appendix 3 xrd data analysis results - university of vermont

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Appendix 3 XRD Data

Analysis Results General Information

Analysis date 11/29/2018 4:38:56 PM Sample name 18CD08A Measurement date 11/29/2018 3:37:54 PM File name Sample 18CD08A.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

1.5e+004

2.0e+004

10 20 30 40 50 -3000

-2000

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Inte

nsity (

cp

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2-theta (deg)

Error

Residual

Meas. data:Sample 18CD08A/Data 1

BG data:Sample 18CD08A/Data 1

Calc. data:Sample 18CD08A/Data 1

Inte

nsity (

cp

s)

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Measurement conditions

XG Cu/30 kV/15 mA Duration time / Scan speed 1 deg/min

Goniometer Step / Sampling step 0.02 deg

Attachment - Measurement axis 2theta/theta

K-beta filter - Scan range 5-55 deg

Incident monochromator - Incident slit -

Receiving monochromator - Vertical divergence slit -

Counter - Receiving slit #1 -

Receiving slit #2 -

Qualitative analysis results

Phase name Formula Figure of merit Phase reg. detail

Quartz, syn Si O2 0.3964336081839039 10850930 (ICDD)

Albite, ordered Na Al Si3 O8 0.743351470458949 90466 (ICDD)

Muscovite-2M1, ferrian K0.96 Na0.04 Al1.71 Fe0.29 ( Al0.91 Si3.09 O10 ) ( O H )1.78 F0.22

0.7560937199920927 10739861 (ICDD)

Phase name Formula Space group Phase reg. detail

Quartz, syn Si O2 154 : P3221 10850930 (ICDD)

Albite, ordered Na Al Si3 O8 2 : C-1 90466 (ICDD)

Muscovite-2M1, ferrian K0.96 Na0.04 Al1.71 Fe0.29 ( Al0.91 Si3.09 O10 ) ( O H )1.78 F0.22

15 : C12/c1,unique-b,cell-1 10739861 (ICDD)

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Inte

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2-theta (deg)


Quartz, syn

Albite, ordered

Muscovite-2M1, ferrian

Inte

nsity (

cps)

Quartz, synAlbite, ordered


- 4 -

Peak list

2-theta (deg) d (A) Height (cps) Int. I(cps¥deg) FWHM(deg) Size Phase name

8.874(3) 9.957(3) 2600(47) 504(5) 0.139(4) 598(15) Muscovite-2M1, ferrian, (0,0,2) 13.847(8) 6.390(4) 384(18) 76.4(19) 0.139(9) 599(37) Albite, ordered, (0,0,1)

17.820(5) 4.9734(15) 478(20) 95.3(14) 0.160(4) 526(13) Muscovite-2M1, ferrian, (0,0,4) 19.63(9) 4.518(19) 20(4) 12.4(14) 0.55(9) 153(26) Muscovite-2M1, ferrian, (1,1,0) 20.860(3) 4.2550(6) 2038(41) 373(4) 0.156(2) 542(8) Quartz, syn, (1,0,0)

22.042(8) 4.0293(14) 310(16) 61.2(15) 0.164(6) 515(18) Albite, ordered, (2,0,-1)

23.005(15) 3.863(3) 101(9) 21.0(15) 0.12(3) 681(155) Albite, ordered, (1,-1,1)

23.511(11) 3.7808(17) 471(20) 86(2) 0.120(10) 708(61) Albite, ordered, (1,1,1)

24.289(9) 3.6614(14) 281(15) 74(2) 0.226(8) 376(14) Albite, ordered, (1,3,0)

25.38(14) 3.506(19) 145(11) 57(13) 0.23(17) 377(279) Albite, ordered, (1,1,-2), 01-073-9861@Muscovite-2M1, ferrian, (1,1,-4)

26.620(7) 3.3459(9) 12724(103) 2509(51) 0.132(12) 647(57) Quartz, syn, (0,1,1), 01-073-9861@Muscovite-2M1, ferrian, (0,2,4)

27.877(6) 3.1978(7) 3284(52) 765(14) 0.132(14) 650(68) Albite, ordered, (0,0,2), 01-073-9861@Muscovite-2M1, ferrian, (1,1,4)

30.15(4) 2.961(3) 133(11) 61(9) 0.38(4) 227(26) Albite, ordered, (1,-3,1), 01-073-9861@Muscovite-2M1, ferrian, (0,2,5)

30.49(3) 2.929(2) 119(10) 26(7) 0.17(6) 503(175) Albite, ordered, (0,2,-2)

30.81(8) 2.900(7) 26(5) 4.9(19) 0.13(11) 670(552) Unknown,

31.200(17) 2.8644(16) 130(10) 26.3(13) 0.163(14) 527(45) Albite, ordered, (1,3,1), 01-073-9861@Muscovite-2M1, ferrian, (1,1,5)

31.96(5) 2.798(4) 37(6) 11.5(19) 0.23(8) 380(130) Albite, ordered, (0,2,2), 01-073-9861@Muscovite-2M1, ferrian, (1,1,-6)

33.277(12) 2.6902(9) 98(9) 9.6(11) 0.080(14) 1084(183) Unknown,

34.487(14) 2.5985(10) 37(6) 6.9(12) 0.17(4) 515(123) Muscovite-2M1, ferrian, (1,3,0) 34.99(2) 2.5626(17) 100(9) 32(3) 0.29(3) 299(27) Albite, ordered, (2,4,-1), 01-073-9861@Muscovite-2M1, ferrian, (2,0,-2)

36.058(9) 2.4888(6) 189(13) 35.5(14) 0.143(11) 610(49) Albite, ordered, (2,-2,1), 01-073-9861@Muscovite-2M1, ferrian, (0,0,8)

36.508(5) 2.4591(3) 860(27) 148(2) 0.129(5) 675(28) Quartz, syn, (1,1,0), 00-009-0466@Albite, ordered, (2,2,1), 01-073-9861@Muscovite-2M1, ferrian, (2,0,2)

37.37(4) 2.404(2) 61(7) 23.1(18) 0.34(3) 257(24) Albite, ordered, (2,4,0), 01-073-9861@Muscovite-2M1, ferrian, (0,2,7)

39.420(6) 2.2839(3) 544(21) 91.9(18) 0.147(5) 601(22) Quartz, syn, (1,0,2), 00-009-0466@Albite, ordered, (1,-1,-3)

40.243(5) 2.2391(3) 337(17) 51.8(10) 0.128(5) 688(27) Quartz, syn, (1,1,1), 01-073-9861@Muscovite-2M1, ferrian, (0,4,1)


42.446(6) 2.1279(3) 766(25) 147(3) 0.137(8) 651(37) Quartz, syn, (2,0,0), 00-009-0466@Albite, ordered, (0,6,0), 01-073-9861@Muscovite-2M1, ferrian, (1,3,5)

45.507(4) 1.99160(15) 976(29) 198(3) 0.160(4) 561(16) Muscovite-2M1, ferrian, (0,0,10) 45.768(7) 1.9808(3) 316(16) 59(3) 0.148(10) 609(41) Quartz, syn, (0,2,1), 00-009-0466@Albite, ordered, (0,6,1)


49.17(3) 1.8515(10) 58(7) 9.1(18) 0.11(4) 815(303) Albite, ordered, (4,0,-3), 01-073-9861@Muscovite-2M1, ferrian, (1,3,-8)

50.105(6) 1.8191(2) 1389(34) 265(5) 0.134(7) 683(37) Quartz, syn, (1,1,2)

51.11(3) 1.7858(9) 124(10) 17(3) 0.12(3) 790(170) Albite, ordered, (2,0,-4)

53.27(2) 1.7182(7) 42(6) 10.2(11) 0.22(3) 421(55) Muscovite-2M1, ferrian, (2,0,8)

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54.872(6) 1.67176(18) 551(21) 117(4) 0.150(8) 623(33) Quartz, syn, (0,2,2), 01-073-9861@Muscovite-2M1, ferrian, (1,5,2)

Lattice constants

Angular correction

No correction

Use External standard parameters

Use internal standard data

Analysis results

File name a (A) b (A) c (A) alpha (deg) beta (deg) gamma (deg)

Sample 18CD08A 4.917324 4.917324 5.412406 90.000000 90.000000 120.000000

Sample 18CD08A 8.146709 12.791253 7.162381 94.260002 116.599998 87.669998

Sample 18CD08A 5.212120 9.040412 20.078019 90.000000 95.680000 90.000000

Phase name a (A) b (A) c (A) alpha (deg) beta (deg) gamma (deg)

Quartz, syn 4.917324 4.917324 5.412406 90.000000 90.000000 120.000000

Albite, ordered 8.146709 12.791253 7.162381 94.260002 116.599998 87.669998

Muscovite-2M1, ferrian 5.212120 9.040412 20.078019 90.000000 95.680000 90.000000

Sample 18CD08A Sample 18CD08A 0

0.5

1

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3.5

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5.5

6

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Latt

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(a

ng

.)

Data set

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Quantitative analysis results (RIR)

Phase name Content(%)

Quartz, syn 28.1(6)

Albite, ordered 8.3(3)

Muscovite-2M1, ferrian 63.7(14)

Sample 18CD08A

0 20 40 60 80

Quartz, syn

Albite, ordered


Unknown

Wt(%)

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Analysis date 11/30/2018 10:43:51 AM Sample name 18CD08B Measurement date 11/29/2018 4:53:43 PM File name Sample 18CD08B.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

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10 20 30 40 50

-500

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Inte

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cps)

2-theta (deg)

Error

Residual

Meas. data:Sample 18CD08B/Data 1

BG data:Sample 18CD08B/Data 1

Calc. data:Sample 18CD08B/Data 1

Inte

nsity (

cps)

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Receiving slit #2 -



Biotite-1M K.78 Na.22 Mg1.63 Fe.85 Ti.33 Al1.35 Si2.84 O11 ( O H )

1.581493551503799 10760884 (ICDD)

Albite, calcian, ordered ( Na , Ca ) Al ( Si , Al )3 O8 1.275845969642784 411480 (ICDD)

amphibole, sodium magnesium titanium(III) catena-silicate fluoride Na0.85 ( Na1.02 Mg0.98 ) Mg3 ( Mg1.83 Ti0.17 ) Si8 O22 F2

1.906567364574769 10896410 (ICDD)

Clinochlore-1M, chromian Mg5.1 Al1.2 Si3 Cr.7 O10 ( O H )8 2.992215961700575 10721385 (ICDD)

Magnesiohornblende ( Na0.36 K0.15 ) ( Ca0.75 Na0.25 )2 ( Mg2.64 Fe1.3 Al0.91 Ti0.15 ) ( Si0.81 Al0.19 )8 O22.1 ( O H )1.9

1.646427541407685 10720459 (ICDD)

chlorite Mg2.5 Fe1.65 Al1.5 Si2.2 Al1.8 O10 ( O H )8

1.691073799200048 10721234 (ICDD)


Biotite-1M K.78 Na.22 Mg1.63 Fe.85 Ti.33 Al1.35 Si2.84 O11 ( O H )

12 : C12/m1,unique-b,cell-1 10760884 (ICDD)

Albite, calcian, ordered ( Na , Ca ) Al ( Si , Al )3 O8 2 : C-1 411480 (ICDD)

amphibole, sodium magnesium titanium(III) catena-silicate fluoride Na0.85 ( Na1.02 Mg0.98 ) Mg3 ( Mg1.83 Ti0.17 ) Si8 O22 F2


Clinochlore-1M, chromian Mg5.1 Al1.2 Si3 Cr.7 O10 ( O H )8 2 : C-1 10721385 (ICDD)




5 : C121,unique-b,cell-1 10721234 (ICDD)

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10 20 30 40 50

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Inte

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2-theta (deg)

Meas. data:Sample 18CD08B/Data 1

Biotite-1M

Albite, calcian, ordered

amphibole, sodium magnesium titanium(III

) catena-silicate fluoride

Clinochlore-1M, chromian

Magnesiohornblende

chlorite

Inte

nsity (

cps)

Biotite-1MAlbite, calcian, ordered

amphibole, sodium magnesium titanium(III) catena-silicate fluorideClinochlore-1M, chromian

Magnesiohornblendechlorite

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Peak list


6.264(13) 14.10(3) 335(24) 68(6) 0.172(16) 483(44) Clinochlore-1M, chromian, (0,0,1), 01-072-1234@chlorite, (0,0,1)

7.26(4) 12.17(7) 149(16) 104(9) 0.49(8) 171(29) Unknown,

8.734(6) 10.117(6) 1786(55) 699(8) 0.248(8) 335(10) Biotite-1M, (0,0,1)

10.541(4) 8.385(3) 2975(70) 458(7) 0.115(4) 726(28) amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (1,1,0), Magnesiohornblende, (1,1,0)

12.505(7) 7.073(4) 995(41) 204(5) 0.159(6) 526(19) chlorite, (0,0,2)

13.859(8) 6.385(4) 301(22) 49(2) 0.093(14) 903(139) Unknown,

18.794(13) 4.718(3) 279(22) 58(2) 0.171(10) 493(30) amphibole, sodium magnesium titanium(III) 01-072-1234@catena-silicate fluoride, (2,0,0), chlorite, (0,0,3)

20.868(12) 4.253(2) 218(19) 33(2) 0.142(8) 595(35) Clinochlore-1M, chromian, (1,-1,1), 01-072-1234@chlorite, (1,1,1)

21.18(2) 4.192(4) 79(11) 9.9(11) 0.12(2) 721(142) amphibole, sodium magnesium titanium(III) catena-silicate fluoride, (2,2,0)

22.060(12) 4.026(2) 230(20) 35.8(17) 0.140(9) 602(41) Albite, calcian, ordered, (2,0,-1), 01-072-1234@chlorite, (1,1,-2)

22.84(3) 3.890(5) 39(8) 10.0(15) 0.23(3) 361(54) Albite, calcian, ordered, (1,-1,1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (1,3,-1), 01-072-0459@Clinochlore-1M, chromian, (0,2,-2), 01-072-1234@Magnesiohornblende, (1,3,-1), chlorite, (0,2,2)

23.57(2) 3.772(4) 123(14) 21(2) 0.15(2) 555(72) Albite, calcian, ordered, (1,1,1) 24.214(11) 3.6725(17) 200(18) 60(3) 0.177(13) 480(34) Biotite-1M, (1,1,-2), 00-041-1480@Albite, calcian, ordered, (2,0,0), 01-072-1385@Clinochlore-1M, chromian, (1,-1,2)

25.173(9) 3.5348(12) 660(33) 106(6) 0.147(8) 577(31) chlorite, (0,0,4)

