611712:37 CJP TALPEN

Client Sample ID: CK-3 Lab Sample ID: 400-132588-4 Date Collected: 01/1111712:15 Matrix: Solid

E Date Received: 01/12/1716:57 Percent Solids: 2S.7

Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 5035 339330 01122117 07:44 RS TAL PEN

Total/NA Analysis 8260C 339331 0112211712:41 RS TALPEN

Total/NA Prep 3546 338556 01116117 09:16 ROT TAL PEN

Total/NA Analysis 82700 338741 01117117 13:48 MAM TAL PEN

Total/NA Prep 5035 338604 0111611711:00 MKA TALPEN

Total/NA Anatysls MAVPH 50 338571 01116117 21:18 MKA TALPEN


Total/NA Analysis 80818 5 338706 0111711719:42 TD TALPEN

Total/NA Prep 3546 339010 01119117 07:20 ROT TALPEN

Total/NA Analysis MA-EPH 339632 0112411718:50 RM TAL PEN

Tota!INA Prep 3546 339010 01119117 07:20 ROT TALPEN

Total/NA Analysis MA-EPH 339633 01124117 23:02 RM TALPEN

Total/NA Prep 3050B 338440 0111511711:30 ON1 TALPEN

Total/NA Analysis 6010C 338689 0111611715:55 RJB TAL PEN

Soluble Leach DJ Leach 338576 01116117 09:57 KJR TALPEN

Soluble Analysis 353.2 3.38609 0111611712:20 KJR TALPEN

Total/NA Prep 3060A 339244 01120117 17:00 CLM TAL PEN

Total/NA Analysis 7196A 339470 0112311712:07 CLM TALPEN

Total/NA Prep 9012B 339068 0111811710:53 BAB TALPEN

Total/NA Analysis 9012B 339005 01118117 17:37 BAB TAL PEN

Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date C.ollected: 01/1111712:30 Matriic S.olid Date Re.ceived: 01112/1716:57

Batch Batch Dllutlon Batch Prepared Prep-Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 7471A 337950 01115117 12:43 JAP TALPEN

Total/NA Analysis 7471A 338612 01116117 09:56 JAP TALPEN

Total/NA Analysis Moisture 338607 0111611712:37 CJP TALPEN


of140 2/1/2017


Client Sample ID: CK-4 Lab Sample ID: 400-132588,5 Date Collected: 01/11/1712:30 Matrix: Solid Date Received; 01/12/17 16:57 Percent Solids: 20.9

Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 5035 339330 01/22111()7:44 RS TAL PEN

Total/NA Analysis 8260C 339331 01/22/17 13:06 RS TAL PEN


Total/NA Analysis 8270D 338741 01/17/1714:21 MAM TAL PEN

Total/NA Prep 5035 338604 01/16/1711:00 MKA TAL PEN

Total/NA Analysis MAVPH 50 338571 01/16/17 22:17 MKA TAL PEN

Total/NA Prep 3546 338557 01/16/17 09:24 RDT TAL PEN m Total/NA Analysis 8081B 5 338706 01/17/17 20:12 TD TAL PEN


Total/NA Analysis MA-EPH 339632 01/24/1718:59 RM TAL PEN

Total/NA Prep 3546 339010 01/19/17 07:20 RDT TALPEN

Total/NA _Analysis MA-EPH 339633 01/24/17 23:11 RM TAL PEN

Total/NA Prep 30508 338440 01/15/1711:30 DN1 TAL PEN

Total/NA Analysis 6010C 338689 01/16/1.7 16;08 RJ8 TAL PEN

Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TAL PEN

Soluble Analysis 353.2 338609 01/16/1712:21 KJR TAL PEN

Total/NA Prep 3060A 339244 01/20/1717:00 CLM TALPEN

Total/NA Analysis 7196A 339470 01/23/1712:07 CLM TALPEN

Total/NA Prep 90128 339068 01/18/1710:53 BAB TALPEN


Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01/11/1713:15 Matrix: Solid Date Received: 01112/1716:57


Total/NA Prep 7471A 337950 01/15/17 12:43 JAP TALPEN

Total/NA Analysis 7471A .338612 01/16/17 09:57 JAP TALPEN

Total/NA Analysis Moisture 338607 01/16/1712:37 CJP TAL PEN

Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01/1111713:15 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 48 .• 8



Total/NA Prep 5035 339082 01119/ft bi\:59 BSW TALPEN

Total/NA Analysis 8260G 50 339083 01/19/1712:21 cs TALPEN


Total!NA Analysis 8270D 338741 01/1711714:54 MAM TAL PEN

Total/NA Prep 5035 338604 01/16/1711:00 MKA TALPEN

Total/NA Analysis MAVPH 50 338571 01/17/1710:52 MKA TALPEN


Total/NA Analysis 80818 2 338801 01/17/1721:10 MAM TAL PEN


of 140 2/1/2017


Client Sample ID: CK•5 Lab Sample ID: 400-1325BB-6 Date Collected: 0111111713:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8

Batch Batch Dilution Batch Pr~pared


total/NA Pi€p 3546 339010 01/19)1701:20 ROT TAL PEN Total/NA Analysis MA-EPH 339632 01124117 18:02 RM TAL PEN



Total/NA Prep 30508 338440 0111511711:30 ON1 TAL PEN

Total/NA Analysis 6010C 338689 0111611716:11 RJB TAL PEN

Soluble Leach DI Leach 338576 01116117 09:57 KJR TALPEN E -Soluble Analysis 353.2 338609 0111611712:22 KJR TALPEN

Total/NA Prep 3060A 339244 0112011717:00 CLM TALPEN

Total/NA Analysis 7196A 339470 0112311712:03 CLM TALPEN

Total/NA Prep 90128 339068 0111811710:53 BAB TALPEN

Total/NA Ana_lysts 90128 339005 0111811717:30 BAB TAL PEN

C.lient Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01113/17 09:30 Matrix: Solid Date Received: 01/14/17 08:32


Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 ()i/15111'12:43 ON1 TALPEN

Total/NA Analysis 7471A 338612 0111611712:14 JAP TAL PEN

Total/NA Analysis Moisture 338696 0111711714:08 JNJ TAL PEN

Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01/13/17 09.:30 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9


Total/NA Prep 50.35 339082 01/19117 08:59 SSW TALPEN

Total/NA Analysis 8260C 339083 0111911715:35 cs TALPEN

TotaUNA Prep 3546 338817 0111811709:33 ROT TAL PEN Total/NA Analysis 82700 338966 01119117 00:09 MAM TAL PEN


