closure report for housekeeping category corrective action
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NevadaDOE/NV/l 1718--289
EnvironmentalRestorationProject
Closure ReportFor Housekeeping CategoryCorrective Action Unit 297Nevada Test Site, Nevada
Controlled Copy Number:
Revision: O
March 1999
Distribution A - Approved for public release; further dissemination unlimited.
Environmental RestorationDivision— —=2$&&
U.S. Department of EnergyNevada Operations Office
Available to the public from:
U. S. Department of CommerceNational Technical Information Service5285 Port Royal RoadSpringfield, VA 22161(703) 487-4650
Available electronically at http://www.doe.~ ov/bridgQ Available to the U.S. Department ofEnergy and its contractors in paper from:
U.S. Department of EnergyOffIce of Scientific and Technical InformationP.O. BOX 62Oak Ridge, TN 37831-0062(423) 576-8401.
Reference herein to any specific commercial product, process, or service by trade name,trademark, manufacturer, or otherwise, does not necessarily constitute or imply its endorsement,recommendation, or favoring by the U.S. Government or any agency thereof or its contractors orsubcontractors.
DOE/NV/l 1718--289
CLOSURE REPORTFOR HOUSEKEEPING CATEGORY
CORRECTIVE ACTION UNIT 297NEVADA TEST SITE, NEVADA
Controlled Copy No.:
Revision: O
Prepared for:U.S. Department of EnergyNevada Operations Office
Under Contract No. DE-AC08-96NV11718
March 1999
closure Report - CAU 297EW vacuumhllllpoil RCCOVqProjectSummaryRevision ODate: Msrch 18.1999
PROJECT SUMMARY
Corrective Action Unit (CAU) 297 is located at the Nevada Test Site Area 25 EngineMaintenance and Disassembly Building (Building 3900). The CAU consists of one CorrectiveAction Site (CAS) 25-25-01 which includes two 38-liter (l O-gallon) metal containers used in aclosed vacuum pump oil recovery system for recirculating oil.
Closure for this site was completed on December 1, 1998 under the guidance of theHousekeeping Category Work Plan (Department of Energy, Nevada Operations Office, 1996) bycompleting the following activities:
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Two 38-liter (1O-gallon) metal containers were removed.
Associated piping was cut, removed, and sealed.
Soil containing petroleum hydrocarbons were excavated to a maximum depth ofapproximately 46 centimeters(18 inches).
The tanks, associated piping, and impacted soil were disposed of in the Area 6 HydrocarbonLandfill on January 14, 1999.
Completing the closure activities at the site identified a hydrocarbon release associated withhistorical operations of the oil recovery system. The petroleum impacted soils are located in asignificant power/utility corridor feeding into the building. The first of the underground utilitieswere identified at a depth of approximately 1 meter (3 feet) below ground surface. Due to theextent of the impacted area, confining work space limitations, proximity to utility lines, andlimitations to the amount of excavated material for housekeeping closure activities, excavationactivities were discontinued. Clean soil was used to bacldlll over the excavated area.
Following the closure requirements of the Housekeeping Work Plan, only one verification soilsample was collected below the removed containers and piping (EMAD-VPOR-1 ). Additionalsamples were collected for quality control (EMAD-VPOR-2) and waste disposition purposes.Samples were analyzed for total petroleum hydrocarbons, Toxicity Characteristic LeachingProcedure (TCLP) volatile organic compounds, TCLP semi-volatile organic compounds, TCLPmetals, polychlorinated biphenyls, and organochlorine pesticides.
The soil sample collected below the oil recovery containers and piping contained petroleumhydrocarbons (as oil) at a concentration of 5,200 milligrams per kilogram (mg/kg). Thisconcentration exceeded the Nevada Administrative Code (NAC) Action Level of 100 mg/kg(NAC 445A.2272). A Spill Notification Report was completed on January 19, 1999 and NevadaDivision of Emergency Management Number 99-0120-3281 was assigned.
Closws Report - CAU 297EMAD Vscuumhmp OilRcwvsryPrOjest Summ8syRevision: ODate Msrch 18, 1999
Polychlorinated biphenyls (Arochlor 1254) were also detected in the excavated waste soils at amaximum concentration of 7.2 mg/kg, however, the concentrations are below the U.S.Environmental Protection Agency (EPA) Preliminary Remediation Goal concentration forindustrial sites of 18 mg/kg (EPA, 1996).
No other constituents were detected above the analytical method detection limit. The analyticalresults and test methods are summarized on Table 1 and are detailed in the analytical datapackage. The table and data package are provided in Appendix A for reference and for use insupporting future characterization and/or closure activities.
Due to the extent of the impacted soil and the work area considerations, the spill associated withthis site will be assignedasCAS25-25-17 under CAU 398. The site will be tracked withinAppendix II of the Federal Facility Agreement and Consent Order u@il corrective actions can becompleted at a fiture date.
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Closure Repon. CAU 297EMAD Vacuom Pump011RecowyReferencesRevision: ODate: March 18, 1999
REFERENCES
Federal Facility Agreement and Consent Order, 1996, Agreed to by the Nevada Division ofEnvironmental Protection, the U.S. Department of Energy, and the U.S. Department ofDefense.
Nevada Administrative Code, 1998, NAC 445A.2272, “Contamination of Soil:Action Levels.” Carson City, NV.
U.S. Department Of Energy, Nevada Operations Office, 1996, Housekeeping CategoryCorrective Action Unit Work Plan, DOEINV-452. Las Vegas, NV.
>U.S. Environmental Protection Agency, 1996, Region 9 Preliminary Remediation Goals,San Francisco, CA.
5
WIW RL. 1A(J 2!EMAD Vacuum PumDOil RecovervSummary TableRevision: OMarch 18, 1999
TABLE 1- SUMMARY OF ANALYTICAL RESULTS FOR CAU 297: EMAD VACUUM PUMP OIL RECOVERY
Lc(1
TCLP ORGANO-TCLP SEMI- TCLP CHLORINE
TPH A Vocs B Vocs c METALS “ PCBS E PESTICIDES F GAMMASAMPLE ID& TYPE (mg/kg) (mg/L) (m@) (mgkg) (mg/kg) (mg/kg) (pcilg)
;MAD-VPOR- 1 5,200 ND ND ND ND ND NA/EDIFICATION
lMAD-VPOR-2)UPLICATE OF 1,700 ND ND ND ND ND NA;MAD-VPOR-I
IMAD-VPOR-3 CS-137 0.165VASTE
4,700 ND ND ND0.7 K-40 24.9
CHARACTERIZATION Arochlor- 1254ND
Ra-226 1.2DRUMS) Th-228 2.28
;MAD-VPOR-4 K-40 19.6VASTE
3,700 ND ND ND7.2 Ra-226 1.01
CHARACTERIZATION Aiochlor-1 254ND
Th-228 1.84LUGGERS) Th-232 1.26
All samples were collected on Dec. 1, 1998.A-TPH: Total (extractable) petroleum hydrocarbons analyzed using U.S. EPA Method 8015 Modified.B-TCLP VOCS: TCLP Volatile organic compounds analyzed using U.S. EPA Method 8260B.C-TCLP Semi-VOCs: TCLP Semi-Volatile Organic Compounds analyzed using U.S. EPA Method 8270C.D-TCL.P Metals: Metals analyzed using U.S. EPA Method 7470. Extraction by Method 1311.13-PCBS:Polychlorinated Biphenyls analyzed using U.S. EPA Method 8082.F-Ch-ganochlorine Pesticides analyzed using U.S. EPA Method 808 IA.TCL.P:Toxicity Characteristic Leaching Procedure (40 CFR, Part 26 1.24).ND: Not detected above laboratory detection limits.NA: Not analyzed.(mg/L or mg/kg or pCi/g): milligrams per Liter (for liquid), milligrams per kilogram (forsoil), picocuries per gram (for gamma spectroscopy).
NEL LABORATORIES ~s Vegas Divisior
Reno ● La? Vegas 4208 Arcata Way, Suite A ● Las Vegas, W 8903[. ..
Phoenix o Irvine (702) 657-101O ● Fax: (702) 657-15771-888-388-3282
CLIENT: Bechtel NevadaP.O. BOX 98521, MIS NTS273Las Vegas, NV 89193-8521
ATTN: Ted Redding
PROJECT NAME: V553 NEL ORDER ID: L9812048PROJECT NUMBER: 17777
Attached are the analytical results for samples in support of the above referenced project,
Sampies were received by NEL in good condition, under chain of custody on 12/3/98.
Samples were analyzed as received.
Shouid you have any questions or comments, please feel free to contact our Client Services department at (702)657-1010.
Some resultshave been flagged as follows:
J - This concentration shouid be considered an estimate due laboratory control sample failure.
Jc - This concentration should be considered an estimate. The continuing calibration check standard did notmeet QC requirements for this analyte.
Jm - This concentration should be considered an estimate due to probable matrix effects.
Some QA results have been flagged as follows:
J - This concentration should be considered an estimate due laboratory control sample failure.