25.51(4) 3.489(6) 107(13) 197(17) 1.72(13) 50(4) Biotite-1M, (0,2,2), 00-041-1480@Albite, calcian, ordered, (1,-3,-1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (1,3,1), 01-072-0459@Clinochlore-1M, chromian, (1,-1,-3), 01-072-1234@Magnesiohornblende, (2,4,0), chlorite, (1,1,-3)

26.489(8) 3.3621(10) 1038(42) 391(9) 0.347(7) 246(5) Biotite-1M, (0,0,3), 00-041-1480@Albite, calcian, ordered, (1,-1,-2), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (1,5,0), Magnesiohornblende, (1,3,1)

27.937(6) 3.1911(7) 2327(62) 570(9) 0.225(4) 381(7) Albite, calcian, ordered, (2,0,-2) 28.228(10) 3.1588(10) 1171(44) 192(5) 0.151(7) 566(25) Biotite-1M, (1,1,2), 00-041-1480@Albite, calcian, ordered, (2,2,0), 01-072-1385@Clinochlore-1M, chromian, (1,-1,3), 01-072-1234@chlorite, (1,1,3)

28.630(8) 3.1153(9) 984(40) 185(5) 0.173(6) 495(16) amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (3,1,0), Magnesiohornblende, (3,1,0)

29.83(3) 2.992(3) 123(14) 24(2) 0.18(2) 473(59) Albite, calcian, ordered, (1,-3,1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,2,1), Clinochlore-1M, chromian, (1,-1,-4)

30.34(2) 2.944(2) 181(17) 37(2) 0.190(16) 453(38) Biotite-1M, (1,1,-3), 00-041-1480@Albite, calcian, ordered, (0,4,-1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (1,5,-1), 01-072-1234@Magnesiohornblende, (1,5,-1), chlorite, (1,1,-4)

31.269(7) 2.8582(6) 73(11) 11.8(18) 0.14(4) 596(146) Albite, calcian, ordered, (1,3,1), 01-072-1385@Clinochlore-1M, chromian, (0,0,5)

31.560(19) 2.8325(17) 145(16) 19(2) 0.12(2) 727(138) Clinochlore-1M, chromian, (0,2,-4), 01-072-1234@chlorite, (0,0,5)

31.78(2) 2.8136(19) 130(15) 17(6) 0.12(4) 745(269) Magnesiohornblende, (3,3,0), 01-072-1234@chlorite, (0,2,4)

32.014(10) 2.7934(8) 332(24) 51(6) 0.14(2) 609(103) amphibole, sodium magnesium titanium(III) catena-silicate fluoride, (3,3,0)

32.469(11) 2.7553(9) 70(11) 5.8(17) 0.08(2) 1113(306) Magnesiohornblende, (3,3,-1) 32.73(3) 2.734(2) 131(15) 25(2) 0.18(2) 482(62) amphibole, sodium magnesium titanium(III) catena-silicate fluoride, (1,5,1)

33.001(12) 2.7120(9) 115(14) 13.2(13) 0.108(18) 801(135) Magnesiohornblende, (1,5,1) 33.99(6) 2.636(4) 39(8) 23(3) 0.46(10) 187(42) Biotite-1M, (1,3,-1), 00-041-1480@Albite, calcian, ordered, (1,-3,-2), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (1,1,-2), 01-072-1234@Clinochlore-1M, chromian, (1,-3,0), chlorite, (1,3,-1)

34.581(10) 2.5916(7) 171(17) 26(2) 0.137(12) 637(54) amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,4,1), 01-072-1234@Clinochlore-1M, chromian, (1,-3,1), chlorite, (1,3,1)

35.077(4) 2.5561(3) 1003(41) 118(3) 0.111(4) 786(28) Clinochlore-1M, chromian, (1,1,-5), 01-072-0459@Magnesiohornblende, (2,4,1)

35.292(11) 2.5411(8) 149(16) 15(3) 0.093(18) 933(178) chlorite, (1,3,-2)

35.62(2) 2.5187(14) 142(15) 63(5) 0.42(4) 210(20) Biotite-1M, (1,1,3), 00-041-1480@Albite, calcian, ordered, (2,4,-1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (2,0,-2), 01-

36.56(4) 2.456(2) 68(11) 10(2) 0.15(4) 601(153) Biotite-1M, (1,3,-2), 00-041-1480@Albite, calcian, ordered, (2,2,1), 01-072-1385@Clinochlore-1M, chromian, (1,-3,2), 01-072-1234@chlorite, (1,3,2)

- 11 -

37.42(3) 2.4015(18) 80(12) 16(2) 0.19(3) 462(82) Albite, calcian, ordered, (3,-1,0), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,6,-1), 01-072-0459@Clinochlore-1M, chromian, (1,3,-3), 01-072-1234@Magnesiohornblende, (3,1,1), chlorite, (0,2,5)

41.25(3) 2.1869(18) 39(8) 7.8(16) 0.10(8) 884(745) Biotite-1M, (1,3,-3), 01-072-0459@Magnesiohornblende, (1,7,1), 01-072-1234@chlorite, (1,3,-4)

42.41(2) 2.1295(11) 124(14) 19(3) 0.14(2) 627(104) amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride, (3,3,-2), 01-072-1234@Magnesiohornblende, (4,4,-1), chlorite, (2,2,2)

43.10(8) 2.097(4) 39(8) 25(3) 0.59(11) 151(28) Biotite-1M, (0,4,2), 00-041-1480@Albite, calcian, ordered, (1,5,1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,0,2), 01-072-0459@Clinochlore-1M, chromian, (0,2,-6), 01-072-1234@Magnesiohornblende, (4,4,0), chlorite, (0,2,6)

44.911(7) 2.0166(3) 1213(45) 246(5) 0.127(9) 705(52) Biotite-1M, (0,0,5), 00-041-1480@Albite, calcian, ordered, (4,0,-2), 01-072-1385@Clinochlore-1M, chromian, (1,-3,-5), 01-072-0459@Magnesiohornblende, (3,5,1), 01-072-1234@chlorite, (2,0,4)

45.832(19) 1.9782(8) 42(8) 22(3) 0.32(8) 278(72) Biotite-1M, (2,2,2), 00-041-1480@Albite, calcian, ordered, (3,-1,1), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (4,0,-2), 01-072-0459@Clinochlore-1M, chromian, (2,-2,3), Magnesiohornblende, (4,2,-2)

48.14(3) 1.8888(11) 80(12) 19.6(18) 0.23(2) 396(42) amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,4,2), 01-072-0459@Clinochlore-1M, chromian, (1,-3,5), 01-072-1234@Magnesiohornblende, (5,1,0), chlorite, (1,3,5)

49.75(2) 1.8311(8) 45(9) 39(4) 0.82(10) 111(13) Biotite-1M, (0,2,5), 00-041-1480@Albite, calcian, ordered, (4,0,-3), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (1,7,-2), 01-072-0459@Clinochlore-1M, chromian, (2,-2,4), 01-072-1234@Magnesiohornblende, (2,8,1), chlorite, (2,2,4)

50.72(3) 1.7984(10) 58(10) 13(3) 0.21(4) 432(85) Albite, calcian, ordered, (1,1,3), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (0,10,0), 01-072-1234@Clinochlore-1M, chromian, (0,4,5), chlorite, (0,4,5)

53.03(3) 1.7254(8) 62(10) 16.2(16) 0.20(3) 464(75) Albite, calcian, ordered, (4,4,-2), 01-089-6410@amphibole, sodium magnesium titanium(III) 01-072-1385@catena-silicate fluoride, (2,2,-3), 01-072-0459@Clinochlore-1M, chromian, (1,-3,6), 01-072-1234@Magnesiohornblende, (5,5,-1), chlorite, (2,4,-2)

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD08B 5.355985 9.274263 10.220678 90.000000 100.160004 90.000000

Sample 18CD08B 8.157731 12.852849 7.109151 93.680000 116.419998 89.389999

Sample 18CD08B 9.745749 18.031295 5.313852 90.000000 102.980003 90.000000

Sample 18CD08B 5.333412 9.239052 14.422593 90.000000 97.080002 90.000000

Sample 18CD08B 9.867903 18.084475 5.337275 90.000000 105.480003 90.000000

Sample 18CD08B 5.348791 9.263270 14.193719 90.000000 96.279999 90.000000


Biotite-1M 5.355985 9.274263 10.220678 90.000000 100.160004 90.000000

Albite, calcian, ordered 8.157731 12.852849 7.109151 93.680000 116.419998 89.389999

amphibole, sodium magnesium titanium(III) catena-silicate fluoride

9.745749 18.031295 5.313852 90.000000 102.980003 90.000000


5.333412 9.239052 14.422593 90.000000 97.080002 90.000000

Magnesiohornblende 9.867903 18.084475 5.337275 90.000000 105.480003 90.000000

chlorite 5.348791 9.263270 14.193719 90.000000 96.279999 90.000000

- 12 -



Biotite-1M 19.6(14)

Albite, calcian, ordered 34(3)

amphibole, sodium magnesium titanium(III) catena-silicate fluoride 18(3)

Clinochlore-1M, chromian 19(3)

Magnesiohornblende 1.4(5)

chlorite 8.1(9)

amphibole, sodium magnesium titanium(III) 01-072-0459@catena-silicate fluoride

Magnesiohornblende


chlorite



Magnesiohornblende



Sample 18CD08B Sample 18CD08B 0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

10.5

11

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 13 -

Sample 18CD08B

0 20 40 60 80

Biotite-1M


amphibole, sodium magnesium titanium(III) catena-silicate fluoride


Magnesiohornblende

Wt(%)

- 14 -


Analysis date 11/30/2018 9:28:01 AM Sample name 18CD08C Measurement date 11/30/2018 8:55:07 AM File name Sample 18CD08C.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

10 20 30 40 50

-2000

-1000

0

1000

2000

Inte

nsity (

cps)

2-theta (deg)

Error

Residual

Meas. data:Sample 18CD08C/Data 1

BG data:Sample 18CD08C/Data 1

Calc. data:Sample 18CD08C/Data 1

Inte

nsity (

cps)

- 15 -









Receiving slit #2 -



Albite, ordered Na Al Si3 O8 0.6811893627986149 90466 (ICDD)

Quartz Si O2 0.6011371552960538 10707344 (ICDD)


0.9277422216023894 10721234 (ICDD)

Anorthite, Na-rich Ca0.85 Na0.14 Al1.94 Si2.06 O8 1.034315319575634 10751436 (ICDD)

Muscovite-2M1, syn K0.964 ( Al1.21 Mg0.75 Fe0.04 ) ( Al0.19 Si3.81 ) O10 ( ( O H )1.2 F0.8 )

0.9766105941315172 10703665 (ICDD)


Albite, ordered Na Al Si3 O8 2 : C-1 90466 (ICDD)

Quartz Si O2 154 : P3221 10707344 (ICDD)


5 : C121,unique-b,cell-1 10721234 (ICDD)

Anorthite, Na-rich Ca0.85 Na0.14 Al1.94 Si2.06 O8 2 : P-1 10751436 (ICDD)



- 16 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

10 20 30 40 50 0

1000

2000

3000

4000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Meas. data:Sample 18CD08C/Data 1

Albite, ordered

Quartz

chlorite

Anorthite, Na-rich

Muscovite-2M1, syn

Inte

nsity (

cps)

Albite, orderedQuartzchlorite

Anorthite, Na-richMuscovite-2M1, syn

- 17 -

Peak list


6.21(3) 14.22(6) 85(12) 30(3) 0.19(6) 429(133) chlorite, (0,0,1)

8.900(4) 9.928(4) 2253(61) 450(6) 0.140(5) 594(20) Muscovite-2M1, syn, (0,0,2) 12.507(14) 7.072(8) 143(15) 30.3(19) 0.14(2) 602(92) chlorite, (0,0,2)

13.892(8) 6.369(4) 822(37) 149(3) 0.114(8) 730(52) Albite, ordered, (0,0,1), 01-075-1436@Anorthite, Na-rich, (0,2,0)

17.816(5) 4.9745(14) 469(28) 85.2(19) 0.123(8) 684(43) Muscovite-2M1, syn, (0,0,4) 19.78(5) 4.485(10) 51(9) 17(2) 0.27(4) 316(53) chlorite, (1,1,-1), 01-075-1436@Anorthite, Na-rich, (1,1,-3), 01-070-3665@Muscovite-2M1, syn, (1,1,0)

20.872(5) 4.2524(10) 1047(42) 175(3) 0.142(3) 594(15) Quartz, (1,0,0), 01-072-1234@chlorite, (1,1,1), 01-075-1436@Anorthite, Na-rich, (0,3,0), 01-070-3665@Muscovite-2M1, syn, (1,1,-2)

22.076(6) 4.0233(12) 785(36) 148(3) 0.159(4) 532(15) Albite, ordered, (2,0,-1), 01-072-1234@chlorite, (1,1,-2), 01-075-1436@Anorthite, Na-rich, (2,0,-2)

23.057(16) 3.854(3) 126(15) 33(2) 0.216(17) 392(31) Albite, ordered, (1,-1,1), 01-072-1234@chlorite, (0,2,2), 01-075-1436@Anorthite, Na-rich, (1,2,-3), 01-070-3665@Muscovite-2M1, syn, (1,1,-3)

23.564(8) 3.7723(12) 670(33) 128(4) 0.156(8) 544(28) Albite, ordered, (1,1,1), 01-075-1436@Anorthite, Na-rich, (1,3,-1)

24.244(9) 3.6681(13) 538(30) 139(4) 0.228(7) 372(11) Albite, ordered, (1,3,0), 01-072-1234@chlorite, (1,1,2), 01-075-1436@Anorthite, Na-rich, (1,-2,-3)

25.46(2) 3.496(3) 185(18) 63(4) 0.26(2) 325(29) Albite, ordered, (1,1,-2), 01-072-1234@chlorite, (0,0,4), 01-075-1436@Anorthite, Na-rich, (1,0,-4), 01-070-3665@Muscovite-2M1, syn, (1,1,-4)

26.633(5) 3.3443(7) 5410(95) 937(43) 0.129(8) 660(43) Quartz, (0,1,1), 01-075-1436@Anorthite, Na-rich, (1,-1,-4), 01-070-3665@Muscovite-2M1, syn, (0,2,4)

26.855(12) 3.3171(14) 1542(51) 269(46) 0.13(2) 673(116) Muscovite-2M1, syn, (0,0,6) 27.932(3) 3.1917(3) 9476(126) 1591(25) 0.120(4) 715(21) Albite, ordered, (0,0,2), 01-075-1436@Anorthite, Na-rich, (0,4,0), 01-070-3665@Muscovite-2M1, syn, (1,1,4)

28.304(18) 3.1505(19) 446(27) 239(30) 0.35(4) 244(30) Albite, ordered, (2,-2,0), 01-072-1234@chlorite, (1,1,3), 01-075-1436@Anorthite, Na-rich, (2,-2,-3)

