145-155 beech street, chelsea, ma, mag910688 - us … beech street : facility/site ... 34. bis...

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 1

5 Post Office Square Suite 100 BOSTON MA 02109-3912

CERTIFIED MAIL - RETURN RECEIPT REQUESTED

JUl 2 1 2015 Mark R Stebbins Managing Member Lawrenceville LLC 1359 Hooksett Road Hooksett NH 031 06

Re Authorization to discharge under the Remediation General Permit (RGP) - for the 145-1 55 Beech Street site located in Chelsea MA Authorization MAG91 0688

Dear Mr Stebbins

Based on the review ofa Notice of Intent (NO I) submitted on your behalfby Kathleen Campbell ofCDW Consultants Inc for the site referenced above the US Environmental Protection Agency (EPA) hereby authorizes you as the named Owner and Operator to discharge in accordance with the provisions oftlhe RGP at this site Your authorization number is listed above

The checklist enclosed with this RGP authorization indicates the pollutants which you are required to monitor Also indicated on the checklist are the effluent limits test methods and minimum levels (MLs) for each pollutant Please note that the checklist does not represent the complete requirements of the RGP Operators must comply with all of the applicable requirements of this permit including influent and effluent monitoring narrative water quality standards record keeping and reporting requirements found in Parts I and II and Appendices I - VIII of the RGP See EPAs website for the complete RGP and other information at httpwwwepagovregionllnpdesmasshtmldgp

Please note the enclosed checklist includes parameters that exceeded or had a reasonable potential to exceed the Appendix III limits The checklist also includes other parameters for which your laboratory reports indicated there was insufficient sensitivity to detect these parameters at the minimum levels (ML) established in Appendix VI of the RGP The metals limits that are included on the checklist are dilution dependent Based on the effluent flow from the treatment system and the low flow of the receiving water Island End River the metals limits are based on the dilution factor of 19 Also see the RGPs Appendix III for Massachusetts facilities

Therefore the following limits will apply to the effluent of this treatment system

Total Suspended Solids (TSS) - 30 mg1 Total Group I Polycyclic Aromatic Hydrocarbons- 10 ug1 Total Group II Polycyclic Aromatic Hydrocarbons - 100 ug1 Chromium (+3) - 190 ug1 Copper - 70 ug1 Lead- 16 ug1 Zinc- 160 ug1 Iron - 1900 ugL and pH range of 65 - 85 standard units (su) Monitoring for chloride tertiary butyl alcohol 14 dioxane and acetone shall be conducted with no effluent limit

This EPA general permit and authorization to discharge will expire on September 9 2015 You have reported this project will terminate on October 1 2015 Please be aware you are required to reapply for coverage after the EPA expired permit has been reissued The reissuance date as well as the reapplication submittal date will be posted on the EPA web site at that time Regardless of your project termination date you are required to submit a Notice ofTermination (NOT) to the attention of the contact person indicated below within thirty (30) days of the termination of the discharge

Thank you in advance for your cooperation in this matter Please contact George Papadopoulos at 617-918-1579 or PapadopoulosGeorgeepagov ifyou have any questions

Sincerely

lU~~yen Thelma Murphy Chief Storm Water and Construction Permits Section

Enclosure

cc Kathleen Campbell PE CDW Consultants Inc Robert Kubit MassDEP Stephen Shea B WSC

2

2010 Remediation General Permit Summary of Monitoring Parametersill

NPDES Authorization Number MAG910688 Authorization Issued July 20 2015 FacilitySite Name 145-155 Beech Street

FacilitySite Address Email address of owner mstebbinsoroconinccom

LeQJal Name of Operator Operator contact name title and Address

Lawrencevil le LLC Mark R Stebbins Managing Member

Email same as above Estimated date of The Project Completion IOctober 1 2015

Contaminated Construction Dewatering Category-Category and Sub-Category Known Contaminated Sites Subcategory

RGI Termination Date September 2015 Receiv ing Water Island End River to Mystic River to Boston Inner Harbor

Monitoring amp Limits are applicable if checked All samples are to be collected as grab samples

Parameter

Effluent LimitlMethodl M L (All Effluent Limits are shown as Daily

Maximum Limit unless denoted by a in that case it will be a Monthly Average

Limit)

v 1 Total Suspended Solids (TSS)

30 mill igramsl iter (mgL) Me1602ML5ugL

2 Tota l Residual Chlorine (TRC) 1

Freshwater = 11 ugL Saltwater= 75 ugL Me3305ML 20ugL

3 Tota l Petroleum Hydrocarbons (TPH) 50 mgL Me 1664AML 50mgL

4 Cyanide (CN) 2 3 Freshwater= 52 ug1 Saltwater= 10 ugL Me 3354ML 10ugL

5 Benzene (B) 5ugL 500 ugL for hydrostatic testing ony Me 8260CML 2 uqL

6 Toluene (T (l imited as ugL total BTEX Me8260C ML 2uqL

7 Ethylbenzene (E) (l imited as ugL total BTEX) Me8260C ML 2ugL

8 (mpo) Xylenes (X) (limited as ugL total BTEX) Me8260C ML 2ugL

9 Total Benzene Toluene Ethyl Benzene and Xylenes (BTEX) 4

100 ugL Me8260C ML 2ugL

3

Parameter

Effluent Limit[Method[ML (All Effluent Limits are shown as Daily


Limit) 10 Ethylene Dibromide (EDB) (12- Dibromoethane)

005 ug1 Me 8260C ML 10ugL

11 Methyl-tert-Butyl Ether 700 ugIMe8260CML 10ugL

v 12tert-Butyl Alcohol (TBA) _(Tertiary Butanol Monitor Only(ug L)Me 8260CML 10ugL

13 tert-Amyl Methyl Ether (TAME)

Monitor Only(ugL)Me8260CML 10ugL

14 Naphthalene 5 20 ugL Me8260CML 2ugL 15 Carbon Tetrachloride 44 ugL Me8260C ML 5ugL 16 12 Dichlorobenzene (o-DCB) 600 ugL Me8260C ML 5ugL

17 13 Dichlorobenzene (m-DCB)

320 ugL Me 8260C ML SugL

118 14 Dichlorobenzene ( p-DCB)

50 ugL Me 8260C ML Sug L

18a Total dichlorobenzene 763 ugL- NH only Me 8260C ML 5ugL 19 11 Dichloroethane (DCA) 70 ugL Me8260C ML 5ugL 20 1 2 Dlchloroethane (DCA) 50 ugL Me8260C ML 5ugL 21 1 1 Dichloroethene (DCE) 32 ugLMe8260C ML 5ugL 22 cis-12 Dlchloroethene (DCE) 70 ugLMe8260C ML 5ugL

23 Methylene Chloride 46 ugLMe 8260C ML 5ugL 24 Tetrachloroethene (PCE) 50 ugLMe8260C ML 5ugL 25 11 1 Trichloro-ethane TCA)

200 ugLMe 8260C ML 5ug L

26 112 Trichloro-ethane (TCA) 50 ugL Me8260C ML 5ugL

27 Trichloroethene (TCEJ 50 ugL Me8260C ML 5ugL 28 Vinyl Chloride (Chloroethene) 20 ugL Me8260C ML 5ugL

29 Acetone Monitor Only(ugL)Me 8260CML 50ugL

30 14 Dioxane Monitor Only Me1624C ML 50ugL

31 Total Phenols 300 ugL Me4201amp4202ML 2 ug L Me 4204 ML SOug L

32 Pentachlorophenol (PCP) 10 ugL Me8270DML 5ugLMe604 amp625ML 10ugL

33 Total Phthalates (Phthalate esters) 6

30 ugL Me8270DML 5ugL Me 606ML 10uqLamp Me625ML 5uqL

34 Bis (2-Ethylhexyl) Phthalat e [Di shy (ethylhexyl) Phthalate]

60 ugL Me8270DML 5ugLMe606ML lOugL amp Me625ML 5ugL

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

100 ugL

a Benzo(a) Anthracene 7 00038 ugL Me8270D ML 5ugL Me 610ML 5ugLamp Me 625ML 5ugL

4

Parameter

Effluent LimitlM~thodlML All Effluent Limits are shown as Daily ~aximum Limit unless denoted by a In that case it w ill be a Monthly Average

