7. lampiran - soegijapranata catholic universityrepository.unika.ac.id/11699/8/12.70.0067 ignatius...

7. LAMPIRAN

7.1. Perhitungan Laju Transmisi Uap Air (WVTR)

Rumus perhitungan laju transmisi uap air / water vapor transmission rate (WVTR)

(ASTM E96, 1995)

Keterangan :

n : Perubahan berat (gram)

t : Waktu (jam)

A : Luas permukaan (m2)

7.1.1. WVTR Edible Film dengan Minyak Sawit 0,75%

WVTR Edible Film Dengan Penambahan Minyak Sawit 0,75% Setelah 1 Jam

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

�� = , � �� = ��,� x 24

Rata – rata = 429,6568� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 367,8121� � ⁄

Rata – rata = 335,6281� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 308,2455� � ⁄

Rata – rata = 310,1736� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 309,2343� � ⁄

Rata – rata = 304,2202 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 309,4938� � ⁄

Rata – rata = 307,0508� � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 305,5489� � ⁄

Rata – rata = 302,5185 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

7.1.2. WVTREdible Film dengan Minyak Sawit 0,5%

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 294,9448� � ⁄

Rata – rata = 496,0324� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 379,1219� � ⁄

Rata – rata = 356,8229� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 351,7021� � ⁄

Rata – rata = 338,5018� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 333,4285� � ⁄

Rata – rata = 328,7171 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 325,6816� � ⁄

Rata – rata = 323,6606� � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 323,7506� � ⁄

Rata – rata = 316,0231 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

7.1.3. WVTR Edible Film dengan Minyak Sawit 0,25%

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 307,5383� � ⁄

Rata – rata = 812,3008� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = . � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 605,3468� � ⁄

Rata – rata = 518,8838� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 460,8464� � ⁄

Rata – rata = 426,3417� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = , � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 412,7340� � ⁄

Rata – rata = 395,8784 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 376,9351� � ⁄

Rata – rata = 371,0335� � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 354,4195� � ⁄

Rata – rata = 342,5067 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

7.1.4. WVTR Edible Film Tanpa Penambahan Minyak Sawit

WVTR Edible Film Dengan Penambahan Minyak Sawit 0% Setelah 1 Jam

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 333,2082� � ⁄

Rata – rata = 884,6363� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Rata – rata = 617,2591� � ⁄

Rata – rata = 529,6922� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 475,8274� � ⁄

Rata – rata = 444,2333� � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 �� = ,, � � = , � � ⁄

Ulangan 4 �� = ,, � � = , � � ⁄

Ulangan 5 �� = ,, � � = , � � ⁄

Ulangan 1 �� = ,, � � , = , � � ⁄

Ulangan 2 �� = ,, � � , = , � � ⁄

Ulangan 3 �� = ,, � � , = , � � ⁄

Ulangan 4 �� = ,, � � , = , � � ⁄

Ulangan 5 �� = ,, � � , = , � � ⁄

Rata – rata = 437,7678� � ⁄

Rata – rata = 412,5209 � � ⁄

Ulangan 1 �� = ,, � � = , � � ⁄

Ulangan 2 �� = ,, � � = , � � ⁄

Ulangan 3 WVTR = ,, x x = , g jam m⁄

Ulangan 1 WVTR = ,, x x , = , g jam m⁄

Rata – rata = 409,7854� � ⁄

Rata – rata = 393,9996� � ⁄

Ulangan 4 WVTR = ,, x x , = g jam m⁄

Rata – rata = 385,2903� � ⁄

Rata – rata = 377,7027 � � ⁄

WVTR Edible Film Dengan Penambahan Minyak Sawit 0% Setelah 2,4 Jam

Ulangan 2 WVTR = ,, x x = , , g jam m⁄

Rata – rata = 371,0568� � ⁄

7.1.3. Uji SPSS WVTR

7.1.3.1. Uji Normalitas

7.1.3.2. Uji Duncan

Jam_ke_1

Duncana

Perlakuan N Subset for alpha = 0.05

Minyak 0,75% 5 429,7568

Minyak 0,5% 5 496,0324

Minyak 0,25% 5 812,3008

Minyak 0% 5 884,6363

Sig. ,621 ,590

Means for groups in homogeneous subsets are

displayed.

a. Uses Harmonic Mean Sample Size = 5,000.

