air sampling test results (data is available for review · pdf filefilter and reagent blanks...

EE3It CORPORATION

July 15. 1985

r;''"i',T:^ _

.!!'- U '.! 2- 02

Project No. 683001

Mr. Richard KarkkainenVertac Chemical Cornoration24th Floor5100 Poolar StreetIIeraphis, TM 38137Mr. James PerryHercules, IncorporatedC/0 Vertac Chemical PlantJacksonville, AR 72076

1984 Air Sampling Test ResultsVertac Chemical PlantJacksonville, Arkansas

Dear Sirs:Enclosed are the air sampling test results associated with the1984 remedial action activities. The results are summarized ontwo niemoranduras dated October 9 , 1984 and October 30, 1984.Certificate of analysis forms from the laboratory are also in-cluded.If you have any questions or require additional information,please call me at your convenience. ^.(^

^<€ ^

Very Truly Yours,Very Truly Yours, ,S^^.a^- /.ps<'<Glcnn D. Schwtrtz \ ( / v^ WGlcnn D. Schwartzcc: P BigelowB Bundy

D CottonA HusakD Keilroan

Regional OfficeIT Corporation • 10 Dull Road. Pittsburgh. Pennsylvania 15235 . 412-243-3230

MemorandumIT CORPORATION

To: B. P. Bundy Date: October 9. 1984

From: [(_ Sessa Projece No. 846543

Subject; Air Sampling Results - Vercac

Preliminary background area air sampling was conducted at the Vertac

plant work sice from August 10 to 14, 1984. Contaminants sampled for

were dioxin and total volatile organic hydrocarbons. North, south,

east, and west perimeter monitoring sites were set up at the plant

perimeters for this and subsequent area monitoring. Dioxin results are

as follows:

LOCATION RESULTS

East perimeter monitoring site None detected

South perimeter monitoring sice None detected

West perimeter monitoring site None detected

North perimeter monitoring site None detected

East perimeter monitoring site None detected

South perimeter monitoring site None detected

West perimeter monitoring site None detected

Central monitoring site near , . -o f f ice trailers Tlone ^ected

SAMPLE NO.

PM-810-007

PM-810-009

PH-810-010

PM-813-013

PM-813-014

PM-813-015PM-813-016

PM-813-017

DATE

8/10/84

8/10/84

8/10/84

8/13/84

8/13/84

8/13/84

8/13/84

8/13/84

Area and personnel air sampling was performed during the actualactivities of pond sludge removal and slurry wall construction. Dioxin

results are:

SAMPLE NO.

850

85.1

853

872

DATE

9/12/84

9/13/84

9/13/84

9/14/84

878 9/14/84

'LOCATION

Central, location; west of theoffice trailer, about 4 feet upNorth perimeter monitoring sicenear slurry wall construction

West perimeter monitoring sitenear pond sludge removalCentral location; west ofoff ice trailerPersonnel sample taken on dozeroperator during pond sludgeremoval activities

RESULTS

None detected

None detected

None detected

None detected

None defected

None of the samples taken for 245-T or 24-D have been analyzed yet by ITCorporation's Middlebrook Pike laboratory in Knoxville, Tennessee due toa heavy work load. Results should be similar to those found for dioxin.

Middlebrook Pike is also doing volatile organic hydrocarbon sample

analyses, but results are not in yet for the same reasons.

Organic vapor analyzer sampling is being done continuously during sicework and has not shown any results.

All resul ts of samples not yet analyzed shall be reported as soon asthey are received.

Dioxin and volatile organics sampling shall be continued for allremaining phases of site work.

RS;rsg

IT COBPOBATION

•- -^ S fe? S t -ymS^ a ? ^Sim9»-=a^IB •l&Ws'a&g &^Si,¥&W&S

STEWABT LABORATORIES DIVISION5815 Middlebrook Pike- Knoxville. Tennessee 37921 • 615-5:: -M01

CERTIFICATE OF ANALYSIS

TO R.-SESSAc/o IT CORP at DIAMOND SHAMROCK80 LISTER AVENEWARK, NJ 07105

DATE REPORTED: verbal report Sept 11 1984PROJECT CODE VERTACORDER NUMBER-PAGE I OF _1_ . !"~