Limit)

v b Benzo(a) Pyrene 1 00038 ugL Me8270D ML SugLMe610ML SuaLamp Me625ML SugL

v c Benzo(b)Fiuoranthene 1 00038 ugL Me8270D ML SugLMe610ML SuaLamp Me625ML SuaL

v d Benzo(k)Fiuoranthene 7 00038 ugL Me8270D ML SugL Me610ML SuaLamp Me625ML SuaL

v e Chrysene 1 00038 ugL Me8270DML SugLMe610ML SugLamp Me625ML SuaL

v f Dibenzo(ah)anthracene 7 00038 ugL Me8270DML SugLMe610ML SugLamp Me625ML S~aL

v g Indeno(123-cd) Pyrene7 00038 ugL Me82700ML SugL Me610ML SuaLamp Me625MLSuaL

100 ugL 36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

v h Acenaphthene XMe8270DML SugLMe610MLSuaL amp Me625ML SuqL

v i Acenaphthylene XMe8270DML SugLMe610MLSuaL amp Me625ML SuaL

v j Anthracene XMe8270DML SugLMe610MLSugL amp Me625ML SuqL

v k Benzo(ghi) Perylene XMe8270DML SugLMe 610MLSuaL amp Me625ML SuaL

v I Fluoranthene XMe8270DML SugLMe610MLSuaL amp Me625ML SugL

v m Fluorene XMe8270DML SugLMe 610MLSuaL amp Me625ML SugL

v n Naphthalene s 20 ug1 I Me8270ML SugL Me610MLSuaL amp Me625ML SugL

v o Phenanthrene XMe8270DML SugLMe610MLSuaL amp Me625ML SugL

v p Pyrene XMe82700ML5ugLMe610ML SugLamp Me625ML SuaL

0000064 ugLMe 608 ML 05 ugL37 Total Polychlorinated Biphenyls (PCBs) s 9

v 38 Chloride Monitor onlvMe 3000 ML 100 ugL

5

Metal Parameters

Total Recoverable Metal Limit

H 10 =~0 mgll CaCO~ Units= uq1

Minimum levei-ML11

Saltwater Limits 39 Antimony 56 10 40 Arsenic 36 20 41 Cadmium 89 10

42 Chromium III (trivalent) 190 15 43 Chromium VI (hexavalent) 503 10

44 Copper 70 15

45 Lead 16 20 46 Mercury 11 02 47 Nickel 82 20 48 Selenium 71 20 49 Silver 22 10

so Zinc 160 15

51 Iron 1900 20

Other Parameters Limit

52 Instantaneous Flow Site specific in CFS

53 Total Flow Site ~ecific in CFS 54 pH Range for Class A amp Class B Waters in MA 65-83 1MonthGrab12

55 pH Range for Class SA amp Class SB Waters in MA 65-85 1MonthGrab12

56 pH Range for Class B Waters in NH 65-8 1MonthGrab12

57 Daily maximum temperature shy Warm water fisheries 83deg F 1MonthGrab13

58 Daily maximum temperature- Cold water fisheries 68deg F 1MonthGrab13

59 Maximum Change in Temperature in MA- Any Class A water body 15degF 1MonthGrab13

60 Maximum Change in Temperature in MA- Any Class B water body- Warm Water 5degF 1MonthGrab13

61 Maximum Change in Temperature in MA - Any Class B water body - Cold water and LakesPonds 3degF 1MonthGrab13

62 Maximum Change in Temperature in MA - Any Class SA water body- Coastal 15degF 1MonthGrab13

63 Maximum Change in Temperature in MA - Any Class SB twater body - July to September 15degF 1MonthGrab13

64 Maximum Change in Temperature in MA - Any Class SB twater body - October to June f4 deg F 1MonthGrab13

Footnotes 1 Although the maximum values for TRC are 11 ug1 and 75 ug1 for freshwater and saltwater respectively the compliance limits are equal to the minimum level (ML) of the test method used as listed in Appendix VI (ie Method 3305 20 ug1)

2 Limits for cyanide are based on EPAs water quality criteria expressed as micrograms per liter There is currently no EPA approved test method for free cyanide Therefore total cyanide must be reported

6

3 Although the maximum values for cyanide are 52 ug1 and 10 ug1 for freshwater and saltwater respectively the compliance limits are equal to the minimum level (ML) of the Method 3354 as listed in Appendix VI (ie 10 ug1)

4 BTEX = sum of Benzene Toluene Ethylbenzene and total Xylenes

5 Naphthalene can be reported as both a purgeable (VOC) and extractable (SVOC) organic compound If both VOC and SVOC are analyzed the highest value must be used unless the QC criteria for one of the analyses is not met In such cases the value from the analysis meeting the QC criteria must be used

6 The sum of individual phthalate compounds(not includin-g the 34 Sis (2shyEthylhexyl) Phthalate The compliance limits are equal to the minimum level (ML) of the test method used as listed in Appendix VI Total values calculated for reporting on NOis and discharge monitoring reports shall be calculated by adding the measured concentration of each constituent If the measurement of a constituent is less than the ML the permittee shall use a value of zero for that constituent For each test the permittee shall also attach the raw data for each constituent to the discharge monitoring report including the minimum level and minimum detection level for the analysis

7 Although the maximum value for the individual PAH compounds is 00038 ug1 the compliance limits are equal to the minimum level (ML) of the test method used as listed in Appendix VI

8 In the November 2002 WQC EPA has revised the definition of Total PCBs for aquatic life as total PCBs is the sum of all homologue all isomer all congener or all Oroclor analysesTotal values calculated for reporting on NOis and discharge monitoring reports shall be calcu lated by adding the measured concentration of each constituent If the measure of a constituent is less than the ML the permittee shall use a value of zero for that constituent For each test the permittee shall also attach the raw data for each constituent to the discharge monitoring report including the minimum level and minimum detection level for the analysis

9Aithough the maximum value for total PCBs is 0000064 ug1 the compliance limit is equal to the minimum level (ML) of the test method used as listed in Appendix VI (ie 05 ug1 for Method 608 or 000005 ug1 when Method 1668a is approved)

10 Hardness Cadmium Chromium III Copper Lead Nickel Silver and Zinc are Hardness Dependent

11 Minimum Level (ML) is the lowest level at which the analytical system gives a

recognizable signal and acceptable calibration point for the analyte The ML represents the lowest concentration at which an analyte can be measured with a known level of confidence The ML is calculated by multiplying the laboratoryshydetermined method detection limit by 318 (see 40 CFR Part 136 Appendix B)

12pH sampling for compliance with permit limits may be performed using field

methods as provided for in EPA test Method 1501

13 Temperature sampling per Method 1701

7

CDW CONSULTANTS INC CIVIL amp ENVIRONMENTAL ENGINEERS

June 22 2015

US Environmental Protection Agency 5 Post Office Square Suite 100 Mail Code OEP06-4 Boston MA 02109-3912 ATTN Remediation General Permit NOI Processing

Re Notice of Intent for Remediation General Permit 145-155 Beech Street Chelsea MA CDW Project 143500

To Whom It May Concern

CDW Consultants Inc (CDW) is submitting this Notice of Intent (NOI) on behalf of Lawrenceville LLC for a Remediation General Permit (RGP) under EPArsquos National Pollutants Discharge Elimination System (NPDES) program The RGP is required to discharge groundwater encountered during construction activities for development of a new hotel at the above-referenced site

Construction activities will take place on approximately 18 acres consisting of three parcels at 145-155 Beech Street Chelsea MA The Site is bounded to the north by Carter Street to the west by Beech Street and to the south and east by State Highway Route 1 owned by the Massachusetts Department of Transportation (MassDOT) The property is listed as a disposal site under the Massachusetts Contingency Plan (MCP) regulations

In December 1999 the Massachusetts Department of Environmental Protection (MassDEP) issued Release Tracking Number (RTN) 3-017917 as a result of releases of oil or hazardous materials on the property The primary contaminant of concern in soil is polychlorinated biphenyls (PCBs) with secondary contaminants consisting of volatile organic compounds (VOCs) petroleum-related compounds and heavy metals Some of these contaminants have also been detected at low concentrations in the groundwater All of the contaminants identified in soil and groundwater are likely related to prior use of the property for the cleaning and re-painting of chemical storage drums in preparation for reuse by the former American Barrel Company (ldquoABCrdquo)

In addition to the NOI application form we have attached Figure 1 Water Flow Schematic Figure 2 Dewatering Treatment System

40 Speen Street Suite 301 Framingham MA 01701 508-875-2657 FAX 508-875-6617 wwwcdwconsultantscom

Page 2

Figure 3 MassDEP Priority Resource Map Documentation of the Results of the ESA Eligibility Determination Endangered Species Act Documentation StreamStats Flow Statistics Report Massachusetts Cultural Resource Information Report ESS Laboratory Analytical Data Report

Please call if you have any further questionsshy

Very truly yoursshyCDW CONSULTANTS INCshy

Kathleen Campbell PE LSP LEED APshyVice Presidentshy

cc Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

NPDES Permit No MAG9l0000 NPDES Permit No NHG9 10000

B Suggested Form for Notice of Intent (NOD for t be Remediation General Permit

1 General facilitysite information Please provide the following information about the site

a) Name offacilitysite l145-155 Beech St Chelsea Facilitysite mailing address

Location of facility site Facility SIC Street 1145-155 Beech St code(s) longitudeJ -71039 I vacant

latitudel43399 I I b) Name of facilitysite owner Lawrenceville LLC Town(Chelsea

Email address of facilitv site owner State Zip County i( mstebbinsproconinccom

I 02150 Isuffolk IMA Telephone no of faci litysite ownerl603-623-881 1 I

Fax no of facilitysite ownerl Owner is (check one) 1 Federal__Q_ 2 StateIribal_Q_ 3 Private bull 4 Other 0 if so describe