Total/NA Analysis 82700 339121 01119117 22:14 KJA TAL PEN

Total/NA Prep 5035 338604 0111611711:30 MKA TALPEN

Total/NA Analysis MAVPH 50 338571 01117117 00:17 MKA TALPEN

Total/NA Prep 3546 338931 0111811712:42 RDT TALPEN

Total/NA Analysis 80818 2 339152 01119117 21:49 TD TALPEN


Total/NA Analysis MA-EPH 339632 0112411719:57 RM TALPEN



Total/NA Prep 30508 338528 01116117 08:55 KWN TALPEN

Total/NA Analysis 6010C 338847 0111711713:01 GESP TALPEN


of 140 2/1/2017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol

Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01/13/17 09:3.0 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9

Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Soluble Leach o-1·teach 338576 01/16/17 09:57 kJR TAL PEN Soluble Analysis 353.2 338609 01/16/17 12:26 KJR TAL PEN

Total/NA Prep 3060A 339244 01/20/17 17:00 CLM TALPEN

Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TAL PEN

Total/NA Prep 9012B 339068 01/18/1710:53 BAB TAL PEN

Total/NA Analysis 90128 339005 01/18/1717:37 BAB TAL PEN

Client Sample ID: CK.7 Lab Sample ID: 400-132650-2 E Date Collected: 01 /13/17 09.:45. Matrix: Solid Date Recelved: 01/14/17 08:32

Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 01/15/17 12:43 DN1 TALPEN

Total/NA Ana!ysls 7471A 338612 01/16/1712:16 JAP TALPEN


Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date collected: 01/13/17 09:45 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 23.3


Total/NA Prep 5035 339082 01/19/17 08:59 BSW TALPEN Total/NA Analysis 8260C 339083 01/19/17 15:58 cs TALPEN

Total/NA Prep 3546 338817 01/18/17 09:33 ROT TAL PEN

To.tal/NA Analysis 82700 338966 01/19/17 00:41 MAM TAL PEN

Total/NA Prep 3546 338817 01/18/17 09:33 ROT TALPEN Total/NA Analysis 82700 339121 01/19/17 22:44 KJA TALPEN

TotallNA Prep 503.5 338604 01/16/1711:30 MKA TALPEN

Total/NA Analysis MAVPH 50 338571 01/17/17 01:16 MKA TALPEN

Total/NA Prep 3546 339357 01/23/17 08:05 ROT TAL PEN Total/NA Analysis 8081B 339881 01/26/1715:18 MAM · TAL PEN

Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN

Total/NA Analysis MA-EPH 339632 01/24/17 20:07 RM TALPEN

Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25/17 00:18 RM TALPEN

Total/NA Prep 3050B 338528 01/16/17 08:55 KWN TALPEN

Total/NA Analysis 6010C 338847 01/17/1713:16 GESP TALPEN


Soluble Analysis 353.2 338609 01/16/17 12:27 KJR TALPEN


Soluble Analysis 353.2 5 338609 01/16/1712:32 KJR TALPEN

Total/NA Prep 3060A 339244 01/20/1717:00 CLM TALPEN

Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TAL PEN


of140 21112017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol

Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3

Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number Or Analyzed Analyst Lab Total/NA Prep 9012B 339068 61/18/1710:5:3 BAB Tl\LPEN Total/NA Analysis 9012B 339005 01/18/1717:37 BAB TALPEN

Client Sample ID:. CK-8 Lab Sample ID: 400-132650-3 Date Collected: 01/13/17 10:10 Matrix: Solid Date Received: 01114117 08:32

Batch Batch Ollutlon Batch Prepared E Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 01115/1712:43 DN1 TALPEN Total/NA Analysis 7471A 338612 01/16/1712:17 JAP TALPEN


Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 0111311710:10 Matrix: Solid Date Received: 01/.14/17 08:32 Percent Solids: 46.4

Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Ana:lyst .Lab

Total/NA Prep 5035 339330 01122/17 07:44 RS TALPEN Total/NA Analysis 8260C 339331 01/2211713:31 RS TALPEN

Total/NA Prep 3546 338817 01/18117 09:33 RDT TALPEN

Total/NA Analysis 82700 338966 01/19117 01:14 MAM TALPEN


Total/NA Analysis 82700 339121 01/19/17 23:14 KJA TALPEN

Total/NA Prep 5035 338604 01/16/1711:30 MKA TALPEN

Total/NA Analysis MAVPH 50 338571 01/17/17 02:16 MKA TALPEN

Total/NA Prep 3546 338931 01118/1712:42 ROT TALPEN

Total/NA Analysis 80818 2 339152 01/19/17 22:50 TD TALPEN

Total/NA Prep 3546 339010 01/19117 07:20 ROT TALPEN

Total/NA Analysis MA-EPH 339632 01/24/17 20:17 RM TALPEN

Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25117 00:27 RM TALPEN


Total/NA Analysis 6010C 338847 01/17/17 13:20 GESP TALPEN

Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TALPEN

Soluble Analysis 353-2 338609 01/16/1712:28 KJR TALPEN

Total/NA Prop 3060A 339244 01/20/17 17:00 CLM TALPEN

Total/NA Analysis 7196A 339470 01/23/1712:07 CLM TALPEN

Total/NA Prep 9012B 339068 01118/1710:53 BAB TALPEN Total/NA Analysis 90128 339005 01/18/17 17:37 BAB TALPEN


of 140 2/1/2017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1

Project/Site: Moffat & Nichol

Client Sample ID: CK-.9 Lab Sample ID: 400-132650-4 Date Collected: 01/13/1710:25 Matrix: Solid

Date Received: 01/14117 08:32

Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 7471A 338513 01/15/1712:43 ON1 TALPEN


Total/NA Analysis Moisture 338696 01/17/1714:08. JNJ TALPEN

Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01/1311710:25 Matrix: Solid

E Date Received: 01114117 08:32 Percent Solids: 52.0

Batch Batch Dllutlon Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab

Total/NA Prep 5035 339082 01/19/1708:59 BSW TALPEN

Total/NA Analysis 8260C 339083 01/19/1716:47 cs TALPEN


Total/NA Analysis 82700 338966 01/19/17 01:47 MAM TAL PEN


Total/NA Analysis 82700 339121 01/19/17 2.3:44 KJA TAL PEN

Total/NA Prep 5035 338604 01/16/1711 :30 MKA TAL PEN

Total/NA Analysis MAVPH 50 338571 01/17/17 03:16 MKA TAL PEN

Total/NA Prep 3546 338931 01/18/1712:42 ROT TALPEN Total/NA Analysis 80818 2 339152 01/19/17 23:20 TD TAL PEN


