appendix e: kentucky divison of water (kd ow

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APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA Appendix E1: 2016 KDOW ESB Fish Tissue Analytical Reports Appendix E2: Table E1- Calculation of Phase I and Phase II Adult and Young-of-the-Year Bluegill Selenium Whole-Body Fish Tissue Concentrations Appendix E3: Table E2- Comparison of Kentucky Environmental Services Branch and Phase I and II Adult and Young-of-the-Year (YOY) Bluegill Tissue Sample Results Appendix E4: 2018 KDOW ESB Fish Tissue Analytical Reports Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

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APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA

Appendix E1: 2016 KDOW ESB Fish Tissue Analytical Reports

Appendix E2: Table E1- Calculation of Phase I and Phase II Adult and Young-of-the-Year Bluegill Selenium Whole-Body Fish Tissue Concentrations

Appendix E3: Table E2- Comparison of Kentucky Environmental Services Branch and Phase I and II Adult and Young-of-the-Year (YOY) Bluegill Tissue Sample Results

Appendix E4: 2018 KDOW ESB Fish Tissue Analytical Reports

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA

Appendix E1: 2016 KDOW ESB Fish Tissue Analytical Reports

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA

Appendix E2: Table E1- Calculation of Phase I and Phase II Adult and Young-of-the-Year Bluegill Selenium Whole-Body Fish Tissue Concentrations

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Table E1: Calculation of Phase I and II Adult and Young-of-the-Year Bluegill Selenium Whole-Body Fish Tissue Concentrations Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

E.W. Brown Station, Herrington Lake, Mercer County, Kentucky

SamplingPhase Source Basis Sample ID Portion

Percent Moisture

(Ramboll/KU)

Selenium(CF and CR)

inmg/kg

Weightof portion

(WF and WR

in grams)

Weight (WWB)in grams

SeleniumWhole-Body Fish

Concentration(WBFC)

Using Equation 1

FF-001(BG)-CI-171004 Fillet 79.2 1.85 75.991FWB-001(BG)-CI-171004 Carcass 66.9 1.68 133.762

FF-001(BG)-CI-171004-FD Fillet 78.8 2.15 75.991FWB-001(BG)-CI-171004-FD Carcass 66.9 1.91 133.762

FF-001(BG)-CI-171004 Fillet 79.2 2.19 75.991FWB-001(BG)-CI-171004 Carcass 66.9 2.01 133.762

FF-001(BG)-CI-171004 Fillet 79.2 8.91 75.991FWB-001(BG)-CI-171004 Carcass 66.9 5.08 133.762

FF-001(BG)-CI-171004-FD Fillet 78.8 10.2 75.991FWB-001(BG)-CI-171004-FD Carcass 66.9 5.78 133.762

FF-001(BG)-CI-171004 Fillet 79.2 10.53 75.991FWB-001(BG)-CI-171004 Carcass 66.9 6.07 133.762

FWB001(BG)-CI-180615 76.2 219.22 1.26

YOY-001-UCI 83.3 5.164 4.14YOY-002-UCI 82.9 11.279 3.72

FWB001(BG)-CI-180615 76.2YOY-001-UCI 83.3YOY-002-UCI 82.9

FWB001(BG)-CI-180615 76.2 52.2 5.28YOY-001-UCI 83.3 0.864 24.8YOY-002-UCI 82.9 1.93 21.8

YOY-001-UCIDUP 76.2 1.13 24.5FWB001(BG)-CI-180615 76.2

YOY-001-UCI 83.3YOY-002-UCI 82.9

Notes: *The Phase II YOY bluegill samples were analyzed as whole-body only.