Address of owner (if different from site)

Street 1359 Hooksett Rd

Town Hooksett State II NH Zip ~ 03106 ICountyl Merrimack

c) Legal name of operator Operator telephone no 1603-623-881 1 Lawrenceville LLC 1Operator email mstebbinsproconinccom Operator fax no f

Operator contact name and title IMark R Stebbins

Address of operator (ifdifferent from Street owner)

I

Town Statel Zipl ICounty (

I

Remediation General Pennit Page lO of22 Appendix V - NOI

----

I

NPDES Permit No MAG910000 NPDES Permit No NHG910000

d) Check Y for yes or N for no for the following 1 Has a prior NPDES permit exclusion been granted for the discharge Y~ N~ ifY numberl 2 Has a prior NPDES application (Form 1 amp 2C) ever been filed for the discharge Y 0 N~ ifY date and tracking I I 3 Is the discharge a new discharge as defined by 40 CFR 1222 Y bull N 0 4 For sites in Massachusetts is the discharge covered under the Massachusetts Contingency Plan (MCP) and exempt from state permitting Y ~ N 0

e) Is sitefacility subject to any State permitting license f) Is the sitefacility covered by any other EPA permit including or other action which is causing the generation of 1 Multi-Sector General Permit Y 0 N~ discharge Y 0 N bull ifY numbed I IfY please list l site identification assigned by the state ofNH or

2 Final Dewatering General Permit Y 0 ifY numbed I -

N bull -

MA IRTN3-17917

2 permit or license assignedJ I

II

3 EPA Construcfon General Pennit Y~N ifY number I

bull

3 state agency contact information name location and telephone number

4 Individual NPDES permit Y 0 ifY numberl I

N~

5 any other water qrljty related individual or general permit Y 0 N~ ifY number I

g) Is the sitefacility located within or does it discharge to an Area of Critical Environmental Concern (ACEC) Y 0 N bull

h) Based on the facilitysite information and any historical sampling data identifY the sub-category into which the potential discharge falls Activitv Category Activitv Sub-Categorv I - Petroleum Related Site Remediation A Gasoline Only Sites _Q_

B Fuel Oils and Other Oil Sites (including Residential Non-Business Remediation Discharges) -rl_ C Petroleum Sites with Additional Contamination D

II - Non Petroleum Site Remediation A Volatile Organic Compound (VOC) Only Sites _D_ B VOC Sites with Additional Contamination D C Primarily Heavy Metal Sites D - shy

ill - Contaminated Construction Dewatering A General Urban Fill Sites 0 B Known Contaminated Sites EJ

Remediation General Permit Page II of22 Appendi- V- NOI

PDES Permit No MAG910000 ~PDES Permit No NHG9l0000

IV - Miscellaneous Related Discharges A Aquifer Pump Testing to Evaluate Formerly Contaminated Sites _D_ B Well DevelopmentRehabilitation at ContaminatedFormerly Contaminated Sites D C Hydrostatic Testing ofPipelines and Tanks __0_ D Long-Term Remediation ofContaminated Sumps and Dikes jJ_ E Short-term Contaminated Dredging Drain Back Waters (if not covered by 401 404 permit) D

pound 2o middot lSCh arge m ormation PI ease prov1 e dd ormation a bout the discharge (attachinga l 1t10na h s ) eets as necessary 1 dme u mg

a) Describe the discharge activities for which the ownerapplicant is seeking coverage Discharge related to construction dewatering activities

b) Provide the following information about each discharge

l) Number of discharge 2) middotwhat is the maximum and average flow rate of discharge (in cubic feet per second ff s) points Max flowl 0023 IIs maximum flow a design value Y _Q_ N~

2 Average flow (include units)fs gpm lis average flow a design value or estimate~ estimate I 3) Latitnde and 1onqitudE ofeach discharae within 100 feet

42398031 -71038338 -71039374 pt I lat long pt2 lat 42399656 long pt3 lat long pt4 lat long

I ~ pt5 lat long pt6 lat long pt7 lat lona pt8 lat long etc

4) If hydrostatic testing 5) ls the discharge intermittent ~ or seasonal_Q_ total volume ofre Is discharge ongoing Y __Q N bull discharge (gals)~ I

c) Expected dates of discharge (mmddyy ) startl 061012015 lend[ 10t1t2015 I d) Please attach a line drawing or flow schematic showing water flow through the facility including

L l sources of intake wMer ~on middot ~ flow from the oneration 3 treatment units and 4 dischane noints and ~rin~ ~

waters(s)JSee Figure 1 amp Figure 3

Remediation General Permit 2 of22 Appendix V - NOI

NPDES Permit No 1AG9l 0000 NPDES Permit No J HG9l 0000

3 Contaminant information a) Based on the sub-category selected (see Appendix III) indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

Parameter CAS

Number Believed Absent

Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof

Maximum daily value Aver~e dailv value

concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod

l T oral Suspended Solids (TSS) 0 El 1 grab 25400 5000 ugll 316000 172 316000 8 6

2 Total Residual Chlorine (TRC) 8 D 3 Total Petroleum Hydrocarbons (TPH) 8 D

4 Cyanide (CN) 57125 rJ D 5 Benzene (B) 7 l 432 8 D 6 Toluene (T) 108883 8 D 7 Ethylbenzene (E) 100414 8 D 8 (mpo) Xylenes (X) l08883

l06423 95476

1330207

El D

9 Total BTEX 2 nla 8 D 10 Ethylene Dibromide (EDB) ( 12shyDibromoethane) 3

106934

IE] D I

l l Methyl-tert-Butyl Ether (oitBE)

1634044 EJ D I

12 tert-Butyl Alcohol (TBA) Tertiary-Butanol)

75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004

Numbering system is provided to allow cross-referencing to Effluent Limits and Monitoring Requirements by Sub-Category included in Appendix ill as well as the Test Methods and Minimum Levels associated with each parameter provided in Appendix VI ~ BTEX =Sum of Benzene Toluene Ethylbenzene total Xylenes 3 EDB is a groundwater contaminant at fuel spill and pesticide application sites in New England

Remediatton General Pennir Page 13 of 22 Appendix V - NOI

NPDES Permit No MAG9 10000 NPDES Permit No NHG9 10000

Minimum Maximum dafuo value Average dailv value SamQle Analvticat Level CAS Believed Believed of Twe Method

Parameter (MLof concentration ~ concentration mus Number Absent Present Samples ~ Used Test ygffi OgU gill grab) method) ow

Method 13 lert-Amyl Methyl 9940508 Ether (TluvlE) rJ Ll l4Naphthalene 9 1203 EJ D 15 Carbon Tetrachloride 56235 [] D 16 l 2 Dichlorobenzene 95501 I EJ D I (o-DCB)

17 13 Dichlorobenzene 541731 rJ D (m-DCB)

18 14 Dichlorobenzene 106467 pound] (p-DCB) D

18a Total 13 D dichloro[)enzene

19 l l Dichloroethane 75343 pound] (DCA) D

20 12 Dichloroethane 107062 EJ D ( DCA)

2 1 I l Dichloroethene 75354 G D (DCE)

22 cis-12 Dichloroetbene 156592 G D (DCE)

23 Methylene Chloride 75092 EJ I D 24 Tetrachloroelhene 127 184 (PCE) G D 25 1 11 Trichloro-ethane 71556 (TCA) G D

I

26 I l 1 Trichloro-ethane 79005 (TCA) El 0

I

27 Trichloroethene 79016 rJ D (TCE) I

Remediation General Permit Page 14 of22 Appendix V -NOt

NP DES Permit No MAG9IOOOO NPDES Permit No NHG910000

Parameter CAS Number

Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of

Maximum daily vatue Average dailv value

concentration gill

mass ow

concentration ruill

mass OYtlTest

Method 28 Vinyl Chloride (Chloroethene)