Jam_ke_2

Duncana

Minyak 0,75% 5 367,8121

Minyak 0,5% 5 379,1219

Minyak 0,25% 5 605,3468

Minyak 0% 5 617,2591

Sig. ,857 ,850

displayed.

Jam_ke_3

Duncana

Minyak 0,75% 5 335,6281

Minyak 0,5% 5 356,8229

Minyak 0,25% 5 518,8838

Minyak 0% 5 529,6922

Sig. ,650 ,817

displayed.

Jam_ke_4

Duncana

Minyak 0,75% 5 308,2455

Minyak 0,5% 5 351,7021

Minyak 0,25% 5 460,8464

Minyak 0% 5 475,8274

Sig. ,280 ,705

displayed.

Jam_ke_5

Duncana

Minyak 0,75% 5 310,1736

Minyak 0,5% 5 338,5018

Minyak 0,25% 5 426,3417

Minyak 0% 5 444,2333

Sig. ,399 ,592

displayed.

Jam_ke_6

Duncana

Minyak 0,75% 5 309,2343

Minyak 0,5% 5 333,4285

Minyak 0,25% 5 412,7340

Minyak 0% 5 437,7686

Sig. ,432 ,417

displayed.

Jam_ke_7

Duncana

Minyak 0,75% 5 304,2202

Minyak 0,5% 5 328,7171

Minyak 0,25% 5 395,8784

Minyak 0% 5 412,5209

Sig. ,394 ,560

displayed.

Jam_ke_8

Duncana

Minyak 0,75% 5 309,4938

Minyak 0,5% 5 325,6816 325,6816

Minyak 0,25% 5 376,9351 376,9351

Minyak 0% 5 409,7854

Sig. ,574 ,088 ,261

Means for groups in homogeneous subsets are displayed.

Jam_ke_9

Duncana

Minyak 0,75% 5 307,0508

Minyak 0,5% 5 323,6606 323,6606

Minyak 0,25% 5 371,0335 371,0335

Minyak 0% 5 393,9996

Sig. ,526 ,083 ,383

Means for groups in homogeneous subsets are displayed.

Jam_ke_10

Duncana

Minyak 0,75% 5 305,5489

Minyak 0,5% 5 323,7506

Minyak 0,25% 5 354,4195 354,4195

Minyak 0% 5 385,2903

Sig. ,085 ,240

displayed.

Jam_ke_11

Duncana

Minyak 0,75% 5 302,5185

Minyak 0,5% 5 316,0231

Minyak 0,25% 5 342,5067 342,5067

Minyak 0% 5 377,7027

Sig. ,137 ,166

displayed.

Jam_ke_12

Duncana

Minyak 0,75% 5 294,9448

Minyak 0,5% 5 307,5383

Minyak 0,25% 5 333,2082 333,2082

Minyak 0% 5 371,0568

Sig. ,139 ,125

displayed.