Total/NA Analysis MA-EPH 339632 01 /24/17 20:37 RM TALPEN

Total/NA Prep 3546 339010 01/19/17 07;20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25/17 00:46 RM TALPEN


Total/NA Analysis 6010C 338847 01/17/1713.:23 GESP TALPEN

Soluble Leach DJ Leach 338576 01/16/17 09:57 KJR TALPEN

Soluble Analysis 353.2 338609 01/16/1712:29 KJR TALPEN

Total/NA Prep 3060A 339244 01/20/17 17:00 CLM TALPEN

Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TALPEN

Total/NA Prep 9012B 339068 01/18/1710:53 BAB TALPEN


Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01113/17 10:45 Matrix: Solid

Date Received: 01114117 08:32



Total/NA Prep 7471A 338513 01115/1712:43 ON1 TALPEN Total/NA Analysis 7471A 338612 01/16/1712:20 JAP TAL PEN



of140 2/1/2017


Client Sample ID: CK-10 Date Collected: 0111311710:45 Date Received: 01114/17 08:32

Prep Type Total/NA Total/NA

Total/NA

Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA Total/NA

Soluble Soluble

Total/NA

Total/NA

Total/NA Total/NA

Batch Type Prep Analysis

Prep

Analysis

Prep Analysis

Prep

Analysis

Prep Analysis

Batch

Method 5035 8260C

3546

82700

3546 82700

5035 MAVPH

3546 80818

Prep 3546

Analysis MA-EPH

Prep 3546 Analysis MA-EPH

Prep 3050B Analysis 6010C

Leach DI Leach Analysis 353.2

Prep 3060A

Analysis 7196A

Prep 90128 Analysis 9012B

Client Sample ID: RB-2 Date Collected: 01/13/17 11 :00 Date Received: 01/14/17 08:32

Prep Type Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA

Total/NA Total/NA

Total/NA Total/NA

Total/NA

Batch

Type Analysis

Prep Analysis

Prep

Analysis

Batch Method

8260C

3520C 82700

3520C

82700

Prep 3520C

Analysis 82700 LL

Analysis MAVPH

Prep 8011

Analysis 8011

Prep 3520C Analysis 8081 B

Prep 3520C

Analysis MA-EPH

Prep 3520C

Lab Chronicle

Run

Run

RERA RERA

Dilution

Factor

50

2

Dilution

Factor 1




Batch Prepared

Number or Analyzed Ana!Yst Lab 339082 01/19/17 08:59 ElSW TAL PEN 339083 01/19/17 17:13 CS TAL PEN

338817 01/18/17 09:33 RDT

338966 01/19/17 02:20 MAM

338817 01/18/17 09:33 RDT 339121 01/20/17 00:15 KJA

338604 01/16/1711:30 MKA 338571 01/17/17 04:15 MKA

338931 01/18/17 12:42 RDT 339152 01/19/17 23:50 TD

339010 01/19/17 07:20 RDT 339632 01124/17 20:47 RM

339010 01/19/17 07:20 RDT 339633 01/25/17 00:55 RM

338528 01/16/17 08:55 KWN

338847 01/17/1713:26 GESP

338576 01/16/17 09:58 KJR 338609 01/16/1712:30 KJR

339244 01 /20/17 17:00 CLM

339470 01/23/17 12:07 CLM

339068 01/18/1710:53 BAB 339005 01/18/1717:37 BAB

TAL PEN

TAL PEN

TAL PEN TAL PEN

TAL PEN

TAL PEN

TAL PEN TAL PEN

TAL PEN

TAL PEN

TAL PEN TALPEN

TALPEN TALPEN

TALPEN TALPEN

TALPEN

TALPEN

TAL PEN TALPEN


Batch Prepared

Number or Analyzed Analyst Lab 338771 01/17/1716:13 CLN TAL PEN

339125 01/19/1715:31 KLR 339672 01/2511710:06 KJA

340079 01 /27 /17 11 :20 KLR 340421 01/31/1716:30 MAM

339125 01/19/1715:31 KLR 339599 01/24/1716:27 S1S

339057 01/19/17 23:24 MKA

339493 01/23/1716:25 KH1 339878 01/27/17 00:38 KH1

339054 01/19/1710:03 KLR 339554 01 /24/17 13:06 TD

339262 01 /20/17 15:54 KLR 339948 01/26/17 17:34 RM

339262 01/20/1715:54 KLR

TALPEN TALPEN

TAL PEN

TALPEN

TALPEN TAL PEN

TALPEN

TALPEN

TALPEN

TALPEN TALPEN

TALPEN TALPEN

TALPEN


of140 2/112017


Client Sample ID: RB-2 Date Collected: 0111311711:00 Date Received: 01114117 08:32

Batch Batch Prep Type Type Method Total/NA Analysis MA-EPH

Total/NA Prep 3010A

TotallNA Analysis 6010C

Total/NA. Prep 7470A

TotallNA Analysis 7470A

Total/NA Prep Distill/CN Total/NA Analysis 335.2

Total/NA Analysis 353.2

Total/NA Analysis 7196A

Laboratory References:

Lab Chronicle

Dilution Batch Prepared

Run Factor Number or Analyzed :3:39950 ()1/26117 20:09

338893 01/1811710:09

339167 01/19117 16:25

338653 01116117 16:27

338941 01/18/17 13:46

338793 01/17/17 09:30

338792 01/17117 14:24

338579 01/16/17 09:36

339253 01/14117 09:18

TAL PEN= TestAmerica Pensacola, 3355 Mclemore Drive, Pensacola, FL 32514, TEL (850)474~1001

of140



Analyst Lab

RM TAL PEN

KWN TAL PEN

GESP TALPEN

JAP TALPEN

JAP TALPEN

BAB TALPEN

BAB TALPEN E KJR TALPEN

JLB TALPEN


21112017


Laboratory: TestAmerica Pensacola

Certification Summary

Unless otherwise noted. al! analy!es for tr1is laboratory were covered under each certification be!o\V,

Authority Louisiana

Program NE LAP

EPA Region Certification ID 6 30976

The following analytes are Included in this report, but are not certified under this certification:

Analysts Method Prep Method Matrix Analyte s26ilc 5035 Solid isol>l.ltyl a1c0ho1

The following analytes are included in this report, but certification is not offered by the governing authority:

Analysis Method Prep Method Matrix Analyte 353.2 · Solid Nitrate Nitrite as N 90128 90128 Solid Cyanide, Total MA~EPH 3520C Water C21-C35 Aromatics MA-EPH 3546 Solid C21-C35 Aromatics Moisture Solid Percent Moisture

of 140


Expiration Date 06-30-17


2/112017

"1J

"' <O (l)

~

"' CJ)

Q. ~ ... 0

~ ;::> 0 ~

.....

