digital.library.unt.edu/67531/metadc708325/m2/1/high_res_d/7554.pdf,.......---------------:-:-~---:---------~--disclaimer...

WSRC-TR-99-000S7

Geotechnical Analysis of Five Shelby Tube Samples from H-Area Retention Basin

-I

r- ~- -------.~

by

C. A. Langton

Westinghouse Savannah River Company Savannah River Site Aiken, South Carolina 29808

W. L. Mhyr.

DOE Contract No. DE-AC09-96SR18500

RECORDS ADMINISTRATION

11111111111111111111111111111111111111111111111111 RD125210

This paper was prepared in connection with work done under the above contract number with the U. S. Department of Energy. By acceptance of this paper, the publisher andlor recipient acknowledges the U. S. Government's right to retain a nonexclusive, royalty-free license in and to any copyright covering this paper, along with the right to reproduce and to authorize others to reproduce all or part of the copyrighted paper.

,.......---------------:-:-~---:---------~- -

DISCLAIMER

This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, nor any of their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof.

This report has been reproduced directly from the best available copy.

Available to DOE and DOE contractors from the Office of Scientific and Technicallnfonnation, P.O. Box 62, Oak Ridge, 1N 37831; prices available from (615) 576-8401.

Available to the public from the National Technical Infonnation Service, U.S. Department of Commerce, 5285 Port Royal Road, Springfield, VA 22161.

-----------------------------~~--- ~-- ~

II I I I I I I I I I I

WSRC-TR-99-OOO57, Rev. 0 ... -, I

February 8,1999

Key Words: H·Area Retention Basin Geotechnical Analysis Soil Characterization

RETENTION: Permanent

GEOTECHNICAL ANALYSIS OF FIVE SHELBY TUBE SAMPLES FROM THE H·AREA RETENTION BASIN (U)

Author

Christine A. Langton, Westinghouse Savannah River Company

Savannah River Technology Center Aiken, SC 29808

And

W. L. Mhyre Raytheon Engineers and Constructors

Savannah River Site Aiken, SC 29808

I Date: February 8, 1999

I I I I I

II

I

Westinl!house Savannah River Companv Savannah River Site Aiken. SC 29808

SAVANNAH RIVER SITE

II I I I I I I I I I I I I I I I I I I

REVIEWS and APPROVALS

Authors

C. Langton waste Processing Technology/

ApprovalslReviews

B. T. Butcher, Level 4 Waste Processing Technology/SRTC

W.E. Skwens, Level 3 waste Processing Technology/SRTC

B.K. Environmental Engineering/WSRC

WSRC-TR-99-OOO57 Rev. 0

February 8, 1999

- &-71 Date

Date

r'Date

I I II

I I I I I I I I I I I I I I I I I

TABLE OF CONTENTS

WSRC-TR-99-OOOS7 Rev. 0

February 8, 1999

SUMMARY 1 BACKGROUND 1 LABORATORY TESTING 3 RESULTS AND DISCUSSION 3

VJSU8l Description/Core Logging 3 Soil Classification Based on Particle Size Analyses 3 Unit Weights As Received and Dried S Natural Moisture, Specific Gravity and Porosity 6 Saturated Vertical Hydraulic Conductivity 6 ~~ 8 Exchangeable Acidity 8 Cation Exchange Capacity 9

CONCLUSIONS 9 REFERENCES 9 QUALITY ASSURANCE 11 ACKNOWLEDGEMENTS 11 APPENDICIES

APPENDIX 1. HRB Shelby Tube Sample Descriptions A-I APPENDIX 2. Particle Size Analyses (Sieve and Hydrometer), Soil Classifications

Specific Gravity Data Sheets A-2 APPENDIX 3. Saturated Vertical Hydraulic Conductivity Data Sheets A-3 APPENDIX 4. Exchangeable Acidity Data Sheets A-4 APPENDIX S. Sodium Concentrations for Cation Exchange Capacity Calculations - A-S APPENDIX 6. Chain of Custody for the HRB Shelby Tube samples A-6

TABLES

Table 1. Soil Classification Based on Particle Size of the HRB Shelby Tube Samples 4 Table 2. Unit Weights of As Received HRB Shelby Tube Samples S Table 3. Unit Weights of Dried HRB Shelby Tube Samples . S Table 4. Natural Moisture Content, Specific Gravity and Porosity ofHRB Samples 6 Table S. Vertical Hydraulic Conductivities <k--) ofHRB Shelby Tube Samples 7 Table 6. Comparison of Water Contents of As Received and Saturated Samples From the

HRB Shelby Tubes 7 Table 7. pH Values for the HRB Shelby Tube Samples 8 Table 8. Exchangeable Acidity of the HRB Shelby Tube Samples 8 Table 9. Cation Exchange Capacity of the HRB Shelby Tube Samples 9 Table 10. Summary of the Geotechnical Properties of the HRB Shelby Tube Siunples - 10 Table 11. Summary of the Geochemical Properties of the HRB Shelby Tube Samples - 10

FIGURES

Figure 1. Locations of the HRB Shelby Tube Samples Analyzed in This Study ---- 2

I I I I I I I I I I I I I I I I I I I

WESTINGHOUSE SAVANNAH RlVER COMPANY SAVANNAH RIVER TECHNOLOGY CENTER

GEOTECHNICAL ANALYSIS OF FIVE SHELBY TUBE SAMPLES FROM THE H-AREA RETENTION BASIN (U)

Christine A. Langton Westinghouse Savannah River Company Savannah River Technology Center, Aiken, SC 29808

W.L.Mhyre Raytheon Engineers & Contractors Savannah River Site Aiken, SC 29808

SUMMARY

WSRC-TR-99..oooS7 February 8, 1999

Page 10fll

Geotechnical and geochemical analyses were performed on five Shelby tube samples collected in the H-Area Retention Basin (HRB) during July and August of 1998. The samples were collected as part of the HRB characterization study. The test results, which are documented in this report, will be used to support the HRB contaminant fate and tranSport modeling/analysis and to evaluate remedial options. The results will also be used as a base line for future treatability studies.

The geotechnical testing was performed in the SRTC low-level radioactive soils characterization laboratory. WSRClSRTC and Raytheon personnel conducted the test program. ASTM and EPA test protocols were used. Sample locations are indicated in Figure 1. The physical and chemical properties of the samples are consistent with the soil types, i.e., clayey sands to sandy clay. Details of the soil classifications are provided in Table 1. Test results are summarized in Tables 2 to 11. Data sheets are provided in the Appendices A-I to A-6.

BACKGROUND

Descriptions of the HRB (281-3H) construction and operating history ire provided elsewhere. I, 2

Samples analyzed in this task were collected as part of the 1998 HRB sampling and characterization program which was conducted to support the Resource Conservation and Recovery Act Facility InvestigationlRemedial Investigation Work Plan (RFJIRI) for the H-Area Retention Basin (HRB) Operable Unit (OU). Results obtained in this study will be-used to support fate and transport analysis, evaluate remedial action objectives, and support human health and ecological risk assessments involved in HRB remediation. They will also be used to support future treatability studies. During the sampling campaign in 1998, Shelby tube samplers were used to collect undisturbed material from the basin at 3 locations (HRBS-04, -OS, and -06) and from three wells (HR3-14C at

WSRC-TR.-99-OOOS7 Febnwy 8, 1999

Page 2 of 11

10.0 to 12.0 feet below land surfiIce (it bls), HR3-1SC at 132.0 to 134.0 it bls., and HR3-16 DL at 6.0 to 8.0 it bls). Five Shelby tubes, which were identified by Environmental Restoration personnel for this series of tests, were relocated to SRTe, 773-A on 12-28-98. They included well samples, HRB-14C, HR3-1SC and HR3-16DL, and samples collected from the basin bottom, HRBS-2S-01, and HRBS-27-01. The samples were sealed and transported to building 772-7B for temporary refrigerated storage. Storage in SRTC was under ambient conditions.

L. A Bagwell, SGS, provided a correlation between the sample locations and the Shelby tube labels. This information is provided below:

SHELBY TUBE LD. HR3-1SC HR3-16DL BRBS-25~1 BRBS-27~1 BRB-14C

C4rresponding well or bore bole Well Well Hole Hole . Well HR3-1SC HR3-16DL BRBS~S BRBS-06 HR3-14C

Date Sampled SAug. 1998 30 June 1998 23 July 1998 27 July 1998 10 July 1998

Ground Elevation (ft above mean sea level) 263.3 254.9 -263 -263 264.S Sample Depth (ft below land SUIfal:e) 132 -134 6-7 0-2.S 0-2.S 8-10 Sample Elevation (ft above mean sea level) 129.3 - 131.3 247.9 - 248.9 260.S -263 260.S -263 2S4.S - 2S6.S Approximate Core Length ~inches~ 12 16 20 IS.s 26

The locations of these samples are shown in Figure 1.

_'~· ____ ~I ____ ~I~~~I~ __ ~t ____ ~I~ __ ~I~ .. . ..... ---_.

.-, ....

-

- I , I !I • !' --

Figure 1. H-Area Retention Basin Sampling Locations



LABORATORY TESTING

WSRC-TR-99.,oooS7 February S, 1999

Page 3 of II

Geoehemcial properties of the soU samples were determined according to the United States Environmental Protection Agency (EPA) SW-S46 methods. Physical and hydrological parameters were determined using American Society for Testing and Materials (ASTM) or United States Army Corps of Engineers (COE) procedures, as applicable. The following tests were conducted: I. Core Logging 2. Particle Size

a. #200 Sieve Analysis (ASTMo.II40) b. Sieve Analysis (ASTMD-421) c. Hydrometer Analysis (ASTMD-422)

3. Unit Weight and Moisture (SRTe Procedure) 4. Natural Moisture (ASTM D-2216) S. Bulk Density (ASTMD-4S31) 6. Specific Gravity ASTM D-SS4) 7. Porosity (calculation) S. Falling Head Permeability - Vertical (ASTM D-SOS4) 9. pH(USEPA) 10. Exchangeable Acidity (US EPA30S.I) II. Cation Exchange Capacity (US EPA 9081)

RESULTS AND DISCUSSION

.Vuual Description/Core Logging

The descriptions of the soU/sediment samples in the HRB Shelby tubes are given in Appendix A-I. The soils were clayey sands to sandy clays. The descriptions are consistent with the soU classifications based on the particle size data reported below.

Soil Classification Based on Particle Size Analyses

Particle size data generated by sieve analyses (ASTM D-421 and ASTM 0.1140) and hydrometer analyses (ASTM D-422) were used to determine the soil classifications of samples from each of the HRB Shelby tubes. A summary of these results and the soU classifications is presented in Table I. The Data sheets with the test results are given in Appendix 2.

Slight differences in the visual descriptions and the soU classifications were anticipated because only a amall portion (about 3 inches) of the core was selected for the particle size analyses. This material was also judged to be the most representative of the core.

The most consolidated section of the core was selected for the hydraulic conductivity tests since the parameter of interest is related to the ability of the strata to act as a confining layer. Representative material was selected for the other tests. Gravel layers were not intentionally included since larger samples are necessary to accurately evaluate the amount and distribution of the gravel and/or cobbles on the physical properties of these soils.

*

WSRC-TR-99-OOOS7 February 8, 1999

Page 4 of 11

Table 1. Soil Oassification Based on Particle Size Analyses of the HRB Shelby Tube Samples.

Coarse Mediu Fine Gravel Sand Sand Sand Silt. Clay Colloid (wi. %)* (wi. %) (wi. %) (wi. %) (wi. % (wi. %) (wi. %)* Classification."

