· 5/1/2013 · tank closure report starwood capital group former new york united medical center...

TANK CLOSURE REPORT

STARWOOD CAPITAL GROUP

FORMER NEW YORK UNITED MEDICAL CENTER

406 BOSTON POST ROAD

PORT CHESTER, NEW YORK 10573-4703

PBS No.: 3-177865

NYSDEC Spill No’s.: 1213776 and 1213913

MAY 2013

ENVIRO-SCIENCES (OF DELAWARE), INC. 781 Route 15 South, 2

nd Floor

Lake Hopatcong, New Jersey 07849

(973) 398-8183 • (973) 398-8037 – Fax

i ENVIRO-SCIENCES (OF DELAWARE), INC.

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013

Table of Contents

Page No.

1.0 INTRODUCTION........................................................................................................1

1.1 Project Overview ...............................................................................................1

1.2 Project Objectives ..............................................................................................2

1.3 Qualified Environmental Professional ...............................................................2

2.0 PHYSICAL SETTING ................................................................................................2

2.1 Physiography ......................................................................................................2

2.2 Topography and Drainage ..................................................................................3

2.3 Soils ...................................................................................................................3

2.4 Hydrogeology .....................................................................................................4

2.5 Geology ..............................................................................................................4

3.0 TECHNICAL OVERVIEW ........................................................................................4

3.1 Decommissioning Activities ..............................................................................4

3.2 Field Observations and Soil Sample Activities .................................................6

4.0 RESULTS .....................................................................................................................7

5.0 CONCLUSIONS AND RECOMMENDATIONS .....................................................7

ii ENVIRO-SCIENCES (OF DELAWARE), INC.

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013

Table of Contents (continued)

FIGURES

Figure 1 USGS Site Location Map

Figure 2 Site Map

Figure 3 Post-Excavation Soil Sample Locations and Excavation Boundaries Map

TABLES

Table 1 Post-Excavation Soil Sample Summary Report

APPENDICES

Appendix A PBS Construction Work Permit

Appendix B Tank Closure Notification Form

Appendix C December 28, 2012 WCDOH Tank Tightness letter

Appendix D Liquid Disposal Documents

Appendix E Tank Disposal Documents

Appendix F Clean Fill Receipts and Certification

Appendix G Photographs of UST Closure

Appendix H Laboratory Analytical Package

1 ENVIRO-SCIENCES (OF DELAWARE), INC.

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013

1.0 INTRODUCTION

Enviro-Sciences, (of Delaware), Inc. (ESI), on behalf of Starwood Capital Group, (Starwood),

has prepared this Tank Closure Report (CR) for submission to the New York State Department

of Environmental Conservation (NYSDEC) and Westchester County Department of Health

(WCDOH). The subject tanks are registered with WCDOH and No. PBS3-177865 has been

assigned. This report provides the results of tank closure activities conducted at the Site in

conjunction with the removal of two 25,000-gallon underground No. 6 heating oil tanks and one

2,000 gallon above ground diesel fuel oil tank. This document has been formatted in general

accordance with the NYSDEC DER-10 Technical Guidance for Site Investigation and

Remediation dated May 3, 2010, NYSDEC CP-51 Soil Cleanup Guidance dated October 21,

2010, Petroleum Bulk Storage Article XXV of the Westchester County Sanitary Code (adopted

March 18, 2010), other applicable NYSDEC protocols and procedures, and generally accepted

industrial practices. All ESI sampling activities were conducted in accordance with the

NYSDEC CP-51 Soil Cleanup Guidance and DER-10 Technical Guidance for Site Investigation

and Remediation.

1.1 Project Overview

This report summarizes activities associated with the decommissioning, removal, and

post-excavation soil sampling pertaining to the two 25,000-gallon No. 6 fuel oil

underground storage tanks (USTs) and one 2,000-gallon diesel fuel above ground storage

tank (AST) located at 406 Boston Post Road, Port Chester, New York 10573-4703. Prior

to the commencement of on-site activities, a Petroleum Bulk Storage (PBS) Work Permit

was obtained from WCDOH for the removal of the two 25,000-gallon No. 6 fuel oil

USTs and one 2,000-gallon diesel fuel AST. Refer to Appendix A for the PBS

Construction Work Permit.

The two 25,000-gallon USTs were installed in 1965 and were used to store No. 6 heating

oil for the three boilers located in the central heating plant, which is adjacent to the tanks.

The 2,000-gallon AST, located behind the central heating plant, was installed in 1999,


and was used to store diesel fuel for an emergency backup generator. Furthermore, a

Tank Closure Notification was submitted to WCDOH in January 2013 (included as

Appendix B). Based on the failed system tightness test for both 25,000-gallon UST’s,

Spill No’s. 1213776 and 1213913 were assigned, one for each tank. Based on the 2,000-

gallon AST being in good condition with no evidence of a release such as staining, and

having secondary containment in the form of double-walled steel construction, a spill

number was not assigned to this tank. Copies of the failed system tightness test

documented by the WCDOH are included as Appendix C.

1.2 Project Objectives

The specific objectives were to remove the tanks to facilitate compliance with the

NYSCEC and the WCDOH protocols and procedures. The specific tasks associated with

preparing this CR included:

Removal and disposal of residual liquids from within the USTs and AST;

Decommissioning and removing two 25,000-gallon USTs and associated

underground piping;

Decommissioning and removing one 2,000-gallon AST and associated above

ground piping;

Assessing impacts to soils during the removal of the USTs and AST;

Disposal of the USTs and AST to a recycling facility;

Excavation and proper disposal of impacted soil;

Collection of post-excavation soil samples for laboratory analysis; and

The preparation of this CR.

1.3 Qualified Environmental Professionals

Mr. John Gear, a Licensed Site Remediation Professional (LSRP #587819) in the state of

New Jersey has directly over seen personnel working on closure activities. Mr. James

Eicher of ESI, certified in subsurface evaluation and closure of USTs, was the onsite

professional overseeing all UST removal activities.

2.0 PHYSICAL SETTING

2.1 Physiography

The subject property consists of a 15.69-acre parcel of land located at 406 Boston Post

Road, Port Chester, Westchester County, New York. The site formerly operated as a


hospital. The site currently has an operating apartment building and office with a guard

shack. The site was constructed during the 1910s and in several phases, was renovated in

the 1980s and 1990s. Renovations reportedly consisted of general interior upgrades.

Project improvements consist of a 12-story, 132-unit apartment building; a five-story

hospital building with two mechanical penthouse floors and a basement; a six-story office

building (Barron Hall) that is joined to the hospital by a pedestrian walkway; a central

boiler plant; and four ancillary buildings consisting of a former laundry facility, a

carpenter shop, and two small garage structures. Additional Project improvements

consist of surface-level asphalt paved parking/drive areas and landscaping. The parcel is

bordered to the northwest with the existing interstate highway (I-287), northeast of the

site is developed with residential properties and a gasoline station. Southeast of the site,

beyond Boston Post Road, is a shopping center (built between 1950 and 1968) and a

gasoline service station and southwest of the site, beyond High Street, is a nursing home

(constructed in 1971). An excerpt from a United States Geological Survey (USGS)

topographic map showing the property’s location is included as Figure 1, and a Site Map

is included as Figure 2, respectively.

2.2 Topography and Drainage

Review of the Mamaroneck, New York – Connecticut Topographic Quadrangle,

published by the United States Geological Survey (USGS 1994), indicate elevations range

from approximately 100 feet above mean sea level (msl) in the northern and central

portions of the site to approximately 70 feet above msl in the eastern and southern portion

of the site. Slope in the general area of the site is to the east southeast. The nearest

surface water feature, Port Chester Harbor, is located approximately 0.8 mile east-

southeast of the site. Observations made during the on-site assessment did not identify

surface water features or vegetation indicative of wetland areas at the site or adjacent

properties.

2.3 Soils

Review of the Soil Survey of Putnam and Westchester Counties, New York, published

by the United States Department of Agriculture Soil Conservation Service (USDA SCS)

and dated September 1994, indicated the site is located in an area comprised of one soil

type known as Udorthents, smoothed (Ub) with estimated slopes between three and

twenty five percent. The Udorthents soil series is considered to be an excessively-

drained soil with a depth of at least 20 inches. This soil is located in areas that have

been altered by cutting and filling and is mainly in and adjacent to urban areas. The


properties and characteristics of the Udorthents soils are so variable that capability sub-

classifications are not assigned.

2.4 Hydrogeology

Review of the Water Resources Data Report for New York, published by the USGS,

indicated the site is located within the surficial aquifer formation with estimated

groundwater levels between 20 and 30 feet below grade surface (bgs). Shallow

groundwater flow is expected to follow the ground level slope of surface elevations

towards the nearest open body of water or intermittent stream. The direction of this flow

at the site is anticipated to be toward the east-southeast. Estimated groundwater levels

may vary due to seasonal fluctuations in precipitation, local usage demands, geology,

underground structures, or dewatering operations.

2.5 Geology

Review of the Geologic Map of Putnam and Westchester Counties, published by the

USGS, 1994, indicated the site is located within the New England uplands physiographic

province of New York, which consists of glacial till materials which is resting over the

Precambrian Hartland formation consisting of bedrock schist. Depth to bedrock in the

vicinity of the site ranges from zero (rock outcrops) to 30 feet bgs.

3.0 TECHNICAL OVERVIEW

The following section describes the activities conducted as part of the CR. All field activities

complied with the NYSDEC DER-10 Technical Guidance for Site Investigation and Remediation

dated May 3 and Petroleum Bulk Storage Article XXV of the Westchester County Sanitary Code

(adopted March 18, 2010), other applicable NYSDEC protocols, and generally accepted industry

practices.

3.1 Decommissioning Activities

From March 18 through March 27, 2013, the UST decommissioning activities were

conducted by Industrial Environmental Contractors Inc. (IEC) Metuchen, New Jersey,

under direct supervision of ESI personnel. All UST decommissioning activities were

performed in accordance with all applicable federal, state, and local regulations, and

included the following activities:


Acquisition of all necessary local permits for removal of two 25,000-gallon

No. 6 fuel oil USTs and one 2,000-gallon diesel fuel oil AST, and completion

and submittal of the Petroleum Bulk Storage Registration and Tank Closure

Notification;

Mark-out of any subsurface utilities near the UST excavation area;

Drained and flushed all residual product remaining in the associated piping,

back into the tanks;

Opened both man-ways of the 25,000-gallon USTs in order to properly vent

and displace vapors prior to entering tanks;

Access was gained through man-ways located on the top of the USTs. All

remaining residual liquid from within the USTs were removed. A total of

2,000 gallons of oil sludge was vacuumed, hauled, and disposed of at Cycle

Chem Inc., located on 217 South First Street in Elizabeth, New Jersey. The

liquid disposal documentation is included as Appendix D;

The top portion of the 2,000-gallon AST was cut open in order to facilitate the

cleaning activities of the tanks interior;

Excavated, visually inspected, screened, and stock piled soils from above and

around the USTs to expose each tank;

Cleaned the interior of the tanks and then removed the USTs from the

subsurface. Upon removal, the tank was secured adjacent to the excavation,

and the exterior of the UST scraped and cleaned for inspection by WCDOH;

ESI inspected both USTs and AST to document its integrity. Holes were not

identified on the outer shell of either UST or AST;

The exterior of the USTs were coated with a tar-like substance;

Following the tank inspection by WCDOH, the tanks were consolidated,

loaded onto a flatbed, secured, and disposed of at Brookfield Resource

Management in Elmsford, New York. The Tank disposal receipts are

included in Appendix E.


