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April 17, 2012Volume 84, Issue 8Pages 3485-3856

LETTERS TO ANALYTICAL CHEMISTRY

ARTICLES

ADDITIONS AND CORRECTIONS

In this issue:

About the Cover: The cover depicts a new approach to analyzing dried blood spot (DBS) samples relying ocoupled to tandem mass spectrometry. The device pictured contains several reagent dra DBS punch adjacent to a pulled glass capillary nanoelectrospray emitter. Artwork by Sthe article.

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LETTERS TO ANALYTICAL CHEMISTRY

Section: Biochemical Methods

Disposable Immunochips for the Detection of Legionella pneumophila Using Electrochemical Impedance SpectroscopyNan Li, Arujun Brahmendra, Anthony J. Veloso, Akriti Prashar, Xin R. Cheng, Vinci W. S. Hung, Cyril Guyard, Mauricio Terebiznik, and Kagan Kerman

pp 3485–3488Publication Date (Web): March 16, 2012 (Letter)DOI: 10.1021/ac3003227

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Anal. Chem.

of 13Analytical Chemistry: Volume 84, Issue 8 (ACS Publications)

13/4/2555http://pubs.acs.org/toc/ancham/84/8

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Stabilizing Nanometer Scale Tip-to-Substrate Gaps in Scanning Electrochemical Microscopy Using an Isothermal Chamber for Thermal Drift SuppressionJiyeon Kim, Mei Shen, Nikoloz Nioradze, and Shigeru Amemiya

pp 3489–3492Publication Date (Web): March 31, 2012 (Letter)DOI: 10.1021/ac300564g

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ARTICLES


High Ion Yields of Carbohydrates from Frozen Solution by UV-MALDIChi-Wei Liang, Po-Jul Chang, Yu-Jiun Lin, Yuan-Tseh Lee, and Chi-Kung Ni

pp 3493–3499Publication Date (Web): March 14, 2012 (Article)DOI: 10.1021/ac3000896

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Ultrafast Kinetic DNA Hybridization Assay Based on the Visualization of Threshold TurbidityXin Shu, Jingzhi Lu, Haipeng Lv, Xu Zhang, Yishu Yan, Jingjing Sun, and Jin Zhu

pp 3500–3506Publication Date (Web): March 29, 2012 (Article)DOI: 10.1021/ac300824a

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Sensitive and Homogeneous Protein Detection Based on Target-Triggered Aptamer Hairpin Switch and Nicking Enzyme Assisted Fluorescence Signal AmplificationLiyun Xue, Xiaoming Zhou, and Da Xing


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Quantitation of Spatially-Localized Proteins in Tissue Samples using MALDI-MRM ImagingElizabeth J. Clemis, Derek S. Smith, Alexander G. Camenzind, Ryan M. Danell, Carol E. Parker, and Christoph H. Borchers

pp 3514–3522Publication Date (Web): February 21, 2012 (Article)DOI: 10.1021/ac202875d

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Section: Immunochemistry

Direct Detection of Antibody Concentration and Affinity in Human Serum Using Microscale ThermophoresisSvenja Lippok, Susanne A. I. Seidel, Stefan Duhr, Kerstin Uhland, Hans-Peter Holthoff, Dieter Jenne, and Dieter Braun

pp 3523–3530Publication Date (Web): March 7, 2012 (Article)DOI: 10.1021/ac202923j

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Section: Electrochemistry

Forced Convection during Feedback Approach Curve Measurements in Scanning Electrochemical Microscopy: Maximal Displacement Velocity with a MicrodiskR. Cornut, S. Poirier, and Janine Mauzeroll

pp 3531–3537Publication Date (Web): March 5, 2012 (Article)DOI: 10.1021/ac203047d

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Microfluidic Digital Isoelectric Fractionation for Rapid Multidimensional Glycoprotein AnalysisJunyu Mai, Gregory J. Sommer, and Anson V. Hatch

pp 3538–3545Publication Date (Web): February 27, 2012 (Article)DOI: 10.1021/ac203076p