7.2. Pendugaan Umur Simpan

7.2.1. Pendugaan Umur Simpan Parameter Angka TBA

7.2.1.1. Angka TBAEdible Film dengan Minyak 0,25% Suhu 25˚C

Hari Absorbansi TBA Rata-

rata Ul 1 Ul 2 Ul 3 Ul 1 Ul 2 Ul 3

0 0,0059 0,0070 0,0063 0,1381 0,1638 0,1474 0,1498

2 0,0056 0,0087 0,0063 0,1310 0,2036 0,1474 0,1607

4 0,0075 0,0068 0,0070 0,1755 0,1591 0,1638 0,1661

6 0,0079 0,0073 0,0072 0,1849 0,1708 0,1685 0,1747

8 0,0073 0,0083 0,0076 0,1708 0,1942 0,1778 0,1810

10 0,0081 0,0093 0,0097 0,1895 0,2176 0,2270 0,2114

12 0,0094 0,0108 0,0115 0,2200 0,2527 0,2691 0,2473

14 0,0158 0,0131 0,0126 0,3697 0,3065 0,2948 0,3237

7.2.1.2. Angka TBA Edible Film dengan Minyak 0,25% Suhu 40˚C

rata Ul 1 Ul2 Ul3 Ul 1 Ul 2 Ul 3

0 0,0056 0,0052 0,0022 0,1310 0,1217 0,0515 0,1014

2 0,0067 0,0096 0,0012 0,1568 0,2246 0,0281 0,1365

4 0,0092 0,0085 0,0094 0,2153 0,1989 0,2200 0,2114

6 0,0100 0,0115 0,0124 0,2340 0,2691 0,2902 0,2644

8 0,0166 0,0161 0,0162 0,3884 0,3767 0,3791 0,3814

10 0,0153 0,0159 0,0179 0,3580 0,3721 0,4189 0,3830

12 0,0198 0,0225 0,0172 0,4633 0,5265 0,4025 0,4641

14 0,0292 0,0263 0,0288 0,6833 0,6154 0,6739 0,6575

0 0,0032 0,0035 0,0037 0,0749 0,0819 0,0866 0,0811

2 0,0005 0,0101 0,0143 0,0117 0,2363 0,3346 0,1942

4 0,0103 0,0101 0,0099 0,2410 0,2363 0,2317 0,2363

6 0,0145 0,0148 0,0142 0,3393 0,3463 0,3323 0,3393

8 0,0212 0,0215 0,0211 0,4961 0,5031 0,4937 0,4976

10 0,0255 0,0259 0,0261 0,5967 0,6061 0,6107 0,6045

12 0,0280 0,0272 0,0394 0,6552 0,6365 0,9220 0,7379

14 0,0456 0,0445 0,0424 1,0670 1,0413 0,9922 1,0335

0 0,0056 0,0063 0,0065 0,1310 0,1474 0,1521 0,1435

2 0,0068 0,0071 0,0064 0,1591 0,1661 0,1498 0,1583

4 0,0085 0,0065 0,0071 0,1989 0,1521 0,1661 0,1724

6 0,0079 0,0092 0,0082 0,1849 0,2153 0,1919 0,1973

8 0,0087 0,0087 0,0099 0,2036 0,2036 0,2317 0,2129

10 0,0103 0,0099 0,0097 0,2410 0,2317 0,2270 0,2332

12 0,0111 0,0148 0,0122 0,2597 0,3463 0,2855 0,2972

14 0,0208 0,0101 0,0179 0,4867 0,2363 0,4189 0,3806

0 0,0028 0,0054 0,0033 0,0655 0,1264 0,0772 0,0897

2 0,0042 0,0055 0,0104 0,0983 0,1287 0,2434 0,1568

4 0,0094 0,0098 0,0087 0,2200 0,2293 0,2036 0,2176

6 0,0131 0,0114 0,0117 0,3065 0,2668 0,2738 0,2824

8 0,0138 0,0134 0,0166 0,3229 0,3136 0,3884 0,3416

10 0,0277 0,0294 0,0152 0,6482 0,6880 0,3557 0,5639

12 0,0292 0,0290 0,0310 0,6833 0,6786 0,7254 0,6958

14 0,0316 0,0322 0,0329 0,7394 0,7535 0,7699 0,7543

0 0,0048 0,0024 0,0065 0,1123 0,0562 0,1521 0,1069

2 0,0093 0,0099 0,0101 0,2176 0,2317 0,2363 0,2285

4 0,0131 0,0124 0,0129 0,3065 0,2902 0,3019 0,2995

6 0,0178 0,0162 0,0176 0,4165 0,3791 0,4118 0,4025

8 0,0193 0,0186 0,0173 0,4516 0,4352 0,4048 0,4306

10 0,0282 0,0335 0,0288 0,6599 0,7839 0,6739 0,7059

12 0,0394 0,0389 0,0383 0,9220 0,9103 0,8962 0,9095

14 0,0437 0,0535 0,0511 1,0226 1,2519 1,1957 1,1567

0 0,0082 0,0056 0,0054 0,1919 0,1310 0,1264 0,1498

2 0,0082 0,0065 0,0064 0,1919 0,1521 0,1498 0,1646

4 0,0081 0,0074 0,0073 0,1895 0,1732 0,1708 0,1778

6 0,0081 0,0079 0,0083 0,1895 0,1849 0,1942 0,1895