30.115(13) 2.9650(13) 253(21) 80(6) 0.20(2) 434(54) Albite, ordered, (1,-3,1), 01-075-1436@Anorthite, Na-rich, (1,-4,0), 01-070-3665@Muscovite-2M1, syn, (0,2,5)

30.488(12) 2.9296(11) 372(25) 82(8) 0.143(19) 602(79) Albite, ordered, (0,2,-2), 01-072-1234@chlorite, (1,1,-4), 01-075-1436@Anorthite, Na-rich, (0,4,-2)

30.83(4) 2.898(3) 82(12) 22(6) 0.17(5) 503(145) Anorthite, Na-rich, (0,3,3) 31.161(13) 2.8678(11) 192(18) 57(3) 0.241(14) 358(21) Albite, ordered, (1,3,1), 01-070-3665@Muscovite-2M1, syn, (1,1,5)

32.11(4) 2.785(3) 55(10) 19(3) 0.20(5) 427(107) Albite, ordered, (0,2,2), 01-075-1436@Anorthite, Na-rich, (1,3,-4), 01-070-3665@Muscovite-2M1, syn, (1,1,-6)

34.49(3) 2.598(2) 89(12) 11(3) 0.10(4) 899(366) chlorite, (1,3,1), 01-075-1436@Anorthite, Na-rich, (1,-3,3), 01-070-3665@Muscovite-2M1, syn, (2,0,0)

35.00(4) 2.562(3) 136(15) 51(5) 0.28(5) 307(53) Albite, ordered, (2,4,-1), 01-072-1234@chlorite, (2,0,-2), 01-075-1436@Anorthite, Na-rich, (1,-4,-3), 01-070-3665@Muscovite-2M1, syn, (2,0,-2)

36.094(8) 2.4864(5) 141(15) 29(2) 0.14(2) 613(103) Albite, ordered, (2,-2,1), 01-070-3665@Muscovite-2M1, syn, (1,1,-7)

36.578(10) 2.4546(7) 331(23) 85(4) 0.162(14) 539(46) Albite, ordered, (2,2,1), 01-070-7344@Quartz, (1,1,0), 01-072-1234@chlorite, (1,3,2), 01-075-1436@Anorthite, Na-rich, (2,-4,0), 01-070-3665@Muscovite-2M1, syn, (2,0,2)

37.017(11) 2.4265(7) 54(9) 5.7(19) 0.07(4) 1183(639) Albite, ordered, (1,5,-1), 01-072-1234@chlorite, (2,0,-3), 01-075-1436@Anorthite, Na-rich, (1,3,3)

37.423(18) 2.4011(11) 152(16) 47(3) 0.18(2) 495(61) Albite, ordered, (2,4,0), 01-072-1234@chlorite, (0,2,5), 01-075-1436@Anorthite, Na-rich, (1,5,-2), 01-070-3665@Muscovite-2M1, syn, (0,2,7)

38.82(3) 2.3179(19) 71(11) 19.9(16) 0.18(5) 493(142) Albite, ordered, (3,3,-1), 01-072-1234@chlorite, (1,1,5), 01-075-1436@Anorthite, Na-rich, (3,-3,-2), 01-070-3665@Muscovite-2M1, syn, (1,1,7)

39.451(8) 2.2822(5) 296(22) 47.2(16) 0.131(9) 671(45) Albite, ordered, (1,-1,-3), 01-070-7344@Quartz, (1,0,2)

40.303(14) 2.2359(7) 121(14) 28.2(14) 0.16(2) 552(74) Quartz, (1,1,1), 01-072-1234@chlorite, (2,0,-4), 01-070-3665@Muscovite-2M1, syn, (2,2,-2)

41.710(19) 2.1637(10) 85(12) 17(2) 0.12(3) 770(204) Anorthite, Na-rich, (3,1,1) 42.458(8) 2.1273(4) 583(31) 120(3) 0.144(11) 620(47) Albite, ordered, (0,6,0), 01-070-7344@Quartz, (2,0,0), 01-072-1234@chlorite, (2,2,2), 01-075-1436@Anorthite, Na-rich, (0,6,0), 01-070-3665@Muscovite-2M1, syn, (1,3,5)

43.46(2) 2.0805(11) 87(12) 11.2(10) 0.109(18) 822(138) Anorthite, Na-rich, (2,-5,-3), 01-070-3665@Muscovite-2M1, syn, (2,2,3)

45.540(7) 1.9902(3) 734(35) 181(6) 0.175(10) 515(28) chlorite, (1,3,-5)

- 18 -

45.823(8) 1.9786(3) 323(23) 65(5) 0.141(16) 639(73) Albite, ordered, (0,6,1), 01-070-7344@Quartz, (2,0,1), 01-070-3665@Muscovite-2M1, syn, (0,0,10)

48.133(15) 1.8889(5) 149(16) 41(2) 0.191(19) 475(47) Albite, ordered, (2,2,2), 01-072-1234@chlorite, (1,3,5), 01-070-3665@Muscovite-2M1, syn, (2,2,5)

49.17(2) 1.8514(9) 66(10) 13(2) 0.15(5) 594(194) Albite, ordered, (4,0,-3), 01-072-1234@chlorite, (2,2,4)

50.157(5) 1.81729(17) 788(36) 188(4) 0.154(10) 593(37) Quartz, (1,1,2), 01-072-1234@chlorite, (1,3,-6), 01-070-3665@Muscovite-2M1, syn, (0,2,10)

50.554(11) 1.8040(4) 159(16) 30(2) 0.138(16) 666(78) Albite, ordered, (1,1,3), 01-070-7344@Quartz, (0,0,3)

51.109(4) 1.78565(12) 318(23) 47(2) 0.116(9) 791(64) Albite, ordered, (2,0,-4), 01-072-1234@chlorite, (1,1,7)

53.21(2) 1.7201(7) 108(13) 23.8(16) 0.17(3) 554(86) chlorite, (2,4,-2)

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD08C 8.140216 12.781058 7.156673 94.260002 116.599998 87.669998

Sample 18CD08C 4.913512 4.913512 5.413751 90.000000 90.000000 120.000000

Sample 18CD08C 5.348291 9.262404 14.192393 90.000000 96.279999 90.000000

Sample 18CD08C 8.153166 12.827196 14.135606 93.370003 116.040001 90.870003

Sample 18CD08C 5.215211 9.055225 19.926545 90.000000 95.614998 90.000000


Albite, ordered 8.140216 12.781058 7.156673 94.260002 116.599998 87.669998

Quartz 4.913512 4.913512 5.413751 90.000000 90.000000 120.000000

chlorite 5.348291 9.262404 14.192393 90.000000 96.279999 90.000000

Anorthite, Na-rich 8.153166 12.827196 14.135606 93.370003 116.040001 90.870003

Muscovite-2M1, syn 5.215211 9.055225 19.926545 90.000000 95.614998 90.000000

- 19 -

Sample 18CD08C Sample 18CD08C 0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 20 -



Albite, ordered 8.5(3)

Quartz 10.5(3)

chlorite 0.65(10)

Anorthite, Na-rich 61.0(4)

Muscovite-2M1, syn 19.29(11)

Sample 18CD08C

0 20 40 60 80

Albite, ordered

Quartz

chlorite

Anorthite, Na-rich

Muscovite-2M1, syn

Wt(%)

- 21 -


Analysis date 11/30/2018 11:05:54 AM Sample name 18CD08D Measurement date 11/30/2018 10:30:19 AM File name Sample 18CD08D.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

1.5e+004

10 20 30 40 50

-2000

-1000

0

1000

2000

Inte

nsity (

cps)

2-theta (deg)

Error

Residual

Meas. data:Sample 18CD08D/Data 1

BG data:Sample 18CD08D/Data 1

Calc. data:Sample 18CD08D/Data 1

Inte

nsity (

cps)

- 22 -









Receiving slit #2 -



Quartz Si O2 2.640076330279654 10741811 (ICDD)

Anorthite, sodian, disordered ( Ca , Na ) ( Si , Al )4 O8 1.693944450866854 411481 (ICDD)

heptamagnesium phyllo-octasilicate difluoride Mg7 Si8 O22 F2 1.632623543714527 10760638 (ICDD)

Phlogopite 1M K ( Co1.7 Ni1.3 ) ( Al Si3 O10 ) ( O H )2

3.061080432720036 10743141 (ICDD)


1.822279071369984 10703665 (ICDD)


Quartz Si O2 152 : P3121 10741811 (ICDD)

Anorthite, sodian, disordered ( Ca , Na ) ( Si , Al )4 O8 2 : P-1 411481 (ICDD)

heptamagnesium phyllo-octasilicate difluoride Mg7 Si8 O22 F2 58 : Pnmn 10760638 (ICDD)

Phlogopite 1M K ( Co1.7 Ni1.3 ) ( Al Si3 O10 ) ( O H )2




- 23 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

10 20 30 40 50 0

1000

2000

3000

4000

5000

6000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Meas. data:Sample 18CD08D/Data 1

Quartz

Anorthite, sodian, disordered

heptamagnesium phyllo-octasilicate difluori

de

Phlogopite 1M

Muscovite-2M1, syn

Inte

nsity (

cps)

QuartzAnorthite, sodian, disordered

heptamagnesium phyllo-octasilicate difluoridePhlogopite 1M

Muscovite-2M1, syn

- 24 -

Peak list


6.30(3) 14.02(8) 80(12) 23(4) 0.22(5) 384(93) Unknown,

8.914(4) 9.912(4) 5378(95) 1697(18) 0.265(3) 314(4) Phlogopite 1M, (0,0,1), 01-070-3665@Muscovite-2M1, syn, (0,0,2)

10.589(9) 8.348(7) 330(23) 63(3) 0.179(8) 466(21) heptamagnesium phyllo-octasilicate difluoride, (1,1,0)

12.60(2) 7.022(13) 132(15) 29(2) 0.193(19) 433(44) Unknown,

13.930(15) 6.352(7) 159(16) 41(2) 0.16(2) 508(61) Anorthite, sodian, disordered, (0,2,0) 17.901(7) 4.951(2) 818(37) 190(3) 0.184(6) 455(14) Phlogopite 1M, (0,0,2), 01-070-3665@Muscovite-2M1, syn, (0,0,4)

19.74(3) 4.493(8) 54(10) 17.9(19) 0.27(3) 316(41) heptamagnesium phyllo-octasilicate difluoride, (0,4,0), 01-074-3141@Phlogopite 1M, (0,2,0), 01-070-3665@Muscovite-2M1, syn, (1,1,0)

20.951(6) 4.2366(12) 1043(42) 211(4) 0.166(4) 508(14) Quartz, (1,0,0), 01-070-3665@Muscovite-2M1, syn, (1,1,-2)

22.103(15) 4.018(3) 177(17) 29.1(18) 0.151(11) 559(39) Anorthite, sodian, disordered, (2,0,-1) 23.02(3) 3.861(5) 47(9) 10.4(10) 0.21(2) 408(47) Phlogopite 1M, (1,1,1), 01-070-3665@Muscovite-2M1, syn, (1,1,-3)

23.572(18) 3.771(3) 104(13) 19.0(12) 0.171(14) 497(41) Anorthite, sodian, disordered, (1,1,1) 24.30(2) 3.659(3) 100(13) 29.6(16) 0.279(17) 304(19) Anorthite, sodian, disordered, (1,3,0), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,3,1)

26.743(3) 3.3307(4) 8016(116) 1899(32) 0.207(4) 413(7) Quartz, (0,1,1), 01-074-3141@Phlogopite 1M, (0,2,2), 01-070-3665@Muscovite-2M1, syn, (0,2,4)

26.897(7) 3.3120(9) 3844(80) 576(28) 0.128(9) 664(45) Phlogopite 1M, (0,0,3)

27.339(10) 3.2595(11) 223(19) 21(2) 0.076(12) 1122(174) heptamagnesium phyllo-octasilicate difluoride, (2,4,0)

27.980(3) 3.1863(3) 2574(66) 443(6) 0.114(4) 752(28) Anorthite, sodian, disordered, (2,0,-2), 01-070-3665@Muscovite-2M1, syn, (1,1,4)

30.477(17) 2.9307(16) 124(14) 25(2) 0.14(3) 630(119) Anorthite, sodian, disordered, (0,2,-2) 31.23(3) 2.862(3) 96(13) 33(3) 0.19(6) 448(144) heptamagnesium phyllo-octasilicate difluoride, (1,5,1), 01-074-3141@Phlogopite 1M, (1,1,-3), 01-070-3665@Muscovite-2M1, syn, (1,1,5)

35.02(5) 2.560(4) 57(10) 29(4) 0.27(12) 320(139) heptamagnesium phyllo-octasilicate difluoride, (1,0,2), 01-074-3141@Phlogopite 1M, (1,3,-1), 01-070-3665@Muscovite-2M1, syn, (2,0,-2)

35.679(12) 2.5144(8) 251(20) 53(2) 0.167(14) 522(44) Anorthite, sodian, disordered, (2,-4,-1), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,6,1)

36.093(12) 2.4865(8) 344(24) 68(2) 0.165(10) 529(33) heptamagnesium phyllo-octasilicate difluoride, (1,7,0), 01-074-3141@Phlogopite 1M, (1,1,3), 01-070-3665@Muscovite-2M1, syn, (1,1,-7)

36.589(8) 2.4539(5) 611(32) 108(3) 0.149(7) 587(27) Quartz, (1,1,0), 01-070-3665@Muscovite-2M1, syn, (1,3,-3)

39.523(8) 2.2782(4) 371(25) 65.4(18) 0.151(8) 582(29) Quartz, (1,0,2), 00-041-1481@Anorthite, sodian, disordered, (3,3,-1)

40.352(11) 2.2333(6) 190(18) 32.0(14) 0.151(10) 584(40) Quartz, (1,1,1), 00-041-1481@Anorthite, sodian, disordered, (2,2,-3), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,4,2), 01-074-3141@Phlogopite 1M, (2,2,0), 01-070-3665@Muscovite-2M1, syn, (2,2,-2)

41.33(3) 2.1828(13) 39(8) 12.1(12) 0.16(5) 570(174) Anorthite, sodian, disordered, (3,-3,-2), 01-070-3665@Muscovite-2M1, syn, (2,2,-3)

41.887(6) 2.1550(3) 166(17) 23.4(11) 0.105(9) 847(74) Muscovite-2M1, syn, (2,2,2) 42.506(9) 2.1250(4) 426(27) 86(2) 0.151(10) 588(39) Quartz, (2,0,0), 01-070-3665@Muscovite-2M1, syn, (1,3,5)

