20 years - indico€¦ · wamhts-4 workshop, barcelona, 16.2.2017 20 years. may 2016 2. may 2016 3...

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1 THEVA Dünnschichttechnik GmbH 2G superconducting tape for magnet applications Markus Bauer WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS

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Page 1: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

1

THEVA Dünnschichttechnik GmbH

2G superconducting tape for magnet applications

Markus Bauer

WAMHTS-4 Workshop, Barcelona, 16.2.2017

20 YEARS

Page 2: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

2

Page 3: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

3

HTS – PRODUCTION LINE

Pilot line features

Modular, fully-automated

Continuous vacuum tape locking

Inline quality control

Production capacity: 150 km/yr (@ 12 mm-width)

Production tape length: 350 m, to be increased

up to 600 m, soon!

Goals

Cost efficient production

Robust process allowing high yield

Implementation of industrial standards

Stringent quality management

Setting worldwide standards

Page 4: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

4

THEVA Pro-Line

simple layer architecture

industrial-grade deposition technique (e-beam evaporation)

in-house designed and manufactured equipment

unique approach – all IP owned by THEVA

2G superconducting tape by PVD

Contact layer

Silver

Superconductor

GdBaCuO

Cap layer

MgO Orientation layer

ISD-MgO

E-polished substrate

Hastelloy C276

Silver

GdBCO

MgO

MgO

Page 5: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

5

ORIENTED BUFFER LAYER

ISD MgO buffer layer

simple process, fast growth > 6 nm/s

tilted substrate (30°)

room temperature

[001]

[110]

MgO

Inclined substrate deposition (ISD)

MgO-Orientation (XRD)

tilt angle of MgO<100> b 30°

in-plane D < 10°

out-of-plane D < 4°

tape direction

Page 6: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

6

tilt leads to overgrowth of

precipitates and misoriented regions

Jc is thickness independent!

Very high Ic possible!

positive effect of the tilt angle

Comparison of laboratory resultswith production tapes

Tunable performance

Page 7: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

7

2,0 µm

Ic > 200 A

12 mm

3,5 µm

Ic > 400 A

12 mm

5,5 µm

Ic > 600 A

12 mm

77 K, self field

Tapestar measurements

first effect of the tilt angle

Tunable performance

60 m

Page 8: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

8

Improving performance on long tapes

2,4 µm

Aug. 2016

Jan. 2017

3,6 µm

340 m, 12 mm

240 m, 12 mm

1000 A

1000 A

Page 9: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

9

THEVA ProLine tapes for magnets

50 µm and 100 µm thick

Cu stabilization

12 mm width

Laminated Plated

5 µm … 20 µm surround coating

optional: pre-tinned

12 mm width available

3.4 mm … 6 mm in development

test pieces available

Page 10: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

10

Mechanical propertiesBending test

0,0

0,2

0,4

0,6

0,8

1,0

1,2

-1,0% -0,5% 0,0% 0,5% 1,0%

RED

UC

ED C

RIT

ICA

L C

UR

REN

T

BENDING STRAIN

TPL4100

Datenreihen1 Datenreihen3

Page 11: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

11

180° 160° 140° 120° 100° 80°

Magnetic field performance

10 T, 4.2 K

6 mm wide tapes

Ic (77K, s.f.) = 310 A

Page 12: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

12

Magnetic Field Performance

more data available!

Typical performance at 25 K … 40 K

Typical Field dependence

0 30 60 90 120 150 180 210 240

0

1

2

3

4

5

lift fa

cto

r

angle [°]

25 K

30 K

35 K

40 K

3 T

0 1 2 3 4 5 6 7 8

0

1

2

3

4

5

6

7 Ic,min

(B || c at 30°)

25 K

30 K

35 K

40 K

lift fa

cto

rmagnetic field [T]

Page 13: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

13

Outlook – additional pinning

Artificial pinning also

effective on ISD-MgO buffer

layer

BaHfO and BrZrO was

tested

also deposition parameters

influence pinning

Increase of performance

0 1 2 3 4 5 6 7 8 91

2

3

4

5

6

789

10

30 K, B//c

Jc (

MA

/cm

2)