8 0,0113 0,0121 0,0092 0,2644 0,2831 0,2153 0,2543

10 0,0106 0,0094 0,0111 0,2480 0,2200 0,2597 0,2426

12 0,0144 0,0177 0,0154 0,3370 0,4142 0,3604 0,3705

14 0,0217 0,0224 0,0202 0,5078 0,5242 0,4727 0,5015

0 0,0032 0,0035 0,0037 0,0749 0,0819 0,0866 0,0811

2 0,0162 0,0173 0,0151 0,3791 0,4048 0,3533 0,3791

4 0,0210 0,0177 0,0169 0,4914 0,4142 0,3955 0,4337

6 0,0239 0,0252 0,0228 0,5593 0,5897 0,5335 0,5608

8 0,0433 0,0214 0,0232 1,0132 0,5008 0,5429 0,6856

10 0,0331 0,0364 0,0286 0,7745 0,8518 0,6692 0,7652

12 0,0557 0,0583 0,0479 1,3034 1,3642 1,1209 1,2628

14 0,0748 0,0649 0,0633 1,7503 1,5187 1,4812 1,5834

0 0,0010 0,0004 0,0011 0,0234 0,0094 0,0257 0,0195

2 0,0174 0,0181 0,0185 0,4072 0,4235 0,4329 0,4212

4 0,0355 0,0283 0,0232 0,8307 0,6622 0,5429 0,6786

6 0,0316 0,0327 0,0321 0,7394 0,7652 0,7511 0,7519

8 0,0370 0,0313 0,0422 0,8658 0,7324 0,9875 0,8619

10 0,0511 0,0576 0,0533 1,1957 1,3478 1,2472 1,2636

12 0,0735 0,0713 0,0776 1,7199 1,6684 1,8158 1,7347

14 0,0748 0,0830 0,0916 1,7503 1,9422 2,1434 1,9453

7.2.1.10. Rata-Rata Angka TBA Edible Film

Konsentrasi Suhu

Angka TBA

Waktu Penyimpanan (hari)

0 2 4 6 8 10 12 14

Minyak

25 0,1497 0,1646 0,1778 0,1895 0,2543 0,2426 0,3705 0,5015

40 0,0811 0,3791 0,4337 0,5608 0,6856 0,7652 1,2628 1,5834

50 0,0195 0,4212 0,6786 0,7519 0,8619 1,2636 1,7347 1,9453

Minyak

25 0,1435 0,1583 0,1724 0,1973 0,2129 0,2332 0,2971 0,3806

40 0,0897 0,1568 0,2176 0,2824 0,3416 0,5639 0,6958 0,7542

50 0,1068 0,2285 0,2995 0,4025 0,4306 0,7059 0,9095 1,1567

Minyak

25 0,1497 0,1607 0,1661 0,1747 0,1810 0,2114 0,2473 0,3237

40 0,1014 0,1365 0,2114 0,2644 0,3814 0,3830 0,4641 0,6575

50 0,0811 0,1942 0,2363 0,3393 0,4976 0,6045 0,7379 1,0335

7.2.1.11. Nilai Ln Rata-Rata

Konsentrasi Suhu

Angka TBA

Waktu Penyimpanan (hari)

0 2 4 6 8 10 12 14

Minyak

25 -1,8991 -1,8042 -1,7271 -1,6634 -1,3692 -1,4163 -0,9929 -0,6902

40 -2,5121 -0,9700 -0,8354 -0,5784 -0,3775 -0,2676 0,2333 0,4596

50 -3,9373 -0,8646 -0,3877 -0,2852 -0,1486 0,2340 0,5508 0,6654

Minyak

25 -1,9414 -1,8433 -1,7579 -1,6230 -1,5469 -1,4559 -1,2137 -0,9660

40 -2,4113 -1,8528 -1,5251 -1,2644 -1,0741 -0,5729 -0,3627 -0,2821

50 -2,2368 -1,4762 -1,2056 -0,9101 -0,8426 -0,3483 -0,0949 0,1456

Minyak

25 -1,8991 -1,8282 -1,7952 -1,7447 -1,7093 -1,5540 -1,3972 -1,1279

40 -2,2887 -1,9914 -1,5540 -1,3303 -0,9639 -0,9597 -0,7677 -0,4193

50 -2,5121 -1,6389 -1,4427 -1,0809 -0,6980 -0,5034 -0,3039 0,0330

7.2.1.12. Kualitas TBA Awal (Q0)

Konsentrasi Minyak (%) Angka TBA Awal Ln

0,75 0,08346 -2,483388

0,50 0,11336 -2,177187

0,25 0,11076 -2,200390

Batas Kritis (Qc) 2 0,693147

7.2.1.13. Unit Kualitas

Konsentrasi Minyak (%) Orde 0 Orde 1

0,75 1,91654 -3,176535

0,50 1,88664 -2,870334

0,25 1,88924 -2,893537

7.2.1.14. Orde Reaksi Konstan

Konsentrasi

Minyak

Reaction Order 0 Reaction Order 1

25 40 50 25 40 50

k R2 k R

0,75 0,02233 0,80722 0,09556 0,91586 0,13044 0,96233 0,08180 0,90452 0,17096 0,84296 0,24582 0,67108

