Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

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http://pubs3.acs.org/acs/journals/toc.page?incoden=ancham&indecade=0&involume=79&inissue=15 (1 of 19)16/8/2550 19:22:42

Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Analytical Chemistry is a peer-reviewed research journal that explores the latest concepts in analytical measurements and the best new ways to increase accuracy, selectivity, sensitivity, and reproducibility.

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Vol. 79, No. 15: August 1, 2007

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EDITORIAL

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Services Offered by Analytical Chemists Royce W. Murray p 5495

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AUDIO

Audio Introduction to the August 1 Cover Rajendrani Mukhopadhyay p 5495

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NEWS

Analytical Currents: How many antibodies work after QD conjugation? | SERS at Pd and Pt surfaces. | How do constituents in plasma membranes move around? | Fast MS of viruses and cells. | Shifting ideas about protein NMR. | Studying protein–DNA interactions inside porous vesicles. | An NMR structure from micrograms of protein. | Watching a transcription factor in action. pp 5497 - 5500

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People: Fréchet wins 2007 Arthur C. Cope Award. | Applications for Kolthoff and Pfizer travel grants. p 5501

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Research Profile: SPR imaging, in living color Laura Cassiday p 5502

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Research Profile: Please squeeze the red blood cells Jennifer Griffiths p 5503

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Research Profile: Continuous separations by acoustic forces Rajendrani Mukhopadhyay p 5504

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Research Profile: Tracking the metabolism of glycosphingolipids in single cells Rajendrani Mukhopadhyay p 5505

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Research Profile: Image and reality in 3D SIMS Elizabeth Zubritsky p 5506

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AC DETECTIVE

Testing their metal Jennifer Griffiths pp 5507 - 5508

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LAB FAB

NMR probe gets new geometry Rajendrani Mukhopadhyay p 5509

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FEATURES

Using the Electrochemistry of the Electrospray Ion Source Gary J. Van Berkel and Vilmos Kertesz pp 5510 - 5520

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AC DETECTIVE

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Fingerprints reveal drug habits Rajendrani Mukhopadhyay p 5521

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FEATURES

Out! Catching Doping Athletes Rajendrani Mukhopadhyay pp 5522 - 5528

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ACCELERATED ARTICLES

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Protocols for Three-Dimensional Molecular Imaging Using Mass Spectrometry Andreas Wucher, Juan Cheng, and Nicholas Winograd pp 5529 - 5539; (Accelerated Article) DOI: 10.1021/ac070692a

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Molecular Commonality Detection Using an Artificial Enzyme Membrane for in Situ One-Stop Biosurveillance Shinya Ikeno, Hitoshi Asakawa, and Tetsuya Haruyama pp 5540 - 5546; (Accelerated Article) DOI: 10.1021/ac0708902

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ARTICLES

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Probing Adenosine Nucleotide-Binding Proteins with an Affinity-Labeled Nucleotide Probe and Mass Spectrometry Haibo Qiu and Yinsheng Wang pp 5547 - 5556; (Article) DOI: 10.1021/ac0622375

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Quantitative Sequencing of Complex Mixtures of Heterochitooligosaccharides by vMALDI-Linear Ion Trap Mass Spectrometry Sophie Haebel, Sven Bahrke, and Martin G. Peter pp 5557 - 5566; (Article) DOI: 10.1021/ac062254u

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Integrated Electrochemical Sensor Array for On-Line Monitoring of Yeast Fermentations E. E. Krommenhoek, J. G. E. Gardeniers, J. G. Bomer, X. Li, M. Ottens, G. W. K. van Dedem, M. Van Leeuwen, W. M. van Gulik, L. A. M. van der Wielen, J. J. Heijnen, and and A. van den Berg pp 5567 - 5573; (Article) DOI: 10.1021/ac0623078