ESI oversaw the removal of the tanks, associated piping, and the excavation of

impacted soils associated with both USTs and AST. All associated piping was

cut off from inside the building and removed from the subsurface;

Approximately four cubic yards of impacted soils is underlain and covered

with plastic sheeting and remains on site for future off-site disposal;

Due to the presence of concrete saddles and a slab beneath the USTs,

collection of post-excavation soil samples were collected from the perimeter

of the subsurface concrete slab as confirmatory samples. Following the

collection of soil confirmation samples, the excavation was backfilled to grade

with the non-impacted stockpiled soils and 294.17 U.S. tons of certified clean

fill supplied by Tilcon Inc. All clean fill brought to the site and used as back

fill material originated from the West Nyack Quarry. Clean fill receipts along

with clean fill certifications are included in Appendix F. Photographs

showing the UST removal activities are included in Appendix G.

3.2 Field Observations and Soil Sampling Activities

From March 18 through 26, 2013, ESI observed and documented the closure of the tanks

and associated piping and removal of both USTs and the AST. On March 26, 2013, ESI

performed the excavation of contaminated soils. On March 25, 26, and 27, 2013, ESI

collected confirmatory post-excavation soil samples. Soils were field screened utilizing a

photoionization detector (PID), visual, and olfactory senses. A small area of impacted

soils was identified near the fill port. Impacted soils were excavated, stock piled on and

covered with plastic sheeting for future off-site disposal. Following the removal of the

tanks and soil excavation activities, confirmatory post excavation soil samples were

collected to document soil conditions. The dimensions of the excavation were

approximately 42 feet in length, 26 feet in width and 13 feet in depth. Impacted soils

were screened with a PID, loaded into a dump truck, staged in a secure holding area, and

covered and underlain with plastic sheeting for proper disposal. 18 post excavation soils

samples were collected: sixteen UST post excavation samples (SW-1 through SW-16)

were collected from 13.0 feet bgs immediately outside the perimeter of the concrete slab

and two pipe run samples (PR-1 and PR-2) were collected from 3.5 feet bgs. All eighteen

samples were analyzed for compounds listed in Table 3, Fuel Oil Contaminated Soil in the

NYSDEC CP-51/Soil Cleanup Guidance document. The excavation was extended to

approximately 15 feet bgs along the east side perimeter of the concrete slab to determine

if groundwater or bedrock was present. Based on observations during closure activities,


groundwater and or bedrock were not encountered during UST removal and post

excavation soil sampling activities. Both USTs were coated with a tar-like substance,

that was applied prior to their installation.

Soil samples were placed directly into laboratory-supplied containers. Once sealed and

labeled, all post-excavation soil sample containers were placed into a sample cooler and

maintained at a temperature of 4 degrees Celsius and transported to Alpha Analytical

Laboratories(Alpha), LLC, Mahwah, New Jersey (NJ Certification No. 14751) for

analysis. The samples were analyzed for compounds listed in Table 3 - Soil Cleanup

Levels for Fuel Oil Contaminated Soil in the NYSDEC CP-51/Soil Cleanup Guidance

document.

4.0 RESULTS

Six of the eighteen soil samples had detections that exceeded NYSDEC Unrestricted Use Soil

Cleanup Objectives (SCO), in 6 NYCRR Part 375-6.8(a). Five of the six sample locations in

which exceedances exist are either beneath or in close proximity to the existing boiler plant

building. The following table summarizes the post excavation soil sampling analytical results

exceeding the NYSDEC Unrestricted Use (SCO):

Contaminants

Unrestricted

Soil Cleanup

Objectives

(mg/kg)

SW-8

(mg/kg)

SW-11

(mg/kg)

SW-12

(mg/kg)

SW-13

(mg/kg)

SW-14

(mg/kg)

PR-1

(mg/kg)

1,2,4-Trimethylbenzene 3.6 ND 0.81 9.4 ND ND ND

Benzene 0.06 ND ND ND ND ND ND

Xylene-Total 0.26 ND ND 5.9 ND ND 0.36 J

Benzo(a)anthracene 1.0 3.8 0.97 ND ND 3.7 0.16 J

Benzo(a)pyrene 1.0 2.9 0.6 ND ND 2.5 0.14 J

Benzo(b)fluoranthene 1.0 3.2 0.66 ND 1.2 3.4 0.17 J

Benzo(k)fluoranthene 0.8 1.8 ND ND ND 1.2 ND

Chrysene 1.0 3.3 1.1 ND ND 3.2 0.19 J

Dibenzo(a,h)anthracene 0.33 0.45 ND ND ND 0.31 ND

Indeno(1,2,3-cd) pyrene 0.5 1.3 0.21 J ND ND 0.95 ND

A summary of all the post-excavation soil sampling results are summarized in Table 1 and Figure

3 depicts all post-excavation soil sampling locations and excavation boundaries. Complete

laboratory analytical packages (on a compact disk) are provided in Appendix H.

5.0 CONCLUSIONS AND RECOMMENDATIONS

Based on an evaluation of the analytical results, the concentrations of impacted soils being within

the same order of magnitude of the NYSDEC SCOs, location of five of the sample locations

being beneath or in close proximity of the existing boiler plant and conversations with the


WCDOH project manager, the following conclusions regarding the conditions encountered at the

site are presented below:

Two, 25,000-gallon No.6 fuel oil UST and associated piping were decommissioned,

removed from the site, and properly disposed.

One 2,000-gallon No. 2 fuel oil AST and associated above ground piping were

decommissioned, removed from the site, and properly disposed.

The results of the CP-51 laboratory analysis for the post excavation soil samples

collected indicate six locations in exceedance of the CP-51 Soil Cleanup Levels.

The low levels of PAHs identified in the post excavation soil samples may be

associated with the tar-like coating that was applied on the exterior of each tank.

1,2,4 trimethylbenzene and total xylene were identified in one sample (SW-12) and

total xylene was identified at an estimated concentration in one sample (PR-1). These

compounds are not typically associated with No. 6 fuel oil.

A small amount of impacted soils was identified near the fill port. Impacted soils will

be disposed of to an off-site facility in the near future.

Based on field observation, the laboratory analytical results, and conversations with the

WCDOH, ESI recommends no further action until the boiler plant building located at 406 Boston

Post Road, Port Chester, New York has been demolished, all debris removed from the area, and

further remediation will be conducted after the building have been removed. The building

demolition is currently planned for May 2014.

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013

ENVIRO-SCIENCES (OF DELAWARE), INC.

FIGURES

SW-8 (9.0') 3/26/2013 Table 3, CP-51Benzo (A) Anthracene 3.8 1.0Benzo (A) Pyrene 2.9 1.0Benzo (B) Fluoranthene 3.2 1.0Benzo (K) Fluoranthene 1.8 0.8Chrysene 3.3 1.0Dibenzo (A,H) Anthracene 0.45 0.33

SW-11 (9.0') 3/26/2013 Table 3, CP-51Chrysene 1.1 1.0

SW-12 (9.0') 3/26/2013 Table 3, CP-51Total Xylenes 5.9 0.261,2,4-Trimethylbenzene 9.4 3.6

SW-13 (9.0') 3/26/2013 Table 3, CP-51Benzo (B) Fluoranthene 1.2 1.0

SW-14 (9.0') 3/26/2013 Table 3, CP-51Benzo (A) Anthracene 3.7 1.0Benzo (A) Pyrene 2.5 1.0Benzo (B) Fluoranthene 3.4 1.0Benzo (K) Fluoranthene 1.2 0.8Chrysene 3.2 1.0Indeno (1,2,3-CD) Pyrene 0.9 0.5

PR-1 (3.5') 3/27/2013 Table 3, CP-51Total Xylenes 0.36 J 0.26

SW-11 (9.0') 3/26/2013 Table 3, CP-51Chrysene 1.1 1.0

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


TABLES

TABLE 1ENVIROSCIENCES (of Delaware), INC.SUMMARY OF POST-EX SOIL SAMPLING RESULTS406 BOSTON POST ROADWESTCHESTER COUNTYPORT CHESTER, NEW YORK 10573-4703PBS No.: 3-177865NYSDEC Spill No’s.: 1213776 and 1213913

NYSDEC

ESI SAMPLE ID UNRESTRICTED SW-1 SW-2 SW-3 SW-4 SW-5 SW-6

SAMPLING DATE USE SOIL 25-MAR-13 25-Mar-13 25-MAR-13 25-MAR-13 25-MAR-13 25-MAR-13

LABORATORY SAMPLE ID CLEANUP L1305016-01 L1305016-02 L1305016-03 L1305016-04 L1305016-05 L1305016-06

SAMPLE DEPTH (feet bgs) OBJECTIVES 13.0 13.0 13.0 13.0 13.0 13.0

Units Qual Qual Qual Qual Qual Qual

General Chemistry

Solids, Total % 81.7 78.6 79.6 82.3 83 73.4

Volatile Organics by 8260/5035

1,2,4-Trimethylbenzene 3.6 mg/kg 0.00072 0.00071 0.00063 0.00068 0.00069 0.00071

1,3,5-Trimethylbenzene 8.4 mg/kg 0.00018 0.00018 0.00016 0.00017 0.00017 0.00018

Benzene 0.06 mg/kg 0.00015 0.00015 0.00013 0.00014 0.00014 0.00015

Ethylbenzene 1.0 mg/kg 0.00018 0.00018 0.00016 0.00018 0.00018 0.00018

Isopropylbenzene NS mg/kg 0.00021 0.00021 0.00018 0.00020 0.00020 0.00021

n-Butylbenzene 12.0 mg/kg 0.00025 0.00025 0.00022 0.00024 0.00024 0.00024

n-Propylbenzene 3.9 mg/kg 0.00016 0.00016 0.00014 0.00015 0.00015 0.00016

Xylene-total 0.26 mg/kg 0.00034 0.00034 0.00030 0.00032 0.00033 0.00034

p-Isopropyltoluene NS mg/kg 0.00024 0.00024 0.00021 0.00023 0.00023 0.00024

sec-Butylbenzene 11.0 mg/kg 0.00026 0.00026 0.00023 0.00024 0.00025 0.00025

tert-Butylbenzene 5.9 mg/kg 0.00070 0.00070 0.00062 0.00067 0.00068 0.00069

Toluene 0.70 mg/kg 0.00014 0.00014 0.00012 0.00013 0.00013 0.00014

Semivolatile Organics by GC/MS

Acenaphthene 20 mg/kg 0.042 0.043 0.043 0.040 0.041 0.046

Acenaphthylene 100 mg/kg 0.038 0.039 0.039 0.037 0.037 0.041

Anthracene 100 mg/kg 0.034 0.035 0.034 0.033 0.033 0.037

Benzo(a)anthracene 1.0 mg/kg 0.23 0.041 0.042 J 0.038 0.039 0.043

Benzo(a)pyrene 1.0 mg/kg 0.25 0.051 0.051 0.048 0.048 0.054

Benzo(b)fluoranthene 1.0 mg/kg 0.30 0.042 0.057 J 0.040 0.040 0.045

Benzo(k)fluoranthene 0.8 mg/kg 0.16 0.040 0.040 0.037 0.038 0.042

Chrysene 1.0 mg/kg 0.21 0.041 0.044 J 0.038 0.039 0.044

Dibenzo(a,h)anthracene 0.33 mg/kg 0.051 J 0.040 0.040 0.038 0.038 0.043

Fluoranthene 100 mg/kg 0.24 0.038 0.071 J 0.036 0.036 0.041

Fluorene 30 mg/kg 0.058 0.060 0.059 0.056 0.057 0.064

Indeno(1,2,3-cd)pyrene 0.5 mg/kg 0.15 J 0.046 0.046 0.044 0.044 0.049

Naphthalene 12 mg/kg 0.067 0.069 0.069 0.065 0.066 0.074

Phenanthrene 100 mg/kg 0.042 J 0.041 0.041 J 0.038 0.039 0.043

Pyrene 100 mg/kg 0.24 0.040 0.064 J 0.038 0.038 0.043

NOTES:

NS - No Standard established.