Well Samples HRB-14C 1 1 9 49 3 37 «34) Clayey Fine Sand HR3-1SC 8 9 8 52 8 15 « 14) Clayey Fme to Med.

Sand HR3-16DL 0 0 16 60 8 16 « 14) Clayey Fine Sand

Basin Samples HRBS-2S-01 0 2 20 22 6 50 «45) Sandy Clay or

Clayey Fine to Med. Sand

HRBS-27-01 2 7 38 24 6 23 «20) Clayey Med. Sand

The gravel and larger cobble size fractions are under represented in this description because the small diameter (2 and 5/8 inch diameter) of the Shelby tubes excluded collection of any larger material which may be present in the strata.

•• The colloidal portion of the sample is a subset of the clay fraction.

... ASTM D-422 provides the following definitions for the various size fractions.

Gravel: . Material passing the 3 inch (7.62 em) sieve and retained on the No.4 sieve (4.75mm);

Sand: Material passing the No.4 sieve (4.75 mm) and retained on the No.200 (75 mm) sieve. a) Coarse sand = Material passing the No.4 (4.75 mm) sieve and retained

on the No.10 (2.00 mm) sieve. b) Medium Sand = Material passing the No. 10 (2.00 mm) sieve and

retained on the No. 40 (425 J1lll) sieve. c) Fine sand = Material passing the No. 40 sieve (425 J1lll) and retained on

the No. 200 sieve (75 J1lll). Silt Size: Material 0.074 to 0.005 mm in diameter. Clay Size: Material smaller than 0.005 mm. Colloids: Material smaller than 0.001 mm.

I I I I I I I I I I I I I I I I .1 I I


Unit Weights of the HRB Shelby Tube Samples As Received and Dried

WSRC-TR-99..()()()57 February 8, 1999

Page 5 of 11

The unit weights of the samples as received and the unit weights of the dry samples are reported in Tables 2 and 3, respectively.

Table 2. Unit Weights of As Received HRB Shelby Tube Samples.

SampleID Wt. Wet Length of Soil (grams) . Wet Soil

(mches) Well Samples

HRB-I4C 782.4 3.652 HR3-15C 654.8 2.25 HR3-16DL 412.5 2.18

Basin Samples HRBS-25-01 672.6 3.125 HRBS-27-01 518.7 2 .

pcf - pounds per cubiC feet

Diameter Soil Core flllches)

2.875 2.875 2.875

2.875 2.875

Volume

S~le (ft')

0.01 0.01 0.01

0.01 0.01

Table 3. Unit Weights of Dried HRB Shelby Tube Samples.

SampieID

Well Samples HRB-14C HR3-15C HR3-16DL

Basin Samples HRBS-25-01 HRBS-27-01

Wt.Dry Soil ,. -,

625.5 460.1 349.5

545.5 463.9

pcf - pounds per cubiC feet

Length of Diameter Dry Soil Soil Core (mches) (mches)

3.652 2.875 2.25 2.875 2.18 2.875

3.125 2.875 2 2.875

Volume sample

(£1:3)

0.01 0.01 0.01

0.01 0.01

UnitWt. Wet (pei)

125.52 170.51 110.86

126.10 151.95

UnitWt dry

(pcf)

100.35 119.81 93.93

102.27 135.90

Natural Moisture, Specific: Gravity and Porosity

WSRC-TR-99-OOO57 February 8, 1999

Page 6 of 11

Natural moisture was c:alculated by determining the weight of water in each Shelby tube sample and c:alcuIating the moisture content relative to the dry weight of the sample (mass water/mass dry soil X 100). The natural moisture contents and the porosities of the samples are listed in Tables 3 and 4, respectively.

Table 4. Natural Moisture Content, Specific: Gravity and Porosity of HRB Shelby Tube Samples.

SlID ample Well Samples

HRB-14C HR3-15C HR3-16DL


Natural Moisture Content

ASTMD 2216 -20.05 29.73 15.27

18.90 10.56

Specific Gravity

ASTMD 854 -

2.24 2.60 2.62

2.64 2.61

Saturated Vertical Hydraulic: Conduc:tivity

Porosity Pore

F raction

0.282 0.262 0.426

0.379 0.166

Samples for the hydraulic conductivity tests were selected from portions of the core which were considered to be intact. The least fractured, most consolidated, highest clay content portions of the .core were selected for the hydraulic conductivity tests because it was assumed that the parameter of interest was the ability of the soil to function as a confining layer. Since the sample length was at least that of the diameter, some of the aamples contained gravel (up to Y:. inch), which was apparent after the aamples were removed from the cell, broken up and dried. Minor defects in the core surfaces (up to 3/8 inch deep and of limited sudiice extent) were patched with similar soil from the core. The samples were oriented in the permeability cell, such that, flow was parallel to the long axis of the core, i.e., vertical conductivities were measured.

Two aamples, HR3-15C and HR3-16DL were remolded after no flow was observed after several hours in the cell. Sample HR3-15C had a very high water content and was compacted as the result of the cell and head pressure applied to the sample during testing.

The samples were saturated to 13 values of greater than 0.95 per the ASTM procedure. Saturation was accomplished in the permeability cell prior to the conductivity measurements. Results are presented in Table 5. In addition, the finalwater content after saturation and completion of the hydraulic conductivity test was determined and reported for each sample used for the hydraulic conductivity measurement. This information is listed in Table 6 along with the water content determined on the as received aample. Data sheets are presented in Appendix 4.

I II I I I I I I I I I I I I I I I I II



Page 7 of II

Table 5. Vertical Hydraulic: Conductivities (k.-...) orHRB Shelby Tube Samples.

Falling Head Hydraulic Conductivity ASTM D-5084 Run 1 Run 2 k Avc•

S8IllJ)le ID (cm/sec) (cm/sec) . (cm/sec) Well Samples

HRB-14C 1.67E-04 2.03E-04 l.85E-04 HR3-15C 1.06E-06 - 1.06E-06 HR3-I6DL 2.67E-OS 2.29E-OS 2.48E-05

Basin Samples HRBS-2S-01 4.02E-06 - 4.02E-06 HRBS-27-01 1.73E-OS 1.78E-OS 1.76E-05

Table 6. Comparison or Water Contents or As Received and Saturated Samples From the HRB Shelby Tubes.

SampleID

Well S8IllJ)les HRB-14C HR3-1SC HR3-16DL

Basin Samples HRBS-2S-01 HRBS-27-01

Water Content As Received

(from Table 2) (wt. % of solid)

20.05 29.73 15.27

18.90 10.56

Water Content After Saturation (from hydraulic conductivity

data sheets) (wt. % of solid)

25.2 32.9 12.0

29.2 17.5

I

Soil pH

WSRC-TR.-99-OOOS7 February 8, 1999

Page sofH

The pH of the soil is a measurement of the H' ion concentration in the pore fluid, which is in equilibrium with the soil, i.e., pH = log (I1CH+). The measurement determines the degree of acidity or alkalinity of the soil materials suspended in water. Deionized water was used to obtain these values per the EPA test method 904SA Results for the HRB Shelby tube samples are listed in Table 7.

Table 7. ph Values for the HRB Shelby Tube Samples.

SamoleID WellSamoles

HRB-14C HR3-1SC HR3-16DL

lBasin Samoles HRBS-25-01 HRBS-27-01

Exchangeable Acidity

pH samole 1

8.7 8

5.9

8.7 5.7

pH I samole2

8.2 7.28 5.14

7.88 4.75

pH Average

8.4S 7.64 5.52

8.29 5.22

Exchangeable acidities of the HRB Shelby tube samples were determined according to EPA Method 305.1. This test measures the mineral acidity of the sample plus the acidity resulting from oxidation and hydrolysis of polyvalent cations, such as, salts of iron and aluminum. Results are summarized in Table 8, and the data sheets are presented in Appendix 4.

Table 8. Exchangeable Acidity of the HRB Shelby Tube Samples.

Acidity (ueq!L) Acidity (ueq!L) Acidity (ueq/L) SamoleID SamoleA SamoieB Average WellSamoles

HRB-14C 90.3 170.5 130.4 HR3-15C 360.1 494.5 427.3 HR3-16DL 251.4 240.8 246.1

Basin Samoles HRBS-25-01 170.0 180.1 160.5 HRBS-27-01 140.9 105.3 123.1

I !

I I



Cation Exchange Capacity


Page 90fll

The cation exchange capacity (CEC) is a measure of the negative charges carried by the soil particles, organic matter and sesquioxides. US EPA Method 9081 was used for these determinations. Results are summarized in Table 9.and analytical data for sodium concentrations of tests solutions are presented in Appendix 5.

Table 9. Cation Exchange Capacity of the HRB Shelby Tube Samples.

CEC (c......tkg soil) CEC (c......tkg soil) CEC (c......tkg soil) SlID amJ>le S I A SIB A ample ample verage Well Samples

HRB-I4C 3.20 3.28 3.24 HRl-15C 4.76 3.47 4.12 HRl-l6DL 1.95 1.17 1.56

!Basin Samples HRBS-25-01 4.42 4.16 4.29 HRBS-27-01 . 3.36 2.71 3.04

CONCLUSIONS

The HRB Shelby tube samples analyzed in this study are clayey sands. One sample from the bottom of the basin, HRBS-25-01, is sandy clay. Geotechnical and geochemical test results obtained in the test program are consistent with the soil types and are summarized in Tables 10 and II, respectively. Data sheets are included in the Appendices A-I to A-6.

REFERENCES

1. WSRC-RP-97-122, Rev. 0, March 1997, "ASCADTM Combined Feasibility Study Proposed Plan Document for the H-Area Retention Basin (281-3H) (U)," Westinghouse Savannah River Company, Aiken, SC.

2. WSRC-RP-98-OO125, Rev. 0, March 1998, "281-3H Retention Basin Treatability Study Work: Plan (U)," Westinghouse Savannah River Company, Aiken, SC.

3. WSRC-RP-99-121, Rev. O.,]amwy 21, 1999, "Task Technical Plan for Geoteclmical Analysis of Five H-Area Retention Basin (HRB) Shelby Tube Samples (U)," Westinghouse Savannah River Company, Aiken, SC.

4. WSRC-RP-99-122, Rev. 0., ]amwy 21,1999, "Task Quality Assurance Plan for Geotechnical Analysis of Five H-Area Retention Basin (HRB) Shelby Tube Samples (U)," Westinghouse Savannah River Company, Aiken, SC.

WSRC-TR-99-OOO57 February 8,1999

Page 10 of 11

Table 10. Summary of the Geotechnical Properties ofthe BRB Shelby Tube Samples.

SampleID

Well Samples HRB-14C HR3-15C HR3-16DL


Ground Elevation Ftabove

....... "".-

264.5 263.3 254.9

-263 -263

Sample Depth

Ftbelow ._ ... -........ _ ......

8 to 10 132 to 134

6t07

o to 2.5 o to 2.5

Sample Elevation

Ft above MSL

254.5 to 256.5 129.3 to 131.3 247.9 to 248.9

260.5 to 263 260.5 to 263

Specific Gravity ASTM - "" .... --.-

2.24 2.6 2.62

2.64 2.61

Natural Unit Wt Moisture

Porosity as Unit Wt ¥o H2O Pore received dry ASTM

A-a __ .. _va. '-" .... ·1 \.1' .... ·1 ---_ ... -

0.282 125.52 100.35 20.05 0.262 170.51 119.81 29.73 0.426 110.86 93.93 15.27

0.379 126.10 102.27 18.90 0.166 151.95 . 135.90 10.56

Table 11. Summary of the Geochemical Properties of the HRB Shelby Tube Samples.