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CdS Nanocrystal-Based Electrochemiluminescence Biosensor for the Detection of Low-Density Lipoprotein by Increasing Sensitivity with Gold Nanoparticle Amplification Guifen Jie, Bo Liu, Hongcheng Pan, Jun-Jie Zhu, and Hong-Yuan Chen pp 5574 - 5581; (Article) DOI: 10.1021/ac062357c

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Quantitative Method for the Profiling of the Endocannabinoid Metabolome by LC-Atmospheric Pressure Chemical Ionization-MS John Williams, JodiAnne Wood, Lakshmipathi Pandarinathan, David Karanian, Benjamin Bahr, Paul Vouros, and Alexandros Makriyannis pp 5582 - 5593; (Article) DOI: 10.1021/ac0624086

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Spectroelectrochemical Sensing Based on Multimode Selectivity Simultaneously Achievable in a Single Device. 20. Detection of Metal Ions in Different Oxidation States Chamika M. Wansapura, Carl J. Seliskar, and William R. Heineman pp 5594 - 5600; (Article) DOI: 10.1021/ac070026+

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Using Statistical Models To Identify Factors That Have a Role in Defining the Abundance of Ions Produced by Tandem MS Sheila J. Barton, Sylvia Richardson, David N. Perkins, Inga Bellahn, Trevor N. Bryant, and John C. Whittaker pp 5601 - 5607; (Article) DOI: 10.1021/ac0700272

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Technique for Quantitative Detection of Specific DNA Sequences Using Alternately Binding Quenching Probe Competitive Assay Combined with Loop-Mediated Isothermal Amplification Hidenori Tani, Tatsuya Teramura, Ken Adachi, Satoshi Tsuneda, Shinya Kurata, Kazunori Nakamura, Takahiro Kanagawa, and Naohiro Noda pp 5608 - 5613; (Article) DOI: 10.1021/ac070041e

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Apoferritin-Templated Synthesis of Encoded Metallic Phosphate Nanoparticle Tags Guodong Liu, Hong Wu, Alice Dohnalkova, and Yuehe Lin pp 5614 - 5619; (Article) DOI: 10.1021/ac070086f

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High-Speed Data Reduction, Feature Detection, and MS/MS Spectrum Quality Assessment of Shotgun Proteomics Data Sets Using High-Resolution Mass Spectrometry Michael R. Hoopmann, Gregory L. Finney, and Michael J. MacCoss pp 5620 - 5632; (Article) DOI: 10.1021/ac0700833

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Application of Dissimilarity Indices, Principal Coordinates Analysis, and Rank Tests to Peak Tables in Metabolomics of the Gas Chromatography/Mass Spectrometry of Human Sweat Yun Xu, Fan Gong, Sarah J. Dixon, Richard G. Brereton, Helena A. Soini, Milos V. Novotny, Elisabeth Oberzaucher, Karl Grammer, and Dustin J. Penn pp 5633 - 5641; (Article) DOI: 10.1021/ac070134w

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Pyrolysis Comprehensive Two-Dimensional Gas Chromatography Study of Petroleum Source Rock Frank Cheng-Yu Wang and Clifford C. Walters pp 5642 - 5650; (Article) DOI: 10.1021/ac070166j

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Reproducibility Assessment of Relative Quantitation Strategies for LC-MS Based Proteomics Yeoun Jin Kim, Ping Zhan, Brian Feild, Steven M. Ruben, and Tao He pp 5651 - 5658; (Article) DOI: 10.1021/ac070200u

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Mass Spectrometric Determination of the Coordination Geometry of Potential Copper(II) Surrogates for the Mammalian Prion Protein Octarepeat Region M. Jake Pushie, Andrew R. S. Ross, and Hans J. Vogel pp 5659 - 5667; (Article) DOI: 10.1021/ac070312l

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Fused-Core Silica Column High-Performance Liquid Chromatography/Tandem Mass Spectrometric Determination of Rimonabant in Mouse Plasma Yunsheng Hsieh, Christine J. G. Duncan, and Jean-Marc Brisson pp 5668 - 5673; (Article) DOI: 10.1021/ac070343g

