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Contaminations,Contaminations, Toxins Toxins and Pesticide and Pesticide Residues in Fruit JuiceResidues in Fruit JuiceResidues in Fruit JuiceResidues in Fruit Juice
ปรารถนา ตั้งตรีรัตน นักวิชาการ
ห&องปฏิบัตกิารชีวเคมีและจุลชีววิทยา
ศูนย ทดสอบและมาตรวิทยา
สถาบนัวิจยัวิทยาศาสตร และเทคโนโลยแีห9งประเทศไทย1
Contaminations and ToxinContaminations and Toxin
Mycotoxins
Metals
2
Radionuclides
Others – Melamine,
Vinylchloride monomer
• Toxic Element
Arsenic Cadmium Lead
• Containers-Juice cartons-Plastic bottle
Source:
Metals
4
Lead Mercury MethylmercuryTin
-Plastic bottle-Glass bottle-Cans
• Environments air, land, and water by human activities
Pesticide Residues : EU Pesticide Residues : EU -- maximum residue levels of maximum residue levels of
pesticides (MRLs)pesticides (MRLs)
16http://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/public/?event=product.selection&language=EN
Pesticide Residues : EU Pesticide Residues : EU -- maximum residue levels of pesticides (MRLs)maximum residue levels of pesticides (MRLs)
17http://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/public/?event=product.selection&language=EN
Pesticide Residues: FDA Pesticide Residues: FDA
18https://www.fda.gov/food/foodborneillnesscontaminants/pesticides/default.htm
Pesticide Residues: Analytical Method(EU) Pesticide Residues: Analytical Method(EU)
• EN16552 : 2018 Foods of plant origin. Multimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE. Modular QuEChERS-method
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clean-up by dispersive SPE. Modular QuEChERS-method
• SANTE/11813/2017 Guidance document on analytical quality control and method validation procedures for pesticide residues and analysis in food and feed.
Toxic element : Analytical Method Toxic element : Analytical Method
- AOAC 972.25 Pb
- AOAC 985.16 Tin in Cans
- AOAC 2011.14 Calcium, Copper, Iron, Magnesium, Manganese, Potassium, Phosphorus,
Sodium, and Zinc in Fortified Food Products.
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Sodium, and Zinc in Fortified Food Products.
- AOAC 2013.06 Arsenic, Cadmium, Mercury, and Lead in Foods by Pressure Digestion and
Inductively Coupled Plasma/Mass Spectrometry.
- AOAC SMPR ® 2015.006 Standard Method Performance Requirements for Quantitation of Arsenic
Species in Selected Foods and Beverages
- IFU N0. R06 Determination of Heavy Metals (2000)
MycotoxinsMycotoxins : Analytical Method : Analytical Method
• IFU No. R02 Determination of Patulin (2005)
• EN 14177:2003 Determination of patulin in clear and cloudy apple juice and puree. HPLC
method with liquid/liquid partition clean-up
• EN 14132:2009 Foodstuffs. Determination of ochratoxin A in barley and roasted coffee. HPLC
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• EN 14132:2009 Foodstuffs. Determination of ochratoxin A in barley and roasted coffee. HPLC
method with immunoaffinity column clean-up
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