J - estimated value.

bgs - Below Ground Surface.

mg/kg - miligrams per kilogram

SHADED Value Exceeds Cleanup Objective.

Qual - Qualifier.


NYSDEC

ESI SAMPLE ID UNRESTRICTED

SAMPLING DATE USE SOIL

LABORATORY SAMPLE ID CLEANUP

SAMPLE DEPTH (feet bgs) OBJECTIVES

Units

General Chemistry

Solids, Total %


1,2,4-Trimethylbenzene 3.6 mg/kg


Benzene 0.06 mg/kg

Ethylbenzene 1.0 mg/kg

Isopropylbenzene NS mg/kg

n-Butylbenzene 12.0 mg/kg

n-Propylbenzene 3.9 mg/kg

Xylene-total 0.26 mg/kg

p-Isopropyltoluene NS mg/kg

sec-Butylbenzene 11.0 mg/kg

tert-Butylbenzene 5.9 mg/kg

Toluene 0.70 mg/kg


Acenaphthene 20 mg/kg

Acenaphthylene 100 mg/kg

Anthracene 100 mg/kg

Benzo(a)anthracene 1.0 mg/kg

Benzo(a)pyrene 1.0 mg/kg

Benzo(b)fluoranthene 1.0 mg/kg

Benzo(k)fluoranthene 0.8 mg/kg

Chrysene 1.0 mg/kg

Dibenzo(a,h)anthracene 0.33 mg/kg

Fluoranthene 100 mg/kg

Fluorene 30 mg/kg

Indeno(1,2,3-cd)pyrene 0.5 mg/kg

Naphthalene 12 mg/kg

Phenanthrene 100 mg/kg

Pyrene 100 mg/kg

NOTES:






Qual - Qualifier.

SW-7 SW-8 SW-9 SW-10 SW-11 SW-12

25-MAR-13 26-MAR-13 26-MAR-13 26-MAR-13 26-MAR-13 26-MAR-13

L1305016-07 L1305016-08 L1305016-09 L1305016-10 L1305016-11 L1305016-12

13.0 13.0 13.0 13.0 13.0 13.0

Qual Qual Qual Qual Qual Qual

77.5 81.8 80.1 80.2 87.7 90.7

0.00071 0.00061 0.00083 0.0007 0.81 9.4

0.00018 0.00015 0.00021 0.00018 0.19 J 2.5

0.00015 0.00013 0.00017 0.00014 0.0078 0.0071

0.00018 0.00016 0.00021 0.00018 0.0098 0.85

0.00021 0.00018 0.00024 0.00020 0.011 0.38

0.00024 0.00021 0.00029 0.00024 0.071 1.4

0.00016 0.00013 0.00018 0.00015 0.0084 1.1

0.00034 0.00029 0.00039 0.00033 0.214 J 5.9

0.00024 0.00020 0.00028 0.00023 0.013 0.69

0.00026 0.00022 0.00030 0.00025 0.014 0.75

0.0007 0.0006 0.00081 0.00068 0.037 0.034

0.00014 0.00012 0.00016 0.00014 0.0074 0.60

0.044 0.66 0.084 0.042 0.15 0.074

0.040 0.075 0.076 0.038 0.14 0.067

0.035 2.0 0.068 0.052 J 0.57 0.06

0.041 3.8 0.08 0.17 0.97 0.088

0.052 2.9 0.29 J 0.16 0.60 0.073

0.043 3.2 0.082 0.21 0.66 0.069

0.04 1.8 0.078 0.088 J 0.25 J 0.069

0.042 3.3 0.08 0.15 1.1 0.071

0.041 0.45 0.079 0.04 0.14 0.07

0.039 8.7 0.075 0.32 1.7 0.066

0.061 0.51 0.12 0.059 0.62 J 1.0

0.047 1.3 0.091 0.084 J 0.21 J 0.08

0.070 0.13 0.14 0.068 0.25 1.2

0.041 5.6 0.08 0.13 3.0 0.07

0.041 6.8 0.079 0.30 1.9 0.07


NYSDEC

ESI SAMPLE ID UNRESTRICTED

SAMPLING DATE USE SOIL

LABORATORY SAMPLE ID CLEANUP

SAMPLE DEPTH (feet bgs) OBJECTIVES

Units

General Chemistry

Solids, Total %




Benzene 0.06 mg/kg

Ethylbenzene 1.0 mg/kg

Isopropylbenzene NS mg/kg

n-Butylbenzene 12.0 mg/kg

n-Propylbenzene 3.9 mg/kg

Xylene-total 0.26 mg/kg

p-Isopropyltoluene NS mg/kg

sec-Butylbenzene 11.0 mg/kg

tert-Butylbenzene 5.9 mg/kg

Toluene 0.70 mg/kg


Acenaphthene 20 mg/kg

Acenaphthylene 100 mg/kg

Anthracene 100 mg/kg

Benzo(a)anthracene 1.0 mg/kg

Benzo(a)pyrene 1.0 mg/kg

Benzo(b)fluoranthene 1.0 mg/kg

Benzo(k)fluoranthene 0.8 mg/kg

Chrysene 1.0 mg/kg

Dibenzo(a,h)anthracene 0.33 mg/kg

Fluoranthene 100 mg/kg

Fluorene 30 mg/kg

Indeno(1,2,3-cd)pyrene 0.5 mg/kg

Naphthalene 12 mg/kg

Phenanthrene 100 mg/kg

Pyrene 100 mg/kg

NOTES:






Qual - Qualifier.

SW-13 SW-14 SW-15 SW-16 PR-1 PR-2

26-MAR-13 26-MAR-13 26-MAR-13 26-MAR-13 27-MAR-13 27-MAR-13

L1305016-13 L1305016-14 L1305016-15 L1305016-16 L1305111-01 L1305111-02

13.0 13.0 13.0 13.0 3.5 3.5

Qual Qual Qual Qual Qual Qual

79.1 82.2 79.8 85.9 85.3 85.6

0.00067 0.00068 0.00066 0.00061 0.64 0.00063

0.00017 0.00017 0.00017 0.00015 0.19 J 0.00016

0.00014 0.00014 0.00014 0.00012 0.0087 0.00013

0.00017 0.00018 0.00017 0.00016 0.054 J 0.00016

0.00020 0.00020 0.00019 0.00018 0.012 0.00018

0.00023 0.00024 0.00023 0.00021 0.08 0.00022

0.00015 0.00015 0.00014 0.00013 0.07 J 0.00014

0.00032 0.00032 0.00031 0.00029 0.36 J 0.00030

0.00022 0.00023 0.00022 0.00020 0.085 0.00021

0.00024 0.00024 0.00024 0.00022 0.052 J 0.00023

0.00066 0.00067 0.00065 0.00059 0.041 0.00062

0.00013 0.00013 0.00013 0.00012 0.076 J 0.00012

0.043 0.68 0.042 0.039 0.079 0.039

0.039 0.059 J 0.038 0.035 0.072 0.036

0.035 2.1 0.099 J 0.038 J 0.064 0.032

0.91 3.7 0.38 0.17 0.16 J 0.24

0.87 2.5 0.39 0.16 0.14 J 0.23

1.20 3.4 0.48 0.22 0.17 J 0.30

0.53 1.2 0.20 0.088 J 0.073 0.13

0.94 3.2 0.38 0.17 0.19 J 0.26

0.12 0.31 0.12 0.037 0.074 0.038 J

0.58 7.9 0.72 0.39 0.20 J 0.40

0.06 0.80 0.059 0.054 0.11 0.055

0.40 0.95 0.22 0.10 J 0.085 0.16

0.07 0.066 0.068 0.063 0.31 J 0.063

0.041 5.7 0.29 0.16 0.22 J 0.093 J

0.60 6.4 0.61 0.31 0.075 0.37

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDICES

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX A

Petroleum Bulk Storage Work Permit

WESTCHESTER COUNTY DEPARTMENT OF HEALTH OFFICE OF ENVIRONMENTAL HEALTH RISK CONTROL

145 Huguenot Street, New Rochelle, NY 10801

PETROLEUM BULK STORAGE WORK PERMIT APPLICATION

PBS No. 3- Date

FACILITY Name

TYPE OF WORK TANK ID(s) FEE (ea.) TOTAL

Address

Remove tank

200

City/Town/Village

Zip

Close tank in place

200

Contact Person

Telephone

Repair tank

145

CONTRACTOR Name

Recondition tank (relining)

145

Address

Repair/replace piping

100

City

State

Zip

Install aboveground tank Quantity: 145

Contact Person

Telephone

Install underground tank Quantity: 145

INSTRUCTIONS • Identify existing tanks by PBS ID numbers as they appear on the

PBS registration certificate. • Indicate the contractor that will be responsible for writing the report

required by the Department. The contractor must be familiar with PBS and environmental regulations.

• Proof of worker’s compensation and disability insurance or proof of exemption must be submitted with the application.

Install piping system Quantity: 100

Install non-stationary tank storage area Quantity: 145

TOTAL FEE

DO NOT BEGIN WORK UNTIL A VALID PERMIT HAS BEEN OBTAINED

03/11

JMaguire

Typewritten Text

Port Chester

JMaguire

Typewritten Text

10573

JMaguire

Typewritten Text

Jim Maguire

JMaguire

Typewritten Text

973-398-8183

JMaguire

Typewritten Text

Industrial Environmental Contracting, Inc.