B (T)

0 mol.% (GB pinning)

2.1 mol.% (Extended pinning)

8.6 mol.% (Random pinning)

0 mol.% (Production sample: BL15083)

Page 14: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

EUROPEAN DEVELOPMENT OF SUPERCONDUCTING TAPES

The research leading to these results has received funding from the European Union’s Seventh Framework Programme

(FP7/2007-2013) under grant agreement nº 280432

http://www.eurotapes.eu

Tapestar system

14

77 K

State of the art:

• existing magnetoscan device Tapestar

• measurement of Ic along the type with 1

mm resolution at high speed

• well known, used worldwide

Page 15: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

EUROPEAN DEVELOPMENT OF SUPERCONDUCTING TAPES

The research leading to these results has received funding from the European Union’s Seventh Framework Programme

(FP7/2007-2013) under grant agreement nº 280432

http://www.eurotapes.eu

Advanced Tapestar System withInversion of Hall-Scanning data

previous

New:

2D-Ic map

New:

2D-Ic map

previous

Page 16: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

16

H2020 Project : EcoSwing

• The idea is to replace a PM generator with a

superconducting generator

• full scale multi-megawatt direct-drive superconducting wind generator

• Installation on an existing modern wind turbine in Thyborøn, Denmark(3.6 MW, 15 rpm, 128 m rotor)

• THEVA is responsible for all HTS tapes and HTS coil manufacturing

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

Page 17: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

17

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

40% lower weight

PM Superconductor

• All roads capability: We limit the diameter to < 4 m

• Low cost design: ‘No frills’ for superconductors

• Low weight design: Optimized for low top head mass

Page 18: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

18

Subscale Test Coil

in LN2 conductioncooled

Ic 216 A 215 An 37 44

pole assembly

- magnetic pole piece- non magnetic

mechanical support- conduction cooling

77K

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

test coil #1- single layer- 10 turns

LN2 test

Page 19: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

19

Lap Joints

• 10 cm long lap joints (12 mm)

• Solder: In97Ag3

• highly reproducible

• typical: 4.8 n or 60 ncm² @ 77 K

Development of highly reproducible joints

portableSPS controlledjoint soldering

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

Page 20: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

20

Per coil: about 200 turns with 500 m of

copper laminated HTS wire

double pancake, insulated design,

potted using commercial resin,glass

fiber reinforced

Use of casting mold for smooth surface

optimum mechanical and thermal

contact

operating temperature < 30 K,

conduction cooled with cold heads

+ 30 coils will be produced coil pole assembly

1,4 m

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

EcoSwing Generator Coils

Page 21: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

21

Generator coilType testing

operatingconditions

“EcoSwing has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No656024.” “Herein we reflect only the author's view. The Commission is not responsible for any use that may be made of the information it contains.”

Page 22: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

22

Summary

Pilot production line with 150 km/a (12 mm) capacity at THEVA

Ic up to

• 600 A (77K, s.f.) or 500 A/cm at 60 m

• 400 A on 200 m + long tapes

Different types and thicknesses of Cu stabilization available

12 mm wide tapes can be delivered immediately

3.4 mm … 6 mm wide tapes to be available soon!

Coil winding and casting process developed

HTS coils with size up to 1,4 m can be produced

Advanced Tapestar system with 2D-Ic-mapping

Ask for offers or samples: [email protected] or [email protected]

Page 23: 20 YEARS - Indico€¦ · WAMHTS-4 Workshop, Barcelona, 16.2.2017 20 YEARS. May 2016 2. May 2016 3 HTS –PRODUCTION LINE Pilot line features Modular, fully-automated Continuous vacuum

May 2016

THEVA Dünnschichttechnik GmbH|Rote-Kreuz-Str. 8|D-85737 Ismaning

Germany|Tel.: +49 89 923346 0|Web.: www.theva.de|Mail.: [email protected]

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Thank you!