Exchangeable Acidi1

IWell Samples HRB-14C 8.45 130.4 3.24 HR3-15C 7.64 427.1 4.12 HR3-16DL 5.52 246.1 1.56

[Basin samples HRBS-25-01 8.29 160.5 4.29 HRBS-27-01 5.22 123.1 3.04

Vertical Hydraulic

ConductMty Kave.

'-"'~"'''''I

l.8SE-04

2.48E-05

4.02E-06 1.76E-05

-------------------


QUALITY ASSURANCE

WSRC-TR·99-OOOS7 February 8,1999

Page 11 of 11

Testing was conducted in accordance with ASTM standard practices and SRS procedures. Results are recorded in Laboratory Notebook WSRC-NB·98-OO204. The Task Technical Plan and Task Quality Assurance Plan for this effort are documented in WSRC-RP·99-OO122 and WSRC-RP.99-OO121, respectively. The Chain of Custody documentation for the Shelby Tube Samples is provided in Appendix 6.

ACKNOWLEDGEMENTS

Wyman Pope Jr. and Clyde N. Shramek, Raytheon Engineers & Constructors, perfonned the geotechnical testing. Frances Wakefield and Cathey Coffey perfonned the geochemical testing. Cecil Woodard and Lynda Wmgard opened the Shelby tubes and extracted the samples.

WSRC-TR.-99-OOOS7 . Febnwy 8,1999

I Page AI-I

I I I I

APPENDIX. 1.

HRB Shelby Tube Sample Descriptions I I I I I I I I I I I I I, I

• '. I I

• I I I

• I I I I I

• I I I I

Visual Descriptions of the HRB Shelby Tube Samples

HRB-14C

WSRC-TR.-99-OOO57 February 8,1999

Page M-l

Approximately 26 inches of core was recovered from the Shelby tube. The upper 7 inches was disturbed and contained about 60 volume % large (up to 1.5 inches) quartzite gravel plus sand, silt and clsy. The gravel is subangular, hard and dense. This section of core is mottled yellow/red/white.

The lower 19 inches is a silty clsyey sand and contained no gravel. A few of the largest particles were less than 0.5 inches. The structure of this portion of the core is uniform and the color is mottled yellow/redlwhite.

HR3-15C Approximately 12 inches of core was recovered from this Shelby tube. A few pieces of quartzite gravel were recovered from the top of the sample. The first 7 inches consisted of an organic rich silty sand which was grayish brown in color, mottled, and contained b1sck charcoal particles (up to 3/8 inch), soft white agglomerates of white clsyand clear quartz sand, light gray, dense quartzite (up to 3/8 inch).

The next 2 inches was a sandy silt which was similar to the material directly above it except this lsyer did not contain the carbon and the quartzite gravel was larger (up to 0.5 inches).

The bottom 3 inches of this core was very wet fine silty sand. It is greenish yellow and is not cohesive. This layer contains no gravel.

HR3-16DL Approximately 16 inches of core was recovered from the Shelby tube. The upper 13 inches consists of wet mottled gray brown silty sand. It contains a sma1l amount of light gray, dense, subangu1ar quartzite gravel up to 1.5 inches in size. This section of core also contains a few root or twig fragments.

The bottom 3 inches of this core consists of wet, yellowish silty sand with orange mottling.

BRBS-25-01 Approximately 20 inches of core was recovered from the Shelby tube. Several pieces of quartzite gravel were present at the very top of the tube sample.

The remaining sample is a clayey, silty sand containing 5-10 volume % hard, dense light gray quartzite gravel up to 1.5 inches in size plus soft aggregates (less than 1 inch in size) of clear quartz sand. The quartz sand aggregates break/crumble very easily. The core is mottled red/yellow/orange and tends to fracture along the red mottling. Some layers have more sand than the others. The core fractured along the red (weathered) zones both perpendicular to and diagonal to the long axis of the core.

l

HRB8-27-01

WSRC-TR-99-OOOS7 February 8,1999

Page AI-3

Approximately 20 inches of core was recovered from the shelby tube. Black organic rich liquid was observed above the top plug in the tube. About 3 inches of sand and gravel coated with black organic material was recovered just below the plug. This material was not sampled.

The next 5 inches of core contain fine clayey silty sand without gravel. It is mottled. This section is similar to the bottom 5 inches of this core except the sand is finer.

The next 4 inches of core consisted of a clayey, silty sand which contained about 20 volume % of the dense quartzite gravel and also about 20 volume % of the soft clear quartz sand agglomerates in a white clay matrix. The color of this core is mottled yellow/redlwhite.

The next 2 inches consist of a few large quartzite gravel. This material was unconsolidated after removing it from the tube.

The bottom 5 inches of this core consisted of calyey, silty sand containing and soft clear quartz sand agglomerates up to 1.5 inches in size.



"

o

D

o v. we. t:. ..

Bottom

Bottom

Bottom

-. , Bottom

Bottom

ORB Shelby Tube Samples

.3 II, ..,ct S

BRB3-15C 12 inches Top

HRB3-16DL 16 inches Top

, • . HRB5-25-01 20 inches Top

II

.... 0 t-iled :Ie'! r~/oin .

HRB5-27-01 15.5 inches Top

HR·14 26 inches Top

,~

•

• WSRC·TR-OOOS7 February 8, 1999

AI-4

)0 -.

.

Sample: J.lR~ - ,<Ie Date: 1-.7/-'11 Tedaniclan: e. 1

DistaDcc fiom bottom of core 0-/'1"';'" ,9- ~(."

1 SoU JttQup name I ~e.:!n ;X:.'Id 'fD ,,~.I" a-/dL._ G "II!" .1 2 Group Symbol v <J • 4 4 '

3 VoL % Cobbles - 0 JJ 'IStlnJ -fine/course IV,," u'2.

4 Vol % Sand "30 - '10 '7

to'l~ .e. fine/mcdlcoursc 5 VoL % fines (po -70 7) ?o70 6 Particle angularity

Angular/subangl - 54-" subroundlround 7 Particle shape £r~ .. f)-

F1at, clongatM, flat . -and elo 5 r rl'J"la r

8 Maximum particle V. - 4Upf I:>r 1 '$'1 size I{ "OC.Cc< .... IJlh 'I

9 Hardness of course sand and large _. -particles

10 Plasticity of fines PAsl.c.. /Il~ (JIP;/"

11 Dry Strength 'Y wJorod: None, low, med., 1./.11 h.. 1 .. • .... hildt. v. hi~ 12 Dilatancy

None slow, rapid .... -13 Toughness - -

Low med. hiM 14 Color />1o#/~ ..J, 1:;'~~eJ~

I em moist condition) .J..I~ ci«,

15 Odor '" ~.o • IIJ,~

16 Moisture MDlSl \J../e.A .. Dry, moist, wet

17 Reaction with HCL -' -none, weak, strong

18 Consistency i),<;lvrbeJ v. soft, soft, firm, V. ~,r(\'>

hard v. hard 19 Structure ~ n. ,J, .. I.e.!. 20 Cementation

.~ -5tr'''''' *,~ .. ~ 11')

Weak. mod. strong I,..i e-\: u.....i../, 21 Local name 23 Comments fw,-t/kJ. VIS""" bd (,...0

roots, root holes, ~~ft; e-mica, surface

coatings on coarse A~o ' .1 grains. caving of hole, difficulty excavating

..t..

I'

,

,

. . , "'"

of 13. 1I1~);F I(

"

.

.

I I II

I I I I I I I I I I I I I I I II


wsac-m,QQQS1 Af·(j"

Samnle: AA'3 -is"C Date: 1-" , -., r Technician: C. ~"'l r.... ofB, f( lfu.~ Dis\aDCO IioIIlboUom ofcoro ,,_ ~ ",Jo..: '3 -, t:; ,10 - 1"'1 I I.:J 01- '/

1 SOU'RroUD name .t:. lc;.I~, <l:A ..I .-: . , . I_~, ., ... 11" Q, .... e., 2 Group Symbol 'IT " " ~ ; , 3 Vol % Cobbles

0 100 7-fine.lCOUISC ;:).0 70 2~7. 4 Vol % Sand '1 0 _/00

' ". '.

finelmcdlCOUISC 1""0 ,. (oS 7.- -~ . 5 VoL % fines 5,7+- ? 10 "?,, /1)£ 7~ '5 7· -6 Particle angularity <; ... b .... j"l.r

AnguIar/subangl I .to s "j, "'.<mol..!

sub~ -7 Particle shape

.If""'~'j" /"'''- flo. t -l-o In~.i. F1at, elongated, fiat and el' - .'

8 Maximum particle J.. It " , ',* /I

si7.e . :;> 9 Hardness of course Q"I!lM~.r.. ~~"".h, I-e. .q ..... r~.ic...

sand and large - h"..- J ..... ,..J. h...r..L

Darticles 10 Plasticity of fines NiTf r/~'G s ... ..,,, !VA C'!>c;. ... ~ -&G_~

11 Dry Strength

.~o~med., low I .. oJ . to iJ tJA

12 Dilatan . cy -None. slow. nmid - - -13 Toughness.

Low~ med.. hi~h - - - -14 Color ''f'II-.· ". '. _.' I~"IS~ ~"h .. -t- .

I em moist condition) . t'::,,' Q/i«.J ~~!':dl~ b!:1.. do.r 1(,., lfn" .. ,,-,, 1';...., .. ;<. t..

15 Odor J\fo ... e ~" .... '1I.1A # '. I~ 16 Moisture '.

v I nrv.- moist. wet ~~.;"" .t.[ v. tue-t ¥.~f NA.

17 Reaction with BCL ' - - -none. weak, strong -

18 Consistency v. ~ft, soft, firm, 1m v. hard

~"c;. J,.. '7" ++ 'Soft rJA 19 Structure -M. £. "..... ..c. ~ 1:2. .,. ;,...,# O,sl-.. ," he J IV-r\.

20 Cementation no'" c.~e" ~e.' p

weak. mod. strong - - - . -21 Local name -23 Comments

boHom ~~ t, ...... t:. ,,,,f,.,,e.J

roots. root holes, (J.re.. .;....,.c. .. ..1. mica,surfIoc Sloel ''1 -/.1J<- #'

<;"''''f 'Co ~ .los''''''' jr.L., -coatings on coarse . . grains. caving of {;..-f,,.,J '" ,t-n-.. -Ivrc...-

hole. cfifficulty . ~~-k.l~. excavatiM ~ 1/. , .. , ... 1

WSRC·TR

Sample: 1-1R. ~ • J~ l>L . Date: 1-1'-f9 Techniclan: C .1... ...... -I.,..4!.. A1~ Distance &om bottom ofcorc o -3 "I~ 3 -7-, 7 ~ 16 •

1 son IlI'OIlD name "',IJL~·~";lA~ mdJ...c~~ ... rk~ ... ,. ~....l

2 Group Symbol • d"y,,:! ........ .!. u

.

3 VoL % Cobbles t. J /<> L$/o fine/course -

4 Vol % Sand 5"Cr~ ,

finelmcdlcourse sn+ 57)t-

5 VoL % fines ~() 7" .5V- 5lJ-6 Particle angularity 'S"~ "'''1 -/.,..

AnguJar/subang/ 9<lb ,,,un./eJ 5«.mc- .sa.,.,.., e.. subroundlround Q~ ... +~,-?c..

7 Particle shape .1(' ~l4l1 ... " FJat. elongated, flat - r "',. . ~. .-

andelo I . et ..... Vl+ --~ ... -8 Maximum particle ·It I

size 1{_'/f II "Sec.",c.. ;Jq," -e. 9 Hardness of course

sand and large /+ ....... ci s ...... ~ S«. ... -c... particles .