J] - The batch MS and/or MSD were outside acceptance iimits. The batch LCS was acceptable,
Laboratory Manager u
CERTIFICATIONS:Reno Las Vegas S. California
Arizona AZ0520 AZ0518 AZ0583 IdahoCalifornia . 1707 2002 2264 MontanaUS Army Coqs Certified Certified Certified Nevadaof Engineers
Date -
Reno Las Vegas S. CaliforniaCertified CertifiedCertified CertifiedNV033 NV052
Corporate Office & Reno Division ● 1030 Matley Lane ● Reno, NV 89502 ● (702)
CA084
348-2522
NEL LABORATORIESCLIENT Bec~telNevada CLIENT ID: EMAD-VPOR-1PRC)JECT NAME: V553 DATE SAMPLED: 12/1/98PROJECT NUMBER 17777 NEL SAMPLE ID: L98 12048-01
TEST Organochlorine Pesticides by EPA 8081A, Dec. 1996MAll?IX: Solid EXTRACTED: 12/8/98DILUTION: 1 ANALYZED: 12/14/98 ANALYST: JRW
ReportingPARAMETER Result LimitA~tin ND 5. pgkg
alpha-BHCbeta-lBHC
deita.BHC
gamma-BHC (Lindane)
Alpha-chlordane
Gamma-chlordane
Chlordane4.4. -I)DD
4.4.-DDE
4.4. -1)DT
Dieidrin
Endosulfan I
Endosulfan IIEndosulfansulfateEndrir~Endrin aldehydeEndrinketoneHeptach}or
Heptachlor epoxide
Methoxychlor
ND
ND
ND
NDNDNDNDND JC
ND JND JC
NDNDND jC
NDND JC
NDNDND JC
NDND JC
5. pgikg5. pglkg5. J@kg
5. pglkg
5. pgjkg
5. pgikg “
20. llg/Kg
5. pgikg
5. pglkg
5. pglkg
; pglkg-.
5. pgikg
5. pglkg
5. pgikg
5. pglkg
5. pglkg -
5. @kg
5. pglkg
5. I.@@20. pglkg
T’oxaphene ND 60. @cg
QUALN CONTROL DATA:
Surrogate 0/0 Recovery Acceptable Ran~e
Decaclhiorobiphenyl 141 70- 130
Tetraclhloro-m-xy lene 99 70- 130
ND - Not DetectedThis report shall not be reproduced except injidl, without the written approval of the laboratory.
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NEL LABORATORIES——CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-2PROJECT NAME: V553 DATE SAMPLED: 12/1/98PROJECT NUMBER: 17777 NEL SAMPLE ID: L98 12048-02
TEST: Organochlorine Pesticides by EPA 8081A. Dec. 1996
MATRIX: Solid EXTRACTED: 12/8/98DILUTION: 1 ANALYZED: 12/14/98 ANALYST: JRW
PARAMETER Reporting—— Result
Aldrin LimitND
itlpha-BHC 5. pglkgND
beta-BHCj. @@
ND 5. pglkgdelta-BHC NDgamma-BHC(Lindane)
5. @io
ND--
Alpha-chlordane 5. pglkoND
.-
Gitmma-chlordane 5. @kgND
Chlordane 5. ygA!JND 20. p@Q
4.4”-DDD ND .ic
4.4’-DDE5 p;!@.
ND J4.4’-DDIT
5 \lg/Q-.ND JC
Dieldrin5. I@g
NDIindosulfan1 5, Itg;kg
NDEndosulfan11
5 It@g-.Ntl JC
Endosulfansulfate; pg(kg-.
NDfindrin
5. p:, kgND JC
Endrinaldehydei p@g-.
NDEndrin ketone
i pg:@ “-.ND
Hcptach]lor5 @@-.
ND JC
Hep[achlorepoxide5 II@g-.
ND 5. WlkgMethoxychlor ND JC 20. @gToxaphene ND 60. )@+QUAIWY CONTROL DA TA:
S!KM!aEDecachlorobiphenylTetrachloro-m-xy lene
0/0 Recoverv Acceptable Range
137 70- 130I 13 70- 130
ND - Not Detected
This report shall not be reproduced except infull, without the written approval of the laboratory.
NEL LABORATORIES-—CLIENT Bechtel Nevada CLIENT ID: EMAD-VPOR-3
PROJIECTNAME: V553 DATE SAMPLED: 12/1/98
PROJECT NUMBER: 17777 NEL SAMPLE ID: L9812048-03
‘TEST: Organochlorine Pesticides by EPA 8081A, Dec. 1996MATRIX: Solid EXTRACTED: 12/8/98D1LUTION: 1 ANALYZED: 12/14/98 ANALYST: JRW
PARAMETER.—Aldrin
itipha-BHC
beta-BHC
delta-EIHC
gamrnd-BHC (Lindane)
.41pha-chlordane
Garnma-chlordane
Chlordane
-L-$”-DDD4.4--DDE4.4--DDT
Dieldrin
Endosulfan 1
Endosulfan 11
Endosulfan sulfateEndrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychior
ReportingResult
ND
ND
ND
ND
ND
ND
ND
ND
ND .fc
ND J
ND JC
ND
ND
ND JC
ND
ND JC
ND
ND
ND .ic
ND
ND JC
Toxaphene ND 60 pg(i+!
QUALITY CONTROL DATA:
Surro~ate “h Recovew Acceptable Ran~e
Decachiorobiphenyl 113 70- 130
Tetrachloro-m-xylene 94 70- 130
ND - Not DetectedThis report shall not be reproduced except infull, without the wriuen approval of the laboratoy.
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NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-4PROJECT NAME: V553 DATE SAMPLED: 12/1/98
PROJECT NUMBER: 17777 NEL SAMPLE ID: L98 12048-04
TEST: Organochiorine Pesticides by EPA 8081A, Dec. 1996MATRIX: Solid EXTRACTED: 12/8/98DILUTION: 1 ANALYZED: 12/14/98 ANALYST: JRW
ReportingPARAMETER Result
A%Limit
ND 5. pglkg
alpha-13HC ND 5. pgfk.g
beta-BHC ND 5. pgllcg
deita-BHC ND 5. jqglkg
gamma-BHC(Lindane) ND 5. pglkg
Alpha-chiordane ND 5. pglkg
Garnma-chlorciane ND 5. pg/kg
Chlordane ND 20. @Kg
4.4”-DK)D ND JC 5. pglkg
4.-l”-DC)E ND J 5. wglkg
-1.-$”-DDT ND Jc 5. pglkg
Dicldrin ND 5. pglkg
Endosulfan 1 ND 5. pglkg
Endosullfan11 ND JC 5. W@
Endosu!fansulfate ND 5. pglkg
Endrin ND k 5. pglkg
Endrin aldehyde ND j pgJkg -
Endrin ketone ND ~ @kg-.
Heptachlor ND JC 5. pglkg
Heptachlor epoxide ND 5. pglkg
Methoxvchlor ND JC 20. pgikg
Toxaphtme ND 60. pglky
QUALITY CONTROL DATA:
S!!m!a!l ‘/0 Recovew Acceptable Ran~e
Decachlorobiphenyl 125 70- 130
Tetrachloro-m-xylene 102 70- 130
ND - Not DetectedThis report shall not be reproduced except injill, without the written approval of the laboratory.
NEL LABORATORIES.—CLIENT Bechtel Nevada CLIENT ID: EMAD-VPOR-IPRQJECT NAME: V553 DATE SAMPLED: 12/1/98PRt2JECT NUMBER: 17777 NEL SAMPLE ID: L98 12048-01
TEST: PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dec. 1996MA”I’RIX: Solid EXTRACTED: 12/8/98DILUTION: 1 ANALYZED: 12/9/98 ANALYST: JRW
PARAMETER ReportingResult
Arochlor-1016Limit
ND 20. ~lglkgArochlor-1221 ND 20. Ltg/kgArochlor-1232 ND 20, @kgArochlor- 1242 ND 20. }lg/kgArochlor- 1248 ND 20. p@igArochlor-1254 ND 20. )lgikgArocihlor-1260 ND 20. }lg/’kgQUAILITY CONTROL DATA:
Surrogate
DecalchlorobiphenylTetrachloro-m-xy lene
% Recoverv Acceptable Range~(35 70- 130100 70- 130
ND - Not DetectedThis report shall not be reproduced except infull, without tile written approval of the laboratoy.
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NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-2PROJECT NAME: V553 DATE SAMPLED: 12/1/98PROJECT NUMBER: 17777 NEL SAMPLE ID: L98 12048-02
TEST: PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dec. 1996MATRIX: Solid EXTRACTED: 12/8/98 .
DILUTION: 1 ANALYZED: 12!9198 ANALYST: JRW
PARAMETER.—Arochlor-1016
Result
ND
ReportingLimit
~~, @@
Arochlor-1221 ND m. pgikg
Arochlor-1232 ND 20. ~g.kgArochlor-1242 ND 20. @kg
,Arochior-1248 ND 20. pgkg
Arochior-1254 ND 20. pg;kg
Arochlor- 1260 ND Z(), @@
QUALITY CONTROL DATA:
Surrogate % Recoverv Accemablc Rant?e
Decachlorobiphenyl 70 70- 130
Tetrachloro-m-xy lene 78 70- 130
ND - Not DetectedThis report shall not be reproduced except infill, without the written upproval of the laboratory.
