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Supplementary File

Synthesis, Characterization and Antimicrobial Studies of Novel Series of 2,4-

bis(hydrazino)-6-substituted-1,3,5-Triazine and Their Schiff Base Derivatives

Hessa H. Al-Rasheed, Essam N. Sholkamy, Monirah Al Alshaikh, Mohammed R. H. Siddiqui , Ahmed S. Al-Obaidi and Ayman El-Faham*

Table of content

Figure S1: 1H NMR and 13 C NMR for 4a

Figure S2: 1H NMR and 13 C NMR for 4b

Figure S3: 1H NMR and 13 C NMR for 4c

Figure S4: 1H NMR and 13 C NMR for 4d

Figure S5: 1H NMR and 13 C NMR for 4e

Figure S6: 1H NMR and 13 C NMR for 4f

Figure S7: 1H NMR and 13 C NMR for 4g

Figure S8: 1H NMR and 13 C NMR for 4h

Figure S9: 1H NMR and 13 C NMR for 4i

Figure S10: 1H NMR and 13 C NMR for 4j

Figure S11: 1H NMR and 13 C NMR for 4k

Figure S12: 1H NMR and 13 C NMR for 4l

Figure S13: 1H NMR and 13 C NMR for 4m

Figure S14: 1H NMR and 13 C NMR for 5a

Figure S15: 1H NMR and 13 C NMR for 5b

Figure S16: 1H NMR for 5c

Figure S17: 1H NMR and 13 C NMR for 5d

Figure S18: 1H NMR and 13 C NMR for 5e

Figure S19: 1H NMR and 13 C NMR for 5f

Figure S20: 1H NMR and 13 C NMR for 5g

Figure S21: 1H NMR and 13 C NMR for 5h

Figure S22: 1H NMR and 13 C NMR for 5i

Figure S23: 1H NMR and 13 C NMR for 6a

Figure S24: LC-MS for 6a

Figure S25: 1H NMR and 13 C NMR for 6b

Figure S26: 1H NMR and 13 C NMR for 6c

Figure S27: 1H NMR and 13 C NMR for 6d

Figure S28: 1H NMR and 13 C NMR for 6e

Figure S29: 1H NMR and 13 C NMR for 6f

Figure S30: 1H NMR and 13 C NMR for 6g

Figure S31: 1H NMR and 13 C NMR for 6h

Figure S32: 1H NMR and 13 C NMR for 6i

Figure S33: 1H NMR and 13 C NMR for 7a

Figure S34: 1H NMR and 13 C NMR for 7b

Figure S35: 1H NMR and 13 C NMR for 7c

Figure S36: 1H NMR for 7d

Figure S37: 1H NMR and 13 C NMR for 7e

Figure S38: 1H NMR and 13 C NMR for 7f

Figure S39: 1H NMR and 13 C NMR for 7g

Figure S40: 1H NMR and 13 C NMR for 7h

Figure S41: 1H NMR and 13 C NMR for 7i

Figure S42: LC-MS for 7i

Figure S43: 1H NMR and 13 C NMR for 8a

Figure S44: 1H NMR and 13 C NMR for 8b

Figure S45: 1H NMR and 13 C NMR for 8c

Figure S46: 1H NMR and 13 C NMR for 8d

Figure S47: 1H NMR and 13 C NMR for 8e

Figure S48: 1H NMR and 13 C NMR for 8f

Figure S49: 1H NMR and 13 C NMR for 8g

Figure S50: LC-MS for 7a

Figure S51: LC-MS for 7d

Figure S52: LC-MS for 7f

Figure S1: Supplementary spectrum for compound 4a (1H and 13C)

Figure S2: Supplementary spectrum for compound 4b (1H and 13C)

Figure S3: Supplementary spectrum for compound 4c (1H and 13C)

Figure S4: Supplementary spectrum for compound 4d (1H and 13C)

Figure S5: Supplementary spectrum for compound 4e (1H and 13C)

Figure S6: Supplementary spectrum for compound 4f (1H and 13C)

Figure S7: Supplementary spectrum for compound 4g (1H and 13C)

Figure S8: Supplementary spectrum for compound 4h (1H and 13C)

Figure S9: Supplementary spectrum for compound 4i (1H and 13C)

Figure S10: Supplementary spectrum for compound 4j (1H and 13C)

Figure S11: Supplementary spectrum for compound 4k (1H and 13C)

Figure S12: Supplementary spectrum for compound 4l (1H and 13C)

Figure S13: Supplementary spectrum for compound 4m (1H and 13C)

Figure S14: Supplementary spectrum for compound 5a (1H and 13C)

Figure S15: Supplementary spectrum for compound 5b (1H and 13C)

Figure S16: Supplementary spectrum for compound 5c (1H NMR)

Figure S17: Supplementary spectrum for compound 5d (1H and 13C)

Figure S18: Supplementary spectrum for compound 5e (1H and 13C)

Figure S19: Supplementary spectrum for compound 5f (1H and 13C)

Figure S20: Supplementary spectrum for compound 5g (1H and 13C)

Figure S21: Supplementary spectrum for compound 5h (1H and 13C)

Figure S22: Supplementary spectrum for compound 5i (1H and 13C)

Figure S23: Supplementary spectrum for compound 6a (1H and 13C)

Figure S24: LC-MS for compound 6a

Figure S25: Supplementary spectrum for compound 6b (1H and 13C)

Figure S26: Supplementary spectrum for compound 6c (1H and 13C)

Figure S27: Supplementary spectrum for compound 6d (1H and 13C)

Figure S28: Supplementary spectrum for compound 6e (1H and 13C)

Figure S29: Supplementary spectrum for compound 6f (1H and 13C)

Figure S30: Supplementary spectrum for compound 6g (1H and 13C)

Figure S31: Supplementary spectrum for compound 6h (1H and 13C)

Figure S32: Supplementary spectrum for compound 6i (1H and 13C)

Figure S33: Supplementary spectrum for compound 7a (1H and 13C)

Figure S34: Supplementary spectrum for compound 7b (1H and 13C)

Figure S35: Supplementary spectrum for compound 7c (1H and 13C)

Figure S36: Supplementary spectrum for compound 7d (1H NMR)

Figure S37: Supplementary spectrum for compound 7e (1H and 13C)

Figure S38: Supplementary spectrum for compound 7f (1H and 13C)

Figure S39: Supplementary spectrum for compound 7g (1H and 13C)

Figure S40: Supplementary spectrum for compound 7h (1H and 13C)

Figure S41: Supplementary spectrum for compound 7i (1H and 13C)

Figure S42: LC-MS for compound 7i

Figure S43: Supplementary spectrum for compound 8a (1H and 13C)

Figure S44: Supplementary spectrum for compound 8b (1H and 13C)

Figure S45: Supplementary spectrum for compound 8c (1H and 13C)

Figure S46: Supplementary spectrum for compound 8d (1H and 13C)

Figure S47: Supplementary spectrum for compound 8e (1H and 13C)

Figure S48: Supplementary spectrum for compound 8f (1H and 13C)

Figure S49: Supplementary spectrum for compound 8g (1H and 13C)

Figure S50: LC-MS for 7a

Figure S51: LC-MS for 7d

Figure S51: LC-MS for 7f