INDUSTRIAL HYGIENE ANALYSIS REPORTSampleNumber

10-007

10-009

10-010

10-013

10-014

10-015

10-016

0-017

R BLANK

1K082

AnalyzedFor

TCDD

TCDD

TCDD

TCDD

TCDD

TCDD

TCDD

TCDD

TCDD

TCDD

iik,

Method of Analysis

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

EPA JAR EXTRACTION

Resul t s 03 °ND (1.01 ng/n )

ND (1.17 ng/m3)

ND (1.14 ng/m )

ND (1.58 ng/n3)

ND (1.08 ng/m )

ND (0.90 ng/m3)3

ND (1.05 ng/m )

ND (0.78 ng/n )

ND (1.20 ng/f i l ter)

ND (0.23 ppb)

i(^rJ3aArtg? ^ji~ll6i Supervisor: ^N^0 00 Co^Vxt-VU) ^/ i ' ii D a t e S i g n a t u r e D a t e

Chemis t :Signature Date

Reviewed by Industr ial Hygienist :Signature Date

EHIT COStfQSXnOH

IT ANALYTICAL SE^CES58l5Miadlebrook Pike • Knoxville. Tennessee 37921 • 615-538-640)


TO IT CorporationATTN: Ruffie Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTED October 12, 1984PROJECT CODE VER 18554

ORDER NUMBER

Sample Description: Ten (10) hexane extracts received September 5, 1984 '•

Concentration units are total ug's per extract

2,4-D

PM-810-PM-810-PM-810-'PM-810-iPM-810-1PM-810-iPM-810-iPM-810-iFilter IReagent

007009010013014015016017BlankBlank

<0.004<0.004<0.008<0,004<0,004<0.003<0.008<0.004<0.008<0.008

2.4.5-TP ( S i l v e x )

<0.002<0.008<0.002<0.004<0.06<0.0008<0.020<0.004<0.01<0.002

" October. J984January 16. 1988

' Noiapr Puslic^^

c ^--' 'Laboratory Manaoer

J&flL n^& Accrec:ted by the American Aooeiation lor LaboraiorY Accreciiiorion :n ih« c/rmical^y ll OK* [;eia c[ ww-g 31 lufa ;ri tr-e curreni AALA ireciory ol Accrecitea Laboroicnes

i33IT CORPORATION

MemorandumTo B. P. Bundy Date October 30, 1984

From: R. Sesaa Project No. 846543

Subject Air Sampling Results - Vertac C

Sample extracts from air sampling conducted August 10 to 13, 1984, which0

consisted of background area air sampling, were analyzed for pesticides2,4-D and 2,4,5-T in addicion to dioxin (TCDD). The dioxin results werereported October 9, 1984. The results for 2,4-D and 2,4,5-T from these

samples are as follows:

RESULTSSAMP],E NUMBER DATE LOCATION ^ p ^ g ^

PM-810-007 8/10/84 East perimeter None Nonemonitoring sice Detected Detected

PM-810-009 8/10/84 South perimeter None Nonemonitoring site Detected Detected

PM-810-010 8/10/84 West perimeter None Nonemonitoring site Detected Detected

PM-813-013 8/13/84 North perimeter None Nonemonitoring site Detected Detected

PM-S13-014 8/13/84 East perimeter None Nonemonitoring site Detected Detected

PM-S^-^OIS 8/13/84 South perimeter None Nonemonitoring site Detected Detected

PM-813-016 8/13/84 West perimeter None Nonemonitoring site Detected Detected

PH-813-017 8/13/84 Central monitoring None Nonesite near off ice Detected Detectedtrailers

Filter and reagent blanks also showed none detected.

All less-than indications show none detected. "None detected" standsfor both front and back sections of the charcoal Cubes.

Two samples fron this background sampling period were run by pulling' volumes of air through charcoal absorbent tubes. The sample numbers,

dates, and locations were:

SAMPLE NUMBER DATE LOCATION ;

PM-814-026 8/14/84 North perimeter monitoring sitePM-814-027 8/14/84 South perimeter monitoring sice r

<These two samples underwent a series of analyses for the following:

1. Acid extractable organics - priority pollutantanalysis

2. Base-neutral extraccable organics - prioritypollutant analysis

3. Additional organic pollutants - no extraneouspeaks detected.

(See attached results from laboratory.)

No detectable levels of any contaminants were found in these samples.All less-than indications are below the detection limit.