75014 rJ D I

29 Acetone 67641 El D

30 14 Dioxane 123911 D rJ 1 grab 82700 5ugL 7 0 00004 70 0 0002

31 Total Phenols 108952 [] D I 32 Pentachlorophenol (PCP)

87865 rJ D i

33 Total Pbtha1ates (Phthalate esters) ~ rJ D I

34 Bis (2-Ethylhexyl) Phthalate [Dishy(ethylbexyl) Phthalate]

117817

rJ D


rJ D I

a Benzo(a) Anthracene 56553 [I D I b Benzo(a) Pyrene 50328 rl D I c Benzo (b)Fiuoranthene 205992

pound] D I d Benzo(k) Fluoranthene 207089 rJ D e Chrysene 21801 EJ D f Dibenzo(ah)anthracene 53703

rJ D g lndeno( 123-cd) Pyrene

193395 El D

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

pound] D

4 The sum of individual phthalate compounds

Remediation General Permit Page 15 of 22 Appendix V- NOl

NPDES Permit No MAG9IOOOO NPDES Permit No --JHG910000

Parameter CAS N umber

Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof

M aximum dailv value Averfe dailv value

concentration lgffi

~ fg

concentration giD

mass

~Test Method

h Acenaphthene 83329 El D i Acenaphthylene 208968 El D j Anthracene 1201 27 El D k Benzo(ghi) Perylene 191242 El D I F1uoranthene 206440 El D I

m Fluorene 86737 G D I

n Naphthalene 91203 El D o Phenanthrene 85018 El D p Pyrene 129000 El D

37 Toml Polychlorinated Biphenyls (PCBs)

85687 84742 I 17840 84662 131113 117817

El D

38 Chloride 16887006 D El 1 grab 3000 0 1 ugiL 2320000 126 2320000 63

39 Antimony 7440360 El D 40 Arsenic 7440382 El D 4 1 Cadmium 7440439 El 0 42 Chromium m (trivalent) 16065831

El I 0 43 Chromium VI (hexavalent) 18540299 El D 44 Copper 7440508 D El 1 grab 6010C 15 ugJL 74 00004 74 0002

45 Lead 7439921 8 D 46 Mercury 7439976 pound] D 47 Nickel 7440020 El D 48 Selenium 7782492 8 D

49 Silver I 7440224 8 D 50 Zinc 7440666 8 D 51 lron 7439896 D [) 1 grab 6010C 20 ugL 19700 11 19700 05

Other (describe) D D Remediation General Permit Page 16 of22 Appendix V - NOI


Parameter CAS

Number Believed Believed of

Samoles

Sam(le Inpound (eg bullbull grab)

Analvtical Method

Minimum Level

ltMLof

1laximum dailV value Average daitv oalue

concentration gill

mass ~

concentration gill

mass flgtl

Absent Present Used (method) Test

llethod I

D D I

D D

tsc arges w ere metaIs are bred present p ease fil1 out t e o owmg (attac resu ts of any ca c atlons b) F or d h h e 1ev 1 h fi ll h 1 ul )

Step 1 Do any ofthe metals in the influent exceed the effluent limits in Ifves which metals Appendix ill (ie the limits set at zero dilution) Y ~N__pound___ copper iron

Step 2 For any metals which exceed the Appendix m limits calculate the Look up the limit calculated at the corresponding dilution dilution factor (DF) using the formula in Part IA3 c (step 2) of the NOI factor in Appendix IV Do any of the metals in the instructions or as determined by the State prior to the submission ofthis NOI influent have the potential to exceed the corresponding What middot s the dilution factor for ar plicable metals effluent limits in Appendix IV (ie is the influent Metal copper DF 19 concentration above the limit set at the calculated dilution Metal Metal

DF DF

factor) y eN 0 lfY list which metalsiron 19

Metal DF copper iron Etc

4 T t t t _fi 1 d r ea men middot sys em m orma ti on Pl ease descn e t e treatment svstem usm g separatesheets as necessary me u rng

a) A description of the treatment system including a schematic of the proposed or existing treatment system A pump will be utilized to the transport groundwater generated from construction dewatering activities to a frac tank The groundwater will the n pass through a 20-micron bag filter prior to discharge to catch basins along Beech Street and Carter Street Carbon treatment may also be employed for additional treatment following the bag filter Influe nt samples will be collected prior to the frac tank a nd effluent samples will be collected after the bag filter and carbon treatment (if utilized) See Figure 2 for a flow diagram of the proposed treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank El Air stripper D Oilwater separator D IEqualization tanks ol Bag filter[] IGAC filter El

Chlorination D

De-chlorination 0

Other (please describe)

Remediatton General Permit Page 17 of22 Appendix V - NOl

~PDES Permit No MAG9LOOOO NPDES Permit No ~HG9l 0000

c) Proposed average and matimum Oow rates (gallons per minute) for the discharge and the design Oow rate(s) (gallons per minute) of the treatment system Average flow rate ofdischargJ 5 lgpm Maximum flow rate oftreatment systerrJ 10 lgpm

Design flow rate of treatment system Is lgpm

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

-t R ace waters eceiVIng su rf ( ) Pl ease proVIde intionnanon a bout the receiVIng water s usmg ( ) separatesheets as necessary

a) Identify the discharge pathway Direct to Within facility Storm Wetlands D ftbeamp desccibe~---recetvmg (sewer) _Q_ drain El ~ water 0

b) Provide a narrative description of the discharae pathwav includin_g the name(s) of the receiving waters Catch Basins on Beech St ampCarter St to culvert into Island End River to Mystic River to Boston Inner Harbor

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water See Figure 1 amp Figure 3

1 For multiple discharges number the discharges sequentially 2 For indirec t dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus ofnearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving wateJSB(CSO) I e) Provide the reported or calculated seven day-ten year low flow (7Ql0) ofthe receiving water J o0204 lcfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303( d) water quality impaired or limited water Y 0 Ne Ifyes for which pollutant(s) Enterococcus Fecal Coliform Dissolved Oxygen PCB in fish tissue I

Is there a fma l TMDL Y 0 N bull Ifyes for which pollutant(s) r I

Remediation General Permit Page t8 of22 Appendix V - NOI

WDES Permit No MAG91 0000 NPDES Permit No NHG910000

6 ESA and NHPA Eligibility Please provide the following information according to requirements ofPermit Parts LA4 and IA5 Appendices II and VII

a) Using the instructions in Appendix VII and information on Appendix II under which criterion listed in Part LC are you eligible for coverage under this general permit A__ B _Q_ C _Q_ D __Q_ E _Q_ F _Q_ b) If you selected Criterion D or F has consultation with the federal services been completed Y__Q N___QUnderway_Q_

c) Ifconsultation with US Fish and Wildlife Service andor NOAA Fisheries Service was completed was a written concurrence finding that the discharge is not likely to adversely affect listed species or critical habitat received Y ~ N~

middot d) Attach documentation ofESA eligibility as described in the NOI instructions and required by Appendix VII Part LC Step 4

e) Using the instructions in Appendix VII under which criterion listed in Part ILC are you eligible for coverage under this general permit 1 bull 2 0 3 0

f) If Criterion 3 was selected attach all wTitten correspondence with the State or Tribal historic preservation officers including any terms and conditions that outline measures the applicant must follow to mitigate or prevent adverse effects due to activities regulated by the RGP

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Pennit Page 19 of22 Appendix Y - NOi

NPDES Permit No MAG91 0000 NPDES Permit No t HG910000

8 Signature Requirements The Notice oflntent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty oflaw that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the infomration submitted Based on my inquiry ofthe person orpersons who manage the system or those persons directly responsible for gathering the infonnation I certify that the information submitted is to the best ofmy knowledge and beliet true accurate and complete I certify that I am aware that there are significant penalties for submittingfalse information including the possibility offine and imprisonmentfor knowing violations

FacilitySite Namel145-155 B ech St Chelsea

I

1-r-N~Operator signature

Printed Name ampTitlei Mark R Stebbins Managing Member

Date~ 622115

r

I

Remediation General PenniE Page 20 of22 Appendix V - NOI

Page

1 o

f 51

l J

DISCHARGE PT 1

GRAPHIC SCALE 50 0 25 50 100

~-~~~ -- I I I IN FEET )

1 INCH = 50 FT

APPROXIMATE POSSIBLE TREATMENT UNIT LOCATIONS

200

I

NOTES ALL SOIL TESTING PERFORMED ABOVE FABRIC

~- LIMITS OF CONSTRUCTION amp AREA OF POTENTIAL CONSTRUCTION DEWATERING SOURCE OF INTAKE WATER

DISCHARGE PT 2

SEAL

DATE November 11 2014 DRAWN ESW scLpound = so

u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(

~~ L[)lt( L[) w ~Cfl

J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC

40 SPEEN STREETSUITE 301FRAMINGHAM MA 01701

Groundwater Generated from Construction Dewatering

Frac Tank

Possible Carbon Treatment

Catch Basin

Influent Sample

Effluent Sample

20-micron Bag Filter

CDW Consultants Inc

Figure 2

Dewatering Treatment System 145-155 Beech Street

Chelsea MA

Page 2 of 51

MassDEP - Bureau of Waste Site CleanupSite Information Phase 1 Site Assessment Map 500 feet amp 05 Mile Radii 145-155 BEECH ST CHELSEA MA The information shown is the best available at the NAD83 UTM Meters date of printing However it may be incomplete The 5220934mN -7908023mE (Zone 18) responsible party and LSP are ultimately responsible May 22 2015 for ascertaining the true conditions surrounding the

site Metadata for data layers shown on this map can be found athttpwwwmassgovmgis