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Spatially Resolved Characterization of Catalyst-Coated Membranes by Distance-Controlled Scanning Mass Spectrometry Utilizing Catalytic Methanol Oxidation as Gas-Solid Probe Reaction Nan Li, Jens Assmann, Wolfgang Schuhmann, and Martin Muhler pp 5674 - 5681; (Article) DOI: 10.1021/ac070347l

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Statistical Correlation and Projection Methods for Improved Information Recovery from Diffusion-Edited NMR Spectra of Biological Samples Leon M. Smith, Anthony D. Maher, Olivier Cloarec, Mattias Rantalainen, Huiru Tang, Paul Elliott, Jeremiah Stamler, John C. Lindon, Elaine Holmes, and Jeremy K. Nicholson pp 5682 - 5689; (Article) DOI: 10.1021/ac0703754

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Postcolumn Concentration in Liquid Chromatography. On-Line Eluent Evaporation and Analyte Postconcentration in Ion Chromatography Masaki Takeuchi, Purnendu K. Dasgupta, Jason V. Dyke, and Kannan Srinivasan pp 5690 - 5697; (Article) DOI: 10.1021/ac0703799

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Analysis of Cell Surface Carbohydrate Expression Patterns in Normal and Tumorigenic Human Breast Cell Lines Using Lectin Arrays Siyuan Chen, Ting Zheng, Michael R. Shortreed, Caroline Alexander, and Lloyd M. Smith pp 5698 - 5702; (Article) DOI: 10.1021/ac070423k

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Analysis of C-Reactive Protein on Amide-Linked N-Hydroxysuccinimide-Dextran Arrays with a Spectral Surface Plasmon Resonance Biosensor for Serodiagnosis Se-Hui Jung, Jae-Wan Jung, In-Bum Suh, Jong Seol Yuk, Woo-Jin Kim, Eui Yul Choi, Young-Myeong Kim, and Kwon-Soo Ha pp 5703 - 5710; (Article) DOI: 10.1021/ac070433l

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Steady-State Asymmetric Nanospray Dual Ion Source for Accurate Mass Determination within a Chromatographic Separation Nicolas L. Young, Michael C. Sisto, Meggie N. Young, Patrick G. Grant, David W. Killilea, LaTasha LaMotte, Kuang Jen J. Wu, and Carlito B. Lebrilla pp 5711 - 5718; (Article) DOI: 10.1021/ac070446z

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Gene Transfection of Mammalian Cells Using Membrane Sandwich Electroporation Zhengzheng Fei, Shengnian Wang, Yubing Xie, Brian E. Henslee, Chee Guan Koh, and L. James Lee pp 5719 - 5722; (Article) DOI: 10.1021/ac070482y

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

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Characterization of Variable Regions of Monoclonal Antibodies by Top-Down Mass Spectrometry Zhongqi Zhang and Bhavana Shah pp 5723 - 5729; (Article) DOI: 10.1021/ac070483q

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Fully Automated Two-Dimensional Electrophoresis System for High-Throughput Protein Analysis Atsunori Hiratsuka, Hideki Kinoshita, Yuji Maruo, Katsuyoshi Takahashi, Satonari Akutsu, Chie Hayashida, Koji Sakairi, Keisuke Usui, Kisho Shiseki, Hajime Inamochi, Yoshiko Nakada, Kouhei Yodoya, Ichiji Namatame, Yutaka Unuma, Makoto Nakamura, Kosuke Ueyama, Yoshinori Ishii, Kazuyoshi Yano, and Kenji Yokoyama pp 5730 - 5739; (Article) DOI: 10.1021/ac070485a

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Hydroxylated Polychlorinated Biphenyl Detection Based on a Genetically Engineered Bioluminescent Whole-Cell Sensing System Kendrick Turner, Shifen Xu, Patrizia Pasini,, Sapna Deo,, Leonidas Bachas, and Sylvia Daunert pp 5740 - 5745; (Article) DOI: 10.1021/ac0705162