44.362(15) 2.0403(7) 88(12) 7.2(11) 0.076(13) 1179(206) Unknown,

44.90(4) 2.0172(18) 110(14) 80(18) 0.66(17) 135(34) Anorthite, sodian, disordered, (4,0,-2), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,8,1), 01-074-3141@Phlogopite 1M, (2,2,-3), 01-070-3665@Muscovite-2M1, syn, (2,2,-5)

45.543(7) 1.9901(3) 1493(50) 391(21) 0.239(5) 376(8) Anorthite, sodian, disordered, (0,6,1), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (3,7,0), 01-074-3141@Phlogopite 1M, (0,0,5)

50.195(6) 1.8160(2) 1183(44) 200(5) 0.124(7) 737(39) Quartz, (1,1,2), 00-041-1481@Anorthite, sodian, disordered, (2,6,0), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,7,2), 01-070-3665@Muscovite-2M1, syn, (0,2,10)

51.26(9) 1.781(3) 27(7) 10.1(16) 0.28(14) 326(157) heptamagnesium phyllo-octasilicate difluoride, (5,1,1), 01-070-3665@Muscovite-2M1, syn, (2,2,6)

54.64(5) 1.6783(15) 81(12) 33(15) 0.35(7) 269(55) Anorthite, sodian, disordered, (2,-2,-4), 01-076-0638@heptamagnesium phyllo-octasilicate difluoride, (1,10,1), 01-074-3141@Phlogopite 1M, (3,1,0), 01-070-3665@Muscovite-2M1,

54.924(10) 1.6703(3) 360(24) 60(27) 0.139(13) 671(61) Muscovite-2M1, syn, (1,5,2)

- 25 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD08D 4.916444 4.916444 5.402545 90.000000 90.000000 120.000000

Sample 18CD08D 8.193212 12.892743 7.107333 93.377998 115.968002 90.776001

Sample 18CD08D 9.495478 18.043962 5.342004 90.000000 90.000000 90.000000

Sample 18CD08D 5.229393 9.058222 10.132102 90.000000 99.948997 90.000000

Sample 18CD08D 5.211895 9.049468 19.913875 90.000000 95.614998 90.000000

Sample 18CD08D


Quartz 4.916444 4.916444 5.402545 90.000000 90.000000 120.000000


8.193212 12.892743 7.107333 93.377998 115.968002 90.776001

heptamagnesium phyllo-octasilicate difluoride

9.495478 18.043962 5.342004 90.000000 90.000000 90.000000

Phlogopite 1M 5.229393 9.058222 10.132102 90.000000 99.948997 90.000000

Muscovite-2M1, syn 5.211895 9.049468 19.913875 90.000000 95.614998 90.000000

Unknown

- 26 -

Sample 18CD08D Sample 18CD08D 0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 27 -



Quartz 68(6)

Anorthite, sodian, disordered 22(3)

heptamagnesium phyllo-octasilicate difluoride 1.3(10)

Phlogopite 1M 7.0(13)

Muscovite-2M1, syn 2.1(14)

Sample 18CD08D

0 20 40 60 80

Quartz


heptamagnesium phyllo-octasilicate difluoride

Phlogopite 1M

Muscovite-2M1, syn

Wt(%)

- 28 -


Analysis date 11/30/2018 11:53:28 AM Sample name 18CD08E Measurement date 11/30/2018 11:14:15 AM File name Sample 18CD08E.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

1.5e+004

10 20 30 40 50

-2000

-1000

0

1000

2000

Inte

nsity (

cps)

2-theta (deg)

Error

Residual

Meas. data:Sample 18CD08E/Data 1

BG data:Sample 18CD08E/Data 1

Calc. data:Sample 18CD08E/Data 1

Inte

nsity (

cps)

- 29 -









Receiving slit #2 -




Phengite 2M1 ( K0.95 Na0.05 ) ( Al0.76 Fe0.14 Mg0.10 )2 ( Si3.25 Al0.75 ) O10 ( ( O H )1.96 F0.04 )

0.9004370501342535 10742774 (ICDD)

Albite (heat-treated) Na ( Al Si3 O8 ) 1.421974073494508 10896427 (ICDD)

graphite orthorhombic C 0.8159363350211323 10742330 (ICDD)



Phengite 2M1 ( K0.95 Na0.05 ) ( Al0.76 Fe0.14 Mg0.10 )2 ( Si3.25 Al0.75 ) O10 ( ( O H )1.96 F0.04 )


Albite (heat-treated) Na ( Al Si3 O8 ) 2 : C-1 10896427 (ICDD)

graphite orthorhombic C 36 : Cmc21 10742330 (ICDD)

- 30 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

10 20 30 40 50 0

2000

4000

6000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Meas. data:Sample 18CD08E/Data 1

Quartz, syn

Phengite 2M1

Albite (heat-treated)

graphite orthorhombic

Inte

nsity (

cps)

Quartz, synPhengite 2M1

Albite (heat-treated)graphite orthorhombic

- 31 -

Peak list


6.235(14) 14.16(3) 608(32) 237(7) 0.302(13) 275(12) graphite orthorhombic, (0,0,2) 8.919(4) 9.907(5) 2447(64) 656(9) 0.212(4) 393(8) Phengite 2M1, (0,0,2)

12.527(10) 7.060(6) 315(23) 81(3) 0.153(14) 546(50) graphite orthorhombic, (0,0,4) 17.849(6) 4.9654(18) 589(31) 108(2) 0.156(5) 537(16) Phengite 2M1, (0,0,4)

18.87(2) 4.699(6) 63(10) 15.4(12) 0.21(2) 405(41) Albite (heat-treated), 01-074-2330@(0,2,-1), graphite orthorhombic, (0,0,6)

19.84(4) 4.471(8) 39(8) 12.2(12) 0.27(3) 315(40) Phengite 2M1, (1,1,-1)

20.905(4) 4.2458(8) 1468(49) 322(4) 0.188(3) 449(7) Quartz, syn, (1,0,0), 01-074-2774@Phengite 2M1, (1,1,-2)

21.95(2) 4.046(4) 122(14) 18.2(16) 0.135(16) 628(76) Albite (heat-treated), (2,0,-1) 24.347(15) 3.653(2) 77(11) 8.0(12) 0.08(2) 1095(348) Unknown,

25.204(12) 3.5306(17) 180(17) 39(3) 0.162(15) 526(50) graphite orthorhombic, (0,0,8) 25.47(3) 3.495(5) 83(12) 44(6) 0.29(6) 290(58) Phengite 2M1, (1,1,-4), 01-089-6427@Albite (heat-treated), (1,1,-2)

26.591(4) 3.3494(5) 9373(125) 2336(33) 0.198(6) 431(13) Quartz, syn, (1,0,1), 01-074-2774@Phengite 2M1, (0,2,4)

27.87(4) 3.199(5) 254(21) 67(7) 0.24(3) 363(48) Phengite 2M1, (1,1,4), 01-089-6427@Albite (heat-treated), (2,0,-2)

29.90(5) 2.986(5) 87(12) 21(2) 0.21(3) 416(59) Phengite 2M1, (0,2,5), 01-089-6427@Albite (heat-treated), (1,-3,1)

31.38(11) 2.849(10) 44(9) 44(4) 0.77(10) 112(15) Phengite 2M1, (1,1,5), 01-089-6427@Albite (heat-treated), 01-074-2330@(1,3,1), graphite orthorhombic, (0,0,10)



36.082(16) 2.4872(11) 127(15) 19(2) 0.13(2) 694(111) Phengite 2M1, (0,0,8), 01-089-6427@Albite (heat-treated), (3,-1,-2)


39.473(9) 2.2810(5) 490(29) 88(2) 0.159(7) 553(25) Quartz, syn, (1,0,2), 01-089-6427@Albite (heat-treated), (1,-1,-3)

40.300(10) 2.2361(5) 345(24) 64.3(19) 0.162(8) 546(28) Quartz, syn, (1,1,1), 01-074-2774@Phengite 2M1, (1,3,-5), 01-089-6427@Albite (heat-treated), (1,-3,2)

42.458(5) 2.1273(3) 576(31) 99.6(18) 0.135(6) 657(28) Quartz, syn, (2,0,0), 01-074-2774@Phengite 2M1, (1,3,5), 01-089-6427@Albite (heat-treated), 01-074-2330@(0,6,0), graphite orthorhombic, (1,1,0)

45.544(8) 1.9901(3) 650(33) 136(5) 0.157(11) 573(42) Phengite 2M1, (0,0,10), 01-074-2330@graphite orthorhombic, (1,1,5)

45.809(8) 1.9792(3) 570(31) 106(5) 0.142(12) 632(53) Quartz, syn, (2,0,1), 01-089-6427@Albite (heat-treated), (3,-1,1)


50.514(16) 1.8053(5) 72(11) 16.8(15) 0.20(2) 448(48) Quartz, syn, (0,0,3), 01-089-6427@Albite (heat-treated), (3,3,1)

54.50(5) 1.6823(14) 33(7) 8(3) 0.21(8) 452(175) Phengite 2M1, (3,1,-3)

54.895(10) 1.6711(3) 444(27) 94(10) 0.178(10) 525(30) Quartz, syn, (2,0,2), 01-074-2774@Phengite 2M1, (1,5,2), 01-089-6427@Albite (heat-treated), (1,7,-2)

- 32 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD08E 4.915122 4.915122 5.417189 90.000000 90.000000 120.000000

Sample 18CD08E 5.220527 9.056608 20.013553 90.000000 95.746002 90.000000

Sample 18CD08E 8.175219 12.834150 7.165115 94.000000 116.510002 88.129997

Sample 18CD08E 2.458043 4.249861 28.445947 90.000000 90.000000 90.000000


Quartz, syn 4.915122 4.915122 5.417189 90.000000 90.000000 120.000000

Phengite 2M1 5.220527 9.056608 20.013553 90.000000 95.746002 90.000000

Albite (heat-treated) 8.175219 12.834150 7.165115 94.000000 116.510002 88.129997

graphite orthorhombic 2.458043 4.249861 28.445947 90.000000 90.000000 90.000000

Sample 18CD08E Sample 18CD08E 0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 33 -



Quartz, syn 29.2(18)

Phengite 2M1 64.4(15)

Albite (heat-treated) 4.7(11)

graphite orthorhombic 1.6(2)


Sample 18CD08E

0 20 40 60 80

Quartz, syn

Phengite 2M1

Albite (heat-treated)


Unknown

Wt(%)

- 34 -


Analysis date 11/30/2018 12:41:33 PM Sample name 18CD09A Measurement date 11/30/2018 12:02:07 PM File name Sample 18CD09A.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

1.0e+003

2.0e+003

3.0e+003

4.0e+003

5.0e+003

10 20 30 40 50

-500

0

500

Inte

nsity (

cps)

2-theta (deg)

Error

Residual


BG data:Sample 18CD09A/Data 1

Calc. data:Sample 18CD09A/Data 1

Inte

nsity (

cps)

- 35 -









Receiving slit #2 -




Epidote Ca2 Al2.16 Fe0.84 Si3 O13 H 0.9373360981895886 10711538 (ICDD)

Clinochlore ( Mg2.96 Fe1.55 Fe.136 Al1.275 ) ( Si2.622 Al1.376 O10 ) ( O H )8

1.467322547439047 10791270 (ICDD)

Ferroactinolite ( Fe , Ca , Mg , Mn , Na )7 ( Si , Al )8 O22 ( O H )1.9

2.263652409902045 10895380 (ICDD)



Epidote Ca2 Al2.16 Fe0.84 Si3 O13 H 11 : P121/m1,unique-b 10711538 (ICDD)

Clinochlore ( Mg2.96 Fe1.55 Fe.136 Al1.275 ) ( Si2.622 Al1.376 O10 ) ( O H )8


Ferroactinolite ( Fe , Ca , Mg , Mn , Na )7 ( Si , Al )8 O22 ( O H )1.9


- 36 -

10 20 30 40 50

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

10 20 30 40 50 0

500

1000

1500

2000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)


Quartz, syn

Epidote

Clinochlore

Ferroactinolite

Inte

nsity (

cps)

Quartz, synEpidote

ClinochloreFerroactinolite

- 37 -

Peak list


6.34(3) 13.93(6) 177(17) 26(3) 0.07(3) 1138(479) Unknown,

8.807(8) 10.033(9) 881(38) 267(6) 0.224(9) 371(16) Unknown,

9.89(3) 8.94(2) 176(17) 34(3) 0.11(3) 757(221) Ferroactinolite, (0,2,0)

10.622(4) 8.322(3) 2799(68) 429(7) 0.115(4) 727(28) Unknown,

11.06(2) 7.996(15) 87(12) 19(2) 0.13(3) 632(134) Epidote, (1,0,0)

12.565(17) 7.039(9) 162(16) 32(2) 0.13(2) 621(103) Clinochlore, (0,0,2)

17.776(14) 4.986(4) 183(17) 65(2) 0.307(12) 274(11) Epidote, (1,0,-2)

18.84(3) 4.707(7) 44(9) 9.5(13) 0.16(4) 537(137) Clinochlore, (0,0,3)

19.709(19) 4.501(4) 128(15) 16.7(15) 0.08(3) 1048(393) Clinochlore, (1,1,-1), 01-089-5380@Ferroactinolite, (0,4,0)

20.877(6) 4.2515(13) 706(34) 130(5) 0.119(8) 708(48) Quartz, syn, (1,0,0), 01-079-1270@Clinochlore, (1,1,1)

22.06(3) 4.026(5) 158(16) 28(10) 0.17(7) 503(207) Clinochlore, (1,1,-2), 01-089-5380@Ferroactinolite, (2,0,-1)

22.20(2) 4.001(4) 204(18) 41(11) 0.187(17) 453(41) Epidote, (2,0,0)

23.63(5) 3.762(7) 44(9) 24(3) 0.29(6) 289(62) Epidote, (1,1,1)

25.13(5) 3.541(7) 41(8) 14(3) 0.21(11) 403(214) Clinochlore, (0,0,4)

25.605(12) 3.4761(16) 160(16) 18(3) 0.08(2) 1082(290) Epidote, (2,1,-1)

26.687(5) 3.3376(6) 3440(76) 743(10) 0.149(7) 571(26) Quartz, syn, (0,1,1)

27.356(8) 3.2575(9) 229(20) 23(3) 0.070(15) 1227(256) Epidote, (2,1,0)

27.86(3) 3.199(4) 271(21) 71(39) 0.21(15) 399(287) Epidote, (2,0,1)

28.05(4) 3.179(4) 148(16) 19(36) 0.11(11) 806(798) Epidote, (2,0,-3)

28.785(11) 3.0989(11) 565(31) 76(3) 0.112(9) 762(63) Unknown,

30.923(9) 2.8894(8) 507(29) 113(4) 0.151(11) 570(40) Epidote, (1,1,-3)