TestAmerica Pensacola 3355 Mclemore Drive

;Pensacola, FL 32514 Phone (850) 474-1001 Fax (850) 478-2671

Client Information Client Con!act:

f_iennifer Lindquist :company: ,C-K Associates fMdress:: 17170 Perkins Road

n Rouge

;f'horu;!:

""'" ~Jennifer.1indqu1S'"[email protected] Project Name: Moffat & Nichol

""'

!ample Identification }'.,;~;;{:::--.. :;,,.:: · '.:-~·--·~::..-~.- ·~;~_::_.~~~-·;, ~:: ,:~~---·· ·><'-.;··:~~-. :u:-:-1"'0,

~~\:t,j_

Chain of Custody Record

15'"]/oc I r '.iJ...-..JJJb 11.S o-,

Pti.i'ie: ~<' '1.St' /JY.5()

Lab PM:

Wilson, Jason A E-Mait

[email protected]

CarrierTraeking No{sj::

Analysis Requested Due Date Requested:

TAT Requested (days):

PO~

Purchase Order Requested WO#:

f>rofect#:.

40007814 SSOW#;

Matrix (-.

Sample ~

i-IH'I ~ Solid

--Solid --Solid --Solid --Solid --Solid --Solid --Solid

--Solid

Solid 11

z ~

-.:;; ~~

i i ~ ~ ~ _g~~~Sl tu es~g5 ~ -=~~~!:: @ ::; ~ ~ ] g g ~ ~ ~ m ~ N ~

~~~£~:::-; a:itS<tNlma.o ~~~.,.;~~g

~t~~~ .~~J~~~}.~ v

I I I I I I I I

~ ~ ~

::: g t3 r::} Q ~ 0 ~ 0 ' • 0

~ fil ~ Q <( ~ <:> 0 0 0 <:> a ~ ~ ~

~

~ :!

~ 0

c 0 ;;.

l!f 6 7 ii: 0

~ ~ i ~ ~ ~~'.~: ~(. &E ~

J 1../I vl\-'i v

I I I I I

~

~ Q

~ t; ~

TestAmerica TI":!:: l..fu",Dffi_r.{ e,.-v3R0~Af- TE.STJ!'<G

COCNo: 400-61884-25981.1 Page:

Page 1 of3 'JOO#:

I-~ Preservation Codes:

lJ~ A- HCL M - Hexane t;. B-NaOH N-None ji< C-ZnA°"'te O-kNo02

~.t1:'. D- Nitric Acid P - Na204S ~::'.~'; E- NaHS04 Q - NB2S03 ~-~·'; F- MeOH R- Na2S203 ;;gt G-Amchior S - H2S04 ~;~: H -Ascorbic Acid T - TSP Dodecahydrate :;:,q,, 1- lee U -Aceton~ -~ J-OIWater V-MCAA ':"'"'. K-EDTA W-pH4-S 1-" L-EOA Z-Nhor(spocify)

"' Special !nstructionsfNote:

i:":~~:::::.:;;'

R A.00-132540 coc

i~ ~ Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) 1CJCi,ible Hazard lderrtification

" Non-Hazard CJ Rammable OSkin Irritant D Poison B D Unknown CJ Radiological CJ Return To Cfient CJ Disposaf By Lab D Archive For Months

Deliverable Requested: I. !!, Ill, IV, Other (specify)

Empty Kft ReITnquished by:

Relinquished by:

Custody Seals Intact I Custody Seal No.: ti Yes a No

Date:

"baietfirOO'.". Company

I -11-1 omemnie: Company

Dale/Ti.me: company

Special Instructions/QC Requirements:

Time: MethOd of Shipment:

RecQived ti): l°'Jlt?-/17 {)C(ZI W?iif 'D •me: { Com;xiny

Received by: Datefr!!'TI!'!: Company

-~erTem;:um:rture(s)°CandO!Mr~~~ 1<o :7'L& • c.

;i

"U

"' (0 <D

"' .._, Q, ~ ,,. 0

t2 ~

;:;, 0 ~ .._,

TestAmerica Pensacola 3355 Mclemore Drive

Pensacola, FL 32514 '.phone {850) 474-1001 Fax: (850) 478-2671

Client Information


mJ;;)ohr.">o-> LlbPM:

Wilson, Jason A earner Trac!ting -No(s):

E-Mail: Cl~Cootact

Jennifer Lindquist Cornp:;!ny::

?~ q,:,g (~ liason .. wilson@testamericainc .. com

C-K Associates 'Address: D11<>o.rte Reque$llld:

17170 Perkins Road C<r. iTATRequasted {days): Baton Rouge State, Zlp: LA, 70810 Ft.one: PO#:

Purchase Order Requested

-~ :WO#:

l'[email protected] I ~~ Project Name: ?reject#: ~· Moffat & Nichol 40007814 Site: SSOYV#:

Sample Identification

:-~,;-:,::.,.~.;.: .. ,~;~~:::;.:~~~ :.~-:~--~:;~~~~-~~ ~-~;-~-:;:·:-~:::-->~:"$~.t ,, ... ~:0

R ;.-,o,c.\-e '\ i -11-n 1 1 ?~ I

Matrix

c-. ......

1~11 Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid

z ~ w

I " ~ z • ~

z : ~ !§

~ z E

~· ~

I 'Vf v

Analysis Requested

'""(~'§%!!if''-. .~¥·$_,._,_,_.if"~ - ..... ~---~:,_·-~ii; fi::. -§¥~~~~jt~'.

Test America n-IE~s::m;g,.~~"3-

COCNo:

400-61884-25981 .. 2 Page: Page2of3 Job#:

Proservation Codes:

.... A-HCL

""I-~ B-NaOH C- Zn Acelato

:...., D-Nl'.ficAcid E-NaHS04 F-MeOH

1-.;-1··8.- G· Amchlor ~ H-AscofbbAcid

,~4 ~~:w~ ·~-~.,: K-EDTA

L~EDA :@: ~ .. Other:

M-Hexane N-None 0-AsNa02 P-Na204S Q·Na2S03 R-Na2S203 S- H2S04 T - TSP Dodecallydrate LI-Acetone V-MCAA W-pH4-5 Z- other (Specify)

Special Instructions/Note:

'~.:_ ,-.;-;

[i

&e...,~~:-.:;-;,:_;~-:-~;::,~"*-:s~

'iiiifaible Hazard Identification

D Poison B D Unknown CJ Radiological

Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)

DRetum To Client CJ Disposal By Lab D Archive For Months Lf-.l Non-Hazard CJ Flammable DSkin Irritant Deliverable Requested: I, !!. JU, IV, Ottier (specffy)