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Magnetic Field Switching of Nanoparticles between Orthogonal Microfluidic Channels Andrew H. Latham, Anand N. Tarpara, and Mary Elizabeth Williams pp 5746 - 5752; (Article) DOI: 10.1021/ac070520d

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Improvements in Mixing Time and Mixing Uniformity in Devices Designed for Studies of Protein Folding Kinetics Shuhuai Yao and Olgica Bakajin pp 5753 - 5759; (Article) DOI: 10.1021/ac070528n

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

High-Affinity Binding of Cadmium Ions by Mouse Metallothionein Prompting the Design of a Reversed-Displacement Protein-Based Fluorescence Biosensor for Cadmium Detection Antonio Varriale, Maria Staiano, Mose' Rossi, and Sabato D'Auria pp 5760 - 5762; (Article) DOI: 10.1021/ac0705667

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Autonomous Microfluidic Sample Preparation System for Protein Profile-Based Detection of Aerosolized Bacterial Cells and Spores Jeanne C. Stachowiak, Erin E. Shugard, Bruce P. Mosier, Ronald F. Renzi, Pamela F. Caton, Scott M. Ferko, James L. Van de Vreugde, Daniel D. Yee, Brent L. Haroldsen, and Victoria A. VanderNoot pp 5763 - 5770; (Article) DOI: 10.1021/ac070567z

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Spectroscopic Imaging of Latent Fingermarks Collected with the Aid of a Gelatin Tape Camilla Ricci, Steve Bleay, and Sergei G. Kazarian pp 5771 - 5776; (Article) DOI: 10.1021/ac070580j

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Tags for the Stable Isotopic Labeling of Carbohydrates and Quantitative Analysis by Mass Spectrometry Michael J. Bowman and Joseph Zaia pp 5777 - 5784; (Article) DOI: 10.1021/ac070581b

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Comparison of Electrokinetics-Based Multidimensional Separations Coupled with Electrospray Ionization-Tandem Mass Spectrometry for Characterization of Human Salivary Proteins Xueping Fang, Li Yang, Weijie Wang, Tao Song, Cheng S. Lee, Don L. DeVoe, and Brian M. Balgley pp 5785 - 5792; (Article) DOI: 10.1021/ac070611a

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

IR-MALDI-MS Analysis of HPTLC-Separated Phospholipid Mixtures Directly from the TLC Plate Andreas Rohlfing, Johannes Müthing, Gottfried Pohlentz, Ute Distler, Jasna Peter-Katalini , Stefan Berkenkamp, and Klaus Dreisewerd pp 5793 - 5808; (Article) DOI: 10.1021/ac070633x

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Scanning Electrochemical Microscopy with Slightly Recessed Nanotips Peng Sun and Michael V. Mirkin pp 5809 - 5816; (Article) DOI: 10.1021/ac070771m

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Reverse-Phase versus Sandwich Antibody Microarray, Technical Comparison from a Clinical Perspective K. Järås, A. Ressine, E. Nilsson, J. Malm, G. Marko-Varga, H. Lilja, and T. Laurell pp 5817 - 5825; (Article) DOI: 10.1021/ac0709955

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Isolation of N-Linked Glycopeptides from Plasma Yong Zhou, Ruedi Aebersold, and Hui Zhang pp 5826 - 5837; (Article) DOI: 10.1021/ac0623181

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Tuneable Peak Deformations in Chiral Liquid Chromatography Robert Arnell, Patrik Forssén, and Torgny Fornstedt pp 5838 - 5847; (Article) DOI: 10.1021/ac062330t

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Polymer Monoliths with Low Hydrophobicity for Strong Cation-Exchange Capillary Liquid Chromatography of Peptides and Proteins Binghe Gu, Yun Li, and Milton L. Lee pp 5848 - 5855; (Article) DOI: 10.1021/ac0623585