31.853(15) 2.8071(13) 225(19) 38(3) 0.160(17) 539(57) Epidote, (0,2,0), 01-079-1270@Clinochlore, (0,2,4), 01-089-5380@Ferroactinolite, (3,3,0)

32.096(19) 2.7864(16) 175(17) 28(3) 0.15(2) 577(94) Epidote, (2,1,1)

33.094(12) 2.7046(10) 162(16) 22(3) 0.108(19) 802(145) Ferroactinolite, (1,5,1)

33.456(18) 2.6762(14) 229(20) 74(4) 0.26(2) 336(26) Epidote, (0,2,1), 01-079-1270@Clinochlore, (1,1,4)

33.84(2) 2.6470(16) 91(12) 15(3) 0.13(3) 650(138) Epidote, (1,2,0), 01-079-1270@Clinochlore, (1,3,-1)

34.558(12) 2.5933(9) 254(21) 35.8(17) 0.132(9) 659(45) Epidote, (3,1,-1), 01-079-1270@Clinochlore, (1,3,1), 01-089-5380@Ferroactinolite, (0,6,1)

35.20(3) 2.5475(18) 81(12) 19(4) 0.16(3) 554(120) Clinochlore, (2,0,1), 01-089-5380@Ferroactinolite, (2,4,1)

35.508(11) 2.5261(7) 206(19) 46(4) 0.14(2) 617(95) Epidote, (2,0,2), 01-079-1270@Clinochlore, (1,3,-2), 01-089-5380@Ferroactinolite, (2,0,-2)

36.194(10) 2.4798(6) 139(15) 12.9(14) 0.082(10) 1062(126) Unknown,

36.613(7) 2.4523(4) 410(26) 55.4(18) 0.120(6) 730(39) Quartz, syn, (1,1,0), 01-071-1538@Epidote, (1,2,-2)

37.510(14) 2.3957(9) 299(22) 57(2) 0.153(16) 573(61) Epidote, (3,1,-3), 01-079-1270@Clinochlore, (2,0,2), 01-089-5380@Ferroactinolite, (3,1,1)

38.528(19) 2.3347(11) 60(10) 9.5(12) 0.15(2) 594(99) Ferroactinolite, (3,5,-1)

39.32(3) 2.2894(18) 84(12) 27(4) 0.30(4) 290(40) Epidote, (2,1,2), 01-079-1270@Clinochlore, (2,2,-1), 01-089-5380@Ferroactinolite, (1,7,-1)

- 38 -

39.503(15) 2.2793(8) 227(19) 36(5) 0.15(2) 589(88) Quartz, syn, (1,0,2), 01-071-1538@Epidote, (2,1,-4), 01-089-5380@Ferroactinolite, (1,1,2)

40.326(17) 2.2347(9) 116(14) 18.2(12) 0.147(14) 599(56) Quartz, syn, (1,1,1), 01-079-1270@Clinochlore, (2,0,-4)

41.817(11) 2.1584(5) 308(23) 52.8(19) 0.157(9) 566(32) Epidote, (4,0,-1), 01-089-5380@Ferroactinolite, (2,6,1)

42.496(8) 2.1255(4) 214(19) 27.6(15) 0.113(8) 791(58) Quartz, syn, (2,0,0), 01-079-1270@Clinochlore, (2,2,2)

42.97(3) 2.1033(13) 79(11) 39(2) 0.45(3) 200(15) Epidote, (3,1,-4), 01-079-1270@Clinochlore, (0,2,6), 01-089-5380@Ferroactinolite, (4,4,-1)

44.325(15) 2.0419(7) 153(16) 28(2) 0.11(2) 801(146) Epidote, (2,0,3)

44.92(3) 2.0161(15) 79(11) 43(5) 0.47(7) 190(29) Epidote, (2,0,-5), 01-079-1270@Clinochlore, (2,2,-4), 01-089-5380@Ferroactinolite, (2,0,2)

45.598(17) 1.9878(7) 164(17) 31(4) 0.15(2) 596(98) Epidote, (4,0,-4), 01-079-1270@Clinochlore, (2,2,3)

45.871(10) 1.9766(4) 273(21) 45(4) 0.135(12) 669(58) Quartz, syn, (2,0,1), 01-071-1538@Epidote, (1,0,-5), 01-089-5380@Ferroactinolite, (2,2,2)

48.60(3) 1.8717(10) 112(14) 54(2) 0.40(2) 230(13) Epidote, (2,2,2), 01-079-1270@Clinochlore, (1,3,5), 01-089-5380@Ferroactinolite, (4,6,-1)

49.18(7) 1.851(2) 17(5) 4.8(15) 0.23(10) 398(171) Clinochlore, (0,2,7), 01-089-5380@Ferroactinolite, (5,3,-1)

50.194(5) 1.81604(18) 662(33) 105(3) 0.132(5) 692(27) Quartz, syn, (1,1,2), 01-079-1270@Clinochlore, (1,3,-6), 01-089-5380@Ferroactinolite, (5,3,0)

51.39(4) 1.7765(14) 38(8) 8.7(11) 0.22(4) 425(82) Epidote, (3,2,-4)

54.30(4) 1.6880(11) 37(8) 7(3) 0.18(5) 531(146) Epidote, (2,0,-6), 01-079-1270@Clinochlore, (3,1,-3), 01-089-5380@Ferroactinolite, (0,0,3)

54.937(17) 1.6700(5) 155(16) 19(3) 0.114(12) 821(83) Quartz, syn, (0,2,2)

- 39 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD09A 4.906037 4.906037 5.396862 90.000000 90.000000 120.000000

Sample 18CD09A 8.869836 5.616189 10.131296 90.000000 115.383003 90.000000

Sample 18CD09A 5.324946 9.223603 14.203174 90.000000 96.349998 90.000000

Sample 18CD09A 9.841122 18.037947 5.235709 90.000000 104.809998 90.000000

Sample 18CD09A


Quartz, syn 4.906037 4.906037 5.396862 90.000000 90.000000 120.000000

Epidote 8.869836 5.616189 10.131296 90.000000 115.383003 90.000000

Clinochlore 5.324946 9.223603 14.203174 90.000000 96.349998 90.000000

Ferroactinolite 9.841122 18.037947 5.235709 90.000000 104.809998 90.000000

Unknown

Sample 18CD09A Sample 18CD09A 0

0.5

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1.5

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4.5

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(a

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Data set

- 40 -



Quartz, syn 40(2)

Epidote 21.9(18)

Clinochlore 5.3(6)

Ferroactinolite 32(4)

Sample 18CD09A

0 20 40 60 80

Quartz, syn

Epidote

Clinochlore

Ferroactinolite

Unknown

Wt(%)

- 41 -


Analysis date 11/30/2018 1:54:38 PM Sample name 18CD09B Measurement date 11/30/2018 12:52:09 PM File name Sample 18CD09B.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

2.0e+003

4.0e+003

6.0e+003

8.0e+003

1.0e+004

10 20 30 40 50

-1000

0

1000

Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 42 -









Receiving slit #2 -




Clinochlore Al2 Mg5 Si3 O10 ( O H )8 1.499701278964685 10741137 (ICDD)

Albite ( Na0.98 Ca0.02 ) ( Al1.02 Si2.98 O8 )

1.217753252795112 10703752 (ICDD)

Biotite K Fe Mg2 ( Al Si3 O10 ) ( O H )2 0.8801452160526145 10801110 (ICDD)

Orthoclase K Al Si3 O8 2.911617847124523 10751592 (ICDD)



Clinochlore Al2 Mg5 Si3 O10 ( O H )8 15 : C12/c1,unique-b,cell-1 10741137 (ICDD)

Albite ( Na0.98 Ca0.02 ) ( Al1.02 Si2.98 O8 )

2 : C-1 10703752 (ICDD)

Biotite K Fe Mg2 ( Al Si3 O10 ) ( O H )2 12 : C12/m1,unique-b,cell-1 10801110 (ICDD)

Orthoclase K Al Si3 O8 12 : C12/m1,unique-b,cell-1 10751592 (ICDD)

- 43 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

10 20 30 40 50 0

1000

2000

3000

4000

5000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Inte

nsity (

cps)

Quartz, synClinochlore

AlbiteBiotite

Orthoclase

- 44 -

Peak list


6.25(2) 14.13(5) 187(18) 62(5) 0.17(4) 476(97) Clinochlore, (0,0,2)

8.771(3) 10.074(3) 6513(104) 1762(14) 0.195(4) 427(8) Biotite, (0,0,1)

10.493(14) 8.424(12) 69(11) 11.7(16) 0.13(2) 660(111) Unknown,

12.517(13) 7.066(8) 325(23) 78(3) 0.166(13) 503(39) Clinochlore, (0,0,4)

13.90(2) 6.367(11) 103(13) 38(3) 0.25(3) 330(39) Albite, (0,0,1)

17.880(11) 4.957(3) 332(24) 74(3) 0.208(9) 404(17) Unknown,

18.85(3) 4.703(7) 88(12) 17(2) 0.18(3) 480(70) Clinochlore, (0,0,6), 01-070-3752@Albite, (0,2,-1)

19.62(3) 4.521(7) 44(9) 17(2) 0.31(4) 271(34) Clinochlore, (0,2,0), 01-080-1110@Biotite, (1,1,0), 01-075-1592@Orthoclase, (0,2,1)

20.903(7) 4.2461(13) 604(32) 110(2) 0.155(5) 546(18) Quartz, syn, (1,0,0), 01-075-1592@Orthoclase, (2,0,-1)

22.036(11) 4.0305(19) 303(22) 52.9(19) 0.153(8) 554(27) Clinochlore, (1,1,-4)

22.950(14) 3.872(2) 127(15) 24.2(11) 0.180(10) 471(26) Clinochlore, (0,2,4), 01-075-1592@Orthoclase, (2,0,0)

23.65(3) 3.759(5) 136(15) 27(3) 0.18(3) 460(78) Clinochlore, (1,1,-5), 01-075-1592@Orthoclase, (1,3,0)

23.94(3) 3.715(5) 155(16) 34(4) 0.20(3) 417(70) Unknown,

24.35(2) 3.653(3) 236(20) 49(4) 0.19(2) 441(52) Clinochlore, (1,1,4), 01-070-3752@Albite, (2,0,0), 01-080-1110@Biotite, (1,1,-2)

25.14(3) 3.539(5) 108(13) 43(5) 0.26(8) 329(104) Clinochlore, (0,0,8), 01-070-3752@Albite, (2,2,-1), 01-075-1592@Orthoclase, (2,2,-1)

25.5(2) 3.49(3) 38(8) 67(12) 1.6(2) 52(7) Clinochlore, (1,1,-6), 01-070-3752@Albite, (1,-3,-1), 01-080-1110@Biotite, (0,2,2), 01-075-1592@Orthoclase, (1,3,-1)

26.519(6) 3.3584(8) 2092(59) 374(89) 0.165(6) 517(18) Clinochlore, (1,1,5), 01-070-3752@Albite, (2,-2,-1)

26.681(6) 3.3383(8) 3946(81) 781(94) 0.18(3) 466(67) Quartz, syn, (0,1,1), 01-080-1110@Biotite, (0,0,3)

26.860(12) 3.3165(14) 1219(45) 199(24) 0.15(2) 562(89) Orthoclase, (2,2,0)

27.82(3) 3.204(3) 275(21) 134(13) 0.46(3) 187(12) Albite, (2,-2,0)

27.998(10) 3.1842(11) 1004(41) 284(14) 0.261(9) 327(11) Clinochlore, (1,1,-7), 01-070-3752@Albite, (2,2,0)

28.720(12) 3.1058(13) 198(18) 16.9(17) 0.079(12) 1083(167) Clinochlore, (1,1,6)

29.814(19) 2.9943(19) 153(16) 47(2) 0.22(2) 387(40) Orthoclase, (1,3,1)

30.440(8) 2.9342(8) 329(23) 55.5(19) 0.132(10) 653(50) Biotite, (1,1,-3), 01-075-1592@Orthoclase, (2,2,-2)

31.35(4) 2.851(3) 99(13) 41(4) 0.38(3) 226(19) Clinochlore, (1,1,7), 01-070-3752@Albite, (1,3,-2)

34.16(6) 2.623(5) 70(11) 22(3) 0.28(7) 314(85) Clinochlore, (1,3,-2), 01-080-1110@Biotite, (1,3,-1), 01-075-1592@Orthoclase, (3,1,-2)

35.598(15) 2.5199(11) 431(27) 107(5) 0.172(19) 505(57) Clinochlore, (1,3,-4), 01-070-3752@Albite, (2,-2,1), 01-080-1110@Biotite, (1,1,3), 01-075-1592@Orthoclase, (3,1,0)

36.09(2) 2.4869(15) 104(13) 24(2) 0.19(3) 470(77) Albite, (1,1,2), 01-075-1592@Orthoclase, (2,4,0)

36.573(14) 2.4549(9) 244(20) 62(3) 0.17(3) 501(76) Clinochlore, (1,1,9), 01-070-3752@Albite, (1,5,-1), 01-080-1110@Biotite, (1,3,-2), 01-075-1592@Orthoclase, (1,5,0)

39.06(2) 2.3041(13) 86(12) 16(2) 0.17(3) 517(99) Biotite, (0,4,0)

39.46(3) 2.2816(15) 141(15) 28(2) 0.18(3) 488(70) Quartz, syn, (0,1,2), 01-074-1137@Clinochlore, (1,1,10), 01-070-3752@Albite, (2,2,-3), 01-080-1110@Biotite, (2,2,0)

40.22(10) 2.240(5) 24(6) 11(2) 0.40(10) 221(57) Quartz, syn, (1,1,1), 01-074-1137@Clinochlore, (1,3,6), 01-070-3752@Albite, (1,-3,2), 01-080-1110@Biotite, (0,4,1), 01-075-1592@Orthoclase, (2,2,-3)

41.25(4) 2.187(2) 40(8) 15(2) 0.32(7) 278(58) Clinochlore, (2,2,-5), 01-070-3752@Albite, (2,-2,-3), 01-080-1110@Biotite, (1,3,-3), 01-075-1592@Orthoclase, (1,5,1)

42.455(12) 2.1274(6) 256(21) 58.8(18) 0.196(11) 454(25) Clinochlore, (0,4,5), 01-070-3752@Albite, (1,5,1), 01-075-1592@Orthoclase, (2,4,1)

- 45 -

42.87(3) 2.1078(12) 63(10) 10.9(10) 0.15(2) 587(90) Clinochlore, (2,2,4), 01-080-1110@Biotite, (0,4,2), 01-075-1592@Orthoclase, (4,0,-2)

44.933(5) 2.0157(2) 491(29) 107(3) 0.149(8) 602(32) Clinochlore, (2,2,-8), 01-070-3752@Albite, (2,0,2), 01-080-1110@Biotite, (0,0,5), 01-075-1592@Orthoclase, (4,2,-2)