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NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID EMAD-VPOR-3PROJECT NAME: V553 DATE SAMPLED: 12/1/98PROJECT NUMBER. 177?7 NEL SAMPLE ID: L9812048-03
TES~ PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dee. 1996MATRIX. Solid EXTRACTED: 12/8/98DILUTION: 1 ANALYZED: 12/9/98 ANALYST: JRW
ReportingPARAMETER Result LimitA=hlor-1016 ND 20. pglkg
Aroclhlor-1221 ND 20. pgikg
Aroclhlor-1232 ND 20. pglkg
Aroclhlor-1242 ND 20. pglkg
Aroclhlor-1248 ND 20. pglkg
Aroclhlor-1254 700 I’%@? 20. pgkg
Aroclhlor-1260 ND 20. pgl!ig
QUALITY CONTROL DATA:
Surrovate 0/0Recovery Accer)tabie Range
Decachlorobiphenyl 122 70- 130Tetrachloro-m-xy iene I 04 70- 130
ND - Not DetectedTitis report shall not be reproduced except injidl, without the written approval of the laborato~.
.
NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-4PROJECT NAME: V553PROJiECT NUMBER: 17777
DATE SAMPLED: 12/1/98NEL SAMPLE ID: L98 12048-04
TEST: PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dec. 1996MATRIX: Solid EXTRACTED: 12/8/98DILUTION: 10 ANALYZED: 12!9198 ANALYST: JRW
ReportingPARAMETER Result LimitA~ior-101 6 ND MO. pgllig
Arochior- 1221 ND m. pglkg
Arochlor- 1232 ND 200. ygkg
Arochlor- 1242 ND 200. p@g
Arochlor-1248 ND 200. @lLg
Arochior-1254 7200 pglkg 200. pgkg
Aroc.hlor-1260 ND 200. pgoig
QUALITY CONTROL DATA:
Surroga& % Recoverv Accer)table Range
Decachlorobiphenyl 110 70- 130
Tetrachloro-m-xy lene 79 70- 130
ND - Not DetectedThis report si~a[lnot be reproduced except injid[, without the written crppro~’alof the Iaboratoty.
NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT JD: Method BlankPROJECT II): v553/17777 DATE SAMPLED: NAPROJECT #: 17777 NEL SAMPLE ID: 981208 PCBS-BLK
TEST: PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dec. 1996METHOD: EPA 8082 ANALYST: JRWMATRIX: Solid EXTRACTED: 12/8/98
ANALYZED: 1~/9/9fj
ReportingPARAMETER Result LimitA~chlor-101 6 ND 20. @cg
Arochior-1221 ND 2(.). pg/lig
Arochlor-1232 ND 20. yg/kgArochlor-1242 ND 20. )lgrkg
Arochlor-1248 ND 20. p@+!
Arochior- 1254 ND 20. }lg/kg
Arochlor- 1260 ND 20. #g/kg
~tlLITY CONTROL DA TA:
SurroEate ‘A)Recovery Accentnblc RanoeDecachlorobiphenyl ]~~ 70- 130Tetrachloro-m-xy lene ]-1~ 70- 130
ND - Not DetectedThis ireportshall not be reproduced ercep! itlfitll, without the written approval of the laborato~.
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NEL LABORATORIESCLIENT: Bechtel NevadaPROJECT ID: V553117777
CLIENT ID: Method B]an~DATE SAMPLED: NA
PROJECT #: 17777 NEL SAMPLE ID: 981208PSTS-BLK
TES-E Organochlorine Pesticides by EPA 8081A, Dec. 1996METHOD: EPA 8081MATRIX: Solid
ANALYST: JRWEXTRACTED: ly8/98ANALYZED: ]~/ 14/98
PARAMETER—— Result Reporting
AldrinND
Limitalpha..BHC
ND5. kglkg
beta-EIHCND
5. pgflig
delta-lBHC 5. pgfkgND
@m’na-BHC(Lindane)ND
5. pglkg
Alpha-chiordane 5. pglkg
Gamrna-chlordaneND
5. pglkgND
5. pglkgChlor(iane
4.4’-DI)DND
20. pg!liig4.4”-DDE
ND
ND5. pgfkg
4,4”-DDTDieldrin
ND5. pglkg5. pglkg
EndosuIfanIND 5. pg/lig
Endosulfin IIND 5. pglkg
EndosulfansulfateND
ND5. llglkg
EndrinND
5. pglkg
Endrin aldehyde
Endrin ketoneND
5. ~gfkg
ND5. pgjkg -
Heptach]orND
- pg;kg.>
Heptach]or epoxide 5. pglkg
Methox~)chiorND
5. pg/kg
ToxaphcneND
20. pglkgND
60. pglkgQUALITY CONTROL DATA:
SUrroPate
Decachlorobipheqy]Tetrachloro-m-xylene
’10 Recovev10887
Acceptable Range70- 13070- 130
ND - N~~tDetectedThis report shall not be reproduced except inful[, without the written approval of the laborato~.
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NEL LABORATORIESCLIENT: Bechtel NevadaPROJECT NAME:
CLIENT ID:V5.53
EMAD-VPOR-IDATE SAMPLED: 12/1/98
PROJECT NUMBER 17777 NEL SAMPLE ID: L9812048-01
TEST TCLP-8 MetalsMATRIX: Solid
TCLP/STLCRESULT REPORTING
PAIUiMETEREXTRACTION
mg/L LIMIT D. F. METHOD DATEArsenic
DIGEST.ED ANALYZEDND 0.5mglL 5
——EPA 6010 ]~/8/98 ]~/9/98
Barium NDl~;9198
5. m~L 5 EPA 6010 12/8/98Cadmium ND]~/9/98 ]39/98
0.05 mg/L 5 EPA 6010 12/8/98Chromium ND
] ~/9/98 1~/9;980.05 mg/L 5 EPA 6010
Lead ND12/8/98
0.25mg/L1~J9/98 ]~/9!98
5 EPA 6010Mercury ND
] ygfgg0.002mglL
~~/9/9810
IW9j98EPA 7470A 12/8/98 ]~/9/98 I~/9/98
Sdenium ND 0.5 mg/L 5 EPA 6010Silver ND
]2/&198 12/9/98 ]: !9:98 ‘0.1 m#L 5 EPA 6010 I~/8/98 1~/9/98 12!9198
.
D.F. - Dilution Factor
ND - Not Detected
This report shall not be reproduced except infull, without the wriuen approval of the laboratoy,
NEL LABORATORIESCLIENT: Bechtel NevadaPRO.IECT NAME:
CLIENT ID:,V553
EMAD-VpOR-2DATE SAMPLED: 12/1/98
PROJECT NUMBER: 17777NEL SAMPLE ID: L98 12048-02
TEST: TCLP-8 MetalsMATRIX: Soiid
TCLP/STLCRESULT REPORTING
PAR,4METEREXTRACTION
—— mg/L LIMIT D. F. METHC)D DATE DICESTED ANALYZEDArsenic ND 0.5 mg/L 5 EPA 6010
——~~/8J9g
Barium ND]~/9/98 1~f9,i98
5. mg/L 5 EPA 6010Cadmium ND
]ygf9g 17j9/980.05 mg/L 5
[~/9/98EPA 6010 .12/8/98
Chromium ND1~J9/98
0.05 mg/L 5I ~/9,198
EPA 6010 12/8/98Lead ND
]~/9f98().~j mg/L 5
]~/9/98EPA 6010 ~-)/g/9g
Mercury ND 0.002 mg/L12/9/98
101~!9/98
EPA 7470ASeltinilum
1~/g/9g I ~f9/98ND
]~!9/980.5 mg/L 5 EPA 6010
Silver ND1y8/9g 1~/9f98 ]~!9,f98
0.1 mg/L 5 EPA 6010 ]~/8/9g ] ~/9/98 ]_)/9198
.
D.F. - Dilution Factor
ND - Nat Detected
This report shall not be reproduced except infull, without the written approval of the laboratory.
NEL LABORATORiES
CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-3PROJECT NAME: V553 DATE SAMPLED: 12/1/98PROJECT NUMBER: 17777 NEL SAMPLE ID: L9812048-03
TEST: TCLP-8 MetalsM14TRIX: Solid
TCLP/STLCRESULT REPORTING EXTRACTION
~ARAMETER mg/L LIMIT D. F. METHOD DATE DIGESTED ANALYZED
Arsenic ND 0.5 m@L 5 EPA 6010 12/8/98 12/9/98 ]~f9f98
Barium ND 5.mg5 5 EPA 6010 12/8/98 12/9/98 ]W9/98
Cadmium ND 0.05mg/L 5 EPA 6010 12/8/98 12/9/98 1~19198
Chromium ND 0.05mg/L 5 EPA 6010 12/8/98 12/9/98 I~/9/98
Lead ND 0.25 mglL 5 EPA 6010 12/8/98 1219/98Mweury ND 0.002mglL 10 EPA 7470A 12/8/98 12/9/98Selenium ND 0.5 mg/L 5 EPA 6010 1218/98 I~/9/98
Silver ND 0.1 mgil 5 EPA 6010 12/8/98 1~/9/98
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●
D.F. - Dilution Factor
ND - Not Detected
This report shall not be reproduced except injiull, ‘without the written approval of the laboratory.