JMaguire

Typewritten Text

50 Hampton Street

JMaguire

Typewritten Text

Metuchen

JMaguire

Typewritten Text

NJ

JMaguire

Typewritten Text

08840

JMaguire

Typewritten Text

David Oliver

JMaguire

Typewritten Text

732-662-7222

JMaguire

Typewritten Text

X

JMaguire

Typewritten Text

001

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

002

JMaguire

Typewritten Text

003

JMaguire

Typewritten Text

$600

JMaguire

Typewritten Text

$600

JMaguire

Typewritten Text

177865

JMaguire

Typewritten Text

2/6/2013

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

(Former) NewYork United Hospital

JMaguire

Typewritten Text

Medical Center

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

406 Boston Post Road

JMaguire

Typewritten Text

GENERAL INSTRUCTIONS. The Work Permit Application may be completed and submitted by the facility’s contractor or by facility personnel. Mail the completed application together with proof of Worker’s Compensation and Disability Insurance (forms DB120.1 and C105.2) and the appropriate fee to: Westchester County Department of Health, 7th Floor - Petroleum Bulk Storage Section, 145 Huguenot Street, New Rochelle, NY 10801. Work permits are valid for 90 days from the issue date. Work must be completed by the Expiration Date listed on the permit. If work has not been completed, a new permit must be obtained. A new Work Permit Application must be filed to change or modify the Work Permit. Work permits are required for the following types of work: Work permits are not required for the following types of work:

• Tank installation • Tank closure • Tank re-lining • Installation of non-stationary tank storage area • Piping repair • Piping installation or replacement

• Dispenser installation/replacement • Cathodic protection system installation or repair • Leak detection system installation or repair • Overfill prevention installation or repair • Bringing interstitial port to grade • Catch basin installation • Fill and vent replacement • Product substitution (a site assessment may be required, contact the Department) • Stage I/Stage II vapor recovery system installation or repair

Facility Information. Enter the name of the facility exactly as it appears on the Petroleum Bulk Storage Registration Certificate. Also enter the facility’s PBS Number and the date in the labeled boxes at the upper right of the form. Contractor Information. Enter the name of the contractor and their valid mailing address; including a contact person and their phone number. The contractor will be responsible for writing the tank closure reports and/or the tank/piping installation reports that are required by this Department. The contractor must be familiar with PBS and environmental regulations and must supply proof of Worker’s Compensation and Disability Insurance. Type of Work. Select the work to be performed at the site. If there is more than one type of work to be performed you may select as many different types of work as necessary on the same application form. Tank ID(s). Enter the identification number of each tank as it appears on the facility’s PBS registration certificate. There is space to enter up to four tank ID numbers on each line in the form. If you require more space for tank ID entries, please use additional forms and fasten them together. In the case of new installations, enter the quantity of tanks, piping systems, or non-stationary tank storage areas to be installed. Fee. The fees are assessed per tank, piping system or non-stationary tank storage area. Total Fee. Enter the total amount of fees for each line of the Type of Work performed, then add each line and enter the Total Fee in the box at the bottom of the column. Submit a check or money order payable to the Westchester County Department of Health. The Department will not accept cash or credit card payments. No refunds will be made for work not performed. If a new tank is being installed at a facility that holds a valid PBS registration, no additional registration fee for that tank is required.

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX B

Tank Closure Notification Form

Office of Environmental Health Risk Control telephone: (914) 813-5161

145 Huguenot Street, 8th Floor fax: (914) 813-4288

New Rochelle, NY 10801 02/12 www.westchestergov.com/health

WESTCHESTER COUNTY DEPARTMENT OF HEALTH PETROLEUM BULK STORAGE

TANK CLOSURE NOTIFICATION Notify the Department at least 48 hours prior to the requested inspection time.

To: Westchester County Department of Health Date: From: Telephone:

FACILITY CONTRACTOR PBS No. Company

Site Name Contact

Address Telephone

City Closure Date

Requested Inspection Time

TANK INFORMATION

Tank ID Capacity Product Stored Type

Removal Closure in place










JMaguire

Typewritten Text

Enviro-Sciences(of Delaware),Inc.

JMaguire

Typewritten Text

973-398-8183

JMaguire

Typewritten Text

3-177865

JMaguire

Typewritten Text

(Former)NewYorkUnitedHosp.MedCenter

JMaguire

Typewritten Text

406 Boston Post Road

JMaguire

Typewritten Text

Port Chester, NY

JMaguire

Typewritten Text

IndustrialEnvironmentalContracting

JMaguire

Typewritten Text

David Oliver

JMaguire

Typewritten Text

732-662-7222

JMaguire

Typewritten Text

001

JMaguire

Typewritten Text

25,000 gallon

JMaguire

Typewritten Text

#6 Heating Oil

JMaguire

Typewritten Text

X

JMaguire

Typewritten Text

002

JMaguire

Typewritten Text

25,000 gallon

JMaguire

Typewritten Text

#6 Heating Oil

JMaguire

Typewritten Text

X

JMaguire

Typewritten Text

003

JMaguire

Typewritten Text

2,000 gallon

JMaguire

Typewritten Text

#2 Heating Oil

JMaguire

Typewritten Text

X

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

JMaguire

Typewritten Text

UST

JMaguire

Typewritten Text

UST

JMaguire

Typewritten Text

AST

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX C

December 28, 2012 WCDOH Tank Tightness Letter

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX D

Liquid Disposal Documents

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX E

Tank Disposal Documents

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX F

Clean Fill Receipts and Certification

TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX G

Photographs of UST Closure

STARWOOD CAPITAL GROUP FORMER NEW YORK UNITED MEDICAL CENTER

406 BOSTON POST ROAD PORT CHESTER, NEW YORK 10573-4703

USTs & AST REMOVAL ACTIVITIES PBS No.: 3-177865



Photograph 2: Photograph 1:



TANK CLOSURE REPORT





PBS No.: 3-177865


MAY 2013


APPENDIX H

Laboratory Analytical Package

L1305016

Enviro-Sciences

STARWOOD CAPITAL

STARWOOD CAPITAL

Client:

Project Name:

Project Number:

04/01/13

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

781 Route 15 S.

2nd Floor

Jim MaguireATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086),PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers.

Lake Hopatcong, NJ 07849

(973) 398-8183Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:04011314:42

Page 1 of 90

L1305016-01

L1305016-02

L1305016-03

L1305016-04

L1305016-05

L1305016-06

L1305016-07

L1305016-08

L1305016-09

L1305016-10

L1305016-11

L1305016-12

L1305016-13

L1305016-14

L1305016-15

L1305016-16

Alpha Sample ID

SW-1

SW-2

SW-3

SW-4

SW-5

SW-6

SW-7

SW-8

SW-9

SW-10

SW-11

SW-12

SW-13

SW-14

SW-15

SW-16

Client ID

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

PORT CHESTER, NY

Sample Location

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:Project Number:

Lab Number: Report Date:

L130501604/01/13

03/25/13 09:20

03/25/13 09:50

03/25/13 10:05

03/25/13 10:25

03/25/13 10:45

03/25/13 11:10

03/25/13 11:40

03/26/13 11:07

03/26/13 10:52

03/26/13 10:40

03/26/13 10:28

03/26/13 10:16

03/26/13 10:03

03/26/13 09:56

03/26/13 09:40

03/26/13 09:31

Collection Date/Time

Serial_No:04011314:42

Page 2 of 90

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:

Project Number:

Lab Number:

Report Date:L1305016

04/01/13

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of

NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample

specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,

followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a

required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is

designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the

associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %

recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods

allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not

narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool

where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight

basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the

back of the report.

In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some

quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the

associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed

along with any associated usability implications.

Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical

Standards requested on the Chain of Custody.

HOLD POLICY

For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30

days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and

made arrangements for Alpha to continue to hold the samples.

Please contact Client Services at 800-624-9220 with any questions.

Serial_No:04011314:42

Page 3 of 90

Case Narrative (continued)

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:

Project Number:

Lab Number:


04/01/13

Report Submission

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

Semivolatile Organics

L1305016-09 and -12 have elevated detection limits due to the dilutions required by matrix interferences

encountered during the concentration of the samples.

L1305016-11 has elevated detection limits due to the dilution required by the matrix interferences encountered

during the concentration of the sample and the analytical dilution required by the sample matrix.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 04/01/13

Serial_No:04011314:42

Page 4 of 90

ORGANICS

Serial_No:04011314:42

Page 5 of 90

VOLATILES

Serial_No:04011314:42

Page 6 of 90

FF

Benzene

Toluene

Ethylbenzene

Methyl tert butyl ether

p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene

1,3,5-Trimethylbenzene


Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by 8260/5035 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.9

1.2

2.5

2.5

2.5

1.2

1.2

6.2

1.2

1.2

1.2

6.2

6.2

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

102

97

99

100

70-130

70-130

70-130

70-130

Acceptance CriteriaSurrogate % Recovery Qualifier

04/01/13

SW-1Client ID:03/25/13 09:20Date Collected:03/26/13Date Received:

PORT CHESTER, NYSample Location:

L1305016-01Lab ID:

Field Prep: Not SpecifiedMatrix: SoilAnalytical Method:Analytical Date:Analyst:

1,8260C03/27/13 14:43BN 82%Percent Solids:

MDL

0.15

0.14

0.18

0.13

0.40

0.34

0.25

0.26

0.70

0.21

0.24

0.16

0.18

0.72

Serial_No:04011314:42

Page 7 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.9

1.2

2.5

2.5

2.5

1.2

1.2

6.2

1.2

1.2

1.2

6.2

6.2


Toluene-d8



100

96

99

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-02Lab ID:



MDL

0.15

0.14

0.18

0.13

0.40

0.34

0.25

0.26

0.70

0.21

0.24

0.16

0.18

0.71

Serial_No:04011314:42

Page 8 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.1

1.6

1.1

2.2

2.2

2.2

1.1

1.1

5.5

1.1

1.1

1.1

5.5

5.5


Toluene-d8



102

97

99

101

70-130

70-130

70-130

70-130


04/01/13



L1305016-03Lab ID:



MDL

0.13

0.12

0.16

0.11

0.36

0.30

0.22

0.23

0.62

0.18

0.21

0.14

0.16

0.63

Serial_No:04011314:42

Page 9 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.4

2.4

2.4

1.2

1.2

6.0

1.2

1.2

1.2

6.0

6.0


Toluene-d8



99

96

97

99

70-130

70-130

70-130

70-130


04/01/13



L1305016-04Lab ID:



MDL

0.14

0.13

0.18

0.12

0.38

0.32

0.24

0.24

0.67

0.20

0.23

0.15

0.17

0.68

Serial_No:04011314:42

Page 10 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.4

2.4

2.4

1.2

1.2

6.0

1.2

1.2

1.2

6.0

6.0


Toluene-d8



107

98

105

103

70-130

70-130

70-130

70-130


04/01/13



L1305016-05Lab ID:


1,8260C03/28/13 02:45JC 83%Percent Solids:

MDL

0.14

0.13

0.18

0.12

0.39

0.33

0.24

0.25

0.68

0.20

0.23

0.15

0.17

0.69

Serial_No:04011314:42

Page 11 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.5

2.5

2.5

1.2

1.2

6.2

1.2

1.2

1.2

6.2

6.2


Toluene-d8



108

99

103

103

70-130

70-130

70-130

70-130


04/01/13



L1305016-06Lab ID:



MDL

0.15

0.14

0.18

0.13

0.40

0.34

0.24

0.25

0.69

0.21

0.24

0.16

0.18

0.71

Serial_No:04011314:42

Page 12 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.9

1.2

2.5

2.5

2.5

1.2

1.2

6.2

1.2

1.2

1.2

6.2

6.2


Toluene-d8



99

98

100

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-07Lab ID:



MDL

0.15

0.14

0.18

0.13

0.40

0.34

0.24

0.26

0.70

0.21

0.24

0.16

0.18

0.71

Serial_No:04011314:42

Page 13 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.1

1.6

1.1

2.1

2.1

2.1

1.1

1.1

5.4

1.1

1.1

1.1

5.4

5.4


Toluene-d8



101

97

99

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-08Lab ID:



MDL

0.13

0.12

0.16

0.11

0.34

0.29

0.21

0.22

0.60

0.18

0.20

0.13

0.15

0.61

Serial_No:04011314:42

Page 14 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.4

2.2

1.4

2.9

2.9

2.9

1.4

1.4

7.2

1.4

1.4

1.4

7.2

7.2


Toluene-d8



101

97

100

99

70-130

70-130

70-130

70-130


04/01/13



L1305016-09Lab ID:



MDL

0.17

0.16

0.21

0.15

0.47

0.39

0.29

0.30

0.81

0.24

0.28

0.18

0.21

0.83

Serial_No:04011314:42

Page 15 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.4

2.4

2.4

1.2

1.2

6.1

1.2

1.2

1.2

6.1

6.1


Toluene-d8



102

97

99

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-10Lab ID:



MDL

0.14

0.14

0.18

0.13

0.39

0.33

0.24

0.25

0.68

0.20

0.23

0.15

0.18

0.70

Serial_No:04011314:42

Page 16 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

150

64

71

ND

ND

ND

ND

ND

190

810

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

66

100

66

130

130

130

66

66

330

66

66

66

330

330


Toluene-d8



105

97

105

97

70-130

70-130

70-130

70-130


04/01/13



L1305016-11Lab ID:



MDL

7.8

7.4

9.8

6.9

21.

18.

13.

14.

37.

11.

13.

8.4

9.5

38.

Serial_No:04011314:42

Page 17 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

600

850

ND

3900

2000

1400

750

ND

380

690

1100

2500

9400

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

60

90

60

120

120

120

60

60

300

60

60

60

300

300


Toluene-d8



100

99

108

95

70-130

70-130

70-130

70-130


04/01/13



L1305016-12Lab ID:



MDL

7.1

6.7

8.9

6.3

19.

16.

12.

12.

34.

10.

12.

7.6

8.6

34.

Serial_No:04011314:42

Page 18 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.3

2.3

2.3

1.2

1.2

5.8

1.2

1.2

1.2

5.8

5.8


Toluene-d8



100

97

102

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-13Lab ID:



MDL

0.14

0.13

0.17

0.12

0.38

0.32

0.23

0.24

0.66

0.20

0.22

0.15

0.17

0.67

Serial_No:04011314:42

Page 19 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.8

1.2

2.4

2.4

2.4

1.2

1.2

6.0

1.2

1.2

1.2

6.0

6.0


Toluene-d8



100

96

99

99

70-130

70-130

70-130

70-130


04/01/13



L1305016-14Lab ID:



MDL

0.14

0.13

0.18

0.12

0.38

0.32

0.24

0.24

0.67

0.20

0.23

0.15

0.17

0.68

Serial_No:04011314:42

Page 20 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.2

1.7

1.2

2.3

2.3

2.3

1.2

1.2

5.8

1.2

1.2

1.2

5.8

5.8


Toluene-d8



100

97

100

99

70-130

70-130

70-130

70-130


04/01/13



L1305016-15Lab ID:



MDL

0.14

0.13

0.17

0.12

0.37

0.31

0.23

0.24

0.65

0.19

0.22

0.14

0.17

0.66

Serial_No:04011314:42

Page 21 of 90

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

1.0

1.6

1.0

2.1

2.1

2.1

1.0

1.0

5.3

1.0

1.0

1.0

5.3

5.3


Toluene-d8



100

98

99

100

70-130

70-130

70-130

70-130


04/01/13



L1305016-16Lab ID:



MDL

0.12

0.12

0.16

0.11

0.34

0.29

0.21

0.22

0.59

0.18

0.20

0.13

0.15

0.61

Serial_No:04011314:42

Page 22 of 90

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

03/27/13 11:311,8260CAnalytical Method:

Analytical Date:

04/01/13

Analyst: BN

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

ND

0.36

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.0

1.5

1.0

2.0

2.0

2.0

1.0

1.0

5.0

1.0

1.0

1.0

5.0

5.0

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 01-04,07-10,13-16 Batch: WG597887-3


Toluene-d8



99

96

99

98

70-130

70-130

70-130

70-130

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

0.12

0.11

0.15

0.10

0.32

0.27

0.20

0.20

0.56

0.17

0.19

0.12

0.14

0.57

Serial_No:04011314:42

Page 23 of 90


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016


Analytical Date:

04/01/13

Analyst: JC

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.0

1.5

1.0

2.0

2.0

2.0

1.0

1.0

5.0

1.0

1.0

1.0

5.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 05-06 Batch: WG597968-3


Toluene-d8



109

99

106

102

70-130

70-130

70-130

70-130


Criteria

MDL

0.12

0.11

0.15

0.10

0.32

0.27

0.20

0.20

0.56

0.17

0.19

0.12

0.14

0.57

Serial_No:04011314:42

Page 24 of 90


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016


Analytical Date:

04/01/13

Analyst: JC

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

50

75

50

100

100

100

50

50

250

50

50

50

250

250

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 11-12 Batch: WG597969-3


Toluene-d8



109

99

106

102

70-130

70-130

70-130

70-130


Criteria

MDL

5.9

5.6

7.4

5.2

16.

14.

9.9

10.

28.

8.4

9.6

6.3

7.2

29.

Serial_No:04011314:42

Page 25 of 90

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

2-Chloroethylvinyl ether

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane


Bromodichloromethane

trans-1,3-Dichloropropene

cis-1,3-Dichloropropene

1,1-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

104

107

104

102

103

100

103

102

102

101

101

104

105

104

100

103

104

98

98

106

96

98

99

97

93

98

92

100

93

92

92

91

98

96

97

92

98

95

91

90

97

87

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

6

8

7

9

5

8

3

9

10

9

10

6

9

7

8

5

9

7

9

9

10

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Volatile Organics by 8260/5035 - Westborough Lab Associated sample(s): 01-04,07-10,13-16 Batch: WG597887-1 WG597887-2

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 26 of 90

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene

trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene

cis-1,2-Dichloroethene

Dibromomethane

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

101

122

111

115

115

107

108

105

100

100

100

103

102

102

106

104

102

106

130

110

106

91

111

104

104

106

98

99

96

91

92

91

96

92

93

99

98

94

95

133

100

104

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

10

9

7

10

8

9

9

9

9

8

9

7

10

9

7

6

8

11

2

10

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 27 of 90

Vinyl acetate

4-Methyl-2-pentanone

1,2,3-Trichloropropane

2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

104

102

98

103

106

106

100

99

100

99

100

99

100

100

100

87

96

101

100

96

106

98

97

90

98

99

95

93

92

93

93

89

89

90

90

92

97

87

91

90

89

100

70-130

70-130

68-130

70-130

70-130

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

6

5

9

5

7

11

7

7

7

6

12

11

11

11

8

11

10

10

11

8

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 28 of 90

Isopropyl Ether

tert-Butyl Alcohol

n-Propylbenzene

1,2,3-Trichlorobenzene




Methyl Acetate

Ethyl Acetate

Acrolein

Cyclohexane

1,4-Dioxane

1,1,2-Trichloro-1,2,2-Trifluoroethane

1,4-Diethylbenzene

4-Ethyltoluene

1,2,4,5-Tetramethylbenzene

Tetrahydrofuran

Ethyl ether

trans-1,4-Dichloro-2-butene

Methyl cyclohexane

Ethyl-Tert-Butyl-Ether

105

89

99

98

100

101

100

104

106

80

95

104

94

106

105

104

100

104

98

92

103

98

88

90

90

91

91

90

99

102

78

86

104

85

97

97

97

95

97

91

82

97

66-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

70-130

70-130

70-130

66-130

67-130

70-130

70-130

70-130

7

1

10

9

9

10

11

5

4

3

10

0

10

9

8

7

5

7

7

11

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 29 of 90

Tertiary-Amyl Methyl Ether

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane




Tetrachloroethene

102

99

103

106

100

109

97

109

106

97

97

96

102

106

99

108

95

108

105

94

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

5

3

1

0

1

1

2

1

1

3

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery



Volatile Organics by 8260/5035 - Westborough Lab Associated sample(s): 05-06 Batch: WG597968-1 WG597968-2


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016


Toluene-d8



97

98

100

100

70-130

70-130

70-130

70-130

98

96

99

100

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

04/01/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04011314:42

Page 30 of 90

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

99

87

108

103

109

102

109

103

92

102

103

100

102

89

100

84

88

88

94

106

96

98

81

107

101

108

103

106

102

91

102

100

99

101

82

94

78

81

85

92

103

94

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

1

7

1

2

1

1

3

1

1

0

3

1

1

8

6

7

8

3

2

3

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 31 of 90

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


98

97

96

100

100

100

109

101

88

133

77

132

106

99

106

108

102

105

96

102

98

95

94

96

98

97

99

108

99

83

115

75

120

106

100

105

102

101

103

95

101

97

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

70-130

70-130

69-130

70-130

3

3

0

2

3

1

1

2

6

15

3

10

0

1

1

6

1

2

1

1

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual

Q

Qual

Serial_No:04011314:42

Page 32 of 90

Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Isopropyl Ether

tert-Butyl Alcohol

n-Propylbenzene





Methyl Acetate

Ethyl Acetate

93

108

103

99

103

104

97

102

98

100

92

109

109

114

104

96

96

102

101

107

106

92

106

100

97

97

102

95

101

96

97

92

108

107

113

100

95

95

100

99

105

110

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

1

2

3

2

6

2

2

1

2

3

0

1

2

1

4

1

1

2

2

2

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 33 of 90

Acrolein

Cyclohexane

1,4-Dioxane


1,4-Diethylbenzene

4-Ethyltoluene


Tetrahydrofuran

Ethyl ether


Methyl cyclohexane



106

103

102

98

102

101

98

106

91

113

104

104

100

109

100

98

93

99

99

97

105

86

115

102

103

101

70-130

70-130

65-136

70-130

70-130

70-130

70-130

66-130

67-130

70-130

70-130

70-130

70-130

3

3

4

5

3

2

1

1

6

2

2

1

1

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016


Toluene-d8



106

98

102

101

70-130

70-130

70-130

70-130

106

99

104

101


04/01/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04011314:42

Page 34 of 90

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane




Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

99

103

106

100

109

97

109

106

97

99

87

108

103

109

102

109

103

92

102

103

100

96

102

106

99

108

95

108

105

94

98

81

107

101

108

103

106

102

91

102

100

99

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

3

1

0

1

1

2

1

1

3

1

7

1

2

1

1

3

1

1

0

3

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 35 of 90

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

102

89

100

84

88

88

94

106

96

98

97

96

100

100

100

109

101

88

133

77

132

101

82

94

78

81

85

92

103

94

95

94

96

98

97

99

108

99

83

115

75

120

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

1

8

6

7

8

3

2

3

2

3

3

0

2

3

1

1

2

6

15

3

10

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual

Q

Qual

Serial_No:04011314:42

Page 36 of 90

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

106

99

106

108

102

105

96

102

98

93

108

103

99

103

104

97

102

98

100

92

109

106

100

105

102

101

103

95

101

97

92

106

100

97

97

102

95

101

96

97

92

108

70-130

70-130

68-130

70-130

70-130

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

0

1

1

6

1

2

1

1

1

1

2

3

2

6

2

2

1

2

3

0

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 37 of 90

Isopropyl Ether

tert-Butyl Alcohol

n-Propylbenzene





Methyl Acetate

Ethyl Acetate

Acrolein

Cyclohexane

1,4-Dioxane


1,4-Diethylbenzene

4-Ethyltoluene


Tetrahydrofuran

Ethyl ether


Methyl cyclohexane


109

114

104

96

96

102

101

107

106

106

103

102

98

102

101

98

106

91

113

104

104

107

113

100

95

95

100

99

105

110

109

100

98

93

99

99

97

105

86

115

102

103

66-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

70-130

70-130

70-130

66-130

67-130

70-130

70-130

70-130

2

1

4

1

1

2

2

2

4

3

3

4

5

3

2

1

1

6

2

2

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 38 of 90

Tertiary-Amyl Methyl Ether 100 101 70-130 1 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016