500 m

1000 ft

MassDEP Phase 1 Site Assessment Map Page 1 of 1

httpmapsmassgisstatemausimagesdepmcpmcphtm 5222015 Page 3 of 51

LKonetzny
Text Box
Figure 3 - MassDEP Priority Resource Map13
LKonetzny
Polygon Line
LKonetzny
Callout
Approximate Site Boundaries13
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout
Discharge to13Receiving Water13

Documentation of the Results of the ESA Eligibility Determination

Using Appendix VII and information in Appendix II of the NPDES RGP the 145-155 Beech St Chelsea project is eligible for coverage under this general permit under Criterion A Chelsea is located in Suffolk County and there are no Endangered Species in Suffolk County according to the Federally Listed Endangered and Threated Species in Massachusetts List Updated 192015 available on the US Fish amp Wildlife Service New England Field Office webpage The 145-155 Beech St Chelsea project is located within 16 of a mile of Everett Everett is located in Middlesex County and there are no Endangered Species in Middlesex County according to the Federally Listed Endangered and Threated Species in Massachusetts List Updated 192015 A copy of the Federally Listed Endangered and Threated Species in Massachusetts List Updated 192015 is attached No designated critical habitats were listed in Suffolk or Middlesex County

An Endangered Species Consultation per the attached instructions which were provided on US Fish amp Wildlife Service New England Field Office webpage was conducted for the following species The Northern Long-eared Bat was listed as ldquoProposed Endangeredrdquo in both counties statewide The Red Knot was listed as ldquoThreatenedrdquo in Suffolk County

The small whorled Pogonia listed as threated in Middlesex County was not evaluated because it is only listed in the Town of Groton The Piping Plover listed as threated in Suffolk County was not evaluated because it is only listed in the Towns of Revere and Winthrop The habitat for the Northern Long-eared Bat is described as mines and caves and a wide variety of forested habitats these habitats are not present within miles of the project The habitat for the Red Knot is described as coastal beaches and rocky shores sand and mud flats these habitats are not present within miles of the project Based on this evaluation no endangered or threatened species or their designated critical habitat are likely to occur in proximity to the storm water discharges or discharge related activities

Page 4 of 51

FEDERALLY LISTED ENDANGERED AND THREATENED SPECIES IN MASSACHUSETTS

COUNTY SPECIES FEDERAL

STATUS GENERAL LOCATIONHABITAT TOWNS

Barnstable

Piping Plover Threatened Coastal Beaches All Towns

Roseate Tern Endangered Coastal beaches and the Atlantic Ocean All Towns

Northeastern beach

tiger beetle Threatened Coastal Beaches Chatham

Sandplain gerardia Endangered Open areas with sandy soils Sandwich and Falmouth

Northern Red-

bellied Cooter Endangered Inland Ponds and Rivers Bourne (north of the Cape Cod Canal)

Red Knot1

Threatened Coastal Beaches and Rocky Shores sand

and mud flats Coastal Towns

Northern Long-

eared Bat

Proposed

Endangered

Winter- mines and caves Summer ndash wide

variety of forested habitats Statewide

Berkshire

Bog Turtle Threatened Wetlands Egremont and Sheffield

Northern Long-

eared Bat

Proposed

Endangered



Bristol

Piping Plover Threatened Coastal Beaches Fairhaven Dartmouth Westport

Roseate Tern Endangered Coastal beaches and the Atlantic Ocean Fairhaven New Bedford Dartmouth

Westport

Northern Red-

bellied Cooter Endangered Inland Ponds and Rivers Taunton

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach

tiger beetle Threatened Coastal Beaches Aquinnah and Chilmark

Sandplain gerardia Endangered Open areas with sandy soils West Tisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened

Forests with somewhat poorly drained

soils andor a seasonally high water table Gloucester Essex and Manchester

Piping Plover Threatened Coastal Beaches

Gloucester Essex Ipswich Rowley

Revere Newbury Newburyport and

Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern

bulrush Endangered Wetlands Montague Warwick

Dwarf

wedgemussel Endangered Mill River Whately

Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened


soils andor a seasonally high water table Hadley

Puritan tiger beetle Threatened Sandy beaches along the Connecticut

River Northampton and Hadley

Dwarf

wedgemussel Endangered Rivers and Streams Hatfield Amherst and Northampton

Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened


soils andor a seasonally high water table Southwick

Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened


soils andor a seasonally high water table Groton

Northern Long-

eared Bat

Proposed

Endangered



Nantucket

Piping Plover Threatened Coastal Beaches Nantucket

Roseate Tern Endangered Coastal beaches and the Atlantic Ocean Nantucket

American burying

beetle Endangered Upland grassy meadows Nantucket

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51




Piping Plover Threatened Coastal Beaches Scituate Marshfield Duxbury Plymouth

Wareham and Mattapoisett

Northern Red-

bellied Cooter Endangered Inland Ponds and Rivers

Kingston Middleborough Carver

Plymouth Bourne Wareham Halifax

and Pembroke

Plymouth Roseate Tern Endangered Coastal beaches and the Atlantic Ocean

Plymouth Marion Wareham and

Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Piping Plover Threatened Coastal Beaches Revere Winthrop

Suffolk Red Knot

1 Threatened

Coastal Beaches and Rocky Shores sand


Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened


soils andor a seasonally high water table Leominster

Northern Long-

eared Bat

Proposed

Endangered



1Migratory only scattered along the coast in small numbers

-Eastern cougar and gray wolf are considered extirpated in Massachusetts -Endangered gray wolves are not known to be present in Massachusetts but dispersing individuals from source populations in Canada may occur statewide -Critical habitat for the Northern Red-bellied Cooter is present in Plymouth County

Updated 01092015

Page 7 of 51

StreamStats Flow Statistics Report Page 2 of 2

ft3s

ft3s

ft3s

ft3s

Statistic Value Unit Prediction Error

(percent) Equivalent years of Interval

record

90-Percent Prediction

Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max

PROBPEREN 064 dim 06 039 085 httppubsusgsgovsir20065031pdfsSIR_2006-5031revpdf (httppubsusgsgovsir20065031pdfsSIR_2006-5031revpdf) Bent_ GC_ and Steeves_ PA_ 2006_ A revised logistic regression equation and an automated procedure for mapping the probability of a stream flowing perennially in Massachusetts US Geological Survey Scientific Investigations Report 2006ndash5031_ 107 p

Bankfull Flows Streamflow Statistics

D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204

httppubsusgsgovwriwri004135 (httppubsusgsgovwriwri004135) Ries_ KG_ III_ 2000_ Methods for estimating low-flow statistics for Massachusetts streams US Geological Survey Water Resources Investigations Report 00-4135_ 81 p

Probability of Perennial Flow Streamflow Statistics

httppubsusgsgovsir20135155 (httppubsusgsgovsir20135155)Bent_ GC_ and Waite_ AM_ 2013_ Equations for estimating bankfull channel geometry and discharge for streams in Massachusetts US Geological Survey Scientific Investigations Report 2013ndash5155_ 62 p_

Accessibility FOIA Privacy Policies and Notices US Department of the Interior | US Geological Survey

URL httpssdevcrusgsgovv3_betaFTreporthtm Page Contact Information StreamStats Help Streamstats Status NewsIntroduction Application Information Page Last Modified 03102015 114525

httpssdevcrusgsgovv3_betaFTreporthtmstate=MAampworkspaceID=MA20150508104 582015 Page 8 of 51

US Fish amp Wildlife Service

145-155 Beech Street Chelsea MA IPaC Trust Resource Report Generated May 27 2015 0154 PM MDT

Page 9 of 51

IPaC Trust Resource Report SVSUA-3PSY5-EL7GU-QQDKY-ERWPZM


IPaC Trust Resource Report

Project Description NAME

145-155 Beech Street Chelsea MA

PROJECT CODE

SVSUA-3PSY5-EL7GU-QQDKY-ERWPZM

LOCATION

Suffolk County Massachusetts

DESCRIPTION

No description provided

US Fish amp Wildlife Contact Information Species in this report are managed by

New England Ecological Services Field Office 70 Commercial Street Suite 300 Concord NH 3301-5094 (603) 223-2541

Endangered Species Proposed candidate threatened and endangered species that are managed by the Endangered Species Program and should be considered as part of an effect analysis for this project

Birds Red Knot Calidris canutus rufa Threatened

CRITICAL HABITAT

No critical habitat has been designated for this species

httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0DM

05272015 0154 IPaC Information for Planning and Conservation Page 2 Version 2019 Page 10 of 51