Empty K"rt Relinquished by:

""'"""~"'!\. ... R(i!inquiShea ~

Refi'.lql.lished by:

Custody SeaJs Intact: I Custody Seal No.; !:.. Yes 6. No

Date: Date.Time.:

Ht-!'l Datatnme:

Date.Time:

Special Instructions/QC Requirements:

Method of Shipment

Ccmp""Y

7 012./ Company

Company Received by:, Date/Time: 1co·l"l',pany

Cooler Temporature{.s-} 0c and Other Rerr.arks:

c--~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~

-u "' (Q (1)

~

"' (X)

a ~ ... 0

~ '3 0 ~

"

T eslAmerica Pensacola 3355 Mclemore D;ive

Pensacola, FL 32514 Phone {850)474-1001 Fax {850) 478-2671

Chain of Custody Record TestArr1erica TIUi.l..~!ffil!>'ENV!~ITT,;t. ~Tr.<l:G

Sam,,le;: fl./. . n f L3b PM: Client Information /'. ·ftlr:> {'CJ fJ J'l.50'\ WTiscin, Jason A

Carrier T i:Jcking NO(Sf. COCNo:

40Q..61884-25981.1 Cfient Comae<: P otie: LJ ? 0- E-Ma11: JenniferLindquist ,!)~ -i?t> /J7.So · [email protected]

Page: Page 1 of3

Company: Job#: C-K Associates

F;-;::'Perldns Road lTATRoq"°"""'°"' I~ C"r Baton Rouge

DueOate RcquestOO: r--,--,--,--An.,....•~ly"s_i_s r .... .i::.te.d

'.m· y·.· ' ... i .:..

l: ·=

t~~::~tion Cod::_ Hemm N-None O-AsNa02 P-Na2043 0,-N82S03 R-N:.2$203 S-H2s04

&a!e,Zip: LA. 70810

"")'j5 755 /OQO Email: [email protected] Project Name:

Moffat & Nichol 0"";.J.o, 'fo.c~f f/CJhor

PO#. Purchase Order-Requested IWO#:

Project#:

40007814 SSOW#:

~Ji

gr~ q

~~ ~ w

~

1~ -!

400-132588 coc

- '

. I j J ~ ~

O]j!~ w ~I" ~ c

: ~ - -;-g

} ! 3

T ~TSP Dodec:ahydrate U-Acetootl V-MCAA W-pH4-5 Z- other (specil)•)

. ··. ·.-·>.---'.'~~-~-

/lit/--<.. i 1-11-11 I '" 1<i b 1 solid 1 1 1 VJ vr vrvrvr "1 v ;,.,-:;.._

0Y '0

7 I 1.~;.g 0 1 Solid 1 1 x1 v1v'1 vr vrvr vr v

7J /3 ;,5t (!, I Solid I '1:. Solid ~, Solid ~"lg;~

~:;,r.'

-::::::~

-~~ Solid

Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)

CJ Return To Client DDisposaf By Lab CJ Archive For. Months

Possible Hazard Identification

D Non-Hazard D Flammable DSkin Irritant DPoisonB DUnknown DRa.diofogicaJ Deliverable Requested: I, n, Ill. IV. Other (specify) Special Instructions/QC Requlremerrts:

Empty Kit Relinquished by. Date: Time: ' I

' Method of Shipment: • • ~ !!

Oater~1me: ( '-· .,; /,. £ o-aierrmie; \[ ' ") OO:mpaoy /I. -1:>--11 W#f\l!f.., 1-i "'r 1 c · v y,,.

Jibrv!A) (U,, ""t:'.it-f{ i //;.;_/;/ j(p_ ~-Mt I R!>linquished by.

CustOOy Seals Intact !Custody Seal No.: t;. Yes .6. No

l°"*'JTime; m--. -1comp.a,.,Y , \Receive!l"b}~· T ··--- (Da:!¢JTome: /

eoo0<Tomperarurn<sJ<cs~ 1

. z,Z/O C. ,

Company

2. 7v~ 7K&

"U

"' "' CD ~

"' <!)

a .... 0

~ '3 0 ~

"

. I ' I TestA~erica .Pensacola 3355 Mclemore Dnve ' Pensacola; FL ~514 Chain of Custody Record ~hone (859)474-1001 Fax (850) 478-2671

Lab PM: CanicrTn"ici:"fng No{~): blient ln~onnation '"'""Pcetv K; r Ii Wilson, Jason A criem CotrtaCt:

1~ennlfer ufidquist f>hone:

2&s-1;ss-100 o '""""' I [email protected] -t-KA.sso~ :Mo-ess: I

17170 PeOOns Road Due D<rte Reqt1=ed:

City.

Baton Rouge !TAT Requested {d<lyS):

.~\:\tj ""' r 1~· j IP,<Chase Ocdec Reque.ted~ I i -• . Ema!l: i [email protected] P1*ctName.: Moffar& rfichol

Si'~ NOLA I ,

Project""#: 40007814 'SSOW#:

I Sample Matrix

Type {~;:· , Sample {C=comp, ~oil,

lSample !kl.entffication Sample Date Time G= rab ITTaT=

i'.~"~::-:·~:'~ ;:-;.~~:: ,;_. ~:;::~·:~;~~~~:~-:.:~~~~'.::.'2~:__ -. If:~~~:.:~;:;~ ;f:::~_,:::·;._, ~~~~%~

c~-& 1I1:3! 11 I oq3r (.;. Solid

r1-?-7 ~--· G- Solid

ci-Z - ~ JOJO G ~""""""

[,J.<- q jQ'JC. r.,. l<;-Cl-1\-to !OUC. r ... s-~6,~ 1100 s vJ

1i§J I~

~alysis Requested

•;.t x u. x ~ n.< u.< >· 0 > 0 a.: ~ .o. .o. ~

:-g~ ~g~ fu :;·~; ;;~:t~ ~ ~ ~ g ~ ~ g ~ ~ ~ ~~~ fil~'.:..g § -~ ·i g .g ~ s g § ~ a ·~ .q- ~ ~ ~ g N ;;. J-~ ·.g ~ . . . . ~. . . v

I II \ I \ I \ nrm 7

f llT }. lv1 vlvlvY

TestAmerica ~L~t."1!0:>.~7,o;t,,'fESTI~

COCNo:

400-B1884-25981.3

::":;~ I of a.. Job#;

I-Prns•Mtt;on coo''"

A-He!.. M-Hexane B-NaOH N-Ncnc C-ZnAC9!a!9 O-AsN302 D - Nitric Acid P- Na204S E - NaHS04 Q- Na2SO$ F-MeOH R-Na2S203 G • Amehlor S - H2S04 H -Ascorbic />.cid T ·ISP Doclecahydrate 1 - roe u-Acetone J-DIWa!er V-MCAll. K-EDTA W-pH.4-5 t.·EDA Z-olt:et{speeiM

r.

Special [nstructions!Note:

~~~~:~·:·::~~::;;:;:2~~~1

m ---------

400.132550 coc ---

PO$Sibte Hazard Identification

CJ No~Hat:ard D Rammable CJSkin Irritant CJ Poisofl B D Unknown DRadiologlcal

Sample_Dis-poSir( (A fee may be assessed if samples are retained longer than 1 month)

D Re.tum To:Qfient D Di5P0.sal Bv Lab D Archive For Months Deliverable Requested: I, 11, Ill, JV, Other (specify}

. . I Em~ kjt Relinquished by;

Fl'PY, ""~nz.::: ~ . " , .. R'"''''"j'"_:' Vl~ 21. v

• ,,,-.Jil

Ref"'GlJWie<lby:. l I

Custtj:ly Seals Intact ICµstody Seal No..: 6. r"fes · b. No

'"

IDate:

j113J17 !-Jth-~l O.fo("rr~'".2 -\~

tc..-l 1 I -4b , Datefnrr.e: 1

C".Qmpany

~/,1 \ 1-\

Company

'Special !nstructio)1s/QC Requirements: i

Time:

R(i"'_"" iJ ,#/./ R"""""""" Iv /}

--···-1 . .,...,

R='-<d°'cf/ F/7/

Melhiid of ShipriWlt:

Date/Time

l /,",//7 O'ateffime:

ll\if/n

dJ- Compa~J't·

I Company'"

l:>o'L Com~ny I)'.\

=·~"""'j'"'"'·c-ll"''"°""""' t .o·c-' t «re. -'2 _o·c 2 , \ ·c. 'I?G.

I I

~ "' (1)

~ ,,. 0

S, ,,. 0

~ j;:; 0 ~ -...

: I TestAmerica Pensacola . I -3355 McLrmore Drive

l(ensaco!~ FL 32514 Phone {8~) 474-1001 Fax (850) 478-2671

Client frtformation Cfient COr!bi:t:

~ennffer ljndquist


Wl!son, Jason A "'·- f<CA.v 1-<J rl<.. lab PM:

E-Ma:l: f lffillnn_wi~on@testamericai~c.com

Phone· t

. a.2<:,-1S'S-f600

Carrier Tracking No(s):

Test America nu;:~ II'< GN'lilaO~.o,l,. TSS>fNC,1

COCNo:

400-61884-25981.4 Paga:

Pa9~ 01.z:f'..a Ob#:

:Company: !

C-K Asso~ates j Analysis Requested iMaress: I 17170 Pej1<ins Road

~" I BalonRoi;ige ~Zip::; LA, 7081tj Ph00$:

! I ,Email: I [email protected] Project Naflie:

:Moffat & ~icho! ·~e: ND'-k

Due Date Requested:

TAT Requested (days):

Pb#: Purchase Order Requested WO#;

Projec:.#:.

;40007814 SSOW*

Sample Type

(O:comp, J Sample Sam le ~enfrfication Sample Date Time G= tab' ~{{':@~~;;:i:<;:~'-~~~~~·:...~v, -,..- -~·~."._.,.~1"~, -~ > o'< ""·~tf/'.:-:-;_ 4:;,~-;:~~~:;i}" • ··~:::~~1 ~~

Matrix c-. ,.,.., ,._..,

~B-~ 11 12fr1 llloo r-.-1;.~ So!ld

Watec

Wat..-

Wat..-

.::'.;;..~ ~·;:,~pf>;;_<--..:r.·"f'_ ~-..;::;,· .;:::!;~ '~""'l'"f~~=•"'"'

Preservation Codes:

A->-lCI.. .,,, B-NaOH

~'i{"· C <Zn Acetate ~ D·Nltf.cAOd ~~ E-NaHS04 <·~~ F-MeQH !J.<i>i G-Amch\or ~ H-AscorbicAcid 4~ !-foe

J-DIW-aw,r K·EDTA L·EOA

M- He:oane

N--0-AsNa02 P-Na204$ O-Na2So3 R-Na2S203 S-H2S04 T -TSP Dodet:ahydra\e U-Acek.ine V-MCM W-pl-14-5 Z:-olher(spedfy}

l""w. flJ #$1JJ '.iC!. e,,_en ict ,

!~~, Special Instructions/Note:

... ~'.

li

_;;.,..