7.69

Dry

Wet

1.74

2.00

2.08

6.47

7.38

209.753

209.753

209.753

209.753

209.753

Percent Solids = 100 - Percent (%) Moisture

Wet

Ramboll/KU

Dry

Ramboll/KU

KESB

209.753KESB

KESB

(DW) Dry Weight = Concentration in Wet Weight/(1-% solids)

BG = Bluegill

ESB = Kentucky Environmental Services Branch

FD = Field Duplicate

FF = Fish Fillet

Cf = Chemical concentration in fish fillet composite sample (mg/kg)

The sample ID includes the sample date, for example "180615" refers to June 15th, 2018 (Phase

mg/kg (DW) = Milligrams per kilogram dry weight

mg/kg (WW) = Milligrams per kilogram wet weight

Pending = Pending the delivery of laboratory results

YOY = Young-of-the-Year

UCI = Upper Curds Inlet

WBFC = Whole body fish chemical concentration (mg/kg)

WBFC Equation 1: WBFC = ([WF/ (WF + WR)] * CF) + ([WR/ (WF + WR)] * CR)

Wf = Weight of fish fillet (g)

Wr = Weight of fish remains or carcass (g)

WWB = Weight of Whole-Body (Wf+Wr)

CI = Curds Inlet

Cr = Chemical concentration in remains composite sample (mg/kg)

DUP = Duplicate sample

FWB = Fish Whole-Body

Whole-Body

Pending Pending

Pending Pending

Phase IIAnalysed as Whole-Body

Phase IIAnalysed as Whole-Body

Phas

e II

Phas

e I KESB

Ramboll/KU

Ramboll/KU

Page 1 of 1

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA

Appendix E3: Table E2- Comparison of Kentucky Environmental Services Branch and Phase I and II Adult and Young-of-the-Year (YOY) Bluegill Tissue Sample Results

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

Table E2: Comparison of Kentucky Environmental Services Branch and Phase I and II Adult and Young-of-the-Year (YOY) Bluegill Tissue Sample Results Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

E.W. Brown Station, Herrington Lake, Mercer County, Kentucky

Species Project Phase Sample Identifier Portion CASNumber Constituent Basis KY ESB

Result (mg/kg)CAP Sample

Result (mg/kg)Percent

Difference

Wet 0.103 0.08 22Dry -- 0.39 --Wet <0.0186 0.0084 NADry -- 0.04 --Wet 2.19 1.85 16Dry -- 8.91 --Wet 9.76 7.45 24Dry -- 35.8 --Wet 0.302 0.24 21Dry -- 0.71 --Wet 0.125 0.105 16Dry -- 0.316 --Wet 2.01 1.68 16Dry -- 5.08 --Wet 40.2 27.9 31Dry -- 84.4 --

Wet 1.26Dry 5.28Wet 4.14

Dry 24.8Wet 3.72

Dry 21.8Notes:

BG mg/kgCAP Ramboll's Corrective Action Plan PendingCI UCIdry wetFF YOY

FWB --KY ESB

The Phase II YOY bluegill samples were analyzed as whole-body only.The sample ID includes the sample date, for example "180615" refers to June 15th, 2018 (Phase II).

Bluegill

Curds Inletdry weight resultsFish FilletFish whole Body Results from KY ESB were wet weight only

Pending

Kentucky Environmental Services Branch

Pending the delivery of laboratory resultsUpper Curds Inletwet weight resultsYoung-of-the-Year

Milligrams per kilogram

7782-49-2

7782-49-2

7782-49-2

Selenium Pending

7440-66-6

YOY-002-UCI

Arsenic (total)

Cadmium

Selenium

Zinc

Arsenic (total)

Cadmium

Selenium

Zinc

FWB001(BG)-CI-180615

YOY-001-UCI Whole-Body

Phas

e II

Blu

egill

(Le

pom

is s

p.)