45.593(7) 1.9880(3) 432(27) 158(4) 0.239(10) 377(15) Clinochlore, (2,0,8), 01-070-3752@Albite, (3,-1,1)

50.156(7) 1.8173(2) 411(26) 84(3) 0.139(11) 661(52) Quartz, syn, (0,0,3), 01-074-1137@Clinochlore, (1,3,-12), 01-070-3752@Albite, (1,1,3)

50.742(5) 1.79771(18) 658(33) 82(3) 0.113(5) 810(36) Albite, (2,0,-4), 01-075-1592@Orthoclase, (2,0,-4)

52.39(3) 1.7448(10) 29(7) 13(2) 0.41(10) 223(53) Clinochlore, (2,2,9), 01-070-3752@Albite, (4,4,-2), 01-080-1110@Biotite, (1,3,4), 01-075-1592@Orthoclase, (2,4,2)

53.10(5) 1.7232(15) 65(10) 15.5(18) 0.22(4) 416(74) Clinochlore, (3,1,-1), 01-070-3752@Albite, (3,-1,-4), 01-075-1592@Orthoclase, (1,3,3)

54.566(16) 1.6804(5) 115(14) 19.1(13) 0.156(19) 598(71) Clinochlore, (3,1,-6), 01-070-3752@Albite, (1,-5,-3), 01-080-1110@Biotite, (1,3,-5), 01-075-1592@Orthoclase, (3,5,-3)

54.878(11) 1.6716(3) 152(16) 16.8(14) 0.103(9) 906(81) Quartz, syn, (0,2,2)

- 46 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD09B 4.884834 4.884834 5.443856 90.000000 90.000000 120.000000

Sample 18CD09B 5.290418 9.162693 28.422562 90.000000 97.147003 90.000000

Sample 18CD09B 8.215106 12.906056 7.218579 94.245003 116.599998 87.800003

Sample 18CD09B 5.342913 9.252239 10.222314 90.000000 100.150002 90.000000

Sample 18CD09B 8.582179 12.993019 7.205038 90.000000 116.050003 90.000000


Quartz, syn 4.884834 4.884834 5.443856 90.000000 90.000000 120.000000

Clinochlore 5.290418 9.162693 28.422562 90.000000 97.147003 90.000000

Albite 8.215106 12.906056 7.218579 94.245003 116.599998 87.800003

Biotite 5.342913 9.252239 10.222314 90.000000 100.150002 90.000000

Orthoclase 8.582179 12.993019 7.205038 90.000000 116.050003 90.000000


0.5

1

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(a

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Data set

- 47 -



Quartz, syn 4.8(6)

Clinochlore 8.7(7)

Albite 10.2(14)

Biotite 64(3)

Orthoclase 12(2)

Sample 18CD09B

0 20 40 60 80

Quartz, syn

Clinochlore

Albite

Biotite

Orthoclase

Wt(%)

- 48 -


Analysis date 11/30/2018 2:54:29 PM Sample name 18CD09C Measurement date 11/30/2018 2:04:00 PM File name Sample 18CD09C.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

2.0e+003

4.0e+003

6.0e+003

10 20 30 40 50

-1000

-500

0

500

1000

Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 49 -









Receiving slit #2 -



Albite, calcian, ordered ( Na , Ca ) Al ( Si , Al )3 O8 1.552847822203883 411480 (ICDD)

Nepheline K Na3 ( Al4 Si4 O16 ) 2.869293889724358 10736265 (ICDD)


3.066015173231709 10720459 (ICDD)


Albite, calcian, ordered ( Na , Ca ) Al ( Si , Al )3 O8 2 : C-1 411480 (ICDD)

Nepheline K Na3 ( Al4 Si4 O16 ) 173 : P63 10736265 (ICDD)



- 50 -

10 20 30 40 50

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500

1000

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4500

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5500

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6500

7000

10 20 30 40 50 0

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cps d

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2-theta (deg)

Inte

nsity (

cps)

Albite, calcian, orderedNepheline

Magnesiohornblende

- 51 -

Peak list


9.836(16) 8.985(15) 233(20) 70(3) 0.17(2) 487(59) Magnesiohornblende, (0,2,0) 10.595(5) 8.343(4) 3925(81) 794(13) 0.161(4) 518(13) Magnesiohornblende, (1,1,0) 12.45(5) 7.10(3) 52(9) 20(2) 0.29(5) 286(52) Unknown,

18.09(4) 4.899(11) 64(10) 31(3) 0.25(6) 341(84) Magnesiohornblende, (1,1,-1) 18.744(13) 4.730(3) 98(13) 15.4(12) 0.08(3) 1015(335) Unknown,

19.665(14) 4.511(3) 118(14) 23.5(18) 0.13(2) 641(105) Magnesiohornblende, (0,4,0) 21.22(3) 4.184(6) 69(11) 15.3(17) 0.14(5) 622(232) Magnesiohornblende, (2,2,0) 22.08(3) 4.023(5) 78(11) 22.6(18) 0.25(2) 337(32) Albite, calcian, ordered, (2,0,-1), 01-072-0459@Magnesiohornblende, (1,1,1)

22.81(3) 3.895(4) 26(7) 16(2) 0.49(11) 171(38) Albite, calcian, ordered, (1,-1,1), 01-073-6265@Nepheline, (2,0,1), 01-072-0459@Magnesiohornblende, (1,3,-1)

23.64(2) 3.760(3) 136(15) 21.6(15) 0.139(15) 610(66) Albite, calcian, ordered, (1,1,1) 24.02(3) 3.702(4) 78(11) 17.3(15) 0.19(3) 448(62) Albite, calcian, ordered, (1,-3,0), 01-072-0459@Magnesiohornblende, (2,2,-1)

25.567(10) 3.4812(14) 110(14) 15.3(15) 0.102(17) 831(134) Albite, calcian, ordered, (1,-3,-1) 26.274(14) 3.3892(17) 261(21) 76(3) 0.17(2) 504(58) Magnesiohornblende, (1,3,1) 27.296(17) 3.265(2) 448(27) 68(4) 0.142(11) 600(46) Nepheline, (2,1,0), 01-072-0459@Magnesiohornblende, (2,4,0)

28.033(7) 3.1804(8) 1306(47) 285(8) 0.131(9) 654(46) Albite, calcian, ordered, (0,0,2) 28.678(4) 3.1103(4) 2259(61) 380(4) 0.134(3) 639(14) Magnesiohornblende, (3,1,0) 29.512(12) 3.0243(12) 111(14) 18.9(11) 0.154(13) 557(48) Nepheline, (2,0,2)

30.399(12) 2.9380(11) 267(21) 50(2) 0.174(9) 493(26) Albite, calcian, ordered, (0,4,-1), 01-072-0459@Magnesiohornblende, (1,5,-1)

30.927(10) 2.8890(9) 289(22) 55(2) 0.175(10) 492(28) Nepheline, (3,0,0)

31.40(2) 2.8465(17) 59(10) 6.0(7) 0.096(19) 901(182) Albite, calcian, ordered, (1,3,1) 31.969(7) 2.7972(6) 415(26) 75.0(16) 0.170(4) 509(13) Magnesiohornblende, (3,3,0) 32.73(3) 2.734(3) 108(13) 36(8) 0.26(9) 328(110) Nepheline, (3,0,1), 01-072-0459@Magnesiohornblende, (3,3,-1)

33.078(10) 2.7059(8) 512(29) 76(7) 0.122(11) 707(61) Magnesiohornblende, (1,5,1) 34.547(11) 2.5941(8) 266(21) 36.6(17) 0.128(10) 676(50) Nepheline, (2,1,2), 01-072-0459@Magnesiohornblende, (0,6,1)

35.138(7) 2.5518(5) 461(28) 73(2) 0.114(9) 765(61) Magnesiohornblende, (2,4,1) 37.89(3) 2.3728(17) 138(15) 38(3) 0.19(4) 462(99) Albite, calcian, ordered, (2,4,0), 01-073-6265@Nepheline, (3,0,2), 01-072-0459@Magnesiohornblende, (3,5,0)

38.515(13) 2.3355(8) 366(25) 62(3) 0.160(13) 551(45) Albite, calcian, ordered, (1,-5,-1), 01-072-0459@Magnesiohornblende, (3,5,-1)

38.78(5) 2.320(3) 86(12) 18(3) 0.20(5) 448(110) Albite, calcian, ordered, (1,1,-3), 01-073-6265@Nepheline, (3,1,1)

39.32(3) 2.2893(18) 101(13) 33(2) 0.30(3) 289(27) Albite, calcian, ordered, (3,3,-1), 01-072-0459@Magnesiohornblende, (1,7,-1)

41.781(14) 2.1602(7) 233(20) 40(2) 0.129(17) 687(90) Nepheline, (4,0,0), 01-072-0459@Magnesiohornblende, (3,3,-2)

44.17(3) 2.0487(12) 74(11) 12.0(12) 0.15(2) 588(94) Nepheline, (1,0,4)

44.996(7) 2.0130(3) 411(26) 81(3) 0.126(9) 715(52) Albite, calcian, ordered, (4,0,-2), 01-073-6265@Nepheline, (3,0,3), 01-072-0459@Magnesiohornblende, (3,5,1)

45.350(7) 1.9981(3) 106(13) 13.8(15) 0.095(18) 949(176) Magnesiohornblende, (3,7,0) 48.232(12) 1.8852(4) 137(15) 19(2) 0.132(15) 690(80) Nepheline, (1,4,0), 01-072-0459@Magnesiohornblende, (5,1,0)

- 52 -

48.67(5) 1.8692(17) 74(11) 26(2) 0.33(5) 274(40) Albite, calcian, ordered, (2,2,2), 01-073-6265@Nepheline, (2,2,3), 01-072-0459@Magnesiohornblende, (4,6,-1)

49.19(2) 1.8508(8) 46(9) 6.3(8) 0.13(3) 707(151) Magnesiohornblende, (4,4,-2) 49.89(7) 1.826(2) 29(7) 28(7) 0.53(18) 173(57) Albite, calcian, ordered, (4,0,0), 01-073-6265@Nepheline, (3,1,3), 01-072-0459@Magnesiohornblende, (2,8,1)

50.46(2) 1.8071(8) 100(13) 31(5) 0.21(4) 432(72) Magnesiohornblende, (5,3,0)

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD09C 8.130365 12.809733 7.085302 93.680000 116.419998 89.389999

Sample 18CD09C 9.981265 9.981265 8.420435 90.000000 90.000000 120.000000

Sample 18CD09C 9.821103 17.998706 5.311962 90.000000 105.480003 90.000000


Albite, calcian, ordered 8.130365 12.809733 7.085302 93.680000 116.419998 89.389999

Nepheline 9.981265 9.981265 8.420435 90.000000 90.000000 120.000000

Magnesiohornblende 9.821103 17.998706 5.311962 90.000000 105.480003 90.000000


1

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3

4

5

6

7

8

9

10

11

12

13

14

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Latt

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sta

nts

(a

ng

.)

Data set

- 53 -



Albite, calcian, ordered 15.8(7)

Nepheline 3.6(2)

Magnesiohornblende 81(3)

Sample 18CD09C

0 20 40 60 80


Nepheline

Magnesiohornblende

Unknown

Wt(%)

- 54 -


Analysis date 11/30/2018 3:22:16 PM Sample name 18CD10A Measurement date 11/30/2018 2:44:51 PM File name 18CD10A.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

2.0e+003

4.0e+003

6.0e+003

8.0e+003

1.0e+004

10 20 30 40 50

-1000

0

1000

Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 55 -









Receiving slit #2 -




Chlorite-serpentine (NR) ( Mg , Al )6 ( Si , Al )4 O10 ( O H )8 1.324620242925983 521044 (ICDD)

Sodalite, (Zn,As) Na6 ( Zn As O4 )6 ·8 H2 O 1.537895440602183 450134 (ICDD)

Muscovite-2M1 K ( Al4 Si2 O9 ( O H )3 ) 1.08592151803028 10703754 (ICDD)



Chlorite-serpentine (NR) ( Mg , Al )6 ( Si , Al )4 O10 ( O H )8 147 : P-3 521044 (ICDD)

Sodalite, (Zn,As) Na6 ( Zn As O4 )6 ·8 H2 O 218 : P-43n 450134 (ICDD)

Muscovite-2M1 K ( Al4 Si2 O9 ( O H )3 ) 15 : C12/c1,unique-b,cell-1 10703754 (ICDD)

- 56 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

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7000

8000

9000

10000

11000

10 20 30 40 50 0

1000

2000

3000

4000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Inte

nsity (

cps)

Quartz, synChlorite-serpentine (NR)

Sodalite, (Zn,As)Muscovite-2M1

- 57 -

Peak list


6.284(13) 14.05(3) 438(27) 119(5) 0.171(17) 487(47) Chlorite-serpentine (NR), (0,0,1) 7.36(3) 12.00(5) 62(10) 25(5) 0.26(8) 322(99) Unknown,

8.920(2) 9.906(2) 6505(104) 1443(11) 0.151(3) 552(11) Muscovite-2M1, (0,0,2)

12.535(7) 7.056(4) 964(40) 210(4) 0.153(7) 546(24) Chlorite-serpentine (NR), (0,0,2) 13.893(5) 6.369(2) 216(19) 19.6(15) 0.04(2) 1962(960) Sodalite, (Zn,As), (1,1,0) 17.866(4) 4.9606(12) 1449(49) 284(4) 0.167(3) 504(10) Unknown,

18.845(11) 4.705(3) 240(20) 42.9(18) 0.156(8) 539(29) Chlorite-serpentine (NR), (0,0,3) 19.889(13) 4.460(3) 125(14) 38(2) 0.252(16) 334(21) Sodalite, (Zn,As), 01-070-3754@(2,0,0), Muscovite-2M1, (0,2,0)

20.892(6) 4.2485(12) 705(34) 148(3) 0.179(4) 470(11) Quartz, syn, (1,0,0), 01-070-3754@Muscovite-2M1, (1,1,-2)

22.30(4) 3.984(6) 95(13) 18(2) 0.12(6) 708(333) Muscovite-2M1, (1,1,2)

22.96(3) 3.870(5) 86(12) 17.6(16) 0.19(2) 439(49) Muscovite-2M1, (1,1,-3)

23.92(3) 3.717(5) 77(11) 22.3(18) 0.27(3) 311(31) Muscovite-2M1, (0,2,3)

25.180(13) 3.5338(17) 571(31) 77(7) 0.111(12) 763(84) Chlorite-serpentine (NR), (0,0,4) 25.20(13) 3.532(18) 100(13) 69(8) 0.59(6) 144(15) Muscovite-2M1, (1,1,3)