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Dual Photonic-Electrochemical Lab on a Chip for Online Simultaneous Absorbance and Amperometric MeasurementsOlga Ordeig, Pedro Ortiz, Xavier Muñoz-Berbel, Stefanie Demming, Stephanus Büttgenbach, César Fernández-Sánchez, and Andreu Llobera

pp 3546–3553Publication Date (Web): March 19, 2012 (Article)DOI: 10.1021/ac203106x

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Label-Free Fluorescent Detection of Ions, Proteins, and Small Molecules Using Structure-Switching Aptamers, SYBR Gold, and Exonuclease IDongmei Zheng, Ruxing Zou, and Xinhui Lou

pp 3554–3560Publication Date (Web): March 16, 2012 (Article)DOI: 10.1021/ac300690r

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Section: Optical, Electron, and Mass Spectroscopy and Other Related Properties

Spatially Resolved Scattering Correlation Spectroscopy Using a Total Internal Reflection ConfigurationHeng Liu, Chaoqing Dong, Xiangyi Huang, and Jicun Ren


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Pd Nanowires as New Biosensing Materials for Magnified Fluorescent Detection of Nucleic AcidLibing Zhang, Shaojun Guo, Shaojun Dong, and Erkang Wang


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Synthesis and Characterization of a Disulfide Reporter Molecule for Enhancing pH Measurements Based on Surface-Enhanced Raman ScatteringLatevi Lawson and Thomas Huser

pp 3574–3580Publication Date (Web): March 20, 2012 (Article)DOI: 10.1021/ac203103s

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Section: Toxicology

Ammunition Identification by Means of the Organic Analysis of Gunshot Residues Using Raman SpectroscopyMaría López-López, Juan José Delgado, and Carmen García-Ruiz

pp 3581–3585Publication Date (Web): March 15, 2012 (Article)DOI: 10.1021/ac203237w

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Section: Air Pollution and Industrial Hygiene

Conductivity for Soot Sensing: Possibilities and LimitationsBenedikt Grob, Johannes Schmid, Natalia P. Ivleva, and Reinhard Niessner

pp 3586–3592Publication Date (Web): March 19, 2012 (Article)DOI: 10.1021/ac203152z

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Section: Enzymes

Luciferase-Based Assay for Adenosine: Application to S-Adenosyl-L-homocysteine HydrolaseEmmanuel S. Burgos, Shivali A. Gulab, María B. Cassera, and Vern L. Schramm


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Massively Parallel Single-Molecule and Single-Cell Emulsion Reverse Transcription Polymerase Chain Reaction Using Agarose Droplet MicrofluidicsHuifa Zhang, Gareth Jenkins, Yuan Zou, Zhi Zhu, and Chaoyong James Yang


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Imaging the Material Properties of Bone Specimens Using Reflection-Based Infrared MicrospectroscopyAlvin S. Acerbo, G. Lawrence Carr, Stefan Judex, and Lisa M. Miller

pp 3607–3613Publication Date (Web): March 13, 2012 (Article)DOI: 10.1021/ac203375d

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Enzymatic Immuno-Assembly of Gold Nanoparticles for Visualized Activity Screening of Histone-Modifying EnzymesZhen Zhen, Li-Juan Tang, Haoxu Long, and Jian-Hui Jiang

pp 3614–3620Publication Date (Web): March 29, 2012 (Article)DOI: 10.1021/ac203385v



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N-Glycan Profiling by Microchip Electrophoresis to Differentiate Disease States Related to Esophageal AdenocarcinomaIndranil Mitra, Zexi Zhuang, Yuening Zhang, Chuan-Yih Yu, Zane T. Hammoud, Haixu Tang, Yehia Mechref, and Stephen C. Jacobson