0,50 0,01519 0,87597 0,05027 0,95483 0,07144 0,93495 0,06523 0,95240 0,15121 0,97289 0,15606 0,96198

0,25 0,01067 0,80164 0,03668 0,94755 0,06338 0,95460 0,04945 0,87394 0,12711 0,96699 0,16481 0,95410

7.2.1.15. Plot Arrhenius

Konsentrasi

Minyak (%)

Orde 0 Orde 1

T (˚C) T (K) 1/T Ln kT 1/T Ln kT

25 298 0,003356 -3,801936176 0,003356 -2,503433895

40 313 0,003195 -2,348008431 0,003195 -1,766338415

50 323 0,003096 -2,036869308 0,003096 -1,403139915

25 298 0,003356 -4,187023920 0,003356 -2,729844057

40 313 0,003195 -2,990382324 0,003195 -1,889103091

50 323 0,003096 -2,638967334 0,003096 -1,857517127

25 298 0,003356 -4,540386159 0,003356 -3,006723245

40 313 0,003195 -3,305436005 0,003195 -2,062713523

50 323 0,003096 -2,758612560 0,003096 -1,802973210

7.2.1.16. Ln kT pada Suhu 25˚C

Koonsentrasi

Minyak (%)

ordo 0 ordo 1

lnkT kT lnkT kT

0,75 -3,71197 0,024429275 -2,489523 0,0829495

0,50 -4,12769 0,016120094 -2,654938 0,0703032

0,25 -4,50756 0,011025296 -2,957217 0,0519633

7.2.1.17. Umur Simpan pada Suhu 25˚C Berdasar Angka TBA

Umur Simpan Orde 0 = Q – Q ��

Umur Simpan Orde 1 = Q – Q��

1. Edible Film Karagenan + Minyak 0,75%

Umur Simpan Orde 1 = − , – , , = , ℎ�

Umur Simpan Orde 0 = − , , = ℎ�

Umur Simpan Orde 0 = – , , = ℎ�

7.2.2. Pendugaan Umur Simpan Parameter Kadar Air

7.2.2.1. Kadar Air Edible Film Tanpa Minyak Sawit Suhu 25˚C

Hari Ul 1 Ul 2 Ul 3 Rata-rata

0 15,14 16,14 14,46 15,25

2 15,45 16,40 18,12 16,66

4 15,46 22,28 17,22 18,32

6 20,16 19,57 20,95 20,23

8 22,66 21,54 20,20 21,47

10 21,68 22,57 21,15 21,80

12 24,20 21,14 22,28 22,54

14 21,17 23,28 22,90 22,45

0 17,05 16,17 16,47 16,56

2 17,34 17,96 16,53 17,28

4 18,65 18,97 19,70 19,11

6 19,54 19,65 19,32 19,50

8 21,51 21,00 22,79 21,77

10 22,62 21,81 22,85 22,43

12 23,61 22,83 21,63 22,69

14 23,95 23,60 21,92 23,16

0 16,80 18,75 16,15 17,23

2 17,93 17,10 18,90 17,98

4 19,62 20,95 19,98 20,18

6 20,74 20,87 21,65 21,09

8 21,70 21,51 22,90 22,04

10 23,95 22,17 22,22 22,78

12 22,62 22,74 24,52 23,29

14 24,77 23,38 24,53 24,23

7.2.2.4. Kadar Air Edible Film dengan Minyak Sawit 0,25% Suhu 25˚C

0 16,83 15,58 16,33 16,25

2 16,92 16,61 16,24 16,59

4 17,73 16,22 17,91 17,29

6 18,13 18,86 16,72 17,90

8 19,20 18,76 17,51 18,49

10 22,93 21,42 19,68 21,34

12 22,31 22,96 24,19 23,15

14 24,30 22,73 22,97 23,33

0 16,53 15,72 17,80 16,68

2 17,50 17,12 19,60 18,07

4 18,53 19,14 19,72 19,13

6 19,10 19,25 19,94 19,43

8 19,75 21,38 20,82 20,65