Toluene-d8



106

98

102

100

70-130

70-130

70-130

70-130

106

99

104

101


04/01/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04011314:42

Page 39 of 90

SEMIVOLATILES

Serial_No:04011314:42

Page 40 of 90

FF

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Parameter Result

J

J

J

J

Dilution Factor

ND

240

ND

230

250

300

160

210

ND

ND

150

ND

42

51

150

240

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

72

76

82

23-120

30-120

18-120


04/01/13



L1305016-01Lab ID:

Field Prep: Not SpecifiedMatrix: Soil Extraction Method:Analytical Method:Analytical Date:Analyst:

1,8270D03/28/13 20:25JB

EPA 3546Extraction Date: 03/27/13 08:14

82%Percent Solids:

MDL

42.

37.

67.

40.

49.

41.

38.

40.

38.

34.

42.

58.

40.

39.

45.

39.

Serial_No:04011314:42

Page 41 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

170

120

210

120

170

120

120

120

170

120

170

210

120

120

170

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

67

68

80

23-120

30-120

18-120


04/01/13



L1305016-02Lab ID:


1,8270D03/28/13 20:49JB


79%Percent Solids:

MDL

43.

38.

69.

41.

51.

42.

40.

41.

39.

35.

43.

60.

41.

40.

46.

40.

Serial_No:04011314:42

Page 42 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

J

J

J

J

Dilution Factor

ND

71

ND

42

ND

57

ND

44

ND

ND

ND

ND

41

ND

ND

64

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

210

120

160

120

120

120

160

120

160

210

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

66

67

74

23-120

30-120

18-120


04/01/13



L1305016-03Lab ID:


1,8270D03/28/13 21:12JB


80%Percent Solids:

MDL

43.

38.

69.

41.

51.

42.

40.

41.

39.

34.

43.

59.

40.

40.

46.

40.

Serial_No:04011314:42

Page 43 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

75

77

86

23-120

30-120

18-120


04/01/13



L1305016-04Lab ID:


1,8270D03/28/13 21:36JB


82%Percent Solids:

MDL

40.

36.

65.

38.

48.

40.

37.

38.

37.

33.

41.

56.

38.

38.

44.

38.

Serial_No:04011314:42

Page 44 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

74

76

80

23-120

30-120

18-120


04/01/13



L1305016-05Lab ID:


1,8270D03/28/13 21:59JB


83%Percent Solids:

MDL

41.

36.

66.

39.

48.

40.

38.

39.

37.

33.

41.

57.

39.

38.

44.

38.

Serial_No:04011314:42

Page 45 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

180

130

220

130

180

130

130

130

180

130

180

220

130

130

180

130

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

84

89

78

23-120

30-120

18-120


04/01/13



L1305016-06Lab ID:


1,8270D03/28/13 22:23JB


73%Percent Solids:

MDL

46.

41.

74.

43.

54.

45.

42.

44.

41.

37.

46.

64.

43.

43.

49.

43.

Serial_No:04011314:42

Page 46 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

170

130

210

130

170

130

130

130

170

130

170

210

130

130

170

130

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

61

65

67

23-120

30-120

18-120


04/01/13



L1305016-07Lab ID:


1,8270D03/28/13 22:46JB


78%Percent Solids:

MDL

44.

39.

70.

41.

52.

43.

40.

42.

40.

35.

44.

61.

41.

41.

47.

41.

Serial_No:04011314:42

Page 47 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


660

8700

ND

3800

2900

3200

1800

3300

ND

2000

1200

510

5600

450

1300

6800

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

320

240

400

240

320

240

240

240

320

240

320

400

240

240

320

240

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

67

78

78

23-120

30-120

18-120


04/01/13



L1305016-08Lab ID:

Field Prep: Not Specified

D

Matrix: Soil Extraction Method:Analytical Method:Analytical Date:Analyst:

1,8270D03/29/13 16:26JB


82%Percent Solids:

MDL

83.

74.

130

79.

98.

81.

77.

79.

75.

67.

84.

120

79.

78.

89.

78.

Serial_No:04011314:42

Page 48 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

290

ND

ND

ND

ND

ND

320

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

330

240

410

240

330

240

240

240

330

240

330

410

240

240

330

240

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

71

76

72

23-120

30-120

18-120


04/01/13



L1305016-09Lab ID:


1,8270D03/28/13 23:33JB


80%Percent Solids:

MDL

84.

75.

140

80.

100

82.

78.

80.

76.

68.

85.

120

80.

79.

91.

79.

Serial_No:04011314:42

Page 49 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

J

J

Dilution Factor

ND

320

ND

170

160

210

88

150

ND

52

93

ND

130

ND

84

300

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

68

74

80

23-120

30-120

18-120


04/01/13



L1305016-10Lab ID:


1,8270D03/28/13 23:57JB


80%Percent Solids:

MDL

42.

38.

68.

40.

50.

41.

39.

40.

38.

34.

43.

59.

40.

40.

45.

40.

Serial_No:04011314:42

Page 50 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

J

J

Dilution Factor

ND

1700

ND

970

600

660

250

1100

ND

570

210

620

3000

ND

210

1900

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

4

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

590

450

740

450

590

450

450

450

590

450

590

740

450

450

590

450

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

71

79

68

23-120

30-120

18-120


04/01/13



L1305016-11Lab ID:

Field Prep: Not Specified

D

Matrix: Soil Extraction Method:Analytical Method:Analytical Date:Analyst:

1,8270D03/29/13 16:50JB


88%Percent Solids:

MDL

150

140

250

140

180

150

140

150

140

120

150

210

140

140

160

140

Serial_No:04011314:42

Page 51 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

290

220

360

220

290

220

220

220

290

220

290

360

220

220

290

220

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

79

87

83

23-120

30-120

18-120


04/01/13



L1305016-12Lab ID:


1,8270D03/29/13 00:44JB


91%Percent Solids:

MDL

74.

66.

120

70.

88.

73.

69.

71.

67.

60.

75.

100

70.

70.

80.

70.

Serial_No:04011314:42

Page 52 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene


ND

580

ND

910

870

1200

530

940

ND

ND

420

ND

ND

120

400

600

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

170

120

210

120

170

120

120

120

170

120

170

210

120

120

170

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

66

69

81

23-120

30-120

18-120


04/01/13



L1305016-13Lab ID:


1,8270D03/29/13 01:07JB


79%Percent Solids:

MDL

43.

38.

70.

41.

51.

42.

40.

41.

39.

35.

44.

60.

41.

41.

46.

41.

Serial_No:04011314:42

Page 53 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

Dilution Factor

680

7900

ND

3700

2500

3400

1200

3200

59

2100

930

800

5700

310

950

6400

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

74

80

79

23-120

30-120

18-120


04/01/13



L1305016-14Lab ID:


1,8270D03/29/13 01:31JB


82%Percent Solids:

MDL

41.

37.

66.

39.

49.

40.

38.

39.

37.

33.

42.

57.

39.

39.

44.

39.

Serial_No:04011314:42

Page 54 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

Dilution Factor

ND

720

ND

380

390

480

200

380

ND

99

280

ND

290

120

220

610

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

160

120

210

120

160

120

120

120

160

120

160

210

120

120

160

120

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

67

72

73

23-120

30-120

18-120


04/01/13



L1305016-15Lab ID:


1,8270D03/29/13 01:54JB


80%Percent Solids:

MDL

42.

38.

68.

40.

50.

42.

39.

40.

38.

34.

43.

59.

40.

40.

46.

40.

Serial_No:04011314:42

Page 55 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

J

J

Dilution Factor

ND

390

ND

170

160

220

88

170

ND

38

110

ND

160

ND

100

310

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

150

110

190

110

150

110

110

110

150

110

150

190

110

110

150

110

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

66

71

75

23-120

30-120

18-120


04/01/13



L1305016-16Lab ID:


1,8270D03/29/13 02:18JB


86%Percent Solids:

MDL

39.

35.

63.

37.

46.

38.

36.

37.

35.

32.

39.

54.

37.

37.

42.

37.

Serial_No:04011314:42

Page 56 of 90


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

03/28/13 18:511,8270DAnalytical Method:

Analytical Date:Extraction Method: EPA 3546Extraction Date: 03/27/13 08:14

04/01/13

Analyst: JB

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

99

160

99

130

99

99

99

130

99

130

160

99

99

130

99

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01-16 Batch: WG597735-1

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

64

66

76

23-120

30-120

18-120


Criteria

MDL

34.

30.

55.

32.

40.

33.

32.

32.

31.

27.

34.

47.

32.

32.

37.

32.