' I ' I ~

I

•

11 •. "" ,

' ! , I I '

Possibfb Ha:rard fdentification

D Noli-Hazard CJ Rammable DSkfn Irritant D Poison B CJ Unknown D Radiological

jDe1iVerab!e Requested: 1, l!,.11!, IV, Other (specify)

Empty Kit Relinquished by:

;R°'"llt~ j • , • . . 'jR.Ooq,.. byc (fl/!lf Jj_ ' 1/1 .,,.-//

~' Rei;nq,,;s.'iQd t>y:. i

I ' Gust.of!~ Seals Intact: fCUsi:ody Seal No.:

Ll (Yes 4 No

-,Sample Dispos<il (A fee maybe assessed if samples are reteined longer than 1 month)

CJ Return To blient D Disposal By Leb CJ Archive For Months Special lnstructiohs/QG Requirements~

I (Time: fMe>lhoci of Shipment -

Cc:mpany -~

eom,,.,.,,

R~"t::~~ R.-.byc ! jl

RecelvOOby: I I

Cooler Tempei3ture(s) °C and Other Remar1cs:

I

'''+-'''

~~i~.--f~

Da~/17 r9. Com~ ;t:-Oatarr.Tne: ' COOi~y

DatE:/Tiine:: &pany

.-.. .,,.-

Tpaanat

Tin

R

THE LEADER IN ENVIRONMENTAL TESTING

ANAL YTICAl REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola 3355 Mclemore Drive Pensacola, FL 32514 Tel: (850)474-1001

Tes!America Job ID: 400-132588-2 CHent Project/Site: Moffat & Nichol

For: C-K Associates 17170 Perkins Road Baton Rouge, Louisiana 70810

g,-w:1-.-Attn: Jennifer Lindquist

Authorized for release by: 211412017 1.:52:23 PM

Jason Wilson, Project Manager I (251 )706-3217 [email protected]

he test results in this report meet all 2003 NELAC and 2009 TN! (equirements for accredited rameters,- exceptions are noted in this report. Tl1is report· may not be reproduced except in full, ct with written .approval fron1 the laboratory. For questions please contact the.Project Manager t/1e e~maif address or telephone nurnber listed on this page.

his ·report has been electronically Sig.ned and authorized by the signatory. Electronic signature is tended to be the legaf/y binding equivalent of a traditionally handwritten signature.

esults relate only to the items tested and the sample(s) as received by the laboratory.

Client C-K Associates Project/Site: Moffat & Nichol

Table of Contents

TestAmerica Job ID: 400-132588·2

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Page 2 of9 T estAmerica Pensacola

2/14/2017

Narrative

Case Narrative Client: C-K Associates Project/Site: Moffat & Nichol

Job ID: 400-132588-2

Laboratory: TestAmerica Pensacola


Job Narrative 400-132588-2

Comments No additional comments.

Receipt The SE\mples were received on 1/12/2017 4:97 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The tempeJatures of the 3 coolers at receipt time were 2.2° c, 2.4° C and 2.7° C.

Metals No analytical or quality issues were noted, other than those described. in the Definitions/Glossary page.

Organic Prep Method(s) 1312: The sample had a noticeable amount of water in it, however the sub-sample did not yield any filtrate from the wet sample. An unaccounted difference of 7 .7 percent between the initial sub-sample and the final portion applied to pressure filtration indicates towards a loss of liquid. The affected sample is as follows: CK-1 (400-132588-1).

No additional analytical or quality issues were noted, other than those descrlbed above or in the Definitions/Glossary page.

Page 3 of9 TestAmerica Pensacola

2/14/2017


Lab Sample ID

400-132588-1

Client Sample ID

CK-1

Matrix

So!ld

Collected

01/11/1711:10

Received

01/12117 16:57

Sample Summary

Page4 of9


2/14/2017



Client Sample ID: CK-1 Date Collected: 0111111711:1.0 Date Received: 01112/1716:&7

Method: 6010C ·Metals (ICP) • SPLP East Analyte Result Quallfier RL

0.010

MDL Unit

0.0020 mgfL Lead 0.0025 J

0



Prepared

02110/17 08:54

Analyzed

02/10/17 17:03

011 Fae

1


Page 5of9


2/14/2017

Definitions/Glossary Client: C-K Associates ProjecVSite: Moffat & Nichol


Qualifiers

Metals

Quallner Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary

Abbreviation These commonly used abbreviations may or may not be present In this report.

• Listed under the "D~ column to designate that the result is reported on a dry weight basis

%R Percent Recovery

CFL Contains Free liquid

CNF Contains no Free liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fae Dilution Factor

DL, RA, RE, IN Indicates a Dilution,. Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concenlration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable ~oncentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL If shown)

POL Practical Quantitafion Limit

QC Quality Control

RER Relative error ratio

RL Reporting limit or Requested Limit (Radiochemistry)

RPO Relative Percent Differen'ce, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEO Toxicity Equivalent Quotient (Dioxin)

Page 6 of9


2114/2017


Method: 6010C ·Metals (ICP)

Lab Sample ID: LCS 400-34174412-A Matrix: Solid Analysis Batch: 341902

Analyte

Lead

Lab Sample ID: LB 400-34142411-D Matrix: Solid Analysis Batch: 341902

Anatyte

Lead


LB LB

Result Qualifier

<0.0020

Sample Sample


Lead 0.0025 J

Lab Sample ID: 400-132588-1 MSD Matrix: Sollcl Analysis Batch: 341902

Sample Sample

Analyte Result Quallfler

Lead 0.0025 J

Spike

Added

1.00

Spike

Added

1.00

Spike

Added

1.00

RL 0.010

LCS LCS


0.890 mglL

MOL Unit

0.0020 mgfL

MS MS Result Quallfier

0.929

MSO MSO

Rt!sult Qualifier

0.913

Unit

mg/L

Unit

mgfL

Page 7 of9



o/nRec.

O o/PRec Limits

89 B0-120

Client Sample ID: Method Blank B Prep Type: SPLP East

o Prep_ared

02/10/17 08:!54

D %Rec

93

Prep Batch: 341744

Analyzed

02110/17 16:47

Dll Fae

1

Client Sample ID: CK-1 Prep Type: SPLP East

Prep Batch: 341744 0/aRec.