NEL LABORATORIES
CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-4
PROJECT NAME: V553 DATE SAMPLED: 12/1/98
PRO.JECT NUMBER: 17777 NEL SAMPLE ID: L98 12048-04
TEST: TCLP-8 MetalsMATRIX: Solid
TCLP/STLCRESULT REPORTING EXTRACTION
PARAMETER mg/L LIMIT D. F. METHOD DATE DIGESTED ANALYZED——Arsenic ND 0.5 mg/L 5 EPA 60 IO }~/8J98 1~/9/98
Barium ND
I ~[9,198
5. mglL 5 EPA 6010 12/8/98 ~~J9/98 ]~,t9f98
Cadmium ND 0.05 mg/L 5 EPA 6010 ]~/8/9fj ] ~/9/98 ~~)9/98
Chromium ND 0.05 mg/L 5 EPA 6010 ] yf3/9f3 ~~J9/98 ] ~/9/98
Lead ND 0.25 mg/L 5 EPA 60 IO i yg/98 ]~/9/98 ]~;9,198
h’lercury ND 0.002 mg/L 10 EPA 7470A \~/8/98 ]~f9,/98 ]~~9/98
Selenium ND 0.5 mg/L 5 EPA 60 IO 1~/8/98 1~/9/98
Silver ND O.I mg/L 5
] w9/9~
EPA 6010 1~/8/9fj \~j9/98 1~/9,198
D.F. - Dilution Factor
ND - Not Detected
This report shall not be reproduced except infull, without the written approval of the laboratory.
NEL LABORATORIESCLIENT Bechtel Nevada CLIENT ID: Method BlankPROJECT ID: V553117777 DATE SAMPLED: NA
PROJECT #: 17777 NEL SAMPLE ID: L12048-HG02-BLK
TEST TCLP by EPA 1311, July 1992& Mercury by EPA 7470A, July 1992MATRIX: TCLP Extract
TCLP/STLCREPORTING EXTRACTION
PARAMETER RESULT LIMIT D. F. METHOD DATE DIGESTED ANALYZED
Mercury ND 0.002mg/L 10 EPA 7470A ]~/8/98 ]~/9/98 ]~/9/98
D.F. - Dilution Factor
ND - Not DetectedThis report shall not be reprodziced txcept infull, witholit the written approval of the laboratoq’.
.
NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID: Method BlankPROJECT ID: v55311 7777 DATE SAMPLED: NAPRO.IECT #: 17777 NEL SAMPLE ID: L12048i-BLK
TEST TCLP by EPA 1311, July 1992&7 Metals by EPA 6010A, July 1992MATRIX: TCLP Extract
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Selenilum
Silver
REPORTINGRESULT LIMIT
ND 0.5mg/LND 5mg/LND 0.05mg/LND 0.05mg/LND 0.25mg/LND 0.5mg/LND 0.1mg/L
D. F.
Y555555
TCLP/STLCEXTRACTION
METHOD DATE DIGESTED ANALYZED
EPA 6010 12/8{98 ]~/9/98 ]~/9/98EPA 6010 t218{98 1~/9/98 ]~f9/98
EPA 6010 12/8/98 ]~/9/98 12/9/98EPA 6010 12/8198 12/9/98 1~/9/98EPA 6010 12t8198 1~/9/98 i~/9/98
EPA 6010 12/8/98 12/9/98 ]~/9/98
EPA 6010 1~/8/98 }~/9J98 ]~f9/98
D.F. - Dilution Factor
ND - Not DetectedThis report shalI not be reproduced except infill, without the written approval of the laboratoq.
.
NEL LABORATORIES
CLIENT: E3echte1Nevada CLIENT ID: EMAD-VPOR-1
PROJECT ID: v553i17777 DATE SAMPLED: 12/1/98PROJECT #: 17777 NEL SAMPLE ID: L9812048-01
TEST: TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260A TCLP EXTRACT DATE: 12/9/98
MATRIIX: Solid EXTRACTED: 1~/] ]/98
DILUTION: 1 ANALYZED: ]~/1 ]/98
Result Reporting
PARAMETER mg/L Limit—.Benzene ND O.I mg/L
Carbon tetrachloride ND (). I mrjL
Chiorobc:nzeme ND 0. I mg/L
Cbloroforrn ND ().I n@
1.4-Dichlorobenzene(p-DCB) ND ().Img/L
1.2-Dichloroethane(1.2-DCA) ND O.I mg‘L
1.l-Dich\oroethene ( 1.1-DCE) ND ().I mg/L
Methyl Ethyl Ketone ND ~.mg/L
‘Ictrwhlcroethene (PCE) ND ().I nlgL
Trichloroethene ND ().I mg/L
Vinj I chloride ND (). I mg/L
QL.!4LlTY COATTROLDA TA:
Surrovatg “h Recovev Acceptable Range
-i-Bromofluorobenzene 86 74- 121
Dibromofluoromethane 93 80- 120
Toluene-d8 99 81- 117
?
ND - Not Detected
r]lls repor~~shall not be reproducedacep( infii], without the written approval of the iaborato~.
NEL LABORATORIES
CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-1
PROJECT ID: V553117777 DATE SAMPLED: 12/1/98
PROJECT #: 17777 NEL SAMPLE ID: L98 12048-01
TEST: TCLP by EPA 1311, July 1992& Semivoiatile Organics by EPA Method 8270C, Dec. 1996METHOD: EPA 8270 TCLP EXTRACT DATE: 12/8/98
MATRIX: Solid EXTRACTED: 1~/]()/98
DILUTION: 1 ANALYZED: ]~/]3/98
Result Reporting .
PARAMETER mg/L Limit
1.-l-Dichlor=ene (p-DCB) ND
2.4-Dinitrotoluene (DNT)
O,In@LND O.I mg/L
Hexach]orobenzene ND O.I mg/L
Hexnchlorobutadiene ND 0. I mg/L
l-kxachloroethane ND 0.1 mgfL
2-\lethylphenol ND 0. I mg.lL
3.Wvlethyiphenol (isomeric pair) ND 0.1 mg/L
Nitrobenzene ND O.I n@L
Pcntachlorophenoi ND 0. I m@L
1’!ridine ND 0.1 tng!L
2.-!.5-Trichlorophenol ND O.I mg!L
2.4.6-Trichltxophenol ND 0. I m#L
@12LITY CONTROL DA TA:
5urroPate 0/0 Recoverv
2.4.6-Tribromophenol 64
2-Fluorobiphenyl 67
?-Fiuorophenol 37
Yitrobenzene-d5 60
?-Terphenyi-d 14 ‘ 69
Phenol-d5 15
Acceptable Range
10- 12343- 116
21- 10035- 114
33- 141
10- 94
,
4D - Not Detected
rilis report sha[[ not be reproduced a~ept infuIl, without the written approval of the laboratory.
NEL LABORATORIES
CLIENr: Bechtel Nevada CLIENT ID: EMAD-VPOR-2
PROJECT ID: V55311?777 DATE SAMPLED: 12/1/98
PROJECT #: 17777 NEL SAMPLE ID: L98 12048-02
TEST: TCLP by EPA 1311, Jttiy 1992 & Volatile Organicsby EPA 8260B, Dec. 1996METHOD: EPA 8260A TCLP EXTIU4CT DATE: 12/9/98
MATRIX: Solid EXTRACTED: 1~/l\/98
D1LUTION: I ANALYZED: 12/11/98
Result Reporting
PARAMETER mg/L Limit—.Benzene ND O.Img/L
Carbon uwachloride ND 0.1 mg/L
Chlorobenzene ND O.l,mg/L
Chloroform ND “O.1mg/L
I A-tlichlorobenzene (p-DCB) ND O.i mg/L
1.~.Di~h\oroeth~e (1,2-DCA) ND 0,1 mg/L
1.I -Dichioroethene ( 1,I -DCE) ND O.I mg/L
Methyl Ethyl Ketone ND 2.mgfL
Tmachloroethene (PCE) ND 0.1 mg/L
Trichloroethene ND O.I m#L
Vinyl chloride ND O.I mg/L
~UALITY CONTROL DATA:
+urro~atc % Recovery Acceptable Ran?e
4-Bromofktorobenzene 87
Dibromofiuoromethane
74- 12195 80- 120
Toluene-d8 99 81- 117
.
4D - Not Detected
‘his repori!shall not be reproduced except injidl, without the written approval of the laborato~
NEL LABORATORIES
CL 1ENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-2PROJECT ID: v553/17777 DATE SAMPLED: 12/1/98PROJECT i+: 17777 NEL SAMPLE ID: L9812048-02
TEST: TCLP by EPA 1311, July 1992& Sernivolatile Organics by EPA Method 8270C, Dec. 1996METHOD: EPA 8270 TCLP EXTRACT DATE: 12/8/98
MATRIX: Solid EXTRACTED: ]~/]0/98
DILUTION: 1 ANALYZED: 1~/]3/98
Result ReportingPARAMETER mg/L Limit
1.-l-t)ichlorc=ene (p-DCB) ND Jm 0. i mg/L
2..$-Dinitrotoluene(DNT) ND 0. I n@L
I-lexttchlorobenzene ND 0. I mg/L
Hwtchlorolmtadiene ND Jm 0.