During the course of work activities at Vertac (pond sludge removal andslurry wall construction) conducted September 12 to September 14,sampling was conducted for dioxin and volatile organics. Dioxin resultsfrom this period have already been reported. The following are resultsfrom samples taken for volatile organics using charcoal-absorbenttubes. Tubes were analyzed for all volatile organic priority pollu-

tants. The only numbers that will appear are those of compoundsdetected.

SAMPLE NUMBER

VER-855

VER-856

VER-858

VER-870

VER-872

VER-875

VER-876

VER-877

VER-882

DATE

9/12/84

9/12/84

9/12/84

9/13/84

9/13/84

9/14/84

9/14/84

9/14/84

9/14/84

LOCATION AREA

Central, west ofoffice trailer

Perimeter areamonitor, west

Perimeter areamonitor north


Perimeter areamonitor west



Central, west ofoffice trailer

Perimeter areamonitor uest

RESULTS

None detected

.005 ppm toluene

Sone detected

.002 ppm toluene

.03 ppm toluene

.02 ppm toluene

None detected

.02 ppn toluene

None detected

Nothing was detected from the field blank. All less-than indicationsare below the detection limit. Only the front sections of these sampleswere analyzed due to the low amounts found.

All results where toluene was present are well below the 100 ppothreshold limit value for occupational toluene exposure.

During the work period when sampling was done (September 12 to 14,1984), the following are results of samples run for both dioxin and2,4,5-T. Results for dioxin have already been submitted. The following

are results for 2,4,5,-T, Samples were taken on glass fiber f i l tercassettes:

SAMPLE NUMBER DATE

VER-852 9/13/84

VER-854

VER-871

VER-873

9/13/84

9/14/84

9/14/84

VER-874 9/14/84

LOCATION

West of officetrailer



West perimeterarea monitor

West of officetrailer

RESULTS

.34 ng/n3

None detected

None detected

None detected

None detected

All results including the blank, except VER-852, are below the detectionlimit. The .34 ng/m3 sample results for 2,4,5-T in Sample 852 is ex-tremely low compared to the TLV for 2,4,5-T of 10 n<(m .

These are all sample results taken to dace.

RS:mad

cc; G. D. SchwartzCentral FileR. L. PalmerSite Copy

EE3ncoapoauioM

IT ANALYTICAL SEkTICES58)5 MiOdlebrook Pike • Knoxville Tennessee 37921 • 615-588-6401


TO' IT CorporationATTN: Raffle Sessa10 Duff RoadPittsburg, PA 15235


ORDER NUMBER

Sample Description: PM-814-027, Front Section Concentration Units: pg/section of^tub

BASE-NEUTRAL EXTRACTABLE ORGANICS - PRIORITY POLLUTANT ANALYSIS ^

acenaphthene NDacenaphthylene NDanthracene NDbenzidine NObenzo(a)anthracene NDbenzo(a)pyrene ND3,4-benzofluoranthene and/or

benzo(k)f1uoranthene NDbenzo(gni )pery1ene NDbis(2-ch1oroethoxy)niethane NDbis(2-ch1oroethyl)ether NDbis(2-ch1oroisopropy1)ether NDb1s(2-ethy1hexy1)phtha1ate ND4-bromophenyl phenyl ether NDbutyl benzylphthalate ND2-chloronaphthalene ND4-chloro-phenyl phenyl ether NDchrysene NDdibenzo(a,h)anthracene ND1.2-dichlorobenzene NO1.3-di'chlorobenzene ND1.4-dichlorobefttene ND3,3'-dich1orobenzidine NDdiethy1phtha1ate NO

Compound

dimethylphthalate NDdi-n-butylphthalate NO2,4-dinitrotoluene NO2,6-dinitrotoluene NDdi-n-octyiphthalate ND1,2-diphenylhydrazine1 NDfluoranthene NDfluorene NDhexachlorobenzene NDhexachlorobutadiene NDhexachlorocyclopentadiene NDhexachloroethane NOindeno(l,2,3-cd)pyrene NDisophorone NDnaphthalene NOnitrobenzene NDN-nitrosodimethy1am1ne NON-nitrosodi-n-propylamine NDN-mtrosodiphenylamine2 NDphenanthrene NOpyrene NDl,2,4-trich1oroben2ene NO2,3,7,8-tetrachlorodibenzo-p-di'oxin ND