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Classification of Cultivation Locations of Panax quinquefolius L Samples using High Performance Liquid Chromatography–Electrospray Ionization Mass Spectrometry and Chemometric AnalysisXiaobo Sun, Pei Chen, Shannon L. Cook, Glen P. Jackson, James M. Harnly, and Peter B. Harrington


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Section: Electric Phenomena

Cold Electron Source with an Electron Multiplier Illuminated by Ultraviolet PhotonsHyun Sik Kim, Seung Yong Kim, and Mo Yang

pp 3635–3639Publication Date (Web): March 12, 2012 (Article)DOI: 10.1021/ac203486u

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SubSection: Inorganic Analytical Chemistry

Determination of the Hydrogen Isotopic Compositions of Organic Materials and Hydrous Minerals Using Thermal Combustion Laser SpectroscopyGeoff Koehler and Leonard I. Wassenaar


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Quantum Dot/Carrier–Protein/Haptens Conjugate as a Detection Nanobioprobe for FRET-Based Immunoassay of Small Analytes with All-Fiber Microfluidic Biosensing PlatformFeng Long, Chunmei Gu, April Z. Gu, and Hanchang Shi


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Spectroscopic Characterization of Coumarin-Stained Beads: Quantification of the Number of Fluorophores Per Particle with Solid-State 19F-NMR and Measurement of Absolute Fluorescence Quantum YieldsAlexandra Huber, Thomas Behnke, Christian Würth, Christian Jaeger, and Ute Resch-Genger


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Triple Signal Amplification of Graphene Film, Polybead Carried Gold Nanoparticles as Tracing Tag and Silver Deposition for Ultrasensitive Electrochemical ImmunosensingDajie Lin, Jie Wu, Min Wang, Feng Yan, and Huangxian Ju


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Section: Optical, Electron, and Mass Spectroscopy and Other Related Properties

Peak–Peak Repulsion in Ion Mobility SpectrometryVahideh Ilbeigi and Mahmoud Tabrizchi


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Section: Industrial Carbohydrates

Positron Lifetime Reveals the Nano Level Packing in Complex Polysaccharide-Rich Hydrolysate MatrixesUlrica Edlund, Yang Yu, Yingzhi Zhu Ryberg, Reinhard Krause-Rehberg, and Ann-Christine Albertsson

pp 3676–3681Publication Date (Web): March 20, 2012 (Article)DOI: 10.1021/ac300152g

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Biopolymer System for Cell Recovery from Microfluidic Cell Capture DevicesAjay M. Shah, Min Yu, Zev Nakamura, Jordan Ciciliano, Matthew Ulman, Kenneth Kotz, Shannon L. Stott, Shyamala Maheswaran, Daniel A. Haber, and Mehmet Toner

pp 3682–3688Publication Date (Web): March 10, 2012 (Article)DOI: 10.1021/ac300190j

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Section: Enzymes

Activity-Based Probes Linked with Laser-Cleavable Mass Tags for Signal Amplification in Imaging Mass Spectrometry: Analysis of Serine Hydrolase Enzymes in Mammalian TissueJunhai Yang, Pierre Chaurand, Jeremy L. Norris, Ned A. Porter, and Richard M. Caprioli


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Section: Magnetic Phenomena

Contactless NMR Spectroscopy on a ChipHerbert Ryan, Suk-Heung Song, Anja Zaß, Jan Korvink, and Marcel Utz


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Section: Toxicology

Amplified Surface Plasmon Resonance and Electrochemical Detection of Pb2+ Ions Using the Pb2+-Dependent DNAzyme and Hemin/G-Quadruplex as a LabelGilad Pelossof, Ran Tel-Vered, and Itamar Willner


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Section: Inorganic Analytical Chemistry

Ultra-High-Sensitive Extraction-Photometric Determination of Sodium Ion Using Flow Injection Analysis with a Chromogenic Calix[4]arene Derivative and a Laser Interferometric Photothermal DetectorDaisuke Tsuda, Yoshio Nakahara, Koji Machitani, Masato Kannaka, Eiji Takahashi, and Keiichi Kimura

pp 3710–3715Publication Date (Web): March 15, 2012 (Article)DOI: 10.1021/ac300250b