Hcxachloroethane ND Jm ().
2-Methy Iplwnol ND ().3..&Methylpihenol(isomericpair) ND 0.
Nitrobenzenc ND Jm ().
Pcntachlorophenol ND ().
Pyridine ND Jm 0.
2.4.5-Trichlorophenol ND 0. I mg/L
2.4.6-Trichlorophenoi ND ().Img/L
m#L
mg/L
m@Lmg/Ln;g/[,
m#L
m#L
>UALITY CONTROL DA TA:
>urro9ate 0/0 Recoverv
2.4.6-Tribronnophenoi 60
J-Fluorobiphenyl 47
:-Fluorophetnol 9 Jm
iitrobenzene-d5 20 Jm
-Terphenyi-d14 “ 65
‘henol-d5 13
Acceptable Range
10- 12343- 116
21- }0035- 114
;3- 141
10- 94
,
(D - Not Detected
‘hixreport shall not be reproduced except infull, without the written approval of the laboratoq.
CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-3PROJECT ID: v553/17777 DATE SAMPLED: 12/1/98PROJECT #: 17777 NEL SAMPLE ID: L9812048-03
TEST TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260A TCLP EXTRACT DATE: 12/9/98MATRIX: Solid EXTRACTED: l~f] 1/98
DILUTION: 1 ANALYZED: 1~/1]/98
Result ReportingPARAMETER mg/L Limit——Ihmzene ND 0. I m@L
Carbon tewachloride ND ().I mg/L
Chlorobenzene ND O.I mg/L
Chloroform ND O.I mg/L
1.4-Dichlorobenzene (p-DCB) “ ND 0.1 mg/L
1.2-Dichloroethane ( 1,2-DCA) ND 0.1 mg/L
1.I -Dichloroethene ( 1,1-DCE) ND O.I m#L
Methyl Ethyl Ketone ND ~, mg/L
Tetrachloroethene(PCE) ND O.I mg/L
Trichioroethene ND 0. I mgll.
Vin} I chloride ND ().I myl.
>(JALITY CONTROL DA TA:
iurrozate 0/0 Recoverv AccetNable Rarwe
$-Bromofluorobenzene 86
Oibromofluoromethane
74- 12193 80- 120
Toluene-d8 99 81- 117
.
JD - Not Detected
‘hisreport shall not be reproduced except infill, withozit the written approval of the laboratoqv.
NEL LABORATORIES
CLIENT Bechtel Nevada CLIENT ID: EMAD-VPOR-3PROJECT ID: V5531’17777 DATE SAMPLED: 12/1/98PROJECT #: 17777 NEL SAMPLE ID: L98 12048-03
TEST: TCLP by EPA 1311, July 1992& Semivolatiie Organics by EPA Method 8270C, Dec. 1996METHOD: EPA 8270 TCLP EXTRACT DATE: 12/8/98MATRIX: Solid EXTRACTED: 12/10/98DILUTION: 1 ANALYZED: 1~/13/98
Result ReportingPARAMETER mg/L—— Limit{.4-Dichlorobenzene(p-DCB) ND Jm 0.1 mg/L2.4-Dinitrotoluene (DNT) ND O.I mg/LI-kmchiorobenzene ND 0.1mg/LHesachlorobutadiene ND Jm 0.1 mg/LHexachloraethane ND Jm 0.1 mg/L2-MethylphenoI ND O.I mg/L3.& Methylphenol (isomeric pair) ND 0.1 mg/LNitrobenzene ND Jrn 0.1mg/LPentachlorophenol ND ().I mg/LPyridine ND Jm 0.1mg/L2.4.5~Trichlorophenol ND 0.1 mr#L2,4.6-Trichlorophenol ND 0.1 mg/L
~U.4LITY CONTROL DATA:
<urro~ate “h Recoverv
1,4,6-Tribromophenol 66?-Fluorobiphenyl 437-Fluorophenol 11Nitrobenzene-d5 17)-Terphenyl-d14 “ 66?henol-d5 13
Acce@able Ranpe
10- 12343- 116
Jm 21- 100Jm 35- 114
33- 141
lo- 94
●
JD - Not Detected
‘his report shall not be reproduced except injidi, without the writtenapprova[of the laborato~.
NEL LABORATORIES
CLIENT: Bechtel Nevada CLIENT ID: EMAD-VPOR-4
PROJECT ID: V553117777 DATE SAMPLED: 12/1/98
PROJECT #: 17777 . NEL SAMPLE ID: L9812048-04
TEST TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260A TCLP EXTRACT DATE: 12/9/98
MATRIX: Solid EXTRACTED: 12/11/98
DILUTION: 1 ANALYZED: 12/1 1/98
Result Reporting
PARAMETER mg/L Limit
‘Benzene ND 0. Img/L
Carbontetrachlorkie ND 0. Img/L
Chlorobenzcne ND 0. i mg/L
Chloroform ND 0. I mg/L
1.4-Dichlorobenzene(p-DCB) ND ().1n@L
~.~-Di~h]oro~th~e (1,2.DCA) ND 0. I n@L
1.1-Dichiorocthene(1, I -DCE) ND 0.1 mg/L
Methyl Ethyl Ketone ND 2. n@L
Tetrachloroethene(PCE) ND 0. i m#L
Trichloroethene ND 0. img/L
Vinyl chloride ND 0.1 m#L
~U4LITY CONTROL DA TA:
<urro~ate ‘A Recoverv Acce~table Ranse
!-Bromofluorobettzene 88 74- 121
Jibromofluoromethan e 95 80- 120
rcduene-d8 99 81- 117
,
.
4D - Not Detected
‘ilis report shall not be reproduced except in~ll, without the written approval of the laboratory.
NEL LABORATORIES—CLIENT: Bechtel Nevada CLIENT ID:PROJECT ID: V55311?777
EMAD-VPOR-4DATE SAMPLED: 12/1/98
PROJECT #: 17777 NEL SAMPLE ID: L98 12048-04
TEST: TCLP by EPA 1311, July 1992& Semivolatile Organics by EPA Method 8270C, Dec. 1996METHOD: EPA 8270 TCLP EXTRACT DATE: 12/8/98MATRIX: Solid EXTRACTED:DILUTION: I
1~/]o/98ANALYZED: 12/13/98
ResultPARAMETER Reporting
mg/L Limit~4-Dichlorobenzene (p-DCB)ND
0. I mg/L2.4-Dinitrotoiuene (DNT)
HtxachlorobenzeneND 0.1 mg/L
He~achlorobutadieneND 0. I mg/L
HexilchloroethaneND O.I mg/L
2-Meth~lphenoiND 0. I mg/LND O.I mg/L3.4-Methylphenol (isomeric pair)
XitrobenzeneND 0. I mg/L
PrntachlorophenoiND O.I mg/L
PyridineND 0.1 mg/LND
2.4.5-Trichlorophenol ND(),I mg/L
2.4.6-Trichioropheno]ND
().I m@L
0. I mg/L,,
Q1-.!-fLlTYCONTROL DATA:
Surrogate 0/0Recoverv7.4.6-Tribromopheno]
~-Fluorobipheny]67
672-Fluorophenoi 35\itrobenzene-d5 58:~-Terphenyi-d 14Phenol-d5
“ 6025
Acceptable Range
10- 12343- ]]6
21- 10035- 114
33- 141
10- 94
.
(D - Not Detected
rhis report shall not be reproduced except inful[, without the written approval of the laboratoq~.
NEL LABORATORIES
CLIENT Bechtel Nevada CLIENT ID: TR120198
PROJECT ID: v553/17777 DATE SAMPLED: 12/1/98
PROJECT #: 17777 NEL SAMPLE ID: L98 12048-05
TEST TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260B TCLP EXTRACT DATE: 12/11/98
MATRIX: Aqueous EXTRACTED: 12/11/98
DILUTION: 1 ANALYZED: 12/11/98
Result ReportingPARAMETER mglL Limit
Benzene Nl) 0.1 mg/L
Carbontetrachloride ND 0.1 mg/L
Chlorobenzene ND O.I mg/L
Chloroform ND 0.1mg/L
1..&Dichlorobenzene(p-DCB) ND O.I mg/L
1.2-Dichloroethane (1.2-DCA) ND O.Img/L
1.l-Dichloroetbenc ( 1,I -DCE) ND O.I m@L
Methyl Ethyl Ketone ND ?.mg/L
Tetrachloroethene(PCE) ND O.I mg/L
Trichloroethene ND O.I mg/L
Vinyl chloride ND 0.1 mg/L
QUALITY CONTROL DATA:
Surrotzate ‘/0 Recoverv Acceptable Range
4-Bromofluorobenzene 86 86- 115
Dibromofluoromethane 95 86- 118
Toluene-d8 99 88- 110
.