Remarks: ND = Not detected- Detected as azobenzene '' Detected as diphenylamine

<50. ' Detected but at a level less than 50 no/section." Isomenc P a i r s

--0'cto"-be'^V '1984.:•/ -'-^ --^ January 1 6 , 1988

^ ^.,Nc; ."Y Puof'c

^1-'<-»^ -<_

Laboratory Manager

^kflLn^k Acc-ediied by rhe An'.encsn As5c;ialion lor Laborolory Accrean^lion ;n thecher^ro^u^T» :.ei3 .:! •esl.na 33 .ttled in the .rurreni AALA C;rec;ory ol Acc-ediled LaDorai

i ;n the chemical•cc-ediled LaDoroionet

DE3IT COBTOIUIIOM

IT-ANALYTICAL SERVICES5 8 1 5 M'caleOrooK Pike* Knoxville Tennessee 37921 • 615-588-6401


TO- IT CorporationATTN: R a f f i e Sessa10 Duff RoadPit tsburg, PA 15Z35


ORDER NUMBER

C-

0Sample Description: Blank

ADDITIONAL ORGANIC POLLUTANTS

Tenta t ive I d e n t i f i c a t i o n ^ ) Concentrat ion Uni ts are jig/Section

No Extraneous Peaks Detected

Remarks : ^^- Ident i f ica t ion is based on computer search of N.B.S. Library.

":' .-, " " " October ;"i9844th

January 16, 1988-pp-:v»3 £,- •/

Laboratory ManagerNcorvBaS^c' ,--'

fLn^k ',;;-?-::'»a ;v •-e Amencan Asio;:o!ior. lor Laboroloiv Accrtanotion in ih* cmnural^y^^»t^^ :.e.-: ;: -esi.-g ss . led ;r. if.e ^ufeni AALA iwciory ot Accr«an»ct Latiorotonf

[E3n COBPOSAI10N

IT ANALYTICAL SERVICES5815 Middlebrook Pike • Knoxvi l ie Tennessee 37921 • 615-588.6401


TO: IT. CorporationATTN: Raff le Sessa10 Duff RoadPittsburg, PA 15235


ORDER NUMBER

Sample Descript ion; B l a n k Concentration Uni t s ; tig/section of tubec

ACID EXTRACTABLE ORGANICS - PRIORITY POLLUTANT ANALYSIS

Compound

2-chloropnenol

2,4-dichlorophenol

2,4-dimethylphenol(m-xy1eno1)

4,6-dinitro-O-cresol

2 ,4-d in i t ropnenol

2-n ' i t rophenol

NDNO

NONONDNO

Compound

4-nitrophenol

p-chloro-m-cresol

pentachlorophenol

phenol

2,4,6-tn'chlorophenol

ND

ND

ND

ND

ND

Remarks: ND = Not detected<50. = Detected but at a level less than 50 ug/sect ion.

3^-" •: ;--: s-=s;-.=ea =e:;-« —.9 -•s Jfh_____^-, " __-Qrt.fihpr, 1984________.•••.•---..'s,is..--.exp:res Janua ry 16, 1'jpS

•>^^^. ^Nciar/ PuaKc

Laboratory Manager

Accredned hy Ihe Aminccn Aiso^anon lor Laboraloiv Accredilaticn in llr ch«mical•:ea o; •esnna as liaaa in !he aimni AALA DirecioTY ol Ac:redned LaBoroionw

EE3IT COBPOBATIOM

IT-ANALYTICAL SERVICES5315 MidGleorook Pike • Knoxville Tennessee 37921 • 615-5fl8-6')0)


TO IT CorporationATTN; Ruff ie Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTED october,15- 1984

PROJECT CODE •E'' wu" \0ORDER NUMBER f-

VOLATILE ORGANIC PRIORITY POLLUTANT ANALYSIS00

Sample Description: VER-877 Front

Compound

acroleinacrylom'tri lebenzenebromoformcarbon te t rachlor idechlorobenzenechlorodibrofnomethanechloroethane2-chloroethyl vinyl etherch lo ro fo rmdich lorobromomethanedi chlorodi f luo ro ine thane1.1-dichloroethane1.2-dichloroethane1.1-dichloroethylene1.2-d tchloropropanecis- l ,3-dichloropropy1ene

Concentrat ionug/ tube

NDNONDNDNDNDNDNDNDNDNDNDNDNDNDND •ND

Compound

trans-l,3-dich1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chlor ide1,1,2,2-tetrachloroethanetet rach1oroethy1eneto luenetrans-l,2-d1ch1oroethy1ene1.1.1-trlch'Ioroethane1.1.2-trichloroethanet r i ch lo roe thy lenet r i ch lo ro f luo romethaneviny l c h l o r i d e