10 Plasticity of fines - - -11 Dry Strength

'. None,low, med., ('I\~ .9 a..,., ~ ~Q..irt ~ hid!. v.hWl

12 Dilatancy -None. slow. llIIlid , - -

13 Toughness - -Lowmed., high r-.

14 Color I fmmoistcondition) ~f. ~:: .. ~~ ,.' 13,,0"''' 'S~ 'Ve.I/otU j,,. .... '1 .'

15 Odor r7 t. :,:,; ... HI 1'1 tV 0 ~ "'- No;'

16 Moisture we:-{ Dry, moist, wet wc.+ we4

17 Reaction with HCL - - -none, weak. strong

18 Consistency v. soft, soft, firm, F,t" yv'I F. ""'" F. r ""'-hard, v. hard

19 Structure ~~,."" ~~"'" 1ObT''''' 'U~. '>-r""

20 Cementation - ~

Weak, mod. strong -21 Local name - --23 Comments

roots, root holes, : ~e .... roc:A.s mica, sur1iIoe

&'1--eX,atjor;; on coarse , grains, caving of ~ .... \,~ hole. difficulty excavatiw!

A ... '

re,.- I I I I I I I I I I I I I I I I I I II

I' I I I I I I I I I I I I I I I I I I

Sample: IH~."S-26-o Distance from boctom ofCOIC

1 Soll ~ lUIIlle 2 Group Symbol

3 VoL % Cobbles finelcoursc

4 Vol % Sand tinelmcdlcourse

5 VoL % fines 6 Particle angularity

AnguIar/subangl subroundlround

7 Particle shape Flat, elongated, flat andelo

8 Maximum particle size

9 Hardness of course sand and large particles'

10 Plasticity offines

11 Dry Strength None, low, med., high, v. hildt .

12 Dilatancy None,slovv,r.apid

13 Toughness Lovv med. hildt

14 Color (m moist condition)

15 Odor 16 Moisture

Dry. moist, wet 17 Reaction with

HCL none, weak. strong

18 Consistency v. soft, soft, firm, har.d, v. hard

19 Structure 20 Cementation

Weak. mod. 21 Local name 23 Comments

roots. root holes, mica, sudiu:e mating" on coarse grains, caving of hole, difficulty excavatiru!:

I wsao.'I'R~

Date: -;21-.,,9 Technician: e.Ln.. .L '+8.~.L U

o~~" ~O-dl f:oUkc, ,,10 .. ~ ~ cc,e- , icJ.""" ~n.c;, .. 11&

. va

I. 5D~ r:.rn'~ /I. 'i"M • k -q,.

,·",..st°1, 7-«I 1...5-~ •

(,0-70

40-30

5,,/' 1

~"I-I,,~."'a r

,J?-.- I '~ 1/

1<J(1rh . ~ s;.{!

r"h'k~I...~J ho..r-i

PI"sf/Co

H ''i~

-

-,.. #(a~ rei. ~ou. :u~ . tJD(\1!.

Mo,s-i

-

F,rm

/J6" .. ~ f"A",'1 ~

S·hD"1

"",,_4.JL w-kl. cS

... 1."1 'reJ ~tI<!: ,-k.. M .. re.. ~A.l '"' \wi.-..

#,--. ''1e...

.. -

Sample: H~S -:)"7-0 , . Date: 1-.:21-99_

L Al~91 I

TedlDician: C. v ..... t-.. of B. "12. tuA" 'I I

Distance from bottom of core 1 SoU RrOUD uame 2 Group Symbol

3 VoL % Cobbles finelcourse

4 Vol % Sand finelmedlcoursc

5 Vol. % fines 6 Particle angularity

Angular/subangl subroundlround

7 Particle shape Flat, elongated, flat and elo

8 Maximum particle size

9 Hardness of course sand and large

I particles 10 P1asticity offines

11 Dry Strength None, low. med .• hisdt.v. hiih

12 Dilatancy. None slow,rapid

13 Toughness Low: med. hi2h

14 Color Cm moist condition)

15 Odor 16 Moisture

I Dry, moist wet 17 Reaction with

HCL none, weak. strong

18 Consistency v. soft, soft, firm, h~d. v. hard

19 Structure 20 Cementation

Weak mod. strong

21 Local name 23 Comments

roots, root holes, mica, SIIdi= coatings on c:oarsc grains. caving of hole, difficulty excaVating

,() --<" S-?" 11'0_ ,<_J . «~~Ik ,1.';;;,,;'

qd •

s..fI ~" .. rh' ~t~ -::-."'s'Oft:!i SV-90 '70

~n ... eobbl~

(.0 ,. to-IS" ;2.0 '7D ,~-IO

IJ.r.!#-::,~ -A=I 'x, .... . .f clEo- S .... b -r

I-;_ .. h~ j

Sof-l s<>6 j: 0 ~ I (S.'z:1:'

,,~ /I I '~

$A~J r"'s=H«. ~J'(.I"" 1"<Ius/DkS,

$".f~ ... ("' ..... V· hOJ'c:l

Pk&-/,e -

t/IeJ -

--- -

m.,.+-"'''' ~'C"'''S ~~;,M:.... 0-" ,~'~ 14 .... rh..!oc,,",

1\)01'1 .... UA.Jlld-e. • c

'rv1o;~ t -- -.

\: ,r N1 CD rc ~ll "/"'" ... ,iI... \4 ...

I~~ ~""~ I~~~~ -~ .. "",~ ... ~ tu~

- -O'~~G

(..QnS .,c"f-'''1 • f OI1C. /<"'j":" f'" 'fA. },,~-te

/'=<'" A <;;~ <-lIer

ii_II " 7/-11. I"/(rl'l AI_ -.cJ ~ ..... <.lu.-. G.-I ~. ""9$d'~; .' _ 'I

S ......... .r 11'/cJx./M 5 .; O-t>

!S,,~t '1,,~ .. h'.;;b~ e"l<..-p-l i?~""'~k ..... J- "0;'; c_l .~ u "In e'" If () -(P"()

/d-:Jt">

Samc. ..... r 0- 'S"

\ I 1~

'. r-+' · ... SOI .t.. f"<lrhA .... 1....,

p)"'s /-,,,

Me,!

--

e~ ... d.SI,"5 '-'

wh,-I-<..

... Io .. ~

~>116 ~ ,,-!r

~

Ft'4<.1 i-'cJ ""r,' .1-""'i<1I:>~ ' . ..-~ Ie~' . , ~

ho<-'-'W -i-r..d.,rC5 !~~. (n!..I.)-",/U$

,

1~4 .. ~ ,- .-/,

~

<3~

I~I!

v.;~ ,~~--

P'/"s~

M-l

---

I I I I I I I I

. i~.-~f.< Q,,,,,

- I I_ •. J

rr'\"'5t

-,

--

O.~~

/)'s+..r~

-a...l-tos

Z~ b.~ot\ odo"'~ 101,uU

I I I I I I !

f""<1~:~ 'r::::!:tti ,,., 'L _ I .... I-.(.1(",," I

I J

I

I

I· 'I I I I I I I I I I I I I I I I I !I

APPENDIX 2.

Particle Size Analyses (Sieve and Hydrometer),

Soil Classifications

and

Specific Gravity Data Sheet

WSRC-TR-99..oooS7 February 8, 1999

PageA2-1

RAYTHEON Engineers & Constructors

WSRc·m.QOO57 AZ-:l

PAGE ...1L OF .ilL

ASTMD75-( N/A ); Particle-Size Analysis

ASTM D422~ 1;' : ASTMC136-(~.A )

Report#: 't1~ ?41ZUIJ'2 *-Ao/I ProjectlWAD#: 71lg ~~

Work Package No.: --...jA~l"/:A-A ___ _ c

QCIR No.: _N.'-"I,YA""--_____ _

TWC: H./tI Lab#: Htze ~/tfC Date Tested: -zblt? ; i

Material Description: CLA.tI/::.t{ GrJe 3o/!D Location: H 1?etPJJrtoN ~fN

Sieve Size

*' C: .. Rllllati'I'e Wl .:t- C:IIRlIlIIItive %I.~ % Passing

Acceptance Retained, grams " Ret:ained-a.

~,q 1,,2.19 '2,/ (,,/1,5

-=tf /0 '!J."1 fnl~·~

/,(,) t/U '7.'1 Ifl1-Z In<§ *."1 Iq,4 ~7.~

. ~_1{1, -ZR>.~ "\

I

I I.

l \

·1 Pan WeIgtrt: t;, -rl? '7 grams

OVenDryWeight b'Z1?,?l7/,Z .. rams

M&TE: IW ... 't4 ICALDUEDATE: 1t/t1fc19 NCR#: "'lit

Criteria

11 Hill qq -q~ '11 1';9 M tpt 10 ~9 , 16 /

"1,7 I

tJ/A Specific Gravity: • 'Z .1?fE;.

[lIyes DNo

Procedure: (! -d12P-dZl

-. I I I

• I I

• I I

• • I I I

• I

• I

- -- ----------------fORIIS.fMP AIR 1s.t7S (7117)

100

gs

go

115

eo 75 - 70 .s::::

C) 115 .-Q) eo ~ 55 >. .0 so '- 45 Q) c: 4:l .-ll. - 35

c: :30 Q)

~ :l5 Q)

:2D a. 15

10

5

RAYTHEON Engineers & Constructors page~ otIS

. Grain Size Distribution Curve Gravel Sand Fines

Coarse Fine Coarse Medium Fine Slit Clav

...........

"'" "" . ""--

'" ~ '" '\

~ \

\ '""'- .

•

3 21.5 1 .75 .5 .38 4· 6 10 18 20 30 40 50 60 70 100 140 200 0.05 0.01 0.005· 0.001 ; 2

0 ,

Sieve Opening. Inches U.S. Standard Sieve Numbers Determined by Hydrometer ;

Grain Size t a Report #: tf/- fAg{ c;t) 512-~I Project #: . H 1?P-7e:N770v ~/N Lab #: t/tze../4e

. ASTM 0 75-( ~ );

RAYTHEON Engineers & Constructors . Particle-Size Analysis

ASTM 0 422-('!i)(~f;' Report#: 'TI- 'Ptl4 ~a>~1? -az:Y

ProjedIWAD #: PM ~/a> !?e7

Work Package No.: -..:M~/J4::1.-___ _

QCIR No.: ----Al!::I!I~t:1.~ ____ _

TWC: iJM Lab#: 1Itz'3-/GC J

Material ~escription: wt!&llk:v. ~ Location: 1/ f?p...$tJ04'I ?-e?IN

Sieve Size

"" CIIRlulali\ll Wl Retained, grams

Date Tested: -=#f..::.~~¢Z"f-LL----

% Passing Acceptance Criteria

tf.c/J. I q{l, 1/

(D 4~.z.. ( .ft?

)

n.01z4 I 1(0

o.C()~. I /)OAII A

Pan Weight 7.It::;C/J_ grams

OVenOryWeight 4t:;'u..lltlil -ms

M&TE: fllJ.14 CALOUEOATE: tI!t7m NCR#: H'I1 Test ¥,I Result / Q Conforming D Nonconforming IZI NfA

Remarks: '* % ftJ(jj ~L .~. l'I 'D,4-TiJ L,_. rmF-Z;:? fflt!.. 6JCt. 6/1rf.I.!4;7P1i. "'z. f7r?tZ~-A1r u: 2YL.