,
iD - Not Detected
‘his report shall not be reproduced ezcept injidl, without the written approval of the laborato~,
NEL LABORATORIESCLIENT: Bechte! Nevada CLIENT ID: Method BlankPROJECT ID: Soil Testing Apex Industrial Use Zone/3745 DATE SAMPLED: NAPROJECT #: 37456-002-16 NEL SAMPLE ID: 121098-E3-TCLP-BLK
TEST: TCLP by EPA 1311, July 1992& Semivolatile Organics by EPA Method 8270C, Dec. 1996METHOD: EPA 8270 TCLP EXTRACT DATE: 12/8/98MATRIX: TCLP Extract EXTR4CTED: 12/10/98
ANALYZED: ]?/13/98
ResultPARAMETER Reporting
mg/L Limit -1..$-Dichiorobenzene(p-DCB) ND —.
2.4-Dinitrotoiuene (DNT) ND0. I mg/L
Hcxachlorobenzene ND0.1 mg/L
Hexachlorobutadiene0.1 mg/L,
NDHtxitchloroethane
0. I mg/L,ND
?-ivlethylphenol ND0.1 mg/L
0.1 mg/L3..l-Methylphenol (isomeric pair)
SitrobenzeneND 0.1 mg/L,ND 0.1 mg/L
Pentachlorophenoi ND 0.1 mg/LPyridine ND2.4.5-Trichlorophenol
0. i mg/LND
2.- L6-Trichlorophenoi(). I mg/L
ND O.I mg/L
QUALITY CONTROL DATA:
5urro~ate
:.4.6-Tribromophenol
~-FluorobiphenylJ-Fluorophenol\itrobenzene-d5~-Terphenyl-d142henoi-d5
ND - Not Detected
‘/i Recoverv Acceptable Range
.67 10- 12367 43- 11643 21- 10060 35-114’ ,62
33- 14129 10- 94
Mis report shall not be reproduced except infull, without the written approval of the laboratory.
NEL LABORATORIESCLIENT Bechtel Nevada CLIENT ID: Method Blank
PROJECT ID: Soil Testing Apex Industrial Use Zone/3745 DATE SAMPLED: NA
PROJECT #: 37456-002-16 NEL SAMPLE ID: 981211-TCLP-BLK
TEST: TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260A TCLP EXTRACT DATE: 12/9/98
MATRIX: TCLP Extract EXTRACTED: 1~/~1/98
ANALYZED: 12/11/98
PARAMETER
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
1.4-Dichiorobenzene(p-DCB)
1.2-Dichloroethane ( 1.2-DCA)
1.I -Dichioroethene ( I. 1.DCE)
\lethyl Ethyl Ketone
Tctrachloroethene(PCE)
Trichloroethene
\“inyi chloride
Resultmg/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
@JALITY CONTROL DATA:
Surrogate 0/0 Recover-v
-LBromofluorobenzene 87
~ibromofluoromethane .91
Toluene-d8 100
SD - Not Detected
This report shall not be reproduced except infull, withou! the written approval of the laboratoq.
ReportingLimit
0.Img/L
O.I mg/L
O.I mg/L
0. I mg/L
O.I mg/L
(). I mg/L
().1rng/L~m@L
0.1 mg/L
().I mg/L
().1mg/L
Acceptable Range
74- 12180- 12081- 117
.
NEL LABORATORIESCLIENT: Bechtel Nevada CLIENT ID: Method BlankPROJECT ID: Soil Testing Apex Industrial Use Zone/3745 DATE SAMPLED: NAPROJECT #: 37456-002-16 NEL SAMPLE ID: 98121 lATCLP-BLK
TEST TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996METHOD: EPA 8260B TCLP EXTIWCT DATE: 12/1 1/98MATRIX: TCLP Extract EXTR4CTED: i2/I ]/98
ANALYZED: 12/1 1/98
ResultPARAMETER Reporting
mg/LLimitBenzene ND
Carbontetrachloride O.I mg/LND O.I mg/LChlorobenzene ND O.I mg/LChloroform ND O.I mg/L1.4-Dichlorobenzene(p-DCB) ND 0.1 mg/L1.2-Dichloroetiae ( 1,2-DCA) ND
1.1-Dich]oroethene ( 1,I.DCE) ND0.1 mg/L
Methyl Ethyl Ketone.0.1 mg/L
ND 2 mg/LTetrachloroetiene (PCE) NDTrichloroethene
O.I mg/LND
Vinyl chloride O.l.mg/LND O.I mg/L
QUALITY CONTROL DATA:
Surrogate ‘/0 Recovery4-Bromofluorobenzene 87Dibromofluorometime 91Toluene-d8
,“100
ND - Not Detected
This report shall not be reproduced except infidl, without the written approva[ of the laboratory.
Acce~table Ranre
86- 11586- 11888- 110
NEL LABORATORIESCLIENT Bechtel NevadaPR03ECT NAME: VS53PROJECT NUMBER 17777
TEST Total Extractable Petroleum Hydrocarbons by EPA Method 8015M, December 1996METHOD: EPA 8015M
MATRIX: Solid ANALYST: SEJ
CLIENT SAMPLE NEL RESULT Reporting SurrogateSAMPLE ID DATE SAMPLE ID mg/kg ~ Limit Recovery* EXTRACTED ANALYZED
EMAD-VPOR-1 12/1/98 L98 12048-01 5200 0 2000. mgl’kg 130 ’70 ~~f9/98 [~/14/98
EMAD-VPOR-2 12/1/98 L98 12048-02 1700 Jm O 100. mg/kg 145 % ~~/9/98 1~/1~/98
EMAD-VPOR-3 12/1/98 L98 12048-03 4700 0 200, mgkg 100 % ]~/9f98 1~/] j/98
EMAD-VPOR-4 12/1/98 L98 12048-04 3700 0 ~0(). mg/kg 130 ‘?40 ~~~$)lgg 1~/1 1,/98
CR: Carbon Range
0 Oil Range Organics (C12 to C32).
Note: The reporting limit for C)ilRange Organics in soil is 50 mg/kg.QUALITY CONTROL DATA (Total for Gas and Diesel Range):
SamDie ID Result Acceptable Range Surrogate Recoverv’ SamDle Number
Blank, 981209STP -BLK ND < 1O.mg/kg 78 % NA
LCS, 981209STP - LCS 61 ~0 57.5- 114 % 107 ?40 NA
.
ND - Not Detected* Surrogate used was Octacosane, acceptance limits 60-121 ?40 for aqueous samples, 54-130% for solid samples.
This report shall not be reproduced except infuIl, without the written approval of the laboratory.
NEL LABORATORIES.
CLIENT Bechtel NevadaPROJECT ID: V553/17777PROJECT #: 17777
TEST C)rganochlorine Pesticides by EPA 8081A, Dec. 1996MATRIX: Solid
PARAMETER
Aldrin
Aldrin
Aldrin
Aldrin
alpha-BHC
alpha-BHC
beta-BHC
beta-BHC
deka-BHC
delta-BHC
gamma-BHC (Lindane)
gamma-BHC (Lindane)
gamma-BHC (Lindane)
gamma-BHC (Lindane)
Alpha-chlordane
Alpha-chlordane
Gamma-chlordane
Gamma-chlordane
4.4’-DDD
4,4’-DDD
4,4’-DDE
4.4”-DDE
4,4”-DDT
-1,4”-DDT
4,4”-DDT
4,4”-DDT
Oieldrin
Ilieldrin
Dieldrin
Dieidrin
%dosulfan I
3ndosulfan I
;ndosulfan 11
%dosulfan 11
;ndosulfan sulfate
%dosulfan sulfate
;ndrin
NEL Samole ID
981208 PSTS-LCS
981208 PSTS-LCSD
L9812048-02-MS
L9812048-02-MSD
981208PSTS-LCS
981208PSTS-LCSD
98 1208PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS
981208 PSTS-LCSD
L9812048-02-MS ““
L9812048-02-MSD
98 1208PSTS-LCS
981208 PSTS-LCSD
981208 PSTS-LCS
981208PSTS-LCSD
981208 PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS
981208PSTS-LCSD
L9812048-02-MS
L9812048-02-MSD
981208 PSTS-LCS
981208 PSTS-LCSD
L98 12048-02-MS
L9812048-02-MSD
981208 PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS “
981208PSTS-LCSD
98 1208PSTS-LCS
981208PSTS-LCSD
981208PSTS-LCS
hdrin 981208PSTS-LCSD
Seik!LAmount
33.3
3>.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3
33.3..! -JJ.J
33.3
33.3
!33.3
33.3
33.5*-I -1JJ.J
23.3
33.3
. . .JJ.J
33.3
33.3. . *JJ.>
33.3
33.3
23.3
33.3
35.3
53.3
33.3
33.3
33.3
33.3
33.3
W!$!L PercentResult Recovery
3~fj
32.33?