Serial_No:04011314:42

Page 57 of 90

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene


Indeno(1,2,3-cd)Pyrene

Pyrene

86

107

78

105

106

96

103

93

100

110

96

95

96

98

102

105

78

100

71

98

96

97

89

87

91

102

89

88

90

91

94

97

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

10

7

9

7

10

1

15

7

9

8

8

8

6

7

8

8

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-16 Batch: WG597735-2 WG597735-3


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

04/01/13

Qual Qual Qual

Serial_No:04011314:42

Page 58 of 90

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

86

91

94

23-120

30-120

18-120

75

80

85


04/01/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04011314:42

Page 59 of 90

INORGANICS&

MISCELLANEOUS

Serial_No:04011314:42

Page 60 of 90

FF


Parameter ResultDilution Factor

Matrix: Soil


L1305016-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed

AnalyticalMethod Analyst

Not Specified

General Chemistry - Westborough LabSolids, Total 81.7 % 10.100 03/27/13 17:09 30,2540G RD

Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 61 of 90

FF



Matrix: Soil


L1305016-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 62 of 90

FF



Matrix: Soil


L1305016-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 63 of 90

FF



Matrix: Soil


L1305016-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 64 of 90

FF



Matrix: Soil


L1305016-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 65 of 90

FF



Matrix: Soil


L1305016-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 66 of 90

FF



Matrix: Soil


L1305016-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 67 of 90

FF



Matrix: Soil


L1305016-08Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 68 of 90

FF



Matrix: Soil


L1305016-09Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 69 of 90

FF



Matrix: Soil


L1305016-10Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 70 of 90

FF



Matrix: Soil


L1305016-11Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 71 of 90

FF



Matrix: Soil


L1305016-12Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 72 of 90

FF



Matrix: Soil


L1305016-13Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 73 of 90

FF



Matrix: Soil


L1305016-14Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 74 of 90

FF



Matrix: Soil


L1305016-15Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 75 of 90

FF



Matrix: Soil


L1305016-16Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305016

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/01/13

MDL

NA

Serial_No:04011314:42

Page 76 of 90

Solids, Total 81.7 83.0 % 2 20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01-16 QC Batch ID: WG597914-1 QC Sample: L1305016-01 Client ID: SW-1

STARWOOD CAPITAL

STARWOOD CAPIT

Project Name:

Project Number:

L1305016Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

04/01/13

Qual

Serial_No:04011314:42

Page 77 of 90

*Values in parentheses indicate holding time in days

L1305016-01A

L1305016-01B

L1305016-01C

L1305016-01D

L1305016-01E

L1305016-01F

L1305016-01G

L1305016-01H

L1305016-02A

L1305016-02B

L1305016-02C

L1305016-02D

L1305016-02E

L1305016-02F

L1305016-02G

L1305016-02H

L1305016-03A

L1305016-03B

L1305016-03C

L1305016-03D

L1305016-03E

L1305016-03F

L1305016-03G

L1305016-03H

L1305016-04A

L1305016-04B

L1305016-04C

5 gram Encore Sampler



Vial MeOH preserved split

Vial Water preserved split


Plastic 2oz unpreserved for TS

Amber 250ml unpreserved




















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A AbsentCooler

Custody SealCooler Information

STARWOOD CAPITAL

STARWOOD CAPITAL

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

Project Name:

Project Number:

L1305016Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type Cooler pHTempdeg C Pres Seal

Container Information

Analysis(*)

04/01/13

Were project specific reporting limits specified? YES

Reagent H2O Preserved Vials Frozen on: 03/26/2013 23:55

Serial_No:04011314:42

Page 78 of 90


L1305016-04D

L1305016-04E

L1305016-04F

L1305016-04G

L1305016-04H

L1305016-05A

L1305016-05B

L1305016-05C

L1305016-05D

L1305016-05E

L1305016-05F

L1305016-05G

L1305016-05H

L1305016-06A

L1305016-06B

L1305016-06C

L1305016-06D

L1305016-06E

L1305016-06F

L1305016-06G

L1305016-06H

L1305016-07A

L1305016-07B

L1305016-07C

L1305016-07D

L1305016-07E

L1305016-07F

L1305016-07G

L1305016-07H

L1305016-08A

L1305016-08B

L1305016-08C

L1305016-08D

L1305016-08E

L1305016-08F

L1305016-08G





































A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

STARWOOD CAPITAL

STARWOOD CAPITAL

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

Project Name:

Project Number:

L1305016Lab Number:

Report Date:



Analysis(*)

04/01/13

Serial_No:04011314:42

Page 79 of 90


L1305016-08H

L1305016-09A

L1305016-09B

L1305016-09C

L1305016-09D

L1305016-09E

L1305016-09F

L1305016-09G

L1305016-09H

L1305016-10A

L1305016-10B

L1305016-10C

L1305016-10D

L1305016-10E

L1305016-10F

L1305016-10G

L1305016-10H

L1305016-11A

L1305016-11B

L1305016-11C

L1305016-11D

L1305016-11E

L1305016-11F

L1305016-11G

L1305016-11H

L1305016-12A

L1305016-12B

L1305016-12C

L1305016-12D

L1305016-12E

L1305016-12F

L1305016-12G

L1305016-12H

L1305016-13A

L1305016-13B

L1305016-13C





































A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

STARWOOD CAPITAL

STARWOOD CAPITAL

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

Project Name:

Project Number:

L1305016Lab Number:

Report Date:



Analysis(*)

04/01/13

Serial_No:04011314:42

Page 80 of 90


L1305016-13D

L1305016-13E

L1305016-13F

L1305016-13G

L1305016-13H

L1305016-14A

L1305016-14B

L1305016-14C

L1305016-14D

L1305016-14E

L1305016-14F

L1305016-14G

L1305016-14H

L1305016-15A

L1305016-15B

L1305016-15C

L1305016-15D

L1305016-15E

L1305016-15F

L1305016-15G

L1305016-15H

L1305016-16A

L1305016-16B

L1305016-16C

L1305016-16D

L1305016-16E

L1305016-16F

L1305016-16G

L1305016-16H






























A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

3.5

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

STARWOOD CAPITAL

STARWOOD CAPITAL

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

Project Name:

Project Number:

L1305016Lab Number:

Report Date:



Analysis(*)

04/01/13

Serial_No:04011314:42

Page 81 of 90

Report Format: DU Report with "J" Qualifiers

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1305016STARWOOD CAPITAL

STARWOOD CAPITAL 04/01/13

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NI

RL

RPD

SRM

Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.

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Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.

Data Qualifiers

A

B

C

D

E

G

H

I

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-

-

-

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Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reported

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.

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Footnotes

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Project Name:

Project Number:

Lab Number:

Report Date:



Data Qualifiers

M

NJ

P

Q

R

RE

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due to obvious interference.

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

J

ND

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Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

30

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.

Project Name:

Project Number:

Lab Number:

Report Date:


STARWOOD CAPITAL

REFERENCES

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Certificate/Approval Program Summary Last revised December 19, 2012 - Westboro Facility

The following list includes only those analytes/methods for which certification/approval is currently held.

For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.

Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 6010C, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8330, 8151A, 8260B, 8260C, 8270C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9030B, 9040B, 9045C, 6010B, 6010C, 6020, 6020A, 7471A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8270D, 8330, 8151A, 8081A, 8081B, 8082, 8082A, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.)

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Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010C, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012B, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C,

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3546, 3580A, 5030B, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 355B0, 3580A, 3630C, 6020A, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C,

Serial_No:04011314:42

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8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.

Serial_No:04011314:42

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Serial_No:04011314:42

Page 90 of 90

L1305111

Enviro-Sciences

STARWOOD CAPITAL

STARWOOD CAPITAL

Client:

Project Name:

Project Number:

04/03/13

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

781 Route 15 S.

2nd Floor

Jim MaguireATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086),PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers.

Lake Hopatcong, NJ 07849

(973) 398-8183Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:04031311:24

Page 1 of 40

L1305111-01

L1305111-02

Alpha Sample ID

PR-1

PR-2

Client ID

PORT CHESTER, NY

PORT CHESTER, NY

Sample Location

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:Project Number:

Lab Number: Report Date:

L130511104/03/13

03/27/13 09:30

03/27/13 09:50

Collection Date/Time

Serial_No:04031311:24

Page 2 of 40

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:

Project Number:

Lab Number:


04/03/13

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of

NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample

specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,

followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a

required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is

designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the

associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %

recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods

allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not

narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool

where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight

basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the

back of the report.

In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some

quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the

associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed

along with any associated usability implications.

Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical

Standards requested on the Chain of Custody.

HOLD POLICY

For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30

days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and

made arrangements for Alpha to continue to hold the samples.

Please contact Client Services at 800-624-9220 with any questions.

Serial_No:04031311:24

Page 3 of 40

Case Narrative (continued)

STARWOOD CAPITAL

STARWOOD CAPITAL

Project Name:

Project Number:

Lab Number:


04/03/13

Report Submission

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

The project location was provided by the project manager.

Semivolatile Organics

L1305111-01 has elevated detection limits due to the dilution required by matrix interferences encountered

during the concentration of the sample.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 04/03/13

Serial_No:04031311:24

Page 4 of 40

ORGANICS

Serial_No:04031311:24

Page 5 of 40

VOLATILES

Serial_No:04031311:24

Page 6 of 40

FF

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

J

J

J

J

J

J

Dilution Factor

ND

76

54

ND

240

120

80

52

ND

ND

85

70

190

640

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

74

110

74

150

150

150

74

74

370

74

74

74

370

370


Toluene-d8



91

102

108

92

70-130

70-130

70-130

70-130


04/03/13

PR-1Client ID:03/27/13 09:30Date Collected:03/27/13Date Received:


L1305111-01Lab ID:



MDL

8.7

8.2

11.

7.7

24.

20.

14.

15.

41.

12.

14.

9.3

10.

42.

Serial_No:04031311:24

Page 7 of 40

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene




ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

1.1

1.6

1.1

2.2

2.2

2.2

1.1

1.1

5.5

1.1

1.1

1.1

5.5

5.5


Toluene-d8



93

103

99

97

70-130

70-130

70-130

70-130


04/03/13



L1305111-02Lab ID:



MDL

0.13

0.12

0.16

0.11

0.36

0.30

0.22

0.23

0.62

0.18

0.21

0.14

0.16

0.63

Serial_No:04031311:24

Page 8 of 40


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111


Analytical Date:

04/03/13

Analyst: BN

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

ND

0.20

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.0

1.5

1.0

2.0

2.0

2.0

1.0

1.0

5.0

1.0

1.0

1.0

5.0

5.0

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 02 Batch: WG598221-3


Toluene-d8



90

103

101

95

70-130

70-130

70-130

70-130


Criteria

MDL

0.12

0.11

0.15

0.10

0.32

0.27

0.20

0.20

0.56

0.17

0.19

0.12

0.14

0.57

Serial_No:04031311:24

Page 9 of 40


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111


Analytical Date:

04/03/13

Analyst: BN

Benzene

Toluene

Ethylbenzene


p/m-Xylene

o-Xylene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Isopropylbenzene

p-Isopropyltoluene

n-Propylbenzene



Parameter Result

ND

10

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

50

75

50

100

100

100

50

50

250

50

50

50

250

250

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 01 Batch: WG598222-3


Toluene-d8



90

103

101

95

70-130

70-130

70-130

70-130


Criteria

MDL

5.9

5.6

7.4

5.2

16.

14.

9.9

10.

28.

8.4

9.6

6.3

7.2

29.