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Microfluidic Rheology of Non-Newtonian Liquids Salvatore Girardo, Roberto Cingolani, and Dario Pisignano pp 5856 - 5861; (Article) DOI: 10.1021/ac062405t

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Determination of Chromium(VI) by Surface Plasmon Field-Enhanced Resonance Light Scattering Zhiqiang Han, Li Qi, Gangyi Shen, Wei Liu, and Yi Chen pp 5862 - 5868; (Article) DOI: 10.1021/ac062453d

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H/D Exchange- and Mass Spectrometry-Based Strategy for the Thermodynamic Analysis of Protein-Ligand Binding Liangjie Tang, Erin D. Hopper, Yan Tong, Jack D. Sadowsky, Kimberly J. Peterson, Samuel H. Gellman, and Michael C. Fitzgerald pp 5869 - 5877; (Article) DOI: 10.1021/ac0700777

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Self-Assembled Monolayers for MALDI-TOF Mass Spectrometry for Immunoassays of Human Protein Antigens Steven M. Patrie and Milan Mrksich pp 5878 - 5887; (Article) DOI: 10.1021/ac0701738

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Isotopic Analysis of N and O in Nitrite and Nitrate by Sequential Selective Bacterial Reduction to N2O

John Karl Böhlke, Richard L. Smith, and Janet E. Hannon pp 5888 - 5895; (Article) DOI: 10.1021/ac070176k

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Identification of Anomeric Configuration of Underivatized Reducing Glucopyranosyl-glucose Disaccharides by Tandem Mass Spectrometry and Multivariate Analysis Joana Simões, Pedro Domingues, Ana Reis, Fernando M. Nunes, Manuel A. Coimbra, and M. Rosário M. Domingues pp 5896 - 5905; (Article) DOI: 10.1021/ac070317i

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

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Assessment of Specific Binding Proteins Suitable for the Detection of Paralytic Shellfish Poisons Using Optical Biosensor Technology Katrina Campbell, Linda D. Stewart, Gregory J. Doucette, Terence L. Fodey, Simon A. Haughey, Natalia Vilariño, Kentaro Kawatsu, and Christopher T. Elliott pp 5906 - 5914; (Article) DOI: 10.1021/ac070342o

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Pressure-Driven Reverse-Phase Liquid Chromatography Separations in Ordered Nonporous Pillar Array Columns Wim De Malsche, Hamed Eghbali, David Clicq, Joris Vangelooven, Han Gardeniers, and Gert Desmet pp 5915 - 5926; (Article) DOI: 10.1021/ac070352p

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Impulse-Driven Heated-Droplet Deposition Interface for Capillary and Microbore LC-MALDI MS and MS/MS J. Bryce Young and Liang Li pp 5927 - 5934; (Article) DOI: 10.1021/ac070383k

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Homogeneous Noncompetitive Immunoassay for 17 -Estradiol Based on Fluorescence Resonance Energy Transfer

Tiina Kokko, Leena Kokko, Timo Lövgren, and Tero Soukka pp 5935 - 5940; (Article) DOI: 10.1021/ac070417o

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Exploitation of Endogenous Protease Activity in Raw Mastitic Milk by MALDI-TOF/TOF Anna Napoli, Donatella Aiello, Leonardo Di Donna, Henrrik Prendushi, and Giovanni Sindona pp 5941 - 5948; (Article) DOI: 10.1021/ac0704863

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Capillary Electrophoresis as a Second Dimension to Isoelectric Focusing for Peptide Separation Jean-Marc Busnel, Niels Lion, and Hubert H. Girault pp 5949 - 5955; (Article) DOI: 10.1021/ac070493r

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Surface Scanning Analysis of Planar Arrays of Analytes with Desorption Electrospray Ionization-Mass Spectrometry Sofie P. Pasilis, Vilmos Kertesz, and Gary J. Van Berkel pp 5956 - 5962; (Article) DOI: 10.1021/ac070527v