37
33.3
32
36
35.6
34
33
32.3
3229
53.6
34.3
30.3
.Z3
33
38
36.5
50.6
37.3
50.9
38.6
11.7
11.6
38.6
37
36.3
43.34~.6
43.3
38.6
30.6
39.6
23.6
38.6
37
4D - Not Detected
‘his report shall not be reproduced except infull, without the written approval of the laborato~,
98
97
96
111
100
96
108
107
102
99
97
96
87
101
103
91
99
99
114
109
152 J
112
153 J
116
35 J1
35 JI
116
111
109
I30
128
130
11692
119
101
116
111
AcceMabie
RPD!WW.73-128
73-128 0.9
73-128 -
73-128 14.5
68- 133 ‘
68- 133
71- 136
71- 136
69- 133
69-133
69- 125
69-125
69- 125
69- 125
63-120
63- 1,20
68-126
68-126
76- 127
76- 12762. 143
62- 143
70- 151
’70-151
70- 151
70:151
84- 135
84-135
84- 135
84-135
57-161
57-161
76-137
76- 137
74- 144.
74- 144 16.4.
75- 146
75-146 4.2
4.-
‘1.1
3. ‘“
0.9 ‘“
i4.i
\q,4
o.
4.6
30.3
77 ;- .-
1.
4.?
17.6
1.6
~~.1
NEL LABORATORIES
CLIENT Bechtel NevadaPROJECT ID: V553/1 7777PROJECT #: 17777
TEST Organochlorine Pesticides by EPA 8081A, Dec. 1996MATRIX: Solid
PARAMETER* * Percent
NEL Sample IDAcceptable
Amount Result Recovery RangeEndrin L9812048-02-Ms 33.3 21 63 JI 75- 146Endnn L9812048-02-MSDEndrin aldehyde
33.3981208PSTS-LCS
Endrin aldehyde33.3
981208 PSTS-LCSD 33.3Endrin ketone 981208 PSTS-LCS 33.3Endrin ketone 981208 PSTS-LCSD 33.3Heptachlor 981208 PSTS-LCSHeptachlor
33.3981208 PSTS-LCSD 33.3
Heptachlor L9812048-02-MSHeptachlor
33.3L9812048-02-MSD 25.3
Heptachlor epoxide 981208 PSTS-LCS 33.3HeptachIor epoxide 981208 PSTS-LCSDMethoxychlor
33.3981208 PSTS-LCS
Methoxychior33.3
981208PSTS-LCSD 33.3
22
44
34.6
37
31
32
31.6
17
18.6
32
32
33.6
32.3
66 J]
132
104
111
93
96
95
51 J]
56 J]
96
96
101
97
75-146
71- 173
71- 173
90- 160
90-160
70- 134
70- 134
70- 134
70-134
75- 129
75- 129
55- 173
55- 173
,
~
4.7
~339
17.6
I.3
9.
0.
3.9
YD - Not Detected
This report shall not be reproduced except infull, without the written approval of the laborato~.
NEL LABORATORIES .-
CLIENT BechtelNevadaPROJECTID: V553/I’7777PROJECT #: 17777
TEST PCB’S (Polychlorinated Biphenyls) by EPA 8082, Dec. 1996MATRIX: Solid
PARAMETER
Arochlor- 1016
Arochlor-1016
Arochlor-1 016
Arochlor-1016
Arochior- 1260
Arochlor- 1260
Arochlor-1260
Arochlor-1260
NEL Samrde ID
981208PCBS-LCS
981208 PCBS-LCSD
L98 12048-02-MS
L9812048-02-MSD
981208PCBS-LCS
981208PCBS-LCSD
L9812048-02-MS
L9812048-02-MSD
M!sAmount
333
333
333
333
333
333---J>>
333
Sek.Result
326
289
354
403
309
261
317
373
PercentRecoverv
98
87
106
12193
78
95
112
Acce@able
Ranze - ~
70-130
70-130 1~.
70-130
70-130 4.1
70-130
70-130 I6.8
48- 129
48-129 ]6.2
,
.
.
‘JD- Not Detected
Vrisreport shall not be reproduced except injidl, without the written approval of the laborato~,
NEL LABORATORIES
CLIENT: i3echtel NevadaPROJECT ID: V553117777PROJECT #: 17777
TEST: TCLP/STLC MetalsMATRIX: Solid ‘
PARAMETER
Arsenic
Arsenic
Arsenic
Mercury
Mercury
Mereury
Silver
Silver
‘Silver
Barium
Barium
Barium
Cadmium
Cadmium
Ctidmium
Chromium
Chromium
Chromium
Lead
Lead
Lead
Selenium
Selenium
Selenium
NEL Samrde ID
L12048i-LCS
L98 12048-02-MS
L9812048-02-MSDLl~04&HGo~.L(-3
L9812048-02-MS
L9812048-02-MSD
L12048i-LCS
L9812048-02-MS
L9812048-02-MSD
L12048i-LCS
L9812048-02-MS
L9812048-02-MSD
L12048i-LCS
L98 12048-02-MS
L9812048-02-MSD
L12048i-LCS
L98 12048-02-MS
L9812048-02-MSD
L12048i-LCS
L9812048-02-MS
L9812048-02-MSD
L 12048i-LCS
L9812048-02-MS
L9812048-02-MSD
.
JD - Not Detected
SlmL SI!EEAmount Result—.
0.5 0.495
0.5 0.51
0.5 0.506
0.005 0.00522
0.05 0.0559
0.05 0.0566
0.5 0,463
0.5 0.466
0.5 0.472
1 1.11
1 0.95
1 0.955().2 0.188
0.2 0.198
0.2 0.197
0.5 0.486
0.5 0.49
0.5 0.494
1 0.927
1 1.05
1 1.01
0.5 0.526
0.5 0.576
0.5 0.531
PercentRecovery
99]02
101
104
112
113
93
93
94l]!
95
96
94
99
99
97
98
99
93
105
101
105
115
106
Acce@aMe
Rm!!?85-115
75-125
75- 125
85-115
“75-125
75-125
85-115
75- 125
75-125
85-li5
75-125
75-125
85-115
75- 125
75- 125
85-115
75- 125
75- 125
85-115
75- 125
75- 125
85- 115
75- 125
75- 125
●
~
0.8
1.2
I.:
0.5
0.5 -
0.8
3.9
8.1
“hisreport shall not be reproduced except infull, without the written approval of the laboratory.
NEL LABORATORIES .
CLIENT Bechtel NevadaPROJECT ID: V553/1 7777PROJECT #: 17777
TEST: TCLP by EPA 1311, July 1992& Semivolatiie Organics by EPA Method 8270C; Dec. 1996MATRIX: Solid
PARAMETER
1,4-Dichlorobenzene (p-DCB)
1,4-Dichlorobenzene (p-DCB)
2.4-Dinitrotoluene (DNT)
2.4-Dinitrotoluene (DNT)
Pentachlorophenol
Pentachlorophenol
$iPi!!&NEL Samr.de ID Amount
121098-E3-TCLP-LCS 80
121098-E3-TCLP-LCSD 80
121098-E3-TCLP-LCS 80
121098-E3-TCLP-LCSD 80:
i21098-E3-TCLP-LCS 80
121098-E3-TCLP-LCSD 80
Sfi!EResult
51.554.2
56.4
61.5
56.8
PercentRecovery
64
68
71
77
71
78
Acce~table
IU!!lz!”!w36-97T’ ‘
36:972 5.1~4&96: ::.
24-96 8.7 ‘
9- 103 ““;-
9- 103 9.6-
.
JD - Not Detected
‘his report shall not be reproduced except injidl, without the written approval of the laborato~.
. .
NEL LABORATORIES
CLIENT: Bechtel NevadaPROJECT ID: V553/l?777 ‘PROJECT #: 17777
TEST TCLP by EPA 1311, July 1992& Volatile Organics by EPA 8260B, Dec. 1996MATRIX: Solid
PARAMETER
1,l-Dichioroethene (1,1-DCE)
1.1-Dichloroethene (1, 1-DCE)
1.l-Dichloroethene (1,1-DCE)
Benzene
Benzene
Benzene
Chlorobenzene
Chlorobenzene
NEL Samde ID
9812 11-TCLP-LCS
L98 12048-02-MS
L9812048-02-MSD
98121 I-TCLP-LCS
L9812048-02-MS
L9812048-02-MSD
981211 -TCLP-LCS
L9812048-02-MS
Chlorobenzene L9812048-02-MSD
Toiuene 98121 I-TCLP-LCS
Toluene L9812048-02-MS
Toluene L9812048-02-MSD
Trichloroethene (TCE) 9812 11-TCLP-LCS
Trichioroethene (TCE) L98 12048-02-MS
Trichloroethene (TCE) L9812048-02-MSD
a!kAmount
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
SlwResult
54.09
41
43
45.9
40
39
49.75
44
42
45
33
34
42.8
38
37
PercentRecovery
108
82
86
92
80
78
100
88
84
90
66 J]
68 J]
86
76
74
Acce~table
!h!uE70-130
61-145
61-145
70-130
76-127
76-127
70-130
75- 130
75- 130
70-130
76-125
76- 125
70- 130
71-120
71- 120
~
4.8
2.5
4.7
2.5
2.7 -
.
*
JD - Not Detected
“hisreport shall not be reproduced except injidi, without the written approval of the laboratory.