Critical Habitats Potential effects to critical habitat(s) within the project area must be analyzed along with the endangered species themselves

There is no critical habitat within this project area



Migratory Birds Birds are protected by the Migratory Bird Treaty Act and the Bald and Golden Eagle Protection Act

Any activity which results in the take of migratory birds or eagles is prohibited unless authorized by the US Fish and Wildlife Service ( ) There are no provisions for1 allowing the take of migratory birds that are unintentionally killed or injured

You are responsible for complying with the appropriate regulations for the protection of birds as part of this project This involves analyzing potential impacts and implementing appropriate conservation measures for all project activities

American Oystercatcher Haematopus palliatus Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0G8

American Bittern Botaurus lentiginosus Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0F3

Bald Eagle Haliaeetus leucocephalus Bird of conservation concern Year-round httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B008

Black-billed Cuckoo Coccyzus erythropthalmus Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0HI

Blue-winged Warbler Vermivora pinus Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0JY

Canada Warbler Wilsonia canadensis Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0LL

Hudsonian Godwit Limosa haemastica Bird of conservation concern Season Migrating httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0JM

Least Bittern Ixobrychus exilis Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0JW

Peregrine Falcon Falco peregrinus Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0FU

Pied-billed Grebe Podilymbus podiceps Bird of conservation concern Season Breeding httpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0JQ


SVSUA-3PSY5-EL7GU-QQDKY-ERWPZMIPaC Trust Resource Report

05272015 0154 Page 5 Information for Planning and ConservationIPaCVersion 2019

Prairie Warbler Dendroica discolor Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0K4

Purple Sandpiper Calidris maritima Bird of conservation concernSeason WinteringhttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0L1

Saltmarsh Sparrow Ammodramus caudacutus Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0MY

Seaside Sparrow Ammodramus maritimus Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0N0

Short-eared Owl Asio flammeus Bird of conservation concernSeason WinteringhttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0HD

Snowy Egret Egretta thula Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0LC

Upland Sandpiper Bartramia longicauda Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0HC

Wood Thrush Hylocichla mustelina Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0IB

Worm Eating Warbler Helmitheros vermivorum Bird of conservation concernSeason BreedinghttpsecosfwsgovspeciesProfileprofilespeciesProfileactionspcode=B0II

Page 13 of 51



RefugesAny activity proposed on National Wildlife Refuge lands must undergo a CompatibilityDetermination conducted by the Refuge If your project overlaps or otherwise impacts aRefuge please contact that Refuge to discuss the authorization process

There are no refuges within this project area

Page 14 of 51



WetlandsImpacts to NWI wetlands and other aquatic habitats from your project may be subject toregulation under Section 404 of the Clean Water Act or other StateFederal Statutes

Project proponents should discuss the relationship of these requirements to their projectwith the Regulatory Program of the appropriate US Army Corps of Engineers District

DATA LIMITATIONS

The Services objective of mapping wetlands and deepwater habitats is to producereconnaissance level information on the location type and size of these resources Themaps are prepared from the analysis of high altitude imagery Wetlands are identifiedbased on vegetation visible hydrology and geography A margin of error is inherent inthe use of imagery thus detailed on-the-ground inspection of any particular site mayresult in revision of the wetland boundaries or classification established through imageanalysis

The accuracy of image interpretation depends on the quality of the imagery theexperience of the image analysts the amount and quality of the collateral data and theamount of ground truth verification work conducted Metadata should be consulted todetermine the date of the source imagery used and any mapping problems

Wetlands or other mapped features may have changed since the date of the imagery orfield work There may be occasional differences in polygon boundaries or classificationsbetween the information depicted on the map and the actual conditions on site

DATA EXCLUSIONS

Certain wetland habitats are excluded from the National mapping program because ofthe limitations of aerial imagery as the primary data source used to detect wetlandsThese habitats include seagrasses or submerged aquatic vegetation that are found inthe intertidal and subtidal zones of estuaries and nearshore coastal waters Somedeepwater reef communities (coral or tuberficid worm reefs) have also been excludedfrom the inventory These habitats because of their depth go undetected by aerialimagery

DATA PRECAUTIONS

Federal state and local regulatory agencies with jurisdiction over wetlands may defineand describe wetlands in a different manner than that used in this inventory There is noattempt in either the design or products of this inventory to define the limits ofproprietary jurisdiction of any Federal state or local government or to establish thegeographical scope of the regulatory programs of government agencies Personsintending to engage in activities involving modifications within or adjacent to wetlandareas should seek the advice of appropriate federal state or local agencies concerningspecified agency regulatory programs and proprietary jurisdictions that may affect suchactivities

Wetland data is unavailable at this time

Page 15 of 51

Flow Statistics Ungaged Site ReportDate Fri May 8 2015 124534 PM GMT-4Site Location MassachusettsNAD 1983 Latitude 423942 ( 42 23 39)NAD 1983 Longitude -710498 (-71 03 00)Drainage Area 0095 mi2

Low Flows Basin Characteristics

100 Statewide Low Flow WRIR00 4135 (0095 mi2)

Regression Equation Valid

Parameter Value Range

Min Max

Drainage Area (square miles)0095 (below min value

161)161 149

Mean Basin Slope from 250K DEM (percent) 0350 032 246

Stratified Drift per Stream Length (square mile per mile)

502 (above max value 129)

0 129

Massachusetts Region (dimensionless) 0 0 1

Warning Some parameters are outside the suggested range Estimates will be extrapolations with unknown errors

Probability of Perennial Flow Basin Characteristics

100 Perennial Flow Probability (0095 mi2)

Parameter ValueRegression Equation Valid Range

Min Max

Drainage Area (square miles) 0095 001 199

Percent Underlain By Sand And Gravel (percent) 766 0 100

Percent Forest (percent) 000 0 100


Bankfull Flows Basin Characteristics

100 Bankfull Statewide SIR2013 5155 (0095 mi2)



Min Max


06)06 329

Mean Basin Slope from 10m DEM (percent)

0986 (below min value 22)

22 239


Low Flows Streamflow Statistics

90-Percent Prediction Prediction Error Equivalent years of

Statistic Value Unit Interval(percent) record

Min Max

D50 00866 ft3s

D60 00788 ft3s

Page 1 of 2StreamStats Flow Statistics Report

582015httpssdevcrusgsgovv3_betaFTreporthtmstate=MAampworkspaceID=MA20150508104Page 16 of 51

Get Results in Report Format

PDF SpreadsheetBelow are the results of your search using the following search criteriaTown(s) ChelseaStreet Name BeechResource Type(s) Area Building Burial Ground Object StructureFor more information about this page and how to use it click here

No Results Found

MHC Home | MACRIS Home

Page 17 of 51

ESS LaboratoryDivision of Thielsch Engineering Inc

BAL Laboratory The Microbiology Division of Thielsch Engineering Inc

CERTIFICATE OF ANALYSIS

Lauren Konetzny

CDW Consultants Inc

40 Speen Street Suite 301

Framingham MA 01701

RE Beech St Chelsea (1435)

ESS Laboratory Work Order Number 1505115

This signed Certificate of Analysis is our approved release of your analytical results These results are

only representative of sample aliquots received at the laboratory ESS Laboratory expects its clients to

follow all regulatory sampling guidelines Beginning with this page the entire report has been paginated

This report should not be copied except in full without the approval of the laboratory Samples will be

disposed of thirty days after the final report has been delivered If you have any questions or concerns

please feel free to call our Customer Service Department

Laurel Stoddard

Laboratory Director

Analytical Summary

The project as described above has been analyzed in accordance with the ESS Quality Assurance Plan

This plan utilizes the following methodologies US EPA SW-846 US EPA Methods for Chemical

Analysis of Water and Wastes per 40 CFR Part 136 APHA Standard Methods for the Examination of

Water and Wastewater American Society for Testing and Materials (ASTM) and other recognized

methodologies The analyses with these noted observations are in conformance to the Quality Assurance

Plan In chromatographic analysis manual integration is frequently used instead of automated

integration because it produces more accurate results

The test results present in this report are in compliance with NELAC Standards A2LA andor client

Quality Assurance Project Plans (QAPP) The laboratory has reviewed the following Sample

Preservations Hold Times Initial Calibrations Continuing Calibrations Method Blanks Blank Spikes

Blank Spike Duplicates Duplicates Matrix Spikes Matrix Spike Duplicates Surrogates and Internal

Standards Any results which were found to be outside of the recommended ranges stated in our SOPs

will be noted in the Project Narrative

185 Frances Avenue Cranston RI 02910-2211 Tel 401-461-7181 Fax 401-461-4486 httpwwwESSLaboratorycomDependability diams Quality diams Service

Page 18 of 51

SMorrell
Reviewed


Client Name CDW Consultants IncClient Project ID Beech St Chelsea ESS Laboratory Work Order 1505115