Concentra t ionug / tube

NDNDNONDNDNDND8.5

NDNDNDNDNDND

Remarks: ND » Not detected<5.0 = Detected but at a level less than 5.0 yg/ tube

15th

December Ib. 1987

Laboratory Manager

JLJ^rBL Ac::":!"ea ^1lhe Ar—ncan Asso;ianon Icr Laborotorv Ac;redilcnicr. .n th« chemical^•^•{alf» •'•e-^ •' •est;"!; =s :.iiea ;n trie curreni AALA Direcicry ot Accreaitea Labonncnes

G3lICOBfOUTIOM

IT ANALYTICAL SERVICES5815 Middlebrook Pike • Knoxville. Tennessee 37921 • 615-583-6401


TO IT CorporationATTN: Ruffle Sessa10 Duff RoadPittsburgh, PA 15235


ORDER NUMBER



acroleinacrylonitrnebenzenebromoformcarbon tetrachloridechlorobenzenechlorodibroniomethanechloroethane2-chloroethyl vinyl etherchloroformdichlorobroniomethanedi chtorodi f luoromethane1.1-dichloroethane1.2-dichloroethane1.1-dichloroethylene1.2-dichloropropanecis-l ,3-dich1oropropy1ene

Concentrationug/tube

NDNDNONONONONONONDNONONONONDNDNO 'NO

trans-l,3-d1ch1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2,2-tetrachloroethanetetrachloroethylenetoluenetrans-l,2-dich1oroethy1ene1.1.1-trichloroethane1.1.2-tr1ch1oroethanetrichloroethylenetr ichlorof luoromethanevinyl chlon'de

Concentrationpg/tube

NONDNDNONONONO5.0

NONONONONDNO

Remarks: ND » Not detected<5.0 " Detected but at a level less than 5.0 ug/ tube

^c" •; ^"c i^sscr-c^d sero.1' T.e 'i-;s^•;: October, 1984

15th

'.'y r=.—.;s3.;-. expires December 16. 1987^ s^~• NolarY ^ibiT?^

Laboratory Manager

•klr|^& Accredited Sy lh« Arnencor. Asso;ialion tor Laboralorv Accredilalion in Ihe chtirucal^^9*J^f Held ot 'esnna as liaed ir the rurreni AALA Directory of Accredited Labon3ton«

EE3ITCOBPOUnON

IT ANALYTICAL SERVICES53)5 MiddiebroOK Pike • Knoxville. Tennessee 37921 • 615 -588 -6401


TO: IT-CorporationATTN: Ruffle Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTEDPROJECT CODE

ORDER NUMBER

October 15, 1984VER 18677



acroleinacrylom'trllebenzenebromoforracarbon tetrachloridechlorobenzenech 1 orodi bromoinetha nechtoroethane2-chloroethyl vinyl etherchloroformdichlorobromomethanedichlorodi f luoromethane1.1-dfchloroethane1.2-dichloroethane1.1-dichtoroethylene1.2-dichloropropanecis-l ,3-dich1oropropy1ene

Concen t ra t ionuq/tube

NONDNDNDNDNDNDNDNDNDNDNDNDNDNDND •ND

Compound

trans-1,3-dichloropropy 1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2,2-tetrachloroethanetetrachloroethylenetoluenetrans-l,2-dich1oroethy1ene1.1.1-trichloroethane1.1.2-trichloroethanetr ichloroethylenet r i ch lo ro f luo romethanevinyl chlor ide


NDNDNDNDNDNDND9.5

NDNDNONDNDND

Remarks: ND .= Not detected<5.0 = Detected but at a level less than 5.0 ug/ tube

Sw:- •_ :- -. i.-i-- r-= M:;r- — - s _ 1 5 t h _— - October. 1984

, December 16. 1987

^€./7^^^My •::r'.~"-3;,c~ exc-'-a .

Laboratory Manager

JL1 r3& A==.-e':.'ed ry '?'e A-Tercan A3so.:iaiion lor LaboTOtoiv Accreditalian in the chernical^^^^[iy» :.e.3 ;; •ey;.-y ss islea ;n irie cun-eni AALA Dirsctory ot Accrwiied LaborCTonti

EQrr coRpounou

IT ANALYTICAL SERVICES5815 Middletirook Pike • Knoxville Tennessee 37921 • 615-588-6401


TO; IT CorporationATTN: R u f f i e Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTED October 15, 1984PROJECT CODE. VER 18677

ORDER NUMBER.