10 23,68 21,98 23,20 22,95

12 23,43 22,76 23,59 23,26

14 23,26 24,71 24,12 24,03

0 16,65 17,78 15,30 16,58

2 18,50 18,12 19,60 18,74

4 20,53 19,14 20,72 20,13

6 21,24 21,10 20,68 21,01

8 21,81 22,62 21,75 22,06

10 24,75 23,37 23,87 24,00

12 23,61 24,93 24,30 24,28

14 25,16 25,97 24,52 25,22

0 19,20 15,58 18,10 17,63

2 19,27 17,35 19,42 18,68

4 18,32 20,22 20,01 19,52

6 20,08 17,88 19,47 19,14

8 21,42 18,83 22,76 21,00

10 20,88 20,59 22,03 20,74

12 22,31 23,46 19,89 21,89

14 22,01 22,35 21,66 22,01

0 18,83 19,56 18,24 18,88

2 19,51 18,95 19,44 19,30

4 18,35 20,80 18,92 19,36

6 20,71 20,93 20,86 20,83

8 22,76 20,85 21,18 21,60

10 22,10 21,70 21,38 21,73

12 22,00 21,81 22,64 22,15

14 23,15 23,97 23,86 23,66

0 17,53 18,16 18,62 18,10

2 18,52 18,83 19,02 18,79

4 20,57 19,12 20,41 20,03

6 21,60 20,84 20,97 21,14

8 22,93 22,42 21,11 22,15

10 22,10 23,70 22,38 22,73

12 22,85 23,52 22,96 23,11

14 24,54 23,63 24,73 24,30

0 18,37 16,95 17,29 17,54

2 20,43 15,48 17,28 17,73

4 20,16 16,68 16,61 17,82

6 19,53 22,18 19,47 20,39

8 21,86 18,93 20,88 20,56

10 21,28 23,02 23,62 22,64

12 24,07 21,28 23,39 22,91

14 22,31 22,90 24,27 23,16

0 19,18 15,72 15,91 16,94

2 15,45 16,37 15,55 15,79

4 19,84 18,58 18,35 18,92

6 21,52 20,69 20,15 20,79

8 21,19 21,60 19,20 20,66

10 24,12 22,32 22,54 22,99

12 22,75 23,62 23,18 23,18

14 23,19 23,47 24,73 23,80

0 16,92 17,53 16,41 16,95

2 18,87 17,95 18,96 18,59

4 19,18 18,58 20,00 19,25

6 19,98 19,42 20,79 20,06

8 21,14 21,52 21,65 21,44

10 22,17 22,98 23,71 22,95

12 23,20 24,64 23,50 23,78

14 25,40 25,02 26,11 25,51

7.2.2.10. Rata-Rata Kadar Air Edible Film

Konsentrasi

Minyak

Kadar Air (%)

Waktu Penyimpanan (Hari)

0 2 4 6 8 10 12 14

Minyak

25 17,54 17,73 17,82 20,39 20,56 22,64 22,91 23,16

40 16,94 15,79 18,92 20,79 20,66 22,99 23,18 23,80

50 16,95 18,59 19,25 20,06 21,44 22,95 23,78 25,51

Minyak

25 17,63 18,68 19,52 19,14 21,00 20,74 21,89 22,01

40 18,88 19,30 19,36 20,83 21,60 21,73 22,15 23,66

50 18,10 18,79 20,03 21,14 22,15 22,73 23,11 24,30

Minyak

25 16,25 16,59 17,29 17,90 18,49 21,34 23,15 23,33

40 16,68 18,07 19,13 19,43 20,65 22,95 23,26 24,03

50 16,58 18,74 20,13 21,01 22,06 24,00 24,28 25,22

Minyak 0%

25 15,25 16,66 18,32 20,23 21,47 21,80 22,54 22,45

40 16,56 17,28 19,11 19,50 21,77 22,43 22,69 23,16

50 17,23 17,98 20,18 21,09 22,04 22,78 23,29 24,23

7.2.2.11. Nilai Ln Rata-Rata

Konsentrasi

Minyak

Kadar Air (%)

Waktu Penyimpanan (Hari)