;M *£<!'[email protected]

,eI J)j /11

Procedure: (! .Iit!-P..cIt! Rev: n

peN's: AlIA Specs:

Rev:

OCPs:

I I I I I I I I I I I I I I I I I I

-------------------POIWS..... . .

.... '~'7S(7IOI) RAYTHEON Engineers & Constructors . Page!1:.. oriK

Grain Size Distribution Curve Gravel Sand Fines

100 Coarse Fine .... ... "'urn Fine . Silt Clav IllS "\. !IO " 115 '" eo 15

...........

... 70 ~ 3> 115 » eo > > 55

'" "<. . "\

'"' eo J

5 45 - 4l = 35 .. - 3)

~ 25 l)

I!D

\ \

\ \

\

"" " 15

10

IS

0 3 21.5 1 .75 .5 .38 4· 6 10 16 20 30 40 50 60 70 100 140 200· 0.05 0.01 0.005 0.001

Sieve Opening, Inches u.S. standard Sieve Numbers Determined by Hydrometer

Report #: 91- fAg 2taJ ?e~1 Grain S...I:.iLze~.z;~~~:.....~~:?_It1_ Project #: tI??e Lab #: tit<. 5 -17C i ~

I ~la

WSRC-TR-G00S7

RAYTHEON Engineers & Constructors PAGE ~OF ,_. AU '1 ASTM 0 75-( "'1ft );

Partlcle-Size Analysis ASTM 0 422~ (c;,t' .. ASTM C 136-( "'In )

Report#: q:J~ f7M.!PCO:;1!:-tml Work Package No.: _..Jk::::.,UIAr.a-___ _

Project/\l\fAD #: f AfZ $1 a:') '?12

TWC: tiM ~ Lab#: HSa -ffetJL

Materialoesc::ption: 2 f1.Ltt'fI:3;1{ FIIJe ~p Location: If flelJr F%1120N 1!a#IH

Sieve Size

10

~'CYIftYlati.e \'til Retained. grams

'ZI /1'("

0_4

b.f}

Pan Weight: ->'.Q- grams

%1.3

M&Te: Iw-'Z4 CALOUEOATe: Illt1flq

QCIR No.: IJft'r

O~Tmed:_¥~~nW~----_

Acceptance % Passing Criteria

~

I,a?

/tK'

<1-P g~

613 ~z

"24 -Zl 1:'0

II 17

tJl!i

f"'I

II Jtz.

Specific Gravity: 'h6:>'Z ~yes DNo

Procedure: e- {l;P-tY'Z/ NCR #: ;.J 1ft Rev: 0

Test c;J . 0 rvI-f!,,'A PCN's: ",III Result Conforming Nonconforming ~ 1''', lilt

Lv

1 1 1 1 1 I 1 1 1 1 1 1 1 1 1 1 1 I

- - - -- - - - -.- - - - - - - - - --A8R ''''73 (7/07)

ItO

IlS

go

EI5

eo 75 - 70 .c

C) EI5 .-Q) eo S fO

>- m .c .... <IS Q) c: .., .-LL - 35

c: :lO

~ 25 Q)

2) 0-

15

10

15

0

RAYTHEON Engineers & Constructors Page./a. Of~


Coarse Fine Coal'Re Medium Fine Silt Clav ~

"'-. "-

-".. '\.

'\. '\.

'\ \

\ \

\ \.

"'- f'-., ~

~

3 21.5 1 .75 .5 .38 4' 8 10 16 20 30 40 50 80 70 100 140 200 0.05 0.01 0.005 0.001

Sieve Opening, Inches U.S. Standard Sieve Numbers Determined by Hydrometer

Grain Size Report #~ Cfl- PM '?lctJ713>~@1 Project #:. y12g.-rerlTfa<l '&t?IN lab #: 1f1Z3 ·-Ito Vi..

I I

~!!i

wsaa.m<OllD5f

RAYTHEON Engineers & Constructors Particle-Size Analysis

ASTM D 422-(6 ')C'bf:'

P~:YIp OF L!. .~. '11

ASTM D 75-( I-ljA ); . ASTM C 136-( t.VA ) Report#: Gf1-PIJ(l.?;(~~~J

ProjectJWAO#: P414~/a? 56

Work Package No.: ..... N~/A ____ _

QCIR No.: _-"A.,.t(A..io...-____ _

TWC: AI 14 Lab #: fIFl,f.. t Z;; ,0/ i

tiy,m Date Tested: _~(l:.~i'/1J...f...7 __

Material Description: c44~i FINe 14!Jb Location: H Pe.rr;'1JoNl !3A.G1tc/

Sieve Size

10

leO 14IJ

-* ...Gtli "ulaayS' VVl Retained. grams

o

I. '5 ((J

1.1. D./J ,.. ,n. "'\

/), tJlftfp

* Clllnlliatilie MA7~ '16 Retal"ed ~ ,.

~.7

J..I A

% Passing

It!):;')

<51 I

?{>I

4~ ,/

Acceptance Criteria

;,J/A (

Pan Weight ;;l/~ /" grams Specific Gravity: 'Z,fiK/ OvenDryWeight _c.f/s....ts./fp'7,.Cf__orams liIyes DNo

NCR#: /JIlt Rev: D Test r ;KI . PCN's: IJI. Result I .'1; ponforming 0 Nonconforming 5?J NlA '1ft

I I!I

I I I I I I I I I I I I I I I. I

- - -........ AIP ASR 18-173 (7m)

-.c C>

'Q) S >. .0 "-Q) C .-U. -C Q)

~ Q)

a.

100

as go

e5

00

75

7D

e5

00

i55

5:l

45

"" :l5

:lO

25

:lO

IS

10

5

o

---------- - --- -RAYTHEON Engineers & Constructors


Coarse Fine Coarse Medium Fine Silt - ""-. '\. , ,

\ , .....

. I'\. ""--' ~

...

, -......... -- ,

~\ pa~ltOf~

Clav I ,

I

-........ r

3 21.5 1 .75 .5 .38 4' 6 10 16 20 30 40 SO 60 70 100 140 200 0.05 0.01 0.005 0.001

SIeve OpenIng, Inches U.S. standard Slave N.Jmbers DetermIned by Hydrometer

Grain Size Report #: 19, fAtt~{a?~;e.· aZ71 Project #: rd ~i?3N77CW ?24~//v Lab #: l~tZi?,Z~"l?1

-

I ia

RAYTHEON Engineers & Constructors Particle-SIze·Analysls

ASTM 0 4Z2.-<1/~)('hf;'

WSRc. TR-G0057

PAGE 1 OF 1& A2-10 - -I ASTM 0 7S{ N/r+ ); .. ASTM C 136-( N/A )

Report #: !l. - e~(!. Z(Ct)~f2. # Cl:2/I Work Package No.: M/t).

ProjectlWAD #: 1:44 ?zftZ5~"8 QCIR No.: IJLA-

TWC: N.j4 LsI!!1(Z.!b2 -'2.1--6/ Date Tested: '2/0</8 Material Description: (!Ltitlft: O.~P Location: f:l grJP-.:b/.QoN 7::A 1;ft:!.~

Sieve * GlIll'ltll" \/Ill -* GURllllme ~ Acceptance SIze Retained. grams % Retal"edfll~.H4 % Passing Criteria

?Ii 0 4h~fl 4. lCO ;.It! -=#4 ll.q 4q/.D ... tj5j

·/0 ~~.(P 4 Z'O.3 '1/ 1.0 ~.fJ "'L.."? ~/

4tJ ,q.z. 31.~ ~:,

)PI. 9.Z ~./ 4 !tJ 14 led- 'Z/·1 ~/

..q(.W /.'1. ?LJ.-;; Zq (). b?74zt; urLt " '2.'1 " O.bZi74 t{P I

1)~ Olt.t;,t; ~6> / I'l L .J> /l, I R!l;411 "J.-.~ ~ /2. 14!.tWtNC~ z4 \ ~t. (Mh~?J1 'Z5 ( b. W"?{1 ~ \ "2/ \ AO~I"""1 .J 'to / ~

A tJ/A Pan Weight I HD' 7.·t grams Specific Gravity: ,,!,lR(

Oven Dry Weight tj 'fA,~/~~.q "lams ijlyes DNa MaTE: {W~Z4 CAL DUE DATE: II/fil'f'i Procedure: r!.-q!P-OZ/ NCR#: iJJA Rev: D Test Q Conforming . 0 Nonconforming rn NlA PCN's: ".1114 Result

Specs: / Remarks: of .J;;ff.ltu. _I. //1/1 l' I ~ L. ~/~D t:::Nz. ",/ ~.,. P-!/ItWMz6N Rev:

DCPs: /A 1:~tJe ~u.,. '1~f&'-I Design Categary/

~ A ..-:..--.-.~ .J :... Level: ,;17 Date: ';!".i:.: r t. nspector: ~JI..~ ',. t-A I'

. IR-r: Level: 71r Date: 'E/..'!Jhr

lV


II

II II


Report Title:

Item #

/

Remarks:

RAYTHEON Engineers & Constructors PAGE a OF ~

summary Report of Testing Activities Continuation Sheet

Remarks

,.M/IZAtt t..i t!. eON i:A:·k! /7 V rrtI 71: ·'.fiTS - /J~71IIf "D?ae4 ('to) t::fJLLll.k:1 !-IlEA-V. C!2.e..ce!2 13 PtIJC:16 ~ Icf-18)

6A-.MP~ . Av'u. #1/P/2!Vtl<J fLNWc171VI7Y 1f!l8-14c:. /, 6~ )(/0-4 c'a4/see.

HIZ?J· Z ~-ol Gj. oz. )( 10-4> eM /-;.ee, IIKYJ. t.1-01 (, <1 ~ x/a .$ &tI/~, ilfl~-I{PDL 2,1(P)( lo-5&t1/'5t:e.

il7Z:'-i'5c:. /. ixPx Ic/(Pea1h5:::,

-ASR 18-173 (711'7)

100

gs

00

as eo 75 - 70 ..c

0) as '0; eo S !is

>- eo .c ... <6 Q) C 4J .-U. - :l5

C 3l Q)

~ 25 Q)

:!O Il. 15

10

5

0

RAYTHEON Engineers & Constructors Page~ Of/~


Coarae Fine Coarse Medium Fine Silt Clav ........ r-.....

...........

~

. '" "-\

\ ,

I

\ I , ", .

.",

"-- . I ~

""-~ i-,-

.