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Fluorescent Derivatization Method of Proteins for Characterization by Capillary Electrophoresis- Sodium Dodecyl Sulfate with Laser-Induced Fluorescence Detection David A. Michels, Lowell J. Brady, Amy Guo, and Alain Balland pp 5963 - 5971; (Article) DOI: 10.1021/ac0705521

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Mass-Transfer Kinetics in a Shell Packing Material for Chromatography Alberto Cavazzini, Fabrice Gritti, Krzysztof Kaczmarski, Nicola Marchetti, and Georges Guiochon pp 5972 - 5979; (Article) DOI: 10.1021/ac070571a

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Quantitative Analysis of Cyanobacterial Toxins by Matrix-Assisted Laser Desorption Ionization Mass Spectrometry Karen L. Howard and Gregory L. Boyer pp 5980 - 5986; (Article) DOI: 10.1021/ac0705723

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Development of Surface Plasmon Resonance Mass Spectrometry Array Platform Dobrin Nedelkov pp 5987 - 5990; (Article) DOI: 10.1021/ac070608r

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Screening and Sequencing of Glycated Proteins by Neutral Loss Scan LC/MS/MS Method Himanshu S. Gadgil, Pavel V. Bondarenko, Michael J. Treuheit, and Da Ren pp 5991 - 5999; (Article) DOI: 10.1021/ac070619k

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Immunoassay on a Power-Free Microchip with Laminar Flow-Assisted Dendritic Amplification Kazuo Hosokawa, Masaki Omata, and Mizuo Maeda pp 6000 - 6004; (Article) DOI: 10.1021/ac070659o

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Detailed Study on the Use of Electrospray Mass Spectrometry To Investigate Speciation in Concentrated Silicate Solutions Stefan A. Pelster, Ferdi Schüth, and Wolfgang Schrader pp 6005 - 6012; (Article) DOI: 10.1021/ac0706729

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Combination of HPLC "Inverted Chirality Columns Approach" and MS/MS Detection for Extreme Enantiomeric Excess Determination Even in Absence of Reference Samples. Application to Camptothecin Derivatives Elena Badaloni, Walter Cabri, Alessia Ciogli, Roberto Deias, Francesco Gasparrini, Fabrizio Giorgi, Aristide Vigevani, and Claudio Villani pp 6013 - 6019; (Article) DOI: 10.1021/ac070776j

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TECHNICAL NOTES

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Rapid Screening of Doping Agents in Human Urine by Vacuum MALDI-Linear Ion Trap Mass Spectrometry Hari Kosanam, P. K. Sai Prakash, C. R. Yates, D. D. Miller, and Suma Ramagiri pp 6020 - 6026; (Technical Note) DOI: 10.1021/ac070118z

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

Controlling Charge on Levitating Drops Ryan T. Hilger, Michael S. Westphall, and Lloyd M. Smith pp 6027 - 6030; (Technical Note) DOI: 10.1021/ac070413j

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Molecular Beacon-Style Hybridization Assay for Quantitative Analysis of Surface Invasive Cleavage Reactions Matthew R. Lockett, Michael R. Shortreed, and Lloyd M. Smith pp 6031 - 6036; (Technical Note) DOI: 10.1021/ac070424c

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Microarray Detection of Duplex and Triplex DNA Binders with DNA-Modified Gold Nanoparticles Abigail K. R. Lytton-Jean, Min Su Han, and Chad A. Mirkin pp 6037 - 6041; (Technical Note) DOI: 10.1021/ac070635h

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Production of Biosensors with Exchangeable Enzyme-Containing Threads Toonika Rinken, Jaak Järv, and Ago Rinken pp 6042 - 6044; (Technical Note) DOI: 10.1021/ac070327j

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

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Analytical Chemistry: Vol.79, Issue 15 (ACS Publications)

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