0 2 4 6 8 10 12 14

Minyak

25 2,864 2,875 2,880 3,015 3,023 3,120 3,132 3,142

40 2,829 2,759 2,940 3,034 3,028 3,135 3,143 3,170

50 2,830 2,923 2,958 2,999 3,065 3,133 3,169 3,239

Minyak

25 2,869 2,927 2,971 2,952 3,045 3,032 3,086 3,091

40 2,938 2,960 2,963 3,037 3,073 3,079 3,098 3,164

50 2,896 2,933 2,997 3,051 3,098 3,124 3,140 3,190

Minyak

25 2,788 2,809 2,850 2,885 2,917 3,061 3,142 3,150

40 2,814 2,894 2,951 2,967 3,028 3,133 3,147 3,179

50 2,808 2,931 3,002 3,045 3,094 3,164 3,190 3,214

Minyak 0%

25 2,724 2,813 2,908 3,007 3,067 3,082 3,115 3,111

40 2,802 2,849 2,950 2,971 3,080 3,110 3,122 3,142

50 2,847 2,889 2,954 3,049 3,093 3,126 3,148 3,160

7.2.2.12. Kualitas Kadar AirAwal (Q0)

Konsentrasi Minyak (%) Kadar air Awal Ln

0,75 17,14 2,842

0,50 18,20 2,902

0,25 16,50 2,803

0 16,32 2,792

Batas Kritis (Qc) 35 3,556

7.2.1.13. Unit Kualitas

Konsentrasi Minyak (%) Orde 0 Orde 1

0,75 17,85778 -0,7138

0,50 16,79778 -0,6538

0,25 18,49778 -0,75185

0 18,68333 -0,76316

7.2.1.14. Orde Reaksi Konstan

Konsentrasi

Minyak

Reaction Order 0 Reaction Order 1

25 40 50 25 40 50

k R2 k R

0,75 0,4757 0,9282 0,5778 0,9098 0,5851 0,9895 0,0235 0,9246 0,0290 0,8862 0,0279 0,9916

0,50 0,3108 0,9308 0,3310 0,9498 0,4409 0,9840 0,0156 0,9267 0,0158 0,9529 0,0210 0,9767

0,25 0,5665 0,9199 0,5360 0,9733 0,5804 0,9741 0,0290 0,9352 0,0263 0,9730 0,0278 0,9541

0 0,5448 0,9185 0,5125 0,9506 0,4917 0,9535 0,0286 0,8995 0,0258 0,9409 0,0241 0,9422

7.2.1.15. Plot Arrhenius

Konsentrasi

Minyak (%)

Orde 0 Orde 1

T (˚C) T (K) 1/T Ln kT 1/T Ln kT

25 298 0,003356 -0,74302 0,003356 -3,74874

40 313 0,003195 -0,5485 0,003195 -3,53898

50 323 0,003096 -0,53591 0,003096 -3,57981

25 298 0,003356 -1,16872 0,003356 -4,16078

40 313 0,003195 -1,10566 0,003195 -4,14859

50 323 0,003096 -0,81891 0,003096 -3,86528

25 298 0,003356 -0,56819 0,003356 -3,54183

40 313 0,003195 -0,62360 0,003195 -3,63709

50 323 0,003096 -0,54411 0,003096 -3,58228

25 298 0,003356 -0,60741 0,003356 -3,5549

40 313 0,003195 -0,66849 0,003195 -3,65644

50 323 0,003096 -0,70983 0,003096 -3,72673

7.2.1.16. Ln kT pada Suhu 25˚C

Koonsentrasi

Minyak (%)

ordo 0 ordo 1

lnkT kT lnkT kT

0,75 -0,72651 0,483596 -3,72254 0,024173

0,50 -1,20698 0,2991 -4,20333 0,014946

0,25 -0,58571 0,556708 -4,88741 0,007541

0 -3,24413 0,039002 -7,97437 0,000344

7.2.1.17. Umur Simpan pada Suhu 25˚C Berdasar Kadar Air

Umur Simpan Orde 0 = Q – Q ��

Umur Simpan Orde 1 = Q – Q��

Umur Simpan Orde 0 = – ,, = , ℎ�

Umur Simpan Orde 0 = − , , = ℎ�

Umur Simpan Orde 1 = , – , , = , ℎ�

4. Edible Film Tanpa Penambahan Minyak

Umur Simpan Orde 0= – , , = ℎ�

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