,

, 3 21.5 1 .75 .5 .38 4' 8 10 18 20 30 40 50 80 70 100 140 200 0.05 0.01 0.005 0.001

Sieve Opening, Inches U.S. Standard Sieve Numbers Determined by Hydrometer

Grain Size Report#: tft- f4&;,itKJ?"P-~~/ Project#:' t/1?e'0!-pa<l ~/d Lab#: t/tZe.t;?- Z7-t::>/

,

I Iga·

-------------------

WSRC.TR-GOO57

I I I I I

I I I I

/

RAYTHEON Engineers & Constructors PAGE ~ OF _

Summary Report of Testing Activities Continuation Sheet

Report No.: q9-f'Ae:~W$-az>/

Remarks

12.e'!:acr6 t:iFII~7M D4z Z-.c",3(9bt' 5rAIJT.;:JA/l.1? "1i::?f';:::;:;.a f1t;.t2.1'fGLe. - -;51£e ANAL Y<"/~ t)~ ~1L:5 :3AMPt..e. ~ It72.e.~/t/e

MJ:~iZ/lfIL P6~ClZIP//c:iJ: Cc..l4l/ec.J ffAI!f54f.izJ

6PE(;lrl{!. 61Z4VI# Z,.;z$ 4~Vg~4-('lZ) ZE.celZ"'-O P~.e ~ INJO 4 !bIZ. PA.tZ7Jae ~ ~(e-e. /JJJALY~{6

5A.lt1f?Le. ~ HtZ13 -z.~ -01 mlelZlt4i.. 7Y-: ~/2.(Pl1cJl'J ~ -tt 14c.J/~t/ hJ.lI?54A1J) ~J7e(!/AC ("7/2 I4vrTl/: 'ZrA,/l~TiVI()8#-19t) 12Ere:R. 11:> 'PlKr~!7 '3ti(p ~ P#!77C(A~v:ee AtJltL Y <£:to

5fi.MPL.E: ; 1112.1370- 27-CP/ IfAIJ:le2., A-L. VEE- -:bC/Z/Pl7cW ~ eu,4tle1ile? SvJp ~PtX. &IZJ4Vr1'f: '2,(gIJ/~7JtJ Df374- '1z ~=IZ 70 PI1C~~ 7ti8 ht- r/tJ(t.,;7t;.U;-~{'le A-1J1tL. y-1Jr~

-:5A-1t1t1.e. ~ '"za ~ I{POL MJ/rretlll'rL -oe~t2.IP1J()t.lJelAt/8/Fr41! ~NC> ?PE:e. GIUIlfIl:,: "2,(p'2.,A-imllr~-'1'Z 7<P....Fed 10 ~e-!7 q (" ID FDe. P,t}-/l.r;c,(..e -::>I&e. AJ.ML.l/-&I{?

~j4,U1~t.e. ~ tilL. ~ -16 ~ . 1V1A-m.tIkl... 7E~IZ.IPI7tJr';~ t!.t...A-l/eV Me1J.1i1IJD -6PIft'.IPlC. Ufll4Wr0 Z<Ia::? 'JZv::1.E.¢. "1D ~6-"S 1/ /("Z.. k:YL rIl1L77t:!t.e -:s Ii¥- AIIlUt../ 17/ ~

I ____ ~ .. ------------------~ Remarks: I ---------------------------

I

A2-13

WSRC-TR-99-OOOS7 February 8, 1999 I

PageA3-1

APPENDIX 3.

Vertical Hydraulic Conductivity Data Sheets for Saturated HRB Shelby Tube Samples


I ASR 11-332 (711'8) RAYTHEON Engineers & Constructors

Hydraulic Conductivity Test


ASTM D 5084-(Q£) )

l~eriaI Desaiptlon: t U41fr-.c! FINe ~I4N.o Lab No.: II (2.6ft./(!

. OStandard Proctor od of CollJPactlon: . . (ASTM D (98)

Water Conteat:

nModified Proctor W(ASTM D 1557)

iameter:

of Permeant Uquid Used: IilDe-Aired Tap Water

f\fai:nttude of Backpressure (psi): ~o

um:

of Specimen After Completion of Coasolldatlon:

Calculations

MethodsA&:D (M~y

/tZJ.

10

MethodC

kaQUAth k .. (aUAt) In (h1Ih2) k = [(a-In)(a~ut)L I At(a-In + a~ut] In (hllb2)

U~ .. a-In"a I k = (aL I -Ut) In (h1Ih2) I ComctioJi to 20 Degrees C I laO =RTk

~est DeonfOrmlng ONonconfOnn1ng

#-, M&TE: 1tA/.-z4 ~AL DUE DATE: IIIN/A I '111m

",CRI: H. Category: 11/~ Procedure: e -4{JP-/YZ! Rev: 0 PCN's: "'/4 .~~ • 'e4.I~/l'!:.o P6e. PAt2A. €>. '7:>.~.1 Spec's: ,lIn. Rev: 11/4 DCF's=-1'4

~ h. ~'1 -r2 ,..::~. -(-I MT74 DrawIng(s): JIA Rev:tiftr DCF's: A1M

~/(f11J:=-17 ~ bJcol. E.~I/UIt4-77c;.1 •

Iaspector: fft i'~JA1t/ Level: :JP Date: 1/~1t1 (J£~

I

RevIewer: r?" ... .~

JF 3:lff Level: Date: ~

ASR 18.J32 (7198) RAYTHEON Engineers & Constructors

Hydraulic Conductivity Test ASTM D 5084-( 10 )

!RePort No.: qq -171ft, ~/CO ~P::> jProJect/W AD No.: P/J.I2. ~I'&:> pz;5 j'rwC: "'/4 iDate{s) of Test: -z!ocI/n !samPle Identification: 1/12 3-/5C

Material Description: (!.t..fIl/~t/ I/le"p. ~ . ILab No.: !lIZ ~-I"7 C. . Work Package No.:. lJiA j<2cmNO.: "'/4

Selectlo~tion: N/A ~dard Proctor ct!odified Proctor

. 1uu(V6~ny

... or ColJlllaction: . (ASI'M D 698) ASI'M D 1557) [l00er: Ftecv!i4l11PtE.

IiIItial Dimensions of Specimen . /Helgbt:. "1.47&t1 ~iameter:· "1,~eM Ir ~h: 10.1/4 ~tIal Water Content: 1/1,1JR llaltial Dry Unit Weigbt: I lit£> fC(.:"

[]IDe-Alred Tap Water DOOer: - -

~ or Permeaat tiquid Used:

tude of Bac:kpnssure (psi): 0 jRaage of Hydraulic Gradient: '2.4 Fn'ect!ve CoasoHdation Stress um: /. z;;, um: 0

Helgbt of Specimen After Completion of CoasoHdatioa: . '4 ~t~.~ -7,9', 6111 . ;(Q.!t(~~

LeagthofSpedmen: --'1. 41 t!d1 jnaaI Diameter: "1.~~

fiiaal Water Content: . ~t./1 /Fiaal Dry Unit Welgbt: ~.{P Pet="

-- OfSaturatioU:;~ ~-'1:::~ • ,'.t~ _ ~ or;; jAverage Hydraulic Conductivity: /.0'i7'Z X to -<;. (!,IU /1e:; . . Calculations

MethodsA&D ~odB../ MethodC

k=QIJAth k .. (aIJAt) In (hlIh1) k .. [(a-ID)(a~ut)L I At(a-ID + a-outlln (hlIh1)

Ua~ut .. IHn co a / k .. (aL I -2At) In (h1Jh2) I Correction to 20 Degrees C . J k20 .. RTk

~est Deoaformiag DNoacoaforming IXI:;~ M&TE:

ItN .. Ztl CAL DUE DATE: . II/17m

~CRI: ,J1tl- II. ~ry: 44 Procedure: tJ -Ql!,P-oZi Rev: e> PCN's:""~ u

: ~ Ve:t..JEIW ;;P1.. 'M112A. E. ~. ~.r Spec's: IJ.~ Rev: I.J J4 DCF'S:A1i4

1~~1 Yf201'"'- v , *, ])M7/ Drawiag(s): JJ ~ Rev:,J~ DCF's: Nlft ~ltll trl"-{) ~ ~. ~v4Wlfn~

Iaspec:tor: 1.1!.. 1;,JI./ff/ Level: .zrr Date: 'o/?/n ~-

LJ ., -----;--;? RevIewer: II';; Level: ... 'P7=. Date: J;ff. .. 17

./ • "


wsac.m.ooon I ASa 11m (7/98)

RAYTHEON Engineers & Constructors

Hydraulic Conducitlvity Test

1'tlQr- 11 6c;./~

I I I I I I I I I I I I

ASTM D 5084-( qo )

~rt No.: <fl. fAt!J/t)/?~loa:>I /ProJectIW AD No.: PA~ ~(a:>:1:1b trwC: N/A pate<s) of Test: 1/Dzt:r:l /samPle IdeDtlflcatlon: I-l tt ~. its> DL

Description: tutV/!.y FM/e. ~NO ItabNo.: H{2:~-I(PVL jlvork Package No.:. N(14 ~NO.: !JIlt

~pedaI Selectlo~tlon: Al/A

Method of Co!llJlllet1on: . ~dard Proctor

.. ASTMD698) ct!odified ProCtor

ASTMD15S7) It1 ~ l:e:N~{T1

Other: Aet.:O " . ~.c-

1alda1 DimmslODS 01 Specimen . /Height: 'l,M. Of,:. joiameter:' -,. ~ r!H1 jteagtb: 44 ~ Water Content: 11i>~ ~~6 InitlaI Dry Unit Weight: q?,qPCr:

GlDe-Aired Tap Water DOOm - -Type of Penneant Liquid Used:

de or Backpn:ssure (psi): "'/A . jRaage ot HydrauUc Gradleat: "Z-$

Fectlve Coasolidation Stress L 1,'7 L IJ /4 : um:

~eIght at Speclmea Alter Completion ot CoasoUdatlon: ",~g, g16" '%fi/.l-It/f/ft,dgrJJIEIr~ /!JnaI1.eIIgtb ot sPectmeu: lR .Q6 c::!41 \&at Diameter:. '1. ~ CIV/

FInal Water Conteut: . I'z.o'% FInal Dry Unit Weight: I Z <:.,.0 YeP

of SaturatIon: i JZA'r-.f::::: /Average' Hydraulic Condnctivfty: t,/(P XIO-'i(JtJ,{/$GC.

Calculations

MethodsA&D ~~ MethodC

kosQUAtb k os (BUAt) In (b1Ib2) k .. (a-lnl(a~L I At(a.fa + a-out] In (b1Ib2)

Ifa1Ut .. a1n os a I k .. (aL I-%At) In (b1Ib2) I. Conec:tloli to zo Degrees C . I laO" RTk

I II 0 r:;,+'1 M&TE: IvJ- .. "'/ ~arormIDg NoaconCormiDg Wzw A - "P(

AL DUE DATE: 1(/1m

1~~~==~~C~~tq~~~:~N~~~~~~~-~e~.~~~~D~V~~~~~J I ;;.~./

Drawing(s):

I Inspecton : Level: 117 Date: :( '2ft't

IRerie1~-~-:~~~!:i:::zt~~~~~ _______ Levd: ;P?-- Date: .:i' -.?,ff

I

------------------, r-----------------

ASIlIS-332 (7/9B) RA Y'fHEON Engineers & Constructors

Hydraulic Conductivity Test ASTM D S084-( ~ )

Materlal Description: ell4-~if r::ltJe 5t.wo ILab No.: Hf2.5 ~ Z!? -0/

WorkPatkageNo.~ Al/a. /<2cmNO.: AljA ..

Method of ColJZPllction: OStandard Proctor

. (ASTM D 698)

liIitial Dimeaslons of Specimen

Irmtial Water Content: . (iP, qtg===== 11Ini=tIal=Dry=Uni=·t=W=eSg=h=t:=/=tJ="Z=.=~=R.=Z:=F====!1 irype of Penneant IJquid Used: ~De-AIrecI Tap Water OOOer: - .