SAMPLE RECEIPT

The following samples were received on May 06 2015 for the analyses specified on the enclosed Chain of Custody Record

The samples and analyses listed below were analyzed in accordance with the 2010 Remediation General Permit (RGP) under the

National Pollutant Discharge Elimination System (NPDES)

Lab Number Sample Name Matrix Analysis1505115-01 DW-1 Ground Water 4500 H+ B 4500-Cl E 6010C 7196A




Page 19 of 51



PROJECT NARRATIVE

Classical Chemistry1505115-01 The maximum holding time listed in 40 CFR Part 136 Table II for pH Dissolved Oxygen Sulfite and

Residual Chlorine is fifteen minutes

Total Residual Chlorine

No other observations noted

End of Project Narrative

DATA USABILITY LINKS

Definitions of Quality Control Parameters

Semivolatile Organics Internal Standard Information

Semivolatile Organics Surrogate Information

Volatile Organics Internal Standard Information

Volatile Organics Surrogate Information

EPH and VPH Alkane Lists




Page 20 of 51



CURRENT SW-846 METHODOLOGY VERSIONS

Prep Methods

3005A - Aqueous ICP and Graphite Furnace Digestion

3020A - Aqueous ICP MS Digestion

3050B - Solid ICP Graphite Furnace ICP MS Digestion

3060A - Solid Hexavalent Chromium Digestion

3510C - Separatory Funnel Extraction

3520C - Liquid Liquid Extraction

3540C - Manual Soxhlet Extraction

3541 - Automated Soxhlet Extraction

3546 - Microwave Extraction

3580A - Waste Dilution

5030B - Aqueous Purge and Trap

5030C - Aqueous Purge and Trap

5035 - Solid Purge and Trap

Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS

7010 - Graphite Furnace

7196A - Hexavalent Chromium

7470A - Aqueous Mercury

7471B - Solid Mercury

8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA

8270D SIM - SVOA Low Level

9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH

9045D - Solid pH (Corrosivity)

9050A - Specific Conductance

9056A - Anions (IC)

9060A - TOC

9095B - Paint Filter

MADEP 04-11 - EPH VPH




Page 21 of 51



Client Sample ID DW-1

Date Sampled 050615 1430

ESS Laboratory Sample ID 1505115-01

Sample Matrix Ground Water

Percent Solids NA

Extraction Method [CALC]

Units ugL

Total Metals

Analyte Results (MRL) MDL Method Limit DF Analyst Analyzed FV BatchIV6010C 1 1Chromium III 1 JLK [CALC]050815 1733 35 (10)




Page 22 of 51







Percent Solids NA

Classical Chemistry

Analyte Results (MRL) MDL UnitsMethod Limit DF Analyst Analyzed Batch7196A ugLHexavalent Chromium 1 JLK CE50656050615 1816 ND (10)

4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)

pH Sample Temp Aqueous pH measured in water at 154 ordmC (NA)

4500-Cl E mgLTotal Residual Chlorine 1 JLK CE50657050615 1836HT ND (001)




Page 23 of 51



Quality Control Data

Analyte Result MRL Units

Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry

Batch CE50656 - General Preparation

Blank

10 ugLHexavalent Chromium ND

LCS

10 4998 90-11099ugLHexavalent Chromium 493

LCS Dup

10 4998 2090-11099 04ugLHexavalent Chromium 495


Blank

001 mgLTotal Residual Chlorine ND

LCS

09960 85-11599mgLTotal Residual Chlorine 099




Page 24 of 51



Notes and Definitions

Z16 Aqueous pH measured in water at 154 ordmC

U Analyte included in the analysis but not detected

HT The maximum holding time listed in 40 CFR Part 136 Table II for pH Dissolved Oxygen Sulfite and Residual

Chlorine is fifteen minutes

Sample results reported on a dry weight basisRelative Percent DifferenceRPD

dryAnalyte NOT DETECTED at or above the MRL (LOQ) LOD for DoD Reports MDL for J-Flagged AnalytesND

MDLMRL

Method Detection LimitMethod Reporting Limit

IVFV

Initial VolumeFinal Volume

sect Subcontracted analysis see attached report123

Range result excludes concentrations of surrogates andor internal standards eluting in that rangeRange result excludes concentrations of target analytes eluting in that rangeRange result excludes the concentration of the C9-C10 aromatic range

Avg Results reported as a mathematical averageNR No Recovery

LOD Limit of Detection

[CALC] Calculated Analyte

LOQ Limit of Quantitation

DL Detection Limit

SUB Subcontracted analysis see attached report[2C] Result was taken from the second column Dual column analysis




Page 25 of 51



ESS LABORATORY CERTIFICATIONS AND ACCREDITATIONS

ENVIRONMENTAL

Department of Defense (DoD) Environmental Laboratory Accreditation Program (ELAP)

A2LA Accredited Testing Cert 286401

httpwwwa2laorgscopepdf2864-01pdf

Rhode Island Potable and Non Potable Water LAI00179

httpwwwhealthrigovfindlabsanalyticalESSpdf

Connecticut Potable and Non Potable Water Solid and Hazardous Waste PH-0750

httpwwwctgovdphlibdphenvironmental_healthenvironmental_laboratoriespdfOutofStateCommercialLaboratoriespdf

Maine Potable and Non Potable Water and Solid and Hazardous Waste RI0002

httpwwwmainegovdhhsmecdcenvironmental-healthwaterdwp-serviceslabcertdocumentsAllLabsxls

Massachusetts Potable and Non Potable Water M-RI002

httppublicdepstatemausLabcertLabcertaspx

New Hampshire (NELAP accredited) Potable and Non Potable Water Solid and Hazardous Waste 2424

httpdesnhgovorganizationdivisionswaterdwgbnhelapindexhtm

New York (NELAP accredited) Non Potable Water Solid and Hazardous Waste 11313

httpwwwwadsworthorglabcertelapcommhtml

New Jersey (NELAP accredited) Non Potable Water Solid and Hazardous Waste RI006

httpdatamine2statenjusDEP_OPRAOpraMainpi_mainmode=pi_by_siteampsort_order=PI_NAMEAampSelect+a+Site=58715

United States Department of Agriculture Soil Permit P330-12-00139

Pennsylvania 68-01752

httpwwwdepwebstatepausportalserverptcommunitylabs13780laboratory_accreditation_program590095

CHEMISTRY


Lead in Paint Phthalates Lead in Childrens Metals Products (Including Jewelry)

httpwwwA2LAorgdirsearchnewnewsearchcfm

CPSC ID 1141

Lead Paint Lead in Childrens Metals Jewelry

httpwwwcpscgovcgi-binlabapplistaspx




Page 26 of 51

Attachment B

Sample and Cooler Receipt Checklist SOP 10_000l

Client CDW Consultants ESS Project ID 15050115

Client Project ID --c---=--o-------ShippedDelivered Via ESS Courier

Date Project Due 5132015 Days For Project 5 Day

Items to be checked upon receipt

1 Air Bill Manifest Present I No 10 Are the samples properly preserved Yes

Air No 11 Proper sample containers used Yes

2 Were Custody Seals Present No 12 Any air bubbles in the VOA vials NA

3 Were Custody Seals Intact NA 13 Holding times exceeded No

4 Is Radiation count lt 100 CPM Yes 14 Sufficient sample volumes Yes

5 Is a cooler present Yes 15 Any Subcontracting needed ~ cooler Temp 24 16 Are ESS labels on correct containers ~ o

I Iced With Ice 17 Were samples received intact es o

6 Was COC included with samples Yes ESS Sample IDs

7 Was COC signed and dated by client Yes Sub lab--------~~~-------shy

8 Does the COC match the sample Yes Analysis ---=----------shy9 Is COC complete and correct Yes TAT~~-----------------------

18 Was there need to call project manager to discuss status If yes please explain

Wets Cc + Cc Sfl ltt -- Oc tyen--~ ~ ~ ~Its- t8VD

Who was called ________ _ By whom

Sample Number Properly Preserved Container Type of Containers Preservative

1 Yes 1 Yes

Vh _ VYI bull I Completed By-j 79 Reviewed By dtpoundY~oyC2nL

250 ml Plastic 1 500 ml Plastic 1 s(g l tO DateTime middot ~

DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51

ESS Laboratory N~O~s 1 5o5115middot

CHAIN OF CUSTODY (20( Page of Turn Time (Standard Other Division ofThielsch Engineering Inc

185 Frances Avenue Cranston RI 02910-2211 Tel (401) 461-7181 Fax (401) 461-4486 wwwesslaboratorycom

If faster than 5 days prOrpproval by laboratory is_r_e_q_u7ir-ed---

~ wher e samples were collected from f Moo RI CT NH NJ NY ME Oeher

rf11rrus lCJtY for any oflhe following MAmiddotMCP Navy USACE Orher

Co Name

rDJ Co(s__~c Project-----__- I P~ect Name lliJChar or less)