Serial_No:04031311:24

Page 10 of 40

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane




Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

91

91

87

91

89

98

89

97

106

100

84

79

89

84

98

88

92

98

100

90

100

87

86

83

83

86

96

86

94

99

96

76

78

82

81

97

85

85

96

96

84

94

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

4

6

5

9

3

2

3

3

7

4

10

1

8

4

1

3

8

2

4

7

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Volatile Organics by 8260/5035 - Westborough Lab Associated sample(s): 02 Batch: WG598221-1 WG598221-2


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 11 of 40

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

98

108

84

111

68

100

94

88

104

106

106

89

101

100

90

84

97

139

113

97

93

92

108

85

100

64

92

87

83

102

102

102

87

96

95

86

81

94

125

91

89

82

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

6

0

1

10

6

8

8

6

2

4

4

2

5

5

5

4

3

11

22

9

13

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 12 of 40

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

83

84

97

95

92

90

98

98

99

104

104

105

107

104

105

89

114

105

106

103

90

80

81

94

85

89

83

95

95

96

102

98

98

100

99

100

85

108

98

100

101

86

70-130

70-130

68-130

70-130

70-130

70-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

4

4

3

11

3

8

3

3

3

2

6

7

7

5

5

5

5

7

6

2

5

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 13 of 40

Isopropyl Ether

tert-Butyl Alcohol

n-Propylbenzene





Methyl Acetate

Ethyl Acetate

Acrolein

Cyclohexane

1,4-Dioxane


1,4-Diethylbenzene

4-Ethyltoluene


Tetrahydrofuran

Ethyl ether


Methyl cyclohexane


90

84

104

108

112

106

105

86

83

75

102

84

104

109

107

107

88

76

92

99

88

87

79

98

106

109

100

100

82

80

72

93

83

94

101

101

103

82

75

90

90

87

66-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

70-130

70-130

70-130

70-130

66-130

67-130

70-130

70-130

70-130

3

6

6

2

3

6

5

5

4

4

9

1

10

8

6

4

7

1

2

10

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 14 of 40


Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane




Tetrachloroethene

88

91

91

87

91

89

98

89

97

106

85

87

86

83

83

86

96

86

94

99

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

3

4

6

5

9

3

2

3

3

7

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery





Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111


Toluene-d8



89

105

101

96

70-130

70-130

70-130

70-130

86

104

99

95


04/03/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04031311:24

Page 15 of 40

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

100

84

79

89

84

98

88

92

98

100

90

100

98

108

84

111

68

100

94

88

104

96

76

78

82

81

97

85

85

96

96

84

94

92

108

85

100

64

92

87

83

102

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

4

10

1

8

4

1

3

8

2

4

7

6

6

0

1

10

6

8

8

6

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 16 of 40

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate



2-Hexanone

Bromochloromethane

2,2-Dichloropropane

1,2-Dibromoethane

1,3-Dichloropropane


106

106

89

101

100

90

84

97

139

113

97

93

83

84

97

95

92

90

98

98

99

102

102

87

96

95

86

81

94

125

91

89

82

80

81

94

85

89

83

95

95

96

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

70-130

68-130

70-130

70-130

70-130

70-130

69-130

70-130

4

4

2

5

5

5

4

3

11

22

9

13

4

4

3

11

3

8

3

3

3

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 17 of 40

Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

p-Chlorotoluene


Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

Acrylonitrile

Isopropyl Ether

tert-Butyl Alcohol

n-Propylbenzene





Methyl Acetate

Ethyl Acetate

104

104

105

107

104

105

89

114

105

106

103

90

90

84

104

108

112

106

105

86

83

102

98

98

100

99

100

85

108

98

100

101

86

87

79

98

106

109

100

100

82

80

70-130

70-130

70-130

70-130

70-130

70-130

68-130

67-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

2

6

7

7

5

5

5

5

7

6

2

5

3

6

6

2

3

6

5

5

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 18 of 40

Acrolein

Cyclohexane

1,4-Dioxane


1,4-Diethylbenzene

4-Ethyltoluene


Tetrahydrofuran

Ethyl ether


Methyl cyclohexane



75

102

84

104

109

107

107

88

76

92

99

88

88

72

93

83

94

101

101

103

82

75

90

90

87

85

70-130

70-130

65-136

70-130

70-130

70-130

70-130

66-130

67-130

70-130

70-130

70-130

70-130

4

9

1

10

8

6

4

7

1

2

10

1

3

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111


Toluene-d8



89

105

100

96

70-130

70-130

70-130

70-130

86

104

99

95


04/03/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04031311:24

Page 19 of 40

SEMIVOLATILES

Serial_No:04031311:24

Page 20 of 40

FF

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

J

J

J

J

J

J

Dilution Factor

ND

200

310

160

140

170

ND

190

ND

ND

85

ND

220

ND

ND

230

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

310

230

380

230

310

230

230

230

310

230

310

380

230

230

310

230

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

75

72

54

23-120

30-120

18-120


04/03/13



L1305111-01Lab ID:


1,8270D03/29/13 13:54RC


85%Percent Solids:

MDL

79.

71.

130

75.

94.

78.

73.

76.

72.

64.

80.

110

75.

74.

85.

75.

Serial_No:04031311:24

Page 21 of 40

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

J

J

Dilution Factor

ND

400

ND

240

230

300

130

260

ND

ND

150

ND

93

38

160

370

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

150

110

190

110

150

110

110

110

150

110

150

190

110

110

150

110

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

80

77

66

23-120

30-120

18-120


04/03/13



L1305111-02Lab ID:


1,8270D03/29/13 14:22RC


86%Percent Solids:

MDL

39.

35.

63.

37.

47.

38.

36.

37.

36.

32.

40.

55.

37.

37.

42.

37.

Serial_No:04031311:24

Page 22 of 40


Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

03/29/13 09:141,8270DAnalytical Method:

Analytical Date:Extraction Method: EPA 3546Extraction Date: 03/28/13 09:49

04/03/13

Analyst: RC

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

99

160

99

130

99

99

99

130

99

130

160

99

99

130

99

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01-02 Batch: WG598038-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

77

78

73

64

67

62

25-120

10-120

23-120

30-120

0-136

18-120


Criteria

MDL

34.

30.

54.

32.

40.

33.

31.

32.

31.

27.

34.

47.

32.

32.

36.

32.

Serial_No:04031311:24

Page 23 of 40

Acenaphthene


Hexachlorobenzene

Bis(2-chloroethyl)ether

2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

3,3'-Dichlorobenzidine

2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene

4-Chlorophenyl phenyl ether

4-Bromophenyl phenyl ether

Bis(2-chloroisopropyl)ether

Bis(2-chloroethoxy)methane

Hexachlorobutadiene

Hexachlorocyclopentadiene

Hexachloroethane

Isophorone

Naphthalene

62

61

68

64

58

64

64

64

41

67

58

73

62

67

72

67

64

51

69

64

64

61

56

64

58

61

61

58

59

44

68

64

68

62

61

66

64

61

50

64

62

59

31-137

38-107

40-140

40-140

40-140

40-140

40-140

28-104

40-140

28-89

40-140

40-140

40-140

40-140

40-140

40-117

40-140

40-140

40-140

40-140

40-140

2

9

6

10

5

5

10

8

7

1

10

7

0

9

9

5

5

2

8

3

8

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 24 of 40

Nitrobenzene

NitrosoDiPhenylAmine(NDPA)/DPA

n-Nitrosodi-n-propylamine

Bis(2-Ethylhexyl)phthalate

Butyl benzyl phthalate

Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene


Indeno(1,2,3-cd)Pyrene

64

63

70

72

70

80

70

68

67

68

70

69

71

68

57

71

68

63

70

69

64

60

66

67

77

74

74

78

71

66

70

70

69

69

70

62

69

69

66

68

69

65

40-140

32-121

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

6

5

4

7

6

8

11

4

2

3

0

0

3

3

8

3

1

5

3

0

2

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 25 of 40

Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene

1,2,4,5-Tetrachlorobenzene

Acetophenone

2,4,6-Trichlorophenol

P-Chloro-M-Cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

4,6-Dinitro-o-cresol

Pentachlorophenol

Phenol

71

66

52

63

28

66

64

54

70

73

62

67

69

66

68

65

31

58

65

66

72

68

65

52

68

34

69

64

55

63

67

61

68

62

65

65

60

35

48

64

65

64

35-142

40-140

47-134

26-129

41-125

40-140

40-140

40-117

14-144

30-130

26-103

25-102

30-130

30-130

30-130

11-114

4-130

10-130

17-109

26-90

4

2

0

8

19

4

0

2

11

9

2

1

11

2

5

8

12

19

2

2

12

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

04/03/13

Qual Qual Qual

Serial_No:04031311:24

Page 26 of 40

2-Methylphenol

3-Methylphenol/4-Methylphenol

2,4,5-Trichlorophenol

Benzoic Acid

Benzyl Alcohol

Carbazole

69

72

61

38

73

72

66

68

65

28

67

71

30-130.

30-130

30-130

40-140

54-128

4

6

6

30

9

1

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

87

85

78

71

81

70

25-120

10-120

23-120

30-120

0-136

18-120

80

77

73

69

76

68


04/03/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:04031311:24

Page 27 of 40

INORGANICS&

MISCELLANEOUS

Serial_No:04031311:24

Page 28 of 40

FF



Matrix: Soil


L1305111-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/03/13

MDL

NA

Serial_No:04031311:24

Page 29 of 40

FF



Matrix: Soil


L1305111-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

STARWOOD CAPITAL

STARWOOD CAPITAL

L1305111

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/03/13

MDL

NA

Serial_No:04031311:24

Page 30 of 40

Solids, Total 85.3 84.6 % 1 20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG598175-1 QC Sample: L1305111-01 Client ID: PR-1

STARWOOD CAPITAL

STARWOOD CAPIT

Project Name:

Project Number:

L1305111Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

04/03/13

Qual

Serial_No:04031311:24

Page 31 of 40


L1305111-01A

L1305111-01B

L1305111-01C

L1305111-01D

L1305111-01E

L1305111-01F

L1305111-01G

L1305111-01H

L1305111-02A

L1305111-02B

L1305111-02C

L1305111-02D

L1305111-02E

L1305111-02F

L1305111-02G

L1305111-02H

















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A AbsentCooler

Custody SealCooler Information

STARWOOD CAPITAL

STARWOOD CAPITAL

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(2)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

NYTCL-8260HLW(14)

TS(7)

NYTCL-8270(14)

Project Name:

Project Number:

L1305111Lab Number:

Report Date:

Sample Receipt and Container Information



Analysis(*)

04/03/13

Were project specific reporting limits specified? YES

Reagent H2O Preserved Vials Frozen on: 03/28/2013 02:58

Serial_No:04031311:24

Page 32 of 40


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:



Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NI

RL

RPD

SRM

Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.

Data Qualifiers

A

B

C

D

E

G

H

I

-

-

-

-

-

-

-

-

Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reported

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.

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Footnotes

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Project Name:

Project Number:

Lab Number:

Report Date:



Data Qualifiers

M

NJ

P

Q

R

RE

-

-

-

-

-

-

due to obvious interference.

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

J

ND

-

-

Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

30

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.

Project Name:

Project Number:

Lab Number:

Report Date:


STARWOOD CAPITAL

REFERENCES

04/03/13

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Certificate/Approval Program Summary Last revised December 19, 2012 - Westboro Facility

The following list includes only those analytes/methods for which certification/approval is currently held.

For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.

Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 6010C, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8330, 8151A, 8260B, 8260C, 8270C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9030B, 9040B, 9045C, 6010B, 6010C, 6020, 6020A, 7471A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8270D, 8330, 8151A, 8081A, 8081B, 8082, 8082A, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.)

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Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010C, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012B, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C,

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3546, 3580A, 5030B, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 355B0, 3580A, 3630C, 6020A, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C,

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8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.

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