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Carbonyl-Reactive Tandem Mass Tags for the Proteome-Wide Quantification of N-Linked GlycansHannes Hahne, Patrick Neubert, Karsten Kuhn, Chris Etienne, Ryan Bomgarden, John C. Rogers, and Bernhard Kuster

pp 3716–3724Publication Date (Web): March 28, 2012 (Article)DOI: 10.1021/ac300197c

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Section: Pharmacology

Anti-Viral Inhibitor Binding to Influenza Neuraminidase by MALDI Mass SpectrometryKavya Swaminathan and Kevin M. Downard


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Dried Blood Spot Analysis by Digital Microfluidics Coupled to Nanoelectrospray Ionization Mass SpectrometrySteve C. C. Shih, Hao Yang, Mais J. Jebrail, Ryan Fobel, Nathan McIntosh, Osama Y. Al-Dirbashi, Pranesh Chakraborty, and Aaron R. Wheeler


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Fluorescently Cationic Conjugated Polymer as an Indicator of Ligase Chain Reaction for Sensitive and Homogeneous Detection of Single Nucleotide PolymorphismYongqiang Cheng, Qing Du, Liyong Wang, Hailian Jia, and Zhengping Li


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Section: Inorganic Analytical Chemistry

Inkjet Printing of Nanoporous Gold Electrode Arrays on Cellulose Membranes for High-Sensitive Paper-Like Electrochemical Oxygen Sensors Using Ionic Liquid ElectrolytesChengguo Hu, Xiaoyun Bai, Yingkai Wang, Wei Jin, Xuan Zhang, and Shengshui Hu


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Section: Organic Analytical Chemistry

Sample Treatment Considerations in the Analysis of Organic Colorants by Surface-Enhanced Raman ScatteringFederica Pozzi, John R. Lombardi, Silvia Bruni, and Marco Leona


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Section: Biochemical Genetics

Multiplex Loop-Mediated Isothermal Amplification Detection by Sequence-Based Barcodes Coupled with Nicking Endonuclease-Mediated PyrosequencingChao Liang, Yanan Chu, Sijia Cheng, Haiping Wu, Tomoharu Kajiyama, Hideki Kambara, and Guohua Zhou


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Section: Surface Chemistry and Colloids

Adsorption of Cd2+ on Carboxyl-Terminated Superparamagnetic Iron Oxide NanoparticlesZhange Feng, Shun Zhu, Denis Ricardo Martins de Godoi, Anna Cristina S. Samia, and Daniel Scherson

pp 3764–3770Publication Date (Web): March 18, 2012 (Article)DOI: 10.1021/ac300392k

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Measuring Dynamics in Weakly Structured Regions of Proteins Using Microfluidics-Enabled Subsecond H/D Exchange Mass SpectrometryTamanna Rob, Peter Liuni, Preet Kamal Gill, Shaolong Zhu, Naresh Balachandran, Paul J. Berti, and Derek J. Wilson

pp 3771–3779Publication Date (Web): March 29, 2012 (Article)DOI: 10.1021/ac300365u

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Gravitational Sedimentation Induced Blood Delamination for Continuous Plasma Separation on a Microfluidics ChipXian-Bo Zhang, Zeng-Qiang Wu, Kang Wang, Jie Zhu, Jing-Juan Xu, Xing-Hua Xia, and Hong-Yuan Chen


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Section: Toxicology

Quantification of Four Major Metabolites of Embryotoxic N-Methyl- and N-Ethyl-2-pyrrolidone in Human Urine by Cooled-Injection Gas Chromatography and Isotope Dilution Mass SpectrometryBirgit K. Schindler, Stephan Koslitz, Swetlana Meier, Vladimir N. Belov, Holger M. Koch, Tobias Weiss, Thomas Brüning, and Heiko U. Käfferlein

pp 3787–3794Publication Date (Web): March 21, 2012 (Article)DOI: 10.1021/ac300439w