VOLATILE ORSANIC PRIORITY POLLUTANT ANALYSIS 00


acroleinacrylom'tri Iebenzenebromoformcarbon tetrachloridechlorobenzenechlorod-fbromo methanechloroethane2-chloroethyl vinyl etherchloroformdichlorobroraomethanedichlorodifluoromethane1.1-di'chloroethane1.2-dichloroethane1.1-dichloroethylene1.2-dichloropropanecis-l,3-dich1oropropy1ene


NONONONDNONDNONONDNONDNDNDNDNDND •ND

Compound

trans-l,3-dich1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2,2-tetrachloroethanetetrachloroethylenetoluenetrans-l,2-dich1oroethy]ene1.1.1-trichloroethane1.1.2-trichloroethanetrichloroethylenetrichlorofluoromethanevinyl chloride

Concentrationtig/tube

NDNDNONDNDNDNO13.NDNDNDNDNDND

Remarks: NO = Not detected<5.0 = Detected but at a level less than 5.0 yg/tube

15th?WCT := c-,3 su^sc-.^ea =e'or°5L;^5.;..-;ec. -eior0 —?T

October, 1984'DTcerabe^lB, 1987

>^<^^^^~

My ccmm.ssior exp:res -

Laboratory ManagerNotarv Pul ic \

Jkflk n k Acc-eaited by ihe American Aawciaiion lor La&oraiory Accreditation in th« rtiamicalW»»^(»» iieia ai tesiino 01 Ufled in me curreni AALA D^edorv o( Accr«lii»d Latioraton»s

03ITCORPOSMION

IT ANALYTICAL SEkSHCES58)5 Middlebrook Pike • Knoxville. Tennessee 3792) • 615-588-6401


TO: IT CorporationATTN: R u f f f e Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTED.PROJECT CODE

ORDER NUMBER


VOLATILE ORGANIC PRIORITY POLLUTANT ANALYSIS


Compound

acroleinacryloni t r l lebenzenebromoformcarbon tetrachloridechlorobenzenechlorodi bromomethanechloroethane2-chloroethyl vinyl etherchloroformdf ch1orobromomethanedi'chlorodifluoromethane1.1-dichloroethane1.2-dichloroethane1.1-dichloroethylene1.2-dichloropropanecis-1,3-dichlcrop ropylene

Concentrationtig/tube

NONONONONDNONONONONONDNONDNONOND •NO

Compound

trans-l,3-d1ch1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2,2-tetrachloroethanetetrachloroethylenetoluenetrans-l,2-d1ch1oroetny1ene1.1.1-trichloroethane1.1.2-trichloroethanetrichloroethylenetn ch1orof1uoromethanevinyl chloride

00


NONDNONONONOND7.0

NONDNONDNDND

Remarks: ND - Not detected<5.0 = Detected but at a level less than 5.0 yg/tube

•3.-.C s^sscr.rec z^'^re T.e '?-..s 15thOctober, 1984

. -,..-r^p.r« Decaqber_16, 1987^•/^2^_ Laboratory HanaQer

JkirfL Accred.led By [he American Asso:ianon lor LabOCTory Accrediltmon in llr ctrmicolw1w»IBP» ;iela c; 'esung 31 iaied in ihe ^Jrrent AALA DirBclOty ol Accrediied Loborclonet

03rr coaroBATioit

IT ANALYTICAL SERVICES58)5 MiddleOrook Pike • Knoxville. Tennessee 37921 • 615-588-6401


TO: IT CorporationATTN: Ruff ie Sessa10 Duff RoadPittsburgh, PA 15235

DATE REPORTEDPROJECT CODE:

ORDER NUMBER:


VOLATILE ORGANIC PRIORITY POLLUTANT ANALYSIS


acroleinacrylonitr'flebenzenebromoformcarbon tetrachloridechlorobenzenechlorodi bromomethanechloroethane2-chloroetnyl vinyl etherchloroformdichlorobromomethanedichlorodifluoroinethane1.1-dichloroethane1.2-dicnloroethane1.1-dicnloroethylene1.2-dichloropropanecis-l,3-dich1oropropy1ene