·tude of Backpressure (psi): 'W 0 ~tft.. -z(i/ti jaange of Hydraulic GradieDt! ~

ElJ'ective ConsoUdatiou Stress L um: I.t? P~I MiDlmwn: r\f 14

~ Leogth of Specimen:

IFinaJ Dry Unit Weight: Cl/."1 PCP

Calc:ulatlons

MethodsA&:D MethodC

t"QUAth k = (BUAI) In (h1Jh2) k = [(a-lD)(a~ut)L f At(a4u + a~utJ In (hllh2)

Jl-m" a-iD .. a k = (aL I -lAt) In (hlIh2) Correction to 20 Degrees C k20 =RTk

'71'-, M&TE: Dc..oformillg ONoucomormillg IXIN/A (W-24

AL DUE DATE: 11/7,

~ry: II Rev: (;> PCN's-J/4 Spec's: 11\4-

Drawing(s): ""fA

~~!1I;.m::::.....-~::;------ Level: :t:tl Date: ?/:ft9 S~Z;..s::~~~~¢.::::.---___ Level:.ilF- Date: .1;1' ff

, , ,

[


I

II

I ASIt 11-332 (7/98) RAYTHEON Engineers & Constructors

Hydraulic Conduc:tivity Test

I I I I I I I I I I I I I I I I

ASTM D 5084-(~ )

jRepol1 No.: CfI- Pfl£ Pta:> "71:5- ti::lJ I /t'roJectlWADNO.: P,4/2. :Ytv~~ /TWC: A~ ~s) of Test: . 'Z/iln jsamPle Idenliflcatlon: rltz"6t? ~-Z7~ &/

~terial Description: t3-tAl/e'l del? ~t<JD ILab No.: f./ IZl9? -'Z7~al

Work Package No.:. "//14 ~NO.: ,JIlt-Selectio~tlon: /Jb4

~dard 1'roetor ct!odified Proctor . fut.d Tl::.N?rrY f\fethod of Co9llJllCClon: . (ASI'M D 698) ASTMDl557) [jJOther: 6/UD ~/I1Pt.6 ~tIaI Dlmens!oas ot Specimen . jnelght: 1.q4~ joiBmeter: 1. !O &11 /Length: AIM Ihltlal Wilta' Content: 10;&% jrmtial Dry Unit Weight: l'¥jq~

l'ype of Permeant Uqufd Used: IIDDe-Aired Tap Water DOther: .

e of Backpressure (psi): t) jRan&e of BydrauIic Gradient: • ~.

~ectIve CoasoUdatlon Stnss l- . um: (.-;; P~f

"'fA , um: ~

~eIght at Spec bnen After Completion of Coasolidatlon: ~~(1. !/i1i.{Zl;;rt 4(c~ ~ Leagth of SpecImen: "1/1~ ~Diameter: ..,-~~

~ Water Conteut: .' ,..,,-7% IFlnaI Dry UnIt Weight: ItJC7 PC~ !' *,...e. f;:.e:/dJl,/U(b

IAverage Hydraulic Conduetlrity: 1.9'51.10-7 eu4j1;fiG. ...., of Saturation: 17 t/~t=. :! 0 /t~

Calculations

MethodsA&D ,..;

(..MCUlodJ!,... MethodC

k"QUAth k .. (aU At) In (blIbl) k .. [(a-ln)(a-ont)L I At(a-in + a-ont] In (hlM)

It a-out .. a-in .. a I k .. (aL f -2At) In (blIbl) I CorreetloJi to 20 Degrees C I k20 .. RTk

DtJEDATE:

Ur'1i n m 'I< I M&TE: L..JConforming ONonCOnfOrming UlNlA I VI! ~ ttl

Procedure: f! - P-#ZI /.I Spee's: . ~.!>_ 3.1

e , ..r I [). TIl Drawing(s):

Inspector:

IReviewer. _...)~~r6j~~_-:::::::=:::;:--______ Level: aT Date:

-::~~~::::2~~~~::::::-'------ Level: .Jf= Date:

I

WSRC-TR-99-OOO57 February 8,1999 I PageA4-1

,

I I I

APPENDIX 4. I Exchangeable Acidity DATA Sheets I

I I I I I I I I I I I I II

-------------------Summary of Data Sheet for Exchangeable Acidity Tests

Vol Vol. O.OlN pH after H201 Boiling Vol. 0.01 N Sample Sample corrected Initial H2S03 addition Added Time NaOH Final

SampleID volume weight for lolids pH (m!) of H2S04 (dro.J)sj (min) (ml) pH HRB-14-C 50 50.1537 49.85 4.42 0.50 3.60 5 4 0.70 8.22 HR3-15C SO 50.019 49.98 6.24 4.00 4.00 55 38 3.80 8.22 HR3-16DL 50 50.2715 49.73 5.89 1.50 3.70 10 11 2.00 8.21 HRB5-25-01 50 50.001 50.00 8.23 8.50 4.01 30 30 5.10 8.21 HRB5-27-01 50 50.3164 49.69 8.56 4.80 4.00 30 30 3.10 8.20 Blank 50 SO 50.00 5.41 0.10 4.01 5 4 0.20 8.2

- - - -

Vol VoL O.OlN pH after H201 Boiling Vol. 0.02 N Sample Sample corrected Initial H2S03 addition Added Time NaOH Final

---~~ -- ~ -----.- .. -- --- --- ------ - --- -- _ .. - - _. - - ------ .--- -HRB-I4-C 50 50.1588 49.84 4.48 0.30 4.00 5 4 1.00 8.22 HR3-15C SO 50.05 49.95 6.46 3.30 4.01 10 13 2.80 8.22 HR3-16DL 50 50.1623 49.84 5.91 1.00 4.00 15 18 1.70 8.21 HRB5-25-01 50 50.0375 49.96 8.24 ·2.00 4.02 5 5 1.90 8.21 HRB5-27-01 SO 50.1228 49.88 8.6 1.75 4.01 10 13 1.40 8.20

Exchangeable Acidity mgIL 90.3 360.1 251.4 170.0 140.9 30.0

Exchangeable Acidity

---170.5 494.5 240.8 180.1 105.3

I ~ ,

i ~ I!lj~ g.~

i .:.; ~~ .90~

> .... ~ ~~111 N\C""-l

APPENDIXS.


PageA5-1

Sodium Concentrations for Cation Exchange Capacity Calculations


- - - - - - - - - - - -Unorrlcal Result. Report By Subml"lon By O~.r.tion

TuesdAY F.bru.ry 09, 1999

- --........ - ..... ~--------- ..... ------_ ...... ---- -- --.- .. -- .. ----- ------ ...... --- ... -_ .. -~. -- .. --- --_ .. ---- .. ------------------

Operat~on: AANA

~- ... ------------------------.------- .. ---------------------------------------------------------------l'IethodlAANA

Ho.,ureIANALYST NAME

Unlt,IPPH

Sub.I"lon_ld I200022330

StatuIICOHPLETE

CondltlonlAPPRDYED ----- .. ---------- .... ,._-- ------------ -- .. -.... -------.. --------------------_ .. ------------... _-Ult'r Sallpte'd Sample Id COMPONENT TeKt V&l~ •

- - -

.. _-----.. ---- ... ---- ---- --~ --- .. --- --, -_ .. -- ------ .. -ISC-A ISC-A ISC-B ISC-B 14C-A 14C-~ I4C-B 14C-B 2S-A 2S-A 25-8 2S-B 27-A 27-A 27-B 27-B I6DL-A 16DL-A 16DL-B 16DL-B BLANK BLANK

30012240~ 30D1224bQ 300122470 300122470 300122471 300122471 300122472 300122472 300122473 300122473 300122474 300122474 300122475 300122475 30012247b J0012247b 300122477 300122477 300122478 30012247B 30012247~ JOOI2247~

----_.' ~ ----------- ------------- -~ ...... ----.. -... ---------- .. _-- ... -... _- ------... -_ ... ----------ANAL.YST NAI'IE HA ANALVST NAME NA ANAL YBT NAME NA ANALVST NAME NA ANALVST NME NA ANALVST NAME NA ANALVST NAHE NA ANALYST NAME HA ANALVST NAHE NA ANAlVST NAME NA ANALVST NAME NA

sec 190.1628 SeG 138.6043 seG 128.0276 seG 131.4818 seG 176.6490 seG 166.3470 seG 135.0168 seG 108.4336 seG 78.1336 seG 46.6014 seG t.~914

- -

~ :il~ crC"l

a~ ~~ .90 0 j> ........

uo lC ... ~:g~

APPENDIX 6.


PageA6-1

Chain of Custody for the HRB Shelby Tube Samples

I I I I I I I I I I

I II

II I Ii I I I I I

0S1l U.B31,.. (Rev 4-2MB) $oM,,, ":1m1.8I Savannah River Technology Center

Analytical Development Section (773-A) Analysis Request

For 24 And 48 Hours Turnaround

Shelby Tubes from old H leler,lion Basin. istirnal'ld rad amounts are in pCi/g.

[g)Red-Radioactive OWhll&-Nonradioactive

C.H.KIST 11'-l6 'Pl-\olJ6 I

LAtdG FOIf:D LA~-rz::,r.

5- '560(.. WSRC-TR-OOOS·

A6-:

16

No

8.

Comments

less than reportable quantities of nuclear mafBrials as Usted In l7.7 1.07

No

DBlue Label OGreen Lebel 0 HP Survey Label I2SIRetumto Customer

EPAISCOHEC Hazardous Wasta

I

MotrtIJ(or. .SoIId SL

SAMPLE 1.0.

CHAIN • OF • CUSTODY (U) W .. 1Inghouoe Savan"oh RI_ Company, Savannah RI_ Slle .. - Rw.O, 12121195 Sample Destination

SAMPLE ANALYsis REQUESTED . i_I iii' ii' I 1 .... 1 PBIII\:J!

~ I .!:'!-en

~ :0 C;

~ Remarks;

F'to..;) \""Vo-I I,JII:d l I I I I I I I I I I I -t-l--I---I-li-i+--+-l-I·-·-·-···--·------·-··-·--··-·--•

.--

-

~rh: Dill.' TIme RlKiat¥ed by: II· IT:m I I .. I I (PrinG 11D.

_ ... (sign, (Sign) (sign, III SMP, n3-62A, Fax 5-5154

5 ~. _ I" ... ,TI..:: .. I_ .......... '--... ___ . III EMS, n3-58A, Fax 5-8041 IilltJ ____ _ III Other .. __ ....... . 1- . I ' , I' L. . I' , +=-:----........ - -.-'-"-'

-------------------~ <;l ;d

~.~

WESTINGHOUSE SAVANNAH RIVER COMPANY SAVANNAH RIVER TECHNOLOGY CENTER

February 11, 1999

To: B. K. Davis, 730-2B cc: B. T. Butcher, 773-43A

W. E. Stevens, 773A W. L. Tamosaitis, 773-A L. Papouchado, 773-A C. G. May, 773-43A L. M. Nelson, 773-43A P. E. Lowe, 773-41A R. F. Blundy, 730-2B L. A. Bagwell, 730-2B D. W. Nix, 730-2B S. A. Kautz, 730-2B W. L. Mhyre, 717-SN M. A. Ditullio, 717-SN

(SJt(4 CoPies) 703-43A) File '(2 copies)

WSRC· TR·99-000S7 February 8, 1999 I


QSR 14·357# (Rev 12-11-96) Swres: 26-1280LOO

Title

Westinghouse Savannah River Company

Document Approval Sheet

Geotechnical Analysis of Five Shelby Tube Samples from H·Area Retention Basin(U) Primary Author/Contact (Must be WSRC) Location Phone No.

C. A. Lan ton 773-43A 5-5806 Organization Code

L3230

Organization (No Abbreviations)

Savannah River Technolo Center

Document No.