Limits

75 - 125

Client Sample ID: CK-1 Prep Type: SPLP East

Prep Batch: 341744 %Rec, RPO

Limits

75 - 125

RPO Limit

2 20


2114/2017

Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132588-2

ProjecUSite: Moffat & Nichol

Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 Date Collected: 01/11/1711:10 Matrix: Solid Date Received: 01/12/17 16:57

Batch Batch 011 1n1t1a1 Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab SPLP East Leach 1312 77.13g 1542 ml 341424 02/08117 11:10 RMC TAL PEN

SPLP East Prep 30:10A 50 ml 50mL 341744 02110/17 08:54 KWN TAL PEN

SPLP East Analysis 6010C 341902 02110/17 17:03 SEH TAL PEN

Client Sample ID: Method Blank Lab Sample ID: L8400-341424/1-D B Date Collected: NIA Matrix: Solid Date Received: N/A

Batch Batch 011 lnltlal Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab SPLP East Leach 1312 100.00 g 2000 ml 341424 02108117 11:10 RMC TAL PEN

SPLP East Prep 3010A 50ml 50ml 341744 02/10/17 OB:54 KWN TAL PEN

SPLP East Analysis 60100 341902 02/10/17 16:47 SEH TAL PEN

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-3417 44/2-A Date Collected: N/A Matrix: Solid Date Received: N/A

Batch Batch 011 Initial Flnar Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 3010A SO ml 50 ml 341744 02/10117 08:54 KWN TALPEN

Total/NA Analysis 60100 341902 02/10117 17:00 SEH TAl PEN

Client Sample ID: CK·1 Lab Sample to: 400-132588-1 MS Date Collected: 01/11/17 11:10. Matrix: Solid

Date Received: 01/12/17 16:57

Batch Batch 011 Initial Final Batch Prepared

Prep Type Type Method Run Factor Amount Amount Nu.mber or Analyzed AnalYS:t Lab SPLP East Leach 1·312· 77.139 1542 ml 34'1';i24 02/08/1711:10 RMC ... TAL PEN

SPlP East Prep 3010A 50 ml 50ml 341744 02/10/17 08:54 KWN TAl PEN

SPLP East Ana.lysis ~010C 341902 02/10/1717:12 SEH TAl PEN

Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 MSD Date Collected: 01/11/1711:10 Matrix: Solid

Date Received: 01/12/1716:57

Batch Batch 011 Initial Flnal Batch Prepared

Prep Type Type Method Run Factor Amount Amount Number or Analyzed -Analyst Lab SPLP East Leach 1312 77.13g 1542 ml 341424 02/08/17"11:10 RMc TAL PEN

SPLP East Prep 3010A 50 ml 50mL 341744 02!10/17 08:54 KWN TAL PEN

SPLP East Analysis 60100 341902 02/10/17 17:15 SEH TAL PEN

Laboratory References:

TAl PEN= TestAmerica Pensacola, 3355 Mclemore Drive, Pensacola, FL 32514, TEL (850)474-1001


Page 8 of9 2/14/2017

-0

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T es'tAmerica Pensacola 3355 McLemore O)ive

Pensacola, FL32514 Phone {850) 474-1001 Fax {850) 478-2671


Som"-;· "/ . fl , f /' il-tfo (d J.r, fl50'\

Lcl>?M: CamerTr:ickins No(s); Client Information Wilson, Jason A C~entConiact:

!Jennifer Lindquist Pli"d;".!;is- 13''? /6'30 E-Majl:

[email protected] company: C-K Associates

IM'= I I' r7170 Perkins RoodTAT Req=stcd (day:>); c°" Due Date RequestOO::

Baton Rouge iState. Zio: LA, 70810 Phone:

~.:!5 ?55 fOQO Email: [email protected];om Project Name;

Moffat & Nichol

5'.";J_o, Yo.c~f fiqhor

P01'

Purchase Order Requested WO#:

Project#.:

40007814 SSON#:

Sample Matrix Type .(--.....

Sample ~ Sampkl Identification Sam le Date

1 lTAnalysisT.j-

1

,. ·~ l· ; I' -· ,,

I 400..132588 coc -! -..1-~~ n.

~ g <()I -

z

i I ~ > • ~ £: .! z

it I I,; ~ .:i:: ~ •• _ .,,, .. =

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TestArnerica n-tli. :.EA-"'B': •1' Sr."!l~ONJ..SW~ 'f!:ST;:<!G

COCNo:

1400-61884-25981.1 Page: Page 1 of3 Jo!:>#;

:·f.;;1: Preservation Codei:

~;r ;=~~H ~~~=r.e '\."~ C-ZnAcetate O-A$N302 ·:~,.,.m 0- NltricAcid ~4> E- NaHS04 ~";0 F-~OH · ',~·~: G - Amch1or I~~~/ H-AscortlicAcid :'/~~,, I-lea ~~ J-D1Water ·,o· K-EDTA

0 ··""'~

~~ ~ ~.

P·Na2CKS Q-Na2S03 R-r-r..zs2os S-H2S04 T ~TSP D:x,iecahydrate u -A<:e:JJ~ V-MCAA W-pH4-5 Z - o!her (specify)

~1-.;.·~:A ~ m. Special lnstructions/Note:

,.?;.'.''·' .er, :. _. " ''-~~'.;.:-.. " ,_._' · ' · ··· · ~ I - I 1-11-1? I Solid

•.::.·· .· . ... :·."'"~·, 'f '1""~·"r;f.'T~"ff ,, .!-~'.-:',,. --, . o. J~l· -.···- __ ,J, ·'" .. "

\I"- '> ,_-,,. ,; !t<cjAds:"\i*f~'' ~ ··.' ... ·

f~

. -c)< -d 1 1~1M2 1 11141 (,, F SoUd 11-1 ~ 1 ~$t-~-t I I r-r I tt1 ~

{J,/\{,'cc,h_ /-JI-/? /Jot? G Sond ~f ~ I I -;;;; /.J~- "<, - l/:.1/-rl I 12 ,:(1 6 I sond TT-I vf vi vfvf'vfvfv I?:' ~le:-'-/ I /-/ i-171 1,;1301 G I So1id I I rvr vt--"1 ;;r Vf Vj vt i '""'"l \":·,;;

/7k'- ~ l1-11-1JI 13Ki 0 i . · · - H!i'~

Sample Disposal (A fee may be assessed if samples are retained fongertharr 1 month)

D Retum To Client CJ Disposal By Lab D Archive For Months

Possible Hazard ldentific<ition

ONon-Hazard DRammabfe DSAfnlrritant DPoisonB 0 unknown DRadiofogicaJ

DeliYerable Requested:!, U, !I!, IV, Other (specify) Special !nstructtons!QC Requirements:

Einpty Kit Relinquished by: jDate: jTime: ~ jMe1hOO <ifShipnent

Custody Seals Intact I Custody Seal No.: t:,. Yes /:. No

v

_v ... pany

CoOO<Te,_rn(sJ°C•~i 2/-/VC., 2, J ~{!_ j:{( & 'II ,

appendix g report entitled new orleans municipal yacht harbor … · 2017-10-02 · sampling and...

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