Bechtel Nevada ColorationANALYTICAL SERVICESLABORATORYP. O. Box 3936, N. Las Vegas, NV 89036 Page
Reported to: Environmental Restoration
CAU 297 EMAD Report Date: 8-DEC-9
J, F. Bonn, M/S NTS306 Sample Defivery Group: B979Batch: 0861
Program: 720
Report No. : ,
Sample Isotope Analysis flesult Error. (lual MDC Result Analysis Sample Size Siza Type Tracer Spike System Packat-item* ● ‘ ● ‘ Identification ‘‘” ● % Flag Units Date Coil Date Units Matrix Yield % RecV % Detector Sample
EMAD-VPOR-3 CS137 , GAM20 1.65E-01 6. IE+O1 5.8E-02 pcilg 12-02-98 12-01-98 5.15E+02 gm SOIL G 05-01 H0177-O-75270
EMAD-VPOR-3 K 40 GAM20 2.49E+01 2.OE+O1 7.OE-01 pcilg 12-02-98 12-01-98 5.15E+02 gm SOIL G 05-01 H01774)-75270
EMAD-VPOR-3 RA226 GAM20 1:20E +00 2,8E+01 1.7E-01 pcilg 12-02-96 12-01-96 5.15E+02 gm So\L G 05-01 HO177-D-75270
EMAD-VPOR-3 TH228 GAM20 2.28E+O0 1.9E+OI 1.6E-01 pcilg 12-02-98 12-01-98 5,15E+02 gm SOIL G 05-01 HO177-@75270
EMAD-VPDR-3 TH232 GAM20 2.41E+O0 3,1E+01 3.3E-01 pcilg 12-02-96 12-01~98 5,15E+02 gm SOIL G 05-01 H0177-D-75270
EMADWDR-4 K 40 GAM20 1.96E +01 2,1E+01 6.5E-01 pCi/g 12-02-98 12-01-98 7,52E+02 gm SOIL G 05-01 HO177-I-75271
EMAD-VPOR-4 RA226 GAM20 1.OIE+OO 3.OE +01 1.5E-01 pcilg 12-02-98 12-01-98 7.52E+02 gm SOIL G 05-01 H0177-1-75271
EMAD-VPOR-4 TH228 GAM20 1.84E+O0 2.OE+O1 1.5E-01 pCi/g 12-02-98 12-01-98 7.52E+02 gm SOiL G 05-01 HO177-I-75271
EMAD-VPOR-4 TH232 GAM20 1.26E+O0 4.lE+O1 3.OE-01 pCilg 12-02-98 12-01-98 7.52E + 02 gm SOiL G 05-01 H0177-1-75271
OA EKG EMPTY BTL U05 No Nucl Det GAM20 0.00EiOO O.OE+OO u O.OE+OO NA 12-02-98 07-01-98 1.00E+OO gm OUAL “05-01 00631-0-00341
Comment: Qualification Flags: Note: % Error is the 2.0 Sigma Er
Data generated from 20 minuta gamma spectroscopy of sampies E = Estimated Quantity
submitted to the laborato~ orr 12/2/98. H = High Recove~ for SampleJ = Result is less than the RDL
Prepared by:‘ate’*
Approved by:‘ate’*g
L = Low Recovery for SampleP = Preliminary RasuksCl = Bad Instrument Quality Control, Result is OKR = Results are Unusable, Resampling is NecessaryU = Result is less than Minimum Detectable Activity
iLevel1
BechtelNevadaColorationANALYTICAL SERVICES LABORATORYP. O. Box 3936, N. Las Vegas, NV 89036
Reported to: Environmental Restoration
CAU 297 EMADJ. F. Bonn, M/S NTS306
Pag
Report Date: 8-DEC-9Sample Defivery Group: B979.
Batch: 0861Program: 500
ReDort No. :
Sample Isotope Analysis Result Error (luai MDA Result Analysis Sample Size Size Type Tracer Spike System Packet-ltar‘‘ ● ‘’ Identification ● ‘ * ● ‘ % Flag Units Date Colt Date Units Matrix Yiald % Ram % Detactor sample
OA EKG EMPTY BTL U05 AM241 GAM20 0.00E +00 O.OE+OO u 2.OE+O1 pci 12-02-8s 07-01-9B 1.00E +00 sm Q(JAL 05-01 00631-0-00341
(IA EKG EMPTY BTL U05 C060 GAM20 0.00E +00 O.OE+00 u 1.3E+01 pci 12-02-98 07-01-96 1.00E+DO sm QUAL 05-01 00631-0-00341
CIA EKG EMPTY BTL U05 CS137 GAM20 0.00E+OO O.OE+OO u 6,2E+O0 pci 12-02-98 07-01-98 1.00E+OO sm QUAL 05-01 t30631-O-00341
OA SP:NAS-A0271 AM241 GilM20 1.BOE+05 B.BE+OO ,2.7E+02 pCi 12-02-98 04-01-92 l,DOE+OO am QUAL 110.8 05-01 006303-16210
OA SPNAS-A0271 C060 GAM20 2.96E+05 8,6E+O0 2.1E+02 pci 12-02-98 04-01-92 1.00E+OO sm f3UAL 99.4 05-01 00630-3-16210
QA SP:NAS-A0271 CS137 GAM20 2.04E+05 B.lE+DO 5.BE+O1 pci 12-02-98 04-01-92 1.00E+OO sm QUAL 100.6 05-01 008303-16210
.
Comment:, Qualification Flags: Note: % Error is the 2.0 Sigma E
Data generated from 20 minute gamma spectroscopy of samples E = Estimated Quantity
submitted to the laboratory on 12/2/98. H = High Recovery for SampleJ = Result is less than the RDL
‘ate:+%f’xL = Low Recovery for Sample
Prepared by: P = Preliminary ResultsQ = Bad Instrument Quality Control, Result is OKR = Results are Unusable, Resampling is Necessary
Approved by: Date: I >/jbJ9g U = Result is less than Minimum Detectable Activity
(’--T. . . F.-z
.-
Bechti Niiiia ->
ANALYTICAL SERWCES LABORA TORYSERWCES REQUEST& ‘CHAINOF CUSTODYRECORD “ Page_ o
wnrxmon: ungmal - I0 M retame.auyramrawy fmwrnmq nnal anmyswCopy 1 -To be retained by Iaboralo
7~ervices LaboratoryCopy 2 -To be reta!ned by Analylicaerformlng Intermedtale analysis
Copy 3 -To be relawred by sampler
BN4
Closure Rqwn. CAU 297EMAD Vscuum PumpOItRemvayDkmbmionListRcwsion: ODate: Msrch IS, Iyjg
DISTRIBUTION LIST
Nevada DeDart ment of Environmental Protection
Paul Liebendorfer 2 (Controlled)*Bureau of Federal FacilitiesDivision of Environmental Protection333 W. Nye Lane, Room 13BCarson City, NV 89706-0866
Michael McKhmon, Las Vegas OffIce 1 (Controlled)*Bureau of Federal Facilities“Divisionof Environmental Protection555 E. Washington, Suite 4300Las Vegas, NV 89010
U.S. Department of Enerw
Janet Appenzeller-Wing 1 (Uncontrolled)*Environmental Restoration DivisionU.S. Department of Energy, Nevada Operations OfficeP.O. BOX98518 M/S 505Las Vegas, NV 89193-8518
Clayton Barrow 1 (Uncontrolled)*Environmental Restoration DivisionU.S. Department of Energy, Nevada Operations OfficeP.O. BOX98518 M/S 505Las Vegas, NV 89193-8518
Sabrina Lawrence 1 (Controlled)*Environmental Restoration DivisionU.S. Department of Energy, Nevada Operations OffIceP.O. BOX98518 M/S 505Las Vegas, NV 89193-8518
DOE Public Reading Facility 1 (Controlled)P.O. BOX98521 M/S NLV040Las Vegas, NV 89193-8521
DOE/Nevada Operations Office 1 (Uncontrolled)Technical Information Resource CenterP.O. BOX98521 ME 505Las Vegas, NV 89193-8521
Closure ReporI - CAU 297EMAD Vacmum Pump Oil RecoveryDkibution LktRevision ODate March 18.1999
DISTRIBUTION LIST (Continued)
U.S. Department of Energy 2 (Uncontrolled)
OffIce of Scientific and Technical Information175 Oak Ridge TurnpikeP.O. BOX62Oak Ridge, TN 37831
Bechtel Nevada
Correspondence ControlBechtel NevadaP.O. BOX98521 ME NLVO08Las Vegas, NV 89193-8521
Jerry BonnBechtel NevadaP.O. BOX98521 M/S NTS306Las Vegas, NV 89193-8521
David CowserBechtel NevadaP.O. BOX98521 M/S NLV082Las Vegas, NV 89193-8521
Ann HeidemaBechtel NevadaP.O. BOX98521 M/S NLV022Las Vegas, NV 89193-8521
Steve NachtBechtel NevadaP.O. BOX98521 M/S NTS306Las Vegas, NV 89193-8521
Jerel NelsonBechtel NevadaP.O. BOX98521 M/S NTS306Las Vegas, NV 89193-8521
1 (Uncontrolled)*
1 (Uncontrolled)*
1 (Uncontrolled)*
1 (Uncontrolled)
1 (Uncontrolled)*
1 (Uncontrolled)*
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