2009 aig portable xrf workshop › qaqc_whitbread.pdfqaqc 2009 aig portable xrf workshop pxrf...
TRANSCRIPT
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2009 AIG Portable XRF Workshop
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QAQC and Data Management of PXRF Data
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What You Need to Remember
● By using a Portable XRF Device to collect assay data,
YOU ARE NOW THE LABORATORY!!!
● So, you need to act like an analytical laboratory:
● Chemistry results are only from what the X Rays see. Sampling statistics need to be taken into account e.g. homogeneity, particle size, surface effects and XRF window size!
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particle size, surface effects and XRF window size!
● Use blanks
● Deal with matrix effects - Use LAB data to verify chemistry and correct via calibration
● use Matrix Matched certified standards to correct factors if the matrix is consistent.
● Watch your detection limits: Longer Tests = better precision within limits
PXRF Workshop
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Also... Adding Value to Your XRF Data
How can I add value to my XRF Data?
● XRF Sampling is NO Different to any other sampling regime
you adopt!... Remember the Data is very valuable (& costly)!
● So, Use good QA/QC Protocols & Data Validation
● Incorporate Standards, Blanks, Field Duplicates and Check
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● Incorporate Standards, Blanks, Field Duplicates and Check
Samples to increase your understanding & confidence
● Rank & Store the Data in a well ordered & structured DB
● Remember that for ASX/TSX Reporting you must abide by
JORC Code / TSX 43-101 – All about Transparency &
Disclosure – so ensure your data is reported correctly!
PXRF Workshop
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REPORTING, DATA SYSTEMS
INTEGRATION
2009 AIG Portable XRF Workshop
PXRF Workshop
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Integrated
Collection, Data
Management
and QAQC –
Innov-X Example
• ioGAS
• ioHUB
• ioQA™Reporter
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QA - Holistic Approach
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In Field Example – Data Imaging
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QAQC
2009 AIG Portable XRF Workshop
PXRF Workshop
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Why do we Care?
Exploration Don't miss a target, asses
targets properly.
Resources Data suitable for publicly
reported estimates. Geomet
implications. Reduce risk
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implications. Reduce risk
Grade Control Minimal misclassification.
Geomet – scheduling
optimisation.
Plant/Tails/Product Reconciliation
PXRF Workshop
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Effect of Fraction Size on Precision
30 second data - Bulk 30 second data -75um
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Tighter precision envelope and lower effective detection limit for -75um data
PXRF Workshop
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Effect of Reading Time on Precision
30 second data -75um 180 second data -75um
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Tighter precision envelope and lower effective detection limit for 180 second data
PXRF Workshop
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Blanks Tests – “Zero” Blank
Limit, eg set at
multiple of DL or
absolute value
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Example of Analytical Problems ‘Over Time’ – Cu Analyses
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Ores45p Cu-ppmDetection Limits (2sd) and CV
3min – 34ppm, 0.026
1 min – 60ppm, 0.045
30 sec– 85ppm, 0.064
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Percent Relative Difference Plots
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Reported Out of Range Data Come From Here
PXRF Workshop
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Error Model - Test against set
Relative Error
This region coloured in
to indicate that this
plot has been used in
the exception
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the exception
reporting
*Also allows for temporal based variations in precision to be assessed
Time context
PXRF Workshop
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Check Assay Example – QQ Plot
Check Assays
30
40
50
Lab
A %
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-5 0 5 10 15 20 25 30 35 40
Lab B %
-10
0
10
20
Lab
A %
PXRF Workshop
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Relative Bias
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Summary
● Jorc/43-101 � Transparency and Disclosure
● Collection of Portable XRF requires the same QAQC as other
analytical data
● Contamination, Accuracy, Precision, Bias all need to be
monitored
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● Sample matrix and sampling statistic effects are crucial
● In field use no longer precludes data systems integration and
analysis. ‘Real time’ analysis is a reality
● QC reporting can now be automated
PXRF Workshop