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Electrothermal Supercharging of Proteins in Native Electrospray IonizationHarry J. Sterling, Catherine A. Cassou, Anna C. Susa, and Evan R. Williams

pp 3795–3801Publication Date (Web): March 12, 2012 (Article)DOI: 10.1021/ac300468a

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Section: Air Pollution and Industrial Hygiene

NIST Gravimetrically Prepared Atmospheric Level Methane in Dry Air Standards SuiteGeorge C. Rhoderick, Jennifer Carney, and Franklin R. Guenther


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Nontargeted Nucleotide Analysis Based on Benzoylhistamine Labeling-MALDI-TOF/TOF-MS: Discovery of Putative 6-Oxo-Thymine in DNAPoguang Wang, David Fisher, Anjana Rao, and Roger W. Giese


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TECHNICAL NOTES

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Section: Pharmaceutical Analysis

Evaluation of Infrared-Reflection Absorption Spectroscopy Measurement and Locally Weighted Partial Least-Squares for Rapid Analysis of Residual Drug Substances in Cleaning ProcessesHiroshi Nakagawa, Takahiro Tajima, Manabu Kano, Sanghong Kim, Shinji Hasebe, Tatsuya Suzuki, and Hiroaki Nakagami

pp 3820–3826Publication Date (Web): March 13, 2012 (Technical Note)DOI: 10.1021/ac202443a


Hierarchically Driven IrO2 Nanowire Electrocatalysts for Direct Sensing of BiomoleculesJun Ho Shim, Yumin Lee, Minkyung Kang, Jaeyeon Lee, Jeong Min Baik, Youngmi Lee, Chongmok Lee, and Myung Hwa Kim

pp 3827–3832Publication Date (Web): March 21, 2012 (Technical Note)DOI: 10.1021/ac300573b

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Electron Paramagnetic Resonance-Based pH Mapping Using Spectral-Spatial Imaging of Sequentially Scanned SpectraShunichi Koda, Jonathan Goodwin, Valery V. Khramtsov, Hirotada Fujii, and Hiroshi Hirata

pp 3833–3837Publication Date (Web): March 15, 2012 (Technical Note)DOI: 10.1021/ac203415w

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Electrochemistry-Assisted Top-Down Characterization of Disulfide-Containing ProteinsYun Zhang, Weidong Cui, Hao Zhang, Howard D. Dewald, and Hao Chen

pp 3838–3842Publication Date (Web): March 26, 2012 (Technical Note)DOI: 10.1021/ac300106y

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Evaluation of High Resolution Magic-Angle Coil Spinning NMR Spectroscopy for Metabolic Profiling of Nanoliter Tissue BiopsiesAlan Wong, Beatriz Jiménez, Xiaonan Li, Elaine Holmes, Jeremy K. Nicholson, John C. Lindon, and Dimitris Sakellariou

pp 3843–3848Publication Date (Web): March 22, 2012 (Technical Note)DOI: 10.1021/ac300153k

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ADDITIONS AND CORRECTIONS



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High-Throughput Analysis of Protein–Protein Interactions in Picoliter-Volume Droplets Using Fluorescence PolarizationJae-Won Choi, Dong-Ku Kang, Hyun Park, Andrew J. deMello, and Soo-Ik Chang

pp 3849–3854Publication Date (Web): March 25, 2012 (Technical Note)DOI: 10.1021/ac300414g

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Correction to Rapid Identification and Quantification of Tumor Cells Using an Electrocatalytic Method Based on Gold NanoparticlesAlfredo de la Escosura-Muñiz, Christian Sánchez-Espinel, Belén Díaz-Freitas, África González-Fernández, Marisa Maltez-da Costa, and Arben Merkoçi

pp 3855–3855Publication Date (Web): March 28, 2012 (Addition/Correction)DOI: 10.1021/ac3007957

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