WSRC· TR-99-00057

Position

Sr. Fellow Scientist

User 10

T6333

Other Authors

W. l. Mh re

Deadline Date for Approval

Has an invention disclosure been submitted related to this information? DYes 0 No

Disclosure No. (If Known) Title Date Submitted _____ _

Do you intend to submit an invention disclosure? OYes 0 No It yes, projected date ______ _

Information Product Description

[gJ Report Type

OOuarterly 0 Annual OFinal OOther __ _ OSemiannual [gJTechnical OTopical Report Dates _____ thru ____ _

o Published Proceedings o Other _______ _

o Conference Type OAbstract OConfPaper OSlides

OJournal Article (Journal Name) _________ _

o Videotape/Multimedia

ConferenceIMeetlngiPresentation

Meeting Title (No Abbreviations)

Meeting Address (City, State, Country)

Meeting Date(s)

o External Web Page ____ (mldIy) thru ____ (mlrJly)

o Software (Additional forms are required (ESTSC Fl and F2)).

o In Public Literature 0 Routing Concurrently Sponsor

Approved for Release 0 Other . f mation in this material to be given external disbribution, approvals by bolh WSRC and, as appropriate, DOE-SR are required. Distribution

e in accordan fth poli ies set forth in WSRC management requirements and procedures (MRP 3.25) and in DOE·SR orders, and Ihe

";iF'9ffi,::'e:::d:;to ' ! ae!uQJJy approved. - 3-l\-9'1

Date

o Limited Ex ain Below Explanations

I understand and ha onsidered whether any potential intellectual property rights (patents, copyrights, etc., in accordance with MP 1.09 and MAP 1.07) or any contractural barriers (CRADAs, Work for Others, etc.) may be involved before authorizing that this document be proposed for public relea concerns were identified, the. se have been discussed and resolved with General CounseJt ~-#--

evE-Stc-\.>t"5 'L.-L.~ Mana er's Name Print ----.M"a"'n-=ag~e"r"s"'S"';g=na"t"ur"'e-..:---==-

Classification Information (To be Completed by Classification Reviewer) Classification (Check One for Each) Classification Guide Topics

Overali Os Dc OUCNI ~ Abstract 0 sOC 0 UCNI 0 U

Title Os Dc OUCNI Ou WSRC Classification ~cer:~~JI({i\')R WSRC;;~i .

TION ANALVSl iI't:. I

icer's Signature

Ex ort Control Review (To be Completed by Ex ort Control Reviewin Omcial) Export Control Related

DYes ~ e~r's Signature

Use Only UC/C Number

58 NOTE OSR 17-8 must be completed in addition to this form when submitting information for review and approval.

K~'~~~

Westinghouse Savannah River Company

March 18, 1999

Ms, W, F, Perrin, Technical Information Officer U. S. Department of Energy - Savannah River Operations Office

Dear Ms. Perrin:

P.O. Box 616 Aiken, SC 29802

WSRC-TR-99-00057 MSD-STI-97 -4198

REQUEST FOR APPROVAL TO RELEASE SCIENTIFICfTECHNICAL INFORMATION

The attached document is submitted for classification and technical approvals for the purpose of external release. Please complete Part II of this letter and return the letter to the undersigned by 4/30/99. The document has been reviewed for classification and export control by a WSRC Classification staff member and has been determined to be Unclassified.

I. DETAILS OF REQUEST FOR RELEASE

Document Number: WSRC-TR-99-00057

Author's Name: C. A. Langton Location: 773-43A

Department: SRTC

Phone 5-5806

Document Title: Geotechnical Analysis of Five Shelby Tube Samples from H-Area Retention Basin

Presentation/Publication: Meeting/Journal:

Location: (J.d- I / Meeting Date:

II. DOE-SR ACTION

Date Received by TIO 03/19/99

!11 Approved for Release 0 Not Approved o Approved Upon Completion of Changes 0 Revise and Resubmit to DOE-SR o Approved with Remarks

Remarks: ______ ~?-~-------------------------------------------------

W£~~DOE-SR Q$R 25-82-Wit (4-89) Stores; 26-15460.00

~7 f Date

r-----------------------------------------~-- ---- -- - -

US DEPARTMENT OF ENERGY

ANNOUNCEMENT OF U. S. DEPARTMENT OF ENERGY (DOE) SCIENTIFIC AND TECHNICAL INFORMATION (STI)

RECORD STATUS (select one):

DOE F 241.l (7-98) p. 1 of 2 (Furmerly DOE F 1332.15) (All oilier versions are obsolete)

K New Revised Data ievised STI Product . ,. . ...... ..... Part I: STI PROOUCT DESCRIPTION

A. STI PRODUCT TYPE (select one)

K .. 1. Technical Report

OMB Control No. 1910 .. 14()(l

a. Type: o Topical o Semiannual o Annual 181 Final Other (specify) ............................................. , ................

b. Reporting Period Immtdd1tYw. ............................. Ihru . ............................... ..... 2. Conference

a. ProductType: ...... Conference Proceedings ..... Conference Paper or Other (abstracts, excerpts, etc.) -b. Conference Information (title, location, dates)

..... 3. Software Manual ( The actual software package should be made available simultaneously. Follow Instructions provided with ESTSC F 1 and ESTSCF2.)

...... 4. Journal Article

a. Type: L Announcement citation onlv _Preprint _Postprtnt

b. Journal Name . ................................................................................................................................................................................................................... c. Volume d. Issue e. Serial idenUfier (e.g., ISSN or CODEN)

...... 5 . S& T Accomplishment Report

...... 6. Book

...... 7. Patent Application a. Date Filed ImnvUcbYm') -1-1-b. Date Plioliiy (mmtdd'yyyy) _1_1_ c. Patent Assignee

..... 8. ThesisJDlssertation

B. STI PRODUCT TITLE G£lI1.I~.~I:IO.\~iAI.Aoi!.ly.$.ill..I1.f.f.iy.II .. Sb£ltI1.Y . .It.dl.II .. SiilIllPll!.$..fx.QmJ:H .. r.eiil.f.l£lI£lnlil:ln.i:liAaill .... , ............................... C. AUTHOR(s) _ c. •. e. .. _l.ftlllll.QIl ..........................

E-mail Address(es):

D. STI PRODUCT IDENTIFIER

- 1. Report Number(s) . W.Sf.lC.,IIHIf1.,a.Qa.~l .................................

- 2. DOE Contract Number(s) _.Q.I:.,AC.Qf1.,f1.eSR1.as.a~ ...... - 3. R&D Project ID(s)

- 4. Other Identifying Number(s)

E. ORIGINATING RESEARCH ORGANIZATION Savannah River Site

F. DATE OF PUBLICATION (mmldcbYm') ................................... G. LANGUAGE (If non-EngJlsh) English

(Grontees and Awardees: Skip to Descn'ptionlAbstroct section at the end ot Part Q

H. SPONSORING ORGANIZATION

I. PUBLISHER NAME AND LOCATION (If other than research organization)

Availabiliiy Ireter requests to [if applicable])

J. SUBJECT CATEGORIES (fist primary one first) 5.8 ................................. , ....................................................................................................................... Keywords ):b!\r.e.ft.R~t~nli.QIl.i:liilai.O •. G!il.l1~lI.o;;lJ.o.\~iAI.Aoi!lI/§.II1 •. Sl1jI..C.biilr.ft~.I~rj~ftlil1.n ....................................................................................

K. DESCRIPTION/ABSTRACT

Geoteclmical aod geochemical anaillses were pedo[med 00 tille Sbelbll tube samples collected in tbe I:I-A[ea R§tention Basin (HRB) during Jul)1 and August of 1998. The samRles were collected as Rad of the HRB characterization stud~. The test results, which are documented in this rel2ort, will be used to sU(1(1ort the HRB contaminant fate and trans(1ort modelinalanal}'sis and to evaluate remedial Ol2tiOns. The results will also be used as a base line for future treatabili!y studies.

US DEPARTMENT OF ENERGY

ANNOUNCEMENT OF U. S. DEPARTMENT OF ENERGY (DOE) SCIENTIFIC AND TECHNICAL INFORMATION (STI)

Part II: 5TI PRODUCT MEDIA/FORMAT and LOCATIONfTRANSMISSION

A. MEDIAiFORMAT INFORMATION

DOEF2411 (p Zoll}

1. Medium of STI product is: .X .. Paper ...... ' Electronic document _ ..... Computer medium ..... Audiovisual material

2. Size of STI product

3. File format: a. If electronic document is posted at site, indicate: 0 html 0 pdfn 0 sgml 0 xml

b. If electronic document is transmilled to OSTI, indicate: 0 html 0 pdfn 0 pdfi 0 msword

_ TIFFG4 _ WP-indicate Version (5.0 or greater) platform/operating system ____ _ _ MS Word-indicate Version (5.0 or greater) platform/operating system _ Postscript

4. If computer medium or audiovisual material: a. Quantity/type (specifY) _________________________________ _

b. Machine compatibility (specifY) ______ _ c. Sound: _ (yes) d. Color _ (yes) e. Tables/Graphics _ (yes)

f. Other information about product format a user needs to know: _______________________ _

B. LOCATIONfTRANSMI5SION INFORMATION

1. STI Product is available at site: Unique URL (of specific STI Produc~

2. STI Product is being transmitted to OSTI:

a._ Electronically via FTP b._ Via Mail or shipment (e.g., Federal Express) (Paper products, electronic documents on CD-ROM, diskettes, videocassettes, etc.)

3. Infonnation Product Filename (oftransmiffed electronic formaQ ................ , ... , .............................................................................................................. ..

C. ADDITIONAL INFORMATION (concerning media/format or location/transmission; for OSTI intemal use only):

(Grantees and Awardees: Skip to Contact section a/ the end of Part III) Part III: STI PRODUCT REVIEW? RELEASE INFORMATION A. ACCESS LIMITATION .lI...... 1. Unlimited Announcement (available /0 U.S. and non·U.S. public)

2. OpenNet (use OpenNet guidance for be/ow): a. If additional source other than making it available through NTIS:

(1) Accession Number (2) Document Location _____________ _

b. Field Office Acronym _____ _

c. Declassification date (mmiddlyyyy) _/_1 __ d. Declassification Status:

_ Declassified _ Sanitized _ Never classified 3. U.S. Dissemination Only

--------

e. OpenNet Document Type

f. OpenNet Document Keywords

g. OpenNet Addressee

4. Copyrighted material; Are there any restrictions based on copyright? __ yes __ no. If yes, list the restrictions

5. Small Busines. Innovation Research (SB/R) Release date (mm/ddlyyyy) ............................... ..

6. Small Business Technology Transfer (STTR) Release date (mm/dd/yyyy) ............................... ..

7. Proprietaryrrrade Secret

8. Patent Pending 9. Protected data __ CRADA __ Other (specify) Release date (mmiddlyyyy) ................................... .

10. Official Use Only (OUO) 11. Program-Directed Special Handling (specifY) ____________________________ _

12. Export ControtllT ARiEAR

13. Unclassified Controlled Nuclear Information (UCNQ

14. Classified Classification LeveVCateaorv of:

a. This form IJ ...................................................................... .. b. The STI Product .U.n.~laSll.ified ........................................... .. 15. Other information relevant to access (specify; for OSTI intemal use only)}

B. OTHER (infonnation useful to include in published announcement record which is not suited for any other field on this form)

C. CONTACT AND RELEASING OFFICIAL 1.Contact (if appropriate, the organization or site contact to include In published citations who would receive any external questions about the content of the

STI Product or the research Information contained therein) • Name and/or Position K.J. Schmidt, Manager STI Program & SIte Support E·mail Phone (803) 725·2321 Organization Westinghouse Savannah River Company

2. Releasing Official L I veri'):' that all necessary re .... iews have been completed (e.g. Patent, Copyright. ECI. UCNI. etc.) ~::ilSed by (name) K. J. Schmidt Datep~':;:-dWi'YYYl ................................ .

digital.library.unt.edu/67531/metadc708325/m2/1/high_res_d/7554.pdf,.......---------------:-:-~---:---------~--disclaimer...

Documents