NDNONDNONONONONONONONDNONONONONO •NO

Compound

trans-l,3-d1ch1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2,2-tet rach1oroethanetet rach1oroetny1enetoluenetrans-l,2-dich1oroethy1ene1.1.1-trichloroethane1.1.2-trichloroethanetricnioroethylenetrich1orofluoromethanevinyl chloride

Remarks: NO .» Not detected<5.0 =• Detected but at a level less than 5.0 ug/tube

;"':.—. —. ;-: s»=sc,-:c93 belcre rr.? l.-. 15th:^;: October. 1984

Pecember^S. 1987————€^.———

My ;cr••.:nlss;crt expires

_^^&/• / } Noiart- PUSH/^NoTart- P U S H / ^

Laboratory Manager

Ac;redned by tha Am»ncan A»o:i<ilion (or Laboratory Accrtditanon in th» chemK'alrield c[ testing as listed in the ;un»nl AAM Directory of Accrediltd Laborotonw

IT.AMALYTICAL SERVICES5815 Middlebrook Pike • Knoxville. Tennessee 37921 • 615-588-6401


TO: IT CorporationATTN: R u f f l e10 Duff RoadPit tsburgh, PA

Sessa

15235

VOLATILE

DATE REPORTEDPROJECT CODE

ORDER NUMBER

ORGANIC PRIORITY POLLUTANT ANALYSIS


(V!^—C

00


acro1e1nacrylomtrilebenzenebromoformcarbon tetrachloridechlorobenzenechlorodibromomethanechlorocthane2-chloroethyl vinyl etherchloroformdichlorobrornomethanedichlorodi f luoronie thane1.1-dichloroethane1.2-dichloroethane1.1-dichloroethylene1.2-dichloropropanecis-l ,3-dich1oropropy1ene


NDNDNONONONONDNONONONDNDNONONOND •ND

Compound

trans-l,3-dicn1oropropy1eneethyl benzenemethyl bromidemethyl chloridemethylene chloride1,1,2.2-tetrachloroethanetetrachtoroethylenetoluenetrans-l,2-di'chloroethy1ene1.1.1-trichloroethane1.1.2-trichloroethanetrichloroethylenetrichlorofluoromethanevinyl chloride


NONDNONDNDNONONONONONDNDNDND

Remarks: NO = Not detected<5.0 = Detected but at a level less than 5.0 ug/tube

3^';rr •c ar.; s-^scrceQ se'or0 rr.e •'- ; 15th.;. October. 1984

My :;.--.-.:5i.cr. -xF-.res December^. 1987 "^ ^ ^^,^.

Laboratory Manager

Jkl n^k Ac:—3.'t<) cy •-.» Ar-er.can Aaoaalion !cr Laborolorv AccrediltBion in lh« cli»micol^HiVwJ^^k :;e-3 -• resn;;g 3s 'isied in ihe ^JTreni AALA Oiroclcry o) AccrBanad Laboreiorw

EH17 COBPO&MIOM

IT ANALYTICAL SERVICES5815 Middlebrook Pike • Knoxville. Tennessee 37921 • 615-5S8-6401


TO: IT CorporationATTN: Ruffie Sessa10 Duff RoadPittsburgh, PA 15235


ORDER NUMBER

Sample Description: Ten (10) hexane extracts received September 5, 1984 "•

Concentration units are total ug's per extract

2,4-D 2.4.5-TP (Si lvex)

0

PM-810-PM-810-iPM-810-iPM-810-iPM-810-IPM-810-IPM-810-IPM-810-IF i l te r IReagent

.007009.010013014015016017BlankBlank

<0.004<0.004<0.008<0.004<0.004<0.003<0.008<0.004<0.008<0.008

<0.002<0.008<0.002<0.004<0.06<0.0008<0.020<0.004<0.01<0.002

• ::" ;L:.s;-.ce^ se'c'e rr.e •'-'cOctober. 1984

12th

., ..xoi.-es January 16. 1988.^pcr^-e^ vf

Laboratory ManagerNotary- Pualic

JkJLn^L Acc'ea:ied by i e Ainencan Association lor Laboratory Accreditation .n ihe cMmical^»^r»j y% tieid cl wilir.a as tistea ;n IM curreni AALA ^irectorv oi Accreaned LoOoraicnw

air sampling test results (data is available for review · pdf filefilter and reagent blanks...

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