7440-38-2

7440-43-9

7782-49-2

7440-66-6

7440-38-2Phas

e I

FF-001(BG)-CI-171004

FWB-001(BG)-CI-171004

Fillet

Carcass7440-43-9

7782-49-2

Page 1 of 1

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

APPENDIX E: KENTUCKY DIVISON OF WATER (KDOW) ENVIRONMENTAL SERVICES BRANCH (ESB) 2016–2018 FISH TISSUE ANALYTICAL DATA

Appendix E4: 2018 KDOW ESB Fish Tissue Analytical Reports

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04359

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 0:05Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030014 Curds Inlet L macrochirus

Program Code: A20

Sample ID: FT18-129AShipment Temp: 0C

Station/Project ID: 6021

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0465$3130T_SECAL 4.70 0.0186

% Moisture % 0.01009540 75.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04359 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04360

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 0:05Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030014 Curds Inlet L macrochirus

Program Code: A20

Sample ID: FT18-129BShipment Temp: 0C

Station/Project ID: 6021

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0470$3130T_SECAL 3.77 0.0188

% Moisture % 0.01009540 75.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04360 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04361

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 0:05Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030014 Curds Inlet L macrochirus

Program Code: A20

Sample ID: FT18-130AShipment Temp: 0C

Station/Project ID: 6021

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0442$3130T_SECAL 7.14 0.0177

% Moisture % 0.01009540 75.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04361 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04362

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 0:05Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030014 Curds Inlet L macrochirus

Program Code: A20

Sample ID: FT18-130BShipment Temp: 0C

Station/Project ID: 6021

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0455$3130T_SECAL 7.16 0.0182

% Moisture % 0.01009540 75.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04362 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04363

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Garrard

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 2:45Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030017 Rocky Fk (Run) L macrochirus

Program Code: A20

Sample ID: FT18-138AShipment Temp: 0C

Station/Project ID: 6024

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0452$3130T_SECAL 3.01 0.0181

% Moisture % 0.01009540 74.5

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04363 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Friday, January 11, 2019

Lab Sample Number: AP04364

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Garrard

Date: 07/19/2018Date: 12/03/2018

Date: 12/03/2018

Time: 2:45Time:12/03/18 15:20Time:12/03/18 15:20

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030017 Rocky Fk (Run) L macrochirus

Program Code: A20

Sample ID: FT18-138BShipment Temp: 0C

Station/Project ID: 6024

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0480$3130T_SECAL 3.04 0.0192

% Moisture % 0.01009540 74.5

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AP04364 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00001

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 01/03/2019

Date: 01/03/2019

Time: 1:30Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr Dam L macrochi

Program Code: A20

Sample ID: FT18-113AShipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0322$3130T_SECAL 2.77 0.0129

% Moisture % 0.01009540 75.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00001 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00002

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 01/03/2019

Date: 01/03/2019

Time: 1:30Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr Dam L macrochi

Program Code: A20

Sample ID: FT18-113BShipment Temp: 0C

Station/Project ID:

Sample Type: Field Split

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0380$3130T_SECAL 3.99 0.0152

% Moisture % 0.01009540 75.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00002 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00003

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 19:55Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herrington HQ Inlet L macroc

Program Code: A20

Sample ID: FT18-119AShipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0460$3130T_SECAL 2.20 0.0184

% Moisture % 0.01009540 73.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00003 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00004

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 19:55Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herrington HQ Inlet L macroc

Program Code: A20

Sample ID: FT18-119BShipment Temp: 0C

Station/Project ID:

Sample Type: Field Split

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0422$3130T_SECAL 2.63 0.0169

% Moisture % 0.01009540 73.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00004 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00005

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 21:00Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030019 Lower Herrington Lk L macroc

Program Code: A20

Sample ID: FT18-122AShipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0465$3130T_SECAL 2.55 0.0186

% Moisture % 0.01009540 75.1

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00005 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00006

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 21:00Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030019 Lower Herrington Lk L macroc

Program Code: A20

Sample ID: FT18-122BShipment Temp: 0C

Station/Project ID:

Sample Type: Field Split

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0422$3130T_SECAL 2.55 0.0169

% Moisture % 0.01009540 75.1

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00006 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00007

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 21:00Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030019 Lower Herrington Lk L macroc

Program Code: A20

Sample ID: FT18-123AShipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0375$3130T_SECAL 2.48 0.0150

% Moisture % 0.01009540 75.0

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00007 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Monday, January 14, 2019

Lab Sample Number: AQ00008

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/03/2019

Date: 01/03/2019

Time: 21:00Time:01/03/19 14:39Time:01/03/19 14:39

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030019 Lower Herrington Lk L macroc

Program Code: A20

Sample ID: FT18-123BShipment Temp: 0C

Station/Project ID:

Sample Type: Field Split

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0430$3130T_SECAL 2.00 0.0172

% Moisture % 0.01009540 75.0

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Environmental Services Branch (ESB) and

has been approved for release.

Michael Goss, Branch Manager

Original report is on file at ESB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00008 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, February 19, 2019

Lab Sample Number: AQ00266

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 01/22/2019

Date: 01/22/2019

Time: 1:30Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr dam Lepomis ma

Program Code: A20

Sample ID: FT18-114AShipment Temp: 0C

Station/Project ID: 860

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0488$3130T_SECAL 2.02 0.0195

% Moisture % 0.01009540 74.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Methyl Mercury Analysis (3350T) has been cancelled.

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00266 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, February 19, 2019

Lab Sample Number: AQ00267

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/19/2018Date: 01/22/2019

Date: 01/22/2019

Time: 1:30Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr dam Lepomis ma

Program Code: A20

Sample ID: FT18-114BShipment Temp: 0C

Station/Project ID: 860

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0472$3130T_SECAL 2.02 0.0189

% Moisture % 0.01009540 74.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Methyl Mercury Analysis (3350T) has been cancelled.

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00267 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, February 19, 2019

Lab Sample Number: AQ00268

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/22/2019

Date: 01/22/2019

Time: 19:55Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herringon HQ Inlet Lepomis m

Program Code: A20

Sample ID: FT18-118AShipment Temp: 0C

Station/Project ID: 6022

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0495$3130T_SECAL 4.15 0.0198

% Moisture % 0.01009540 74.0

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Methyl Mercury Analysis (3350T) has been cancelled.

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00268 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, February 19, 2019

Lab Sample Number: AQ00269

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Mercer

Date: 07/18/2018Date: 01/22/2019

Date: 01/22/2019

Time: 19:55Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herringon HQ Inlet Lepomis m

Program Code: A20

Sample ID: FT18-118BShipment Temp: 0C

Station/Project ID: 6022

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0465$3130T_SECAL 4.12 0.0186

% Moisture % 0.01009540 74.0

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Methyl Mercury Analysis (3350T) has been cancelled.

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00269 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, February 19, 2019

Lab Sample Number: AQ00270

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Garrard

Date: 07/19/2018Date: 01/22/2019

Date: 01/22/2019

Time: 2:45Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky Fk Lepomis

Program Code: A20

Sample ID: FT18-139AShipment Temp: 0C

Station/Project ID: 6024

Sample Type: Field Sample

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0482$3130T_SECAL 2.78 0.0193

% Moisture % 0.01009540 73.9

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Methyl Mercury Analysis (3350T) has been cancelled.

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00270 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Thursday, February 28, 2019

Lab Sample Number: AQ00271

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

David Cravens

David Cravens

Jennifer Clark

Garrard

Date: 07/19/2018Date: 01/22/2019

Date: 01/22/2019

Time: 2:45Time:01/22/19 13:22Time:01/22/19 13:22

Sample Matrix: FISH-WHOLE Collection Method: Composite

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky Fk Lepomis

Program Code: A20

Sample ID: FT18-139BShipment Temp: 0C

Station/Project ID: 6024

Sample Type: Field Split

131

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0460$3130T_SECAL 2.85 0.0184

% Moisture % 0.01009540 73.9

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@PG Container -no pres. pH not tested

Page 1 of 1Sample Number: AQ00271 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00936

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M salmoides

Program Code: A20

Sample ID: FT18-131Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0460$3130T_SECAL 4.16 0.0184

% Moisture % 0.01009540 69.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00936 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00937

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M salmoides

Program Code: A20

Sample ID: FT18-132Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0460$3130T_SECAL 5.97 0.0184

% Moisture % 0.01009540 69.8

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00937 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00938

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M salmoides

Program Code: A20

Sample ID: FT18-133Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0490$3130T_SECAL 3.50 0.0196

% Moisture % 0.01009540 70.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00938 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00939

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M salmoides

Program Code: A20

Sample ID: FT18-134Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0462$3130T_SECAL 4.03 0.0185

% Moisture % 0.01009540 73.6

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00939 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00940

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M salmoides

Program Code: A20

Sample ID: FT18-135Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0482$3130T_SECAL 5.26 0.0193

% Moisture % 0.01009540 71.6

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00940 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, March 26, 2019

Lab Sample Number: AQ00941

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/15/2019

Date: 03/15/2019

Time: 0:45Time:03/15/19 14:45Time:03/15/19 14:45

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M chrysops

Program Code: A20

Sample ID: FT18-136Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0480$3130T_SECAL 5.65 0.0192

% Moisture % 0.01009540 66.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ00941 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01167

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 1:30Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr dam M salmoide

Program Code: A20

Sample ID: FT18-115Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0475$3130T_SECAL 2.62 0.0190

% Moisture % 0.01009540 69.0

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01167 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01168

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 1:30Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr dam M salmoide

Program Code: A20

Sample ID: FT18-116Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0495$3130T_SECAL 2.94 0.0198

% Moisture % 0.01009540 69.5

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01168 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01169

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/25/2019

Date: 03/25/2019

Time: 19:55Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herrington@ HQ In M salmoide

Program Code: A20

Sample ID: FT18-120Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0480$3130T_SECAL 4.58 0.0192

% Moisture % 0.01009540 70.1

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01169 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01170

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/25/2019

Date: 03/25/2019

Time: 19:55Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030015 Herrington @ HQ In I punctat

Program Code: A20

Sample ID: FT18-121Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0468$3130T_SECAL 2.75 0.0187

% Moisture % 0.01009540 73.8

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-4OZF Glass 4 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01170 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01171

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/25/2019

Date: 03/25/2019

Time: 21:00Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030019 Herrington RM 6.1 M salmoide

Program Code: A20

Sample ID: FT18-127Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0485$3130T_SECAL 2.89 0.0194

% Moisture % 0.01009540 70.1

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01171 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01172

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Garrard

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 2:45Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky M salmoide

Program Code: A20

Sample ID: FT18-140Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0490$3130T_SECAL 3.81 0.0196

% Moisture % 0.01009540 70.7

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01172 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01173

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Garrard

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 2:45Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky M salmoide

Program Code: A20

Sample ID: FT18-141Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0462$3130T_SECAL 2.30 0.0185

% Moisture % 0.01009540 68.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01173 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01174

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Garrard

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 2:45Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky M salmoide

Program Code: A20

Sample ID: FT18-142Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0485$3130T_SECAL 2.69 0.0194

% Moisture % 0.01009540 69.3

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01174 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01175

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 1:30Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030007 Herrington nr dam M salmoide

Program Code: A20

Sample ID: FT18-117Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0485$3130T_SECAL 2.12 0.0194

% Moisture % 0.01009540 70.1

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01175 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01176

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Garrard

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 2:45Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky M salmoide

Program Code: A20

Sample ID: FT18-143Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0470$3130T_SECAL 3.48 0.0188

% Moisture % 0.01009540 70.7

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01176 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Tuesday, April 02, 2019

Lab Sample Number: AQ01177

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Garrard

Date: 07/19/2018Date: 03/25/2019

Date: 03/25/2019

Time: 2:45Time:03/25/19 12:55Time:03/25/19 12:55

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030017 Herrington Rocky M salmoide

Program Code: A20

Sample ID: FT18-144Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0485$3130T_SECAL 5.85 0.0194

% Moisture % 0.01009540 68.4

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01177 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Wednesday, April 10, 2019

Lab Sample Number: AQ01343

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/19/2018Date: 03/29/2019

Date: 03/29/2019

Time: 0:05Time:03/29/19 10:20Time:03/29/19 10:20

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030014 Herrington M chrysops x saxa

Program Code: A20

Sample ID: FT18-137Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0472$3130T_SECAL 2.90 0.0189

% Moisture % 0.01009540 66.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01343 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Wednesday, April 10, 2019

Lab Sample Number: AQ01344

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/29/2019

Date: 03/29/2019

Time: 21:00Time:03/29/19 10:20Time:03/29/19 10:20

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030019 Herrington M salmoides

Program Code: A20

Sample ID: FT18-124Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0475$3130T_SECAL 1.95 0.0190

% Moisture % 0.01009540 70.7

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01344 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Wednesday, April 10, 2019

Lab Sample Number: AQ01345

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/29/2019

Date: 03/29/2019

Time: 21:00Time:03/29/19 10:20Time:03/29/19 10:20

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030019 Herrington M salmoides

Program Code: A20

Sample ID: FT18-125Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0490$3130T_SECAL 3.06 0.0196

% Moisture % 0.01009540 70.5

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01345 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Wednesday, April 10, 2019

Lab Sample Number: AQ01346

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/29/2019

Date: 03/29/2019

Time: 21:00Time:03/29/19 10:20Time:03/29/19 10:20

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030019 Herrington M salmoides

Program Code: A20

Sample ID: FT18-126Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0488$3130T_SECAL 2.33 0.0195

% Moisture % 0.01009540 69.8

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01346 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report

To: Division of Water

300 Sower Blvd

Frankfort, KY 40601

Wednesday, April 10, 2019

Lab Sample Number: AQ01347

Re: Fish Tissue Monitoring

ATTN: Melanie Arnold AKGWA:

Facility:County:

Collected By:

Delivered By:

Received By:

Rodney Pierce

Rodney Pierce

Jennifer Clark

Mercer

Date: 07/18/2018Date: 03/29/2019

Date: 03/29/2019

Time: 21:00Time:03/29/19 10:20Time:03/29/19 10:20

Sample Matrix: FISH-WHOLE Collection Method: Grab

REPORT OF ANALYSIS

Sample Description: DOW04030019 Herrington M salmoides

Program Code: A20

Sample ID: FT18-128Shipment Temp: 0C

Station/Project ID:

Sample Type: Field Sample

Container ID:

ENERGY AND ENVIRONMENT CABINET

100 SOWER BOULEVARD, STE. 104

FRANKFORT, KENTUCKY 40601

MATTHEW G. BEVINGOVERNOR

CHARLES G. SNAVELYSECRETARY

ANTHONY R. HATTONCOMMISSIONER

DEPARTMENT FOR ENVIRONMENTAL PROTECTION

CAS NUM CONSTITUENTS UNIT FLAGLOQLAB ACODE RESULT LOD

Selenium mg/Kg DW7782-49-2 0.0480$3130T_SECAL 3.19 0.0192

% Moisture % 0.01009540 70.2

Report Format: DESFinal

This report has been prepared and reviewed by personnel within the Department for Environmental Protection

Laboratory (DEPLAB) and has been approved for release.

Michael Goss, Laboratory Technical Director

Original report is on file at DEPLAB

Case Narrative

Unit Description

DW = Analyzed on a Dry Weight Basis

Container Preservation Status at Sample Login@G-8OZF Glass 8 oz widemouth jar -frozen pH not tested

Page 1 of 1Sample Number: AQ01347 1Report Version

KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D

Corrective Action Site Investigation, Source Assessment, and Risk Assessment Report