26.673(4) 3.3393(5) 6051(100) 1168(23) 0.157(4) 544(13) Quartz, syn, (1,0,1), 01-070-3754@Muscovite-2M1, (0,2,4)

26.885(6) 3.3135(8) 3314(74) 673(23) 0.169(8) 506(23) Unknown,

27.944(15) 3.1903(17) 467(28) 118(4) 0.181(17) 472(45) Sodalite, (Zn,As), (2,2,0) 29.97(2) 2.979(2) 190(18) 57(2) 0.24(3) 352(40) Muscovite-2M1, (0,2,5)

30.840(16) 2.8969(15) 75(11) 9.2(14) 0.10(2) 845(181) Unknown,

31.33(2) 2.8529(18) 186(18) 44(3) 0.191(19) 450(45) Sodalite, (Zn,As), (3,1,0) 31.648(16) 2.8248(14) 133(15) 25(3) 0.15(3) 577(109) Chlorite-serpentine (NR), (0,0,5) 32.106(11) 2.7856(9) 155(16) 33.3(19) 0.147(15) 587(59) Unknown,

34.72(2) 2.5818(15) 280(22) 76(8) 0.22(2) 400(45) Sodalite, (Zn,As), 01-070-3754@(2,2,2), Muscovite-2M1, (2,0,-2)

35.04(3) 2.559(2) 223(19) 65(7) 0.23(4) 377(59) Muscovite-2M1, (1,3,1)

36.113(18) 2.4852(12) 178(17) 46(2) 0.20(2) 436(44) Sodalite, (Zn,As), 01-070-3754@(3,2,0), Muscovite-2M1, (1,3,2)


37.71(5) 2.383(3) 50(9) 20(2) 0.33(4) 270(35) Sodalite, (Zn,As), 01-070-3754@(3,2,1), Muscovite-2M1, (1,3,3)


40.288(12) 2.2367(6) 260(21) 47(2) 0.125(16) 704(90) Quartz, syn, (1,1,1), 01-070-3754@Muscovite-2M1, (0,4,1)

42.500(14) 2.1253(7) 287(22) 82(3) 0.18(2) 489(57) Quartz, syn, (2,0,0), 00-045-0134@Sodalite, (Zn,As), (4,1,1)

44.82(2) 2.0204(10) 68(11) 24(4) 0.29(5) 308(58) Sodalite, (Zn,As), (4,2,0) 45.596(8) 1.9879(3) 1047(42) 368(6) 0.284(6) 317(7) Quartz, syn, (2,0,1), 01-070-3754@Muscovite-2M1, (0,2,9)

48.40(6) 1.879(2) 32(7) 16.1(19) 0.46(5) 196(21) Muscovite-2M1, (2,2,5)

50.132(6) 1.8181(2) 603(32) 118(2) 0.139(8) 658(36) Quartz, syn, (1,1,2)

- 58 -

52.94(5) 1.7280(15) 36(8) 14.6(13) 0.36(4) 255(31) Muscovite-2M1, (1,3,-9)

54.852(8) 1.6723(2) 315(23) 52.0(19) 0.141(8) 664(40) Unknown,

Lattice constants

Angular correction

No correction



Analysis results


18CD10A 4.904076 4.904076 5.390686 90.000000 90.000000 120.000000

18CD10A 5.340000 5.340000 14.104202 90.000000 90.000000 120.000000

18CD10A 8.977849 8.977849 8.977849 90.000000 90.000000 90.000000

18CD10A 5.215531 9.006093 20.115734 90.000000 95.665001 90.000000


Quartz, syn 4.904076 4.904076 5.390686 90.000000 90.000000 120.000000

Chlorite-serpentine (NR)

5.340000 5.340000 14.104202 90.000000 90.000000 120.000000

Sodalite, (Zn,As) 8.977849 8.977849 8.977849 90.000000 90.000000 90.000000

Muscovite-2M1 5.215531 9.006093 20.115734 90.000000 95.665001 90.000000

18CD10A 18CD10A 0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 59 -



Quartz, syn 4.76(14)

Chlorite-serpentine (NR) 0.000000

Sodalite, (Zn,As) 3.75(16)

Muscovite-2M1 91.5(15)

Muscovite-2M1

18CD10A

0 20 40 60 80 100

Quartz, syn


Sodalite, (Zn,As)

Muscovite-2M1

Unknown

Wt(%)

- 60 -


Analysis date 11/30/2018 3:50:45 PM Sample name 18CD10B Measurement date 11/30/2018 3:14:34 PM File name Sample 18CD10B.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0

1000

2000

3000

4000

5000

10 20 30 40 50

-500

0

500

Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 61 -









Receiving slit #2 -



Epidote Ca2 Al0.93 Fe0.05 Al Al0.24 Fe0.76 Si3 O13 H

1.386745245049952 10712387 (ICDD)

Chlorite-serpentine (NR) ( Mg , Al )6 ( Si , Al )4 O10 ( O H )8 1.183545513896287 521044 (ICDD)

Actinolite Ca1.68 Mg4.59 Fe0.48 Na0.1 Al0.23 Si7.92 O22 ( O H )2

1.406354682529557 10800521 (ICDD)


Epidote Ca2 Al0.93 Fe0.05 Al Al0.24 Fe0.76 Si3 O13 H

11 : P121/m1,unique-b 10712387 (ICDD)

Chlorite-serpentine (NR) ( Mg , Al )6 ( Si , Al )4 O10 ( O H )8 147 : P-3 521044 (ICDD)

Actinolite Ca1.68 Mg4.59 Fe0.48 Na0.1 Al0.23 Si7.92 O22 ( O H )2


- 62 -

10 20 30 40 50

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

10 20 30 40 50 0

500

1000

1500

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Inte

nsity (

cps)

EpidoteChlorite-serpentine (NR)

Actinolite

- 63 -

Peak list


6.251(19) 14.13(4) 101(13) 16(3) 0.08(4) 995(522) Chlorite-serpentine (NR), (0,0,1) 9.790(16) 9.027(15) 204(18) 41(3) 0.14(2) 580(100) Epidote, (0,0,1), 01-080-0521@Actinolite, (0,2,0)

10.546(6) 8.382(4) 2772(68) 540(10) 0.140(6) 594(27) Actinolite, (1,1,0)

12.543(5) 7.051(3) 109(13) 21(2) 0.175(16) 476(42) Chlorite-serpentine (NR), (0,0,2) 17.699(4) 5.0070(12) 133(15) 48.0(17) 0.338(12) 248(9) Epidote, (1,0,-2)

18.08(2) 4.903(5) 72(11) 15.5(10) 0.20(2) 416(42) Actinolite, (1,1,-1)

18.78(3) 4.722(8) 48(9) 9.5(16) 0.12(5) 705(277) Chlorite-serpentine (NR), (0,0,3) 19.65(3) 4.515(6) 101(13) 25.8(15) 0.17(2) 485(70) Actinolite, (0,4,0)

21.16(2) 4.195(4) 68(11) 14.5(11) 0.174(19) 484(52) Actinolite, (2,2,0)

22.172(8) 4.0060(14) 356(24) 73.1(17) 0.150(9) 564(35) Epidote, (2,0,0), 01-080-0521@Actinolite, (2,0,-1)

22.84(5) 3.890(8) 47(9) 8.4(15) 0.14(4) 594(165) Actinolite, (1,3,-1)

25.16(3) 3.537(4) 60(10) 8.6(9) 0.136(18) 627(83) Chlorite-serpentine (NR), (0,0,4) 25.589(16) 3.478(2) 106(13) 15.7(9) 0.139(14) 614(61) Epidote, (2,1,-1)

26.228(12) 3.3950(15) 278(22) 69(2) 0.201(10) 423(21) Epidote, (1,0,2), 01-080-0521@Actinolite, (1,3,1)


27.817(6) 3.2046(7) 356(24) 46(2) 0.094(8) 911(74) Epidote, (2,0,1)

28.617(5) 3.1167(5) 1421(49) 279(3) 0.169(3) 507(9) Actinolite, (3,1,0)

29.250(7) 3.0508(7) 125(14) 13.3(9) 0.077(12) 1112(174) Epidote, (0,0,3)

30.406(15) 2.9373(14) 212(19) 44(2) 0.184(11) 468(29) Actinolite, (2,2,1)

30.898(8) 2.8917(8) 337(24) 67(2) 0.183(8) 470(21) Epidote, (1,1,2)


32.138(10) 2.7829(8) 183(17) 19.7(18) 0.095(13) 906(125) Epidote, (2,1,1)

32.702(15) 2.7362(12) 117(14) 18.8(16) 0.143(17) 606(72) Actinolite, (3,3,-1)

33.085(9) 2.7053(7) 436(27) 83(3) 0.165(8) 524(27) Actinolite, (1,5,1)

33.383(15) 2.6818(12) 268(21) 49(7) 0.16(3) 542(96) Epidote, (0,1,3)

33.513(5) 2.6717(4) 363(25) 43(7) 0.106(9) 817(68) Epidote, (3,0,0)

33.858(10) 2.6453(7) 130(15) 22.6(18) 0.148(16) 585(62) Epidote, (1,2,0)

34.547(9) 2.5941(7) 346(24) 64.5(18) 0.155(9) 562(32) Epidote, (3,1,-1), 01-080-0521@Actinolite, (0,6,1)

35.117(11) 2.5533(8) 94(13) 42(2) 0.40(2) 219(14) Actinolite, (0,0,2)


37.557(18) 2.3928(11) 164(17) 38(3) 0.215(19) 407(36) Epidote, (3,1,-3), 01-080-0521@Actinolite, (4,0,-1)

37.83(3) 2.3761(17) 136(15) 26(2) 0.18(3) 487(78) Epidote, (2,2,-1), 01-080-0521@Actinolite, (3,5,0)

38.461(13) 2.3387(7) 244(20) 38(2) 0.147(13) 599(53) Actinolite, (3,5,-1)

38.75(3) 2.322(2) 88(12) 16.6(19) 0.18(3) 496(97) Epidote, (3,0,1), 01-080-0521@Actinolite, (4,2,-1)

- 64 -

39.30(2) 2.2907(13) 123(14) 49(2) 0.374(19) 236(12) Epidote, (1,1,3), 01-080-0521@Actinolite, (1,7,-1)






48.076(17) 1.8910(6) 78(11) 12.0(19) 0.13(3) 688(149) Actinolite, (5,1,0)

48.52(2) 1.8749(7) 244(20) 110(3) 0.385(16) 237(10) Epidote, (2,2,2), 01-080-0521@Actinolite, (4,6,-1)

50.51(4) 1.8056(14) 40(8) 13.9(12) 0.31(4) 293(36) Epidote, (4,0,1), 01-080-0521@Actinolite, (5,3,0)


52.41(4) 1.7443(13) 26(7) 6.1(10) 0.20(5) 464(119) Epidote, (4,2,-2), 01-080-0521@Actinolite, (5,1,-2)



- 65 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD10B 8.878218 5.617360 10.121209 90.000000 115.400002 90.000000

Sample 18CD10B 5.340000 5.340000 14.131771 90.000000 90.000000 120.000000

Sample 18CD10B 9.844477 18.041571 5.274609 90.000000 104.699997 90.000000


Epidote 8.878218 5.617360 10.121209 90.000000 115.400002 90.000000


5.340000 5.340000 14.131771 90.000000 90.000000 120.000000

Actinolite 9.844477 18.041571 5.274609 90.000000 104.699997 90.000000


0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

10.5

11

a b

c

Latt

ice

con

sta

nts

(a

ng

.)

Data set

- 66 -



Epidote 9.3(5)

Chlorite-serpentine (NR) 0.000000

Actinolite 91(4)

Sample 18CD10B

0 20 40 60 80

Epidote


Actinolite

Unknown

Wt(%)

- 67 -


Analysis date 11/30/2018 4:22:08 PM Sample name 18CD10C Measurement date 11/30/2018 3:43:30 PM File name Sample 18CD10C.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

10 20 30 40 50

-2000

-1000

0

1000

2000

Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 68 -









Receiving slit #2 -



Graphite-2H C 1.050129646079356 411487 (ICDD)

Magnetite, zincian, syn ( Zn0.35 Fe0.65 ) Fe2 O4 2.954565110732064 10860510 (ICDD)

Anorthoclase ( Na0.667 K0.333 ) ( Al Si3 O8 ) 1.64757833191667 10751630 (ICDD)


3.153277974650493 10703665 (ICDD)

Rutile, syn Ti O2 2.551661768230729 10714809 (ICDD)


Graphite-2H C 194 : P63/mmc 411487 (ICDD)

Magnetite, zincian, syn ( Zn0.35 Fe0.65 ) Fe2 O4 227 : Fd-3m,choice-2 10860510 (ICDD)

Anorthoclase ( Na0.667 K0.333 ) ( Al Si3 O8 ) 2 : C-1 10751630 (ICDD)



Rutile, syn Ti O2 136 : P42/mnm 10714809 (ICDD)

- 69 -

10 20 30 40 50

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

10 20 30 40 50 0

1000

2000

3000

4000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Inte

nsity (

cps)

Graphite-2HMagnetite, zincian, syn

AnorthoclaseMuscovite-2M1, syn

Rutile, syn

- 70 -

Peak list


8.793(2) 10.048(3) 7912(115) 1812(12) 0.164(3) 507(8) Muscovite-2M1, syn, (0,0,2) 13.677(8) 6.469(4) 555(30) 101(6) 0.135(8) 619(39) Anorthoclase, (1,-1,0)

13.890(10) 6.371(4) 475(28) 94(6) 0.148(14) 566(53) Unknown,

14.95(4) 5.920(14) 38(8) 8.8(10) 0.17(5) 500(142) Anorthoclase, (1,1,-1)

17.608(17) 5.033(5) 188(18) 56(2) 0.253(15) 331(20) Muscovite-2M1, syn, (0,0,4) 20.822(12) 4.263(2) 440(27) 114(4) 0.228(9) 370(15) Muscovite-2M1, syn, (1,1,-2) 22.006(13) 4.036(2) 173(17) 54(3) 0.15(4) 558(142) Muscovite-2M1, syn, (1,1,2) 23.245(13) 3.823(2) 112(14) 39(3) 0.31(3) 277(24) Anorthoclase, (1,1,1)

23.538(16) 3.777(2) 296(22) 62(4) 0.171(14) 497(42) Muscovite-2M1, syn, (0,2,3) 24.312(6) 3.6580(9) 243(20) 108(4) 0.39(3) 216(14) Muscovite-2M1, syn, (1,1,3) 25.57(2) 3.480(3) 167(17) 49(3) 0.271(15) 313(17) Anorthoclase, (1,-1,-2)

26.648(5) 3.3424(7) 7065(109) 1700(18) 0.186(6) 457(14) Graphite-2H, (0,0,2), 01-070-3665@Muscovite-2M1, syn, (0,0,6)