I llgt Jgt ~e~dr- 0- Clr-e~CA-lJoL I LL crco-~

Comacr Person I

La-lt -( Knfl~ ~ nv City

~-V -lt4 he Telephone ~

I ( )ot) 87lt- Jro lt ESSLAB Sample

t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol

I PO l I ~ ~ 3 ) -16 Email Address

I ~o~_~fo ltgtwcciSv 1o_c--lt-CorYmiddot Sample Identification (20 Char or less)

bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~

Tr1 I v w 1gtwmiddot-l ~ ---------

~

L ~middotrD-_( _j_ VcA 0 )

0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID

I SCS1 S Electronic Deliverable Ye No --Format ExceP-s Access_ Po(_ Other

Circle and or Write Required Analysis

~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i

l + 2 Rcsect 61~ -~ ~ ~ 6~ Ngt 00 middot 00 ~ omiddot tj ii 61-- OOJ l ~ a

bUill

Container Type SD~Solid D-Sludge WW-Waste Water GW-Ground Water SW-Surface Water DW-Drinking Water 0-0il W-Wipes F-Filters

Cooler Present _ _No ~nternal Preservation Code 1- NP 2- HCl 3- H2SOo 4- HN03 5- NaOH 6- MeOH 7- Asorbic Acid 8- ZnAcr 9-

Seals Intact Yes _No NA __ [ J Pickup Sampled by louCeJ (ct Q

CoolerTempJ4 m- J~J [ ] Technicians f-C-om-men--~-O-( -J-Oii~C-ltD---J -(Z+G-fgt-~ -~ --()-X_v_o_rypound__0_ Jl----

f-V_ I I Tl P M H bull d5 U( Relinquished by (Signature)

~~ bull PJ1 ~rrIT~ ~JfUkllfllberJD llffitJpJflfr l56Eira Received by (Signature)

RelinqamphliJ by( Sigrurc)

DateTime

J DareTime

I I 1~~ivbd ~gna~re

By circling MA-MCP client acknowledges samples were collected in accordance with MADEP CAM VII A

I (DateTime

I I JeliJquishtd by~(Slgnature) I lDateTime

I Please fax all changes to Chain of Custody in writing

Received by (Signature) DateTime

J 1 (White Lab Copy 2 (Yellow Client Receipt

102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT




Lab Number Sample Name Matrix Analysis1505204-01 North Ground Water 1664A 2540D 3000 4201 4500 CN CE 6010C

7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE

8260B Volatile Organic CompoundsBlank Spike recovery is above upper control limit (B+)CE51130-BS1

Acetone (190 70-130)

Blank Spike recovery is above upper control limit (B+)CE51130-BSD1

Acetone (177 70-130)

8270D(SIM) Semi-Volatile Organic CompoundsSurrogate recovery(ies) above upper control limit (S+)1505204-01

246-Tribromophenol (124 15-110)

Surrogate recovery(ies) below lower control limit (S-)1505204-01

2-Fluorobiphenyl (5 30-130)

Blank Spike recovery is above upper control limit (B+)CE51403-BS2

bis(2-Ethylhexyl)phthalate (162 40-140)



Continuing Calibration recovery is below lower control limit (C-)CYE0202-CCV1

Diethylphthalate (69 70-130)

8270D(SIM) Semi-Volatile Organic Compounds w Isotope DilutionContinuing Calibration recovery is above upper control limit (C+)CYE0181-CCV1

14-Dioxane-d8 (126 80-120)

Continuing Calibration recovery is above upper control limit (C+)CYE0225-CCV1

14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51



Client Sample ID North




Percent Solids NA

Extraction Method 3005A2007

Units ugL

Total Metals

Analyte Results (MRL) MDL Method Limit DF Analyst Analyzed FV BatchIV7010 50 10Antimony 02 1 KJK CE50809051315 143J 13 (20)

7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)

7470A 20 40Mercury 0120 1 RLA CE50910051115 1532 ND (0200)

6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)

7010 50 10Selenium 03 1 KJK CE50809051215 807 ND (20)

7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51







Prepared 51315 1000Analyst TAJInitial Volume 1070

Final Volume 1

Percent Solids NA

Extraction Method 3510C

Units ugL

8082A Polychlorinated Biphenyls (PCB)

Analyte Results (MRL) MDL Method Limit DF Analyzed Sequence Batch8082AAroclor 1016 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)

Recovery Qualifier Limits

30-15064 Surrogate Decachlorobiphenyl

30-15064 Surrogate Decachlorobiphenyl [2C]

30-15068 Surrogate Tetrachloro-m-xylene

30-15064 Surrogate Tetrachloro-m-xylene [2C]




Page 34 of 51







Analyst ZLCInitial Volume 5Final Volume 5

Percent Solids NA

Extraction Method 5030B

Units ugL

8260B Volatile Organic Compounds

Analyte Results (MRL) MDL Method Limit DF Analyzed Sequence Batch8260B111-Trichloroethane 02 1 CE51130CYE0137051115 1805 ND (10)

8260B112-Trichloroethane 02 1 CE51130CYE0137051115 1805 ND (10)

8260B11-Dichloroethane 02 1 CE51130CYE0137051115 1805 ND (10)

8260B11-Dichloroethene 03 1 CE51130CYE0137051115 1805 ND (10)

8260B12-Dichlorobenzene 01 1 CE51130CYE0137051115 1805J 06 (10)


8260B13-Dichlorobenzene 02 1 CE51130CYE0137051115 1805 ND (10)


8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)

8260BCarbon Tetrachloride 01 1 CE51130CYE0137051115 1805 ND (10)

8260Bcis-12-Dichloroethene 02 1 CE51130CYE0137051115 1805 ND (10)

8260BEthylbenzene 01 1 CE51130CYE0137051115 1805 ND (10)

8260BMethyl tert-Butyl Ether 03 1 CE51130CYE0137051115 1805 ND (10)

8260BMethylene Chloride 02 1 CE51130CYE0137051115 1805 ND (20)

8260BNaphthalene 02 1 CE51130CYE0137051115 1805 10 (10)

8260BTertiary-amyl methyl ether 02 1 CE51130CYE0137051115 1805 ND (10)

8260BTertiary-butyl Alcohol 100 1 CE51130CYE0137051115 1805J 147 (250)

8260BTetrachloroethene 02 1 CE51130CYE0137051115 1805 ND (10)

8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)

8260BTrichloroethene 02 1 CE51130CYE0137051115 1805 ND (10)

8260BVinyl Chloride 02 1 CE51130CYE0137051115 1805 ND (10)

8260BXylene O 01 1 CE51130CYE0137051115 1805 ND (10)

8260BXylene PM 02 1 CE51130CYE0137051115 1805 ND (20)


70-13094 Surrogate 12-Dichloroethane-d4

70-13098 Surrogate 4-Bromofluorobenzene

70-13090 Surrogate Dibromofluoromethane

70-13097 Surrogate Toluene-d8




Page 35 of 51







Prepared 51215 1920Analyst VSCInitial Volume 1070

Final Volume 1

Percent Solids NA


Units ugL

8270D(SIM) Semi-Volatile Organic Compounds w Isotope Dilution

Analyte Results (MRL) MDL Method Limit DF Analyzed Sequence Batch8270D14-Dioxane 007 1 CE51243CYE0181051315 2057 70 (02)


15-11562 Surrogate 14-Dioxane-d8




Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL

8270D(SIM) Semi-Volatile Organic Compounds

Analyte Results (MRL) MDL Method Limit DF Analyzed Sequence Batch8270D SIMAcenaphthene 004 1 CE51403CYE0202051515 1038 ND (019)

8270D SIMAcenaphthylene 003 1 CE51403CYE0202051515 1038 ND (019)

8270D SIMAnthracene 003 1 CE51403CYE0202051515 1038J 014 (019)

8270D SIMBenzo(a)anthracene 001 1 CE51403CYE0202051515 1038 006 (005)

8270D SIMBenzo(a)pyrene 001 1 CE51403CYE0202051515 1038J 003 (005)

8270D SIMBenzo(b)fluoranthene 002 1 CE51403CYE0202051515 1038J 004 (005)

8270D SIMBenzo(ghi)perylene 002 1 CE51403CYE0202051515 1038J 003 (019)

8270D SIMBenzo(k)fluoranthene 002 1 CE51403CYE0202051515 1038 ND (005)

8270D SIMbis(2-Ethylhexyl)phthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMButylbenzylphthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMChrysene 001 1 CE51403CYE0202051515 1038J 004 (005)

8270D SIMDibenzo(ah)Anthracene 002 1 CE51403CYE0202051515 1038 ND (005)

8270D SIMDiethylphthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMDimethylphthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMDi-n-butylphthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMDi-n-octylphthalate 019 1 CE51403CYE0202051515 1038 ND (234)

