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1. Page 3/27/20 Page 1 / 12 2 4 6 8 10 12 14 16 18 20 keV 0 2 4 6 8 10 12 14 cps/eV Zn Zn O Si In In Ca Ca Al Mg O bject SEM/EDX Central Facility Textile Technology Department IIT Delhi.

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Page 1: 20-3-14 EDX

1. Page1. Page1. Page

3/27/2014 Page 1 / 12

2 4 6 8 10 12 14 16 18 20keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Si In In In

Ca

Ca

Al Mg

Object

SEM/EDX Central FacilityTextile Technology Department IIT Delhi.

Page 2: 20-3-14 EDX

Spectrum: Object ZnO

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------O 8 K-series 35.54 40.10 67.12 4.7Zn 30 K-series 34.54 38.97 15.96 1.0Si 14 K-series 9.62 10.86 10.35 0.4Al 13 K-series 3.42 3.85 3.83 0.2In 49 L-series 3.32 3.75 0.87 0.3Ca 20 K-series 1.72 1.95 1.30 0.1Mg 12 K-series 0.46 0.51 0.57 0.1------------------------------------------- Total: 88.62 100.00 100.00

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Page 3: 20-3-14 EDX

2 4 6 8 10 12 14 16 18 20keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Si In In In

Ca

Ca

Object

3. Page3. Page3. Page

Page 3 / 12

Spectrum: Object Al(1.5)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 41.72 49.05 21.31 1.4O 8 K-series 33.94 39.91 70.85 5.8Si 14 K-series 5.26 6.18 6.25 0.3In 49 L-series 3.41 4.01 0.99 0.5Ca 20 K-series 0.72 0.85 0.60 0.2------------------------------------------- Total: 85.04 100.00 100.00

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2 4 6 8 10 12 14 16 18 20keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Ca

Ca

In In In

Object

Page 5: 20-3-14 EDX

Spectrum: Object Al(2.0)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 51.34 59.18 27.94 1.8O 8 K-series 31.75 36.60 70.61 6.1In 49 L-series 3.11 3.58 0.96 0.3Ca 20 K-series 0.56 0.64 0.49 0.2------------------------------------------- Total: 86.75 100.00 100.00

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Page 6: 20-3-14 EDX

2 4 6 8 10 12 14 16 18 20keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Si Ca

Ca

In In In

Object

6. Page6. Page6. Page

Page 6 / 12

Spectrum: Object Al(2.5)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 40.27 47.12 20.19 1.5O 8 K-series 35.11 41.07 71.94 6.7Si 14 K-series 4.90 5.74 5.72 0.3In 49 L-series 3.95 4.62 1.13 0.3Ca 20 K-series 1.24 1.45 1.01 0.2------------------------------------------- Total: 85.47 100.00 100.00

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2 4 6 8 10 12 14 16 18 20keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Al In In In

Ca

Ca

Cl Cl

Object

Page 8: 20-3-14 EDX

Spectrum: Object AL(3.0)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 57.24 58.62 28.16 1.9O 8 K-series 32.90 33.69 66.16 5.6Al 13 K-series 3.24 3.31 3.86 0.3In 49 L-series 3.16 3.24 0.89 0.2Ca 20 K-series 0.64 0.66 0.52 0.1Cl 17 K-series 0.47 0.48 0.42 0.1------------------------------------------- Total: 97.65 100.00 100.00

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Page 9: 20-3-14 EDX

0 2 4 6 8 10 12 14 16 18keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Ca

Ca

C In In

In

Al

Object

9. Page9. Page9. Page

Page 9 / 12

Spectrum: Object AL(3.5)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 61.23 61.22 29.22 2.1O 8 K-series 27.67 27.67 53.98 5.5C 6 K-series 4.84 4.83 12.56 1.8In 49 L-series 3.05 3.05 0.83 0.2Al 13 K-series 2.37 2.37 2.74 0.2Ca 20 K-series 0.86 0.86 0.67 0.2------------------------------------------- Total: 100.01 100.00 100.00

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0 2 4 6 8 10 12 14 16 18keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Ca

Ca

In In In

Al

Object

Page 11: 20-3-14 EDX

Spectrum: Object Al(2.0)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 45.20 54.32 24.37 1.6O 8 K-series 32.12 38.61 70.79 6.1Al 13 K-series 2.68 3.22 3.50 0.2In 49 L-series 2.58 3.10 0.79 0.2Ca 20 K-series 0.63 0.75 0.55 0.1------------------------------------------- Total: 83.21 100.00 100.00

11. 11. 11.

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Page 12: 20-3-14 EDX

0 2 4 6 8 10 12 14 16 18keV

0

2

4

6

8

10

12

14

cps/eV

Zn Zn O Si In In In

Ca

Ca

Al

Object

12. 12. 12.

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Spectrum: Object Al(2.5)

El AN Series unn. C norm. C Atom. C Error [wt.%] [wt.%] [at.%] [%]-------------------------------------------Zn 30 K-series 40.18 47.90 20.58 1.7O 8 K-series 34.61 41.26 72.45 7.8In 49 L-series 3.93 4.69 1.15 0.3Si 14 K-series 3.82 4.56 4.56 0.3Ca 20 K-series 0.96 1.15 0.80 0.2Al 13 K-series 0.38 0.45 0.47 0.1------------------------------------------- Total: 83.89 100.00 100.00