27.482(4) 3.2429(4) 8475(119) 1582(17) 0.145(3) 591(14) Muscovite-2M1, syn, (1,1,4) 27.945(4) 3.1902(5) 6938(108) 1308(16) 0.145(4) 588(16) Rutile, syn, (1,1,0)

30.22(3) 2.955(2) 293(22) 123(15) 0.36(3) 238(21) Magnetite, zincian, syn, (2,2,0) 30.48(4) 2.931(4) 151(16) 30(13) 0.15(8) 569(304) Anorthoclase, (0,2,-2)

30.86(2) 2.8952(19) 216(19) 40(6) 0.16(3) 547(109) Anorthoclase, (2,-2,-2), 01-070-3665@Muscovite-2M1, syn, (1,1,5)

31.26(5) 2.859(4) 76(11) 19(3) 0.19(5) 460(135) Anorthoclase, (0,2,2)

34.906(18) 2.5683(13) 83(12) 26(3) 0.23(3) 381(54) Unknown,

35.667(11) 2.5152(7) 496(29) 109(3) 0.148(13) 589(53) Anorthoclase, (2,2,1), 01-070-3665@Muscovite-2M1, syn, (0,0,8)

36.493(13) 2.4601(8) 215(19) 47(3) 0.195(16) 447(35) Anorthoclase, (3,-1,0), 01-071-4809@Rutile, syn, (1,0,1)

37.03(6) 2.426(4) 55(10) 12(2) 0.18(5) 480(138) Magnetite, zincian, syn, (2,2,2), 01-075-1630@Anorthoclase, (1,5,-1), 01-070-3665@Muscovite-2M1, syn, (1,3,3)

37.41(5) 2.402(3) 81(12) 15(3) 0.16(5) 539(173) Anorthoclase, (1,-5,-1), 01-070-3665@Muscovite-2M1, syn, (1,3,-4)

39.450(15) 2.2823(8) 173(17) 26.1(15) 0.142(12) 621(52) Anorthoclase, (2,-4,-2), 01-070-3665@Muscovite-2M1, syn, (1,1,-8)

40.281(11) 2.2371(6) 120(14) 14.2(12) 0.103(12) 858(96) Anorthoclase, (3,-3,-2), 01-070-3665@Muscovite-2M1, syn, (0,4,2)

41.22(3) 2.1885(16) 47(9) 13.6(15) 0.17(6) 535(205) Anorthoclase, (1,3,2), 01-070-3665@Muscovite-2M1, syn, (2,2,2)

41.789(6) 2.1598(3) 685(34) 136(2) 0.161(6) 551(22) Muscovite-2M1, syn, (1,3,5), 01-071-4809@Rutile, syn, (1,1,1)

42.43(2) 2.1284(9) 243(20) 58(3) 0.18(2) 497(65) Graphite-2H, (1,0,0), 01-075-1630@Anorthoclase, (1,5,-2), 01-070-3665@Muscovite-2M1, syn, (1,3,-6)

43.5(2) 2.078(11) 8(4) 4.2(19) 0.4(2) 211(111) Anorthoclase, (1,3,-3), 01-070-3665@Muscovite-2M1, syn, (0,4,4)

44.992(19) 2.0132(8) 196(18) 46(3) 0.219(17) 410(31) Anorthoclase, (3,-1,1), 01-070-3665@Muscovite-2M1, syn, (0,0,10), 01-071-4809@Rutile, syn, (2,1,0)

45.56(3) 1.9893(12) 142(15) 36(5) 0.24(4) 378(61) Muscovite-2M1, syn, (1,3,-7) 45.78(4) 1.9802(14) 95(13) 20(5) 0.19(5) 468(126) Muscovite-2M1, syn, (2,0,6) 47.03(4) 1.9305(16) 31(7) 9(2) 0.27(6) 341(72) Magnetite, zincian, syn, (3,3,1), 01-075-1630@Anorthoclase, (2,4,-3)

48.87(4) 1.8622(13) 72(11) 24.0(17) 0.31(3) 290(28) Anorthoclase, (4,0,0), 01-070-3665@Muscovite-2M1, syn, (1,3,-8)

- 71 -

49.83(6) 1.8284(19) 90(12) 26(6) 0.27(9) 333(113) Anorthoclase, (1,1,3)

50.142(8) 1.8178(3) 401(26) 59(6) 0.139(11) 660(52) Muscovite-2M1, syn, (2,2,6) 50.53(2) 1.8048(7) 162(16) 34.8(19) 0.202(18) 455(40) Anorthoclase, (1,5,2)

51.27(4) 1.7804(13) 74(11) 15.2(15) 0.19(3) 480(84) Anorthoclase, (1,-7,-1), 01-070-3665@Muscovite-2M1, syn, (1,3,8)

53.24(3) 1.7191(8) 72(11) 26(3) 0.18(8) 509(213) Magnetite, zincian, syn, (4,2,2), 01-075-1630@Anorthoclase, (2,-6,1), 01-070-3665@Muscovite-2M1, syn, (1,5,-2)

- 72 -

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD10C 2.462839 2.462839 6.690082 90.000000 90.000000 120.000000

Sample 18CD10C 8.400150 8.400150 8.400150 90.000000 90.000000 90.000000

Sample 18CD10C 8.346477 13.054333 7.199718 91.180000 116.309998 90.139999

Sample 18CD10C 5.297006 9.197246 20.239069 90.000000 95.614998 90.000000

Sample 18CD10C 4.514793 4.514793 2.935935 90.000000 90.000000 90.000000


Graphite-2H 2.462839 2.462839 6.690082 90.000000 90.000000 120.000000

Magnetite, zincian, syn 8.400150 8.400150 8.400150 90.000000 90.000000 90.000000

Anorthoclase 8.346477 13.054333 7.199718 91.180000 116.309998 90.139999

Muscovite-2M1, syn 5.297006 9.197246 20.239069 90.000000 95.614998 90.000000

Rutile, syn 4.514793 4.514793 2.935935 90.000000 90.000000 90.000000


0.5

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Data set

- 73 -



Graphite-2H 32(6)

Magnetite, zincian, syn 2.6(14)

Anorthoclase 34(10)

Muscovite-2M1, syn 8(3)

Rutile, syn 24(5)

Sample 18CD10C

0 20 40 60 80

Graphite-2H

Magnetite, zincian, syn

Anorthoclase

Muscovite-2M1, syn

Rutile, syn

Wt(%)

- 74 -


Analysis date 11/30/2018 4:41:11 PM Sample name 18CD10D Measurement date 11/30/2018 4:11:30 PM File name Sample 18CD10D.raw Operator administrator Comment

Measurement profile

10 20 30 40 50

0.0e+000

5.0e+003

1.0e+004

1.5e+004

10 20 30 40 50

-2000

-1000

0

1000

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Inte

nsity (

cps)

2-theta (deg)

Inte

nsity (

cps)

- 75 -









Receiving slit #2 -



Quartz Si O2 0.7022758946607339 10707344 (ICDD)

Biotite 1M, aluminous barian ( K1.78 Na0.14 Ba0.08 ) ( Mg2.21 Fe1.65 Al1.86 Ti0.28 ) ( Al2.64 Si5.36 O20 ) O2.7 ( O H )1.3

0.8858837736261436 10882193 (ICDD)

Anorthoclase ( Na0.667 K0.333 ) ( Al Si3 O8 ) 1.524569235157798 10751630 (ICDD)


Quartz Si O2 154 : P3221 10707344 (ICDD)

Biotite 1M, aluminous barian ( K1.78 Na0.14 Ba0.08 ) ( Mg2.21 Fe1.65 Al1.86 Ti0.28 ) ( Al2.64 Si5.36 O20 ) O2.7 ( O H )1.3


Anorthoclase ( Na0.667 K0.333 ) ( Al Si3 O8 ) 2 : C-1 10751630 (ICDD)

- 76 -

10 20 30 40 50

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8000

9000

10000

11000

12000

13000

14000

15000

16000

10 20 30 40 50 0

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4000

5000

Inte

gra

ted Inte

nsity (

cps d

eg)

2-theta (deg)

Inte

nsity (

cps)

QuartzBiotite 1M, aluminous barian

Anorthoclase

- 77 -

Peak list


8.843(3) 9.992(3) 9149(123) 1807(15) 0.140(3) 595(13) Biotite 1M, aluminous barian, (0,0,1) 13.945(12) 6.345(5) 346(24) 92(3) 0.148(16) 566(62) Anorthoclase, (1,1,0)

14.99(4) 5.906(17) 30(7) 6.9(15) 0.21(4) 395(74) Unknown,

17.691(7) 5.0092(19) 234(20) 50.0(16) 0.158(10) 533(35) Biotite 1M, aluminous barian, (0,0,2) 20.882(8) 4.2505(16) 625(32) 153(4) 0.221(6) 381(11) Quartz, (1,0,0)

22.091(16) 4.020(3) 263(21) 47(5) 0.169(12) 500(35) Unknown,

22.55(4) 3.940(6) 62(10) 14(3) 0.21(6) 411(126) Biotite 1M, aluminous barian, (1,1,1) 23.601(17) 3.767(3) 361(25) 93(4) 0.15(3) 583(127) Anorthoclase, (1,-3,0)

24.22(3) 3.672(4) 169(17) 59(3) 0.29(2) 295(24) Biotite 1M, aluminous barian, (1,1,-2), 01-075-1630@Anorthoclase, (2,0,0)

25.629(11) 3.4730(14) 329(23) 88(3) 0.196(12) 433(27) Anorthoclase, (1,1,-2)

26.673(6) 3.3394(7) 5007(91) 1266(14) 0.208(5) 411(9) Quartz, (0,1,1), 01-088-2193@Biotite 1M, aluminous barian, (0,0,3)

27.560(7) 3.2339(8) 2237(61) 423(14) 0.130(10) 659(51) Anorthoclase, (0,4,0)

27.999(8) 3.1841(9) 2985(71) 730(17) 0.166(11) 516(33) Anorthoclase, (2,2,0)

29.76(3) 3.000(3) 79(11) 68(7) 0.79(9) 109(12) Anorthoclase, (1,-3,1)

30.54(6) 2.925(5) 112(14) 44(13) 0.36(5) 242(32) Biotite 1M, aluminous barian, (1,1,-3), 01-075-1630@Anorthoclase, (1,3,1)

30.913(17) 2.8903(16) 183(17) 23(5) 0.11(3) 768(183) Anorthoclase, (0,2,-2)

31.33(7) 2.852(6) 53(9) 10(3) 0.17(4) 510(126) Anorthoclase, (0,4,1)

32.31(3) 2.768(3) 33(7) 23(3) 0.62(11) 140(24) Anorthoclase, (1,3,-2)

34.27(16) 2.615(12) 54(10) 63(9) 1.1(2) 80(15) Biotite 1M, aluminous barian, (2,0,-1) 34.564(14) 2.5929(10) 207(19) 22(2) 0.099(14) 878(127) Unknown,

35.04(6) 2.558(4) 51(9) 15(4) 0.27(7) 319(81) Anorthoclase, (2,4,-1)

35.43(4) 2.532(3) 141(15) 55(8) 0.37(4) 238(23) Biotite 1M, aluminous barian, (1,1,3), 01-075-1630@Anorthoclase, (1,-1,2)

35.714(11) 2.5120(7) 472(28) 64(5) 0.128(13) 680(66) Biotite 1M, aluminous barian, (2,0,-2) 36.57(2) 2.4550(13) 178(17) 48(2) 0.252(14) 347(20) Quartz, (1,1,0), 01-075-1630@Anorthoclase, (2,-4,0)

37.46(6) 2.399(4) 48(9) 11.5(15) 0.22(4) 392(72) Anorthoclase, (1,-5,-1)

39.500(10) 2.2795(6) 236(20) 36.9(16) 0.118(11) 747(70) Quartz, (1,0,2), 01-088-2193@Biotite 1M, aluminous barian, (2,2,0), 01-075-1630@Anorthoclase, (2,-4,-2)

40.329(11) 2.2345(6) 138(15) 18.3(11) 0.116(12) 761(75) Quartz, (1,1,1)

41.276(16) 2.1854(8) 67(11) 15.3(14) 0.17(2) 520(75) Unknown,

41.738(8) 2.1623(4) 244(20) 46.5(18) 0.145(11) 614(47) Anorthoclase, (3,-3,0)

42.486(10) 2.1259(5) 307(23) 52(3) 0.145(13) 615(54) Quartz, (2,0,0), 01-075-1630@Anorthoclase, (3,-1,-3)

42.700(14) 2.1158(7) 160(16) 33(3) 0.185(16) 482(42) Anorthoclase, (1,5,-2)

43.769(11) 2.0665(5) 72(11) 8.2(8) 0.104(14) 864(117) Anorthoclase, (2,4,1)

45.068(13) 2.0099(5) 265(21) 57(3) 0.197(11) 455(25) Biotite 1M, aluminous barian, (0,0,5), 01-075-1630@Anorthoclase, (3,-1,1)

45.81(3) 1.9792(13) 90(12) 62(3) 0.64(4) 141(9) Quartz, (2,0,1), 01-088-2193@Biotite 1M, aluminous barian, (2,0,-4), 01-075-1630@Anorthoclase, (3,1,1)

- 78 -

48.3(2) 1.882(8) 14(5) 8.3(18) 0.57(19) 161(55) Anorthoclase, (3,-5,-1)

50.198(7) 1.8159(2) 638(33) 103(4) 0.123(8) 747(50) Quartz, (1,1,2)

50.615(18) 1.8019(6) 145(16) 36(2) 0.22(2) 426(49) Quartz, (0,0,3), 01-075-1630@Anorthoclase, (2,6,-2)

Lattice constants

Angular correction

No correction



Analysis results


Sample 18CD10D 4.917765 4.917765 5.407237 90.000000 90.000000 120.000000

Sample 18CD10D 5.333321 9.236875 10.238814 90.000000 100.029999 90.000000

Sample 18CD10D 8.292087 12.969264 7.152801 91.180000 116.309998 90.139999


Quartz 4.917765 4.917765 5.407237 90.000000 90.000000 120.000000

Biotite 1M, aluminous barian

5.333321 9.236875 10.238814 90.000000 100.029999 90.000000

Anorthoclase 8.292087 12.969264 7.152801 91.180000 116.309998 90.139999

Sample 18CD10D Sample 18CD10D 0

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Data set

- 79 -



Quartz 11.7(5)

Biotite 1M, aluminous barian 58.8(15)

Anorthoclase 29.5(15)

Sample 18CD10D

0 20 40 60 80

Quartz

Biotite 1M, aluminous barian

Anorthoclase

Unknown

Wt(%)

appendix 3 xrd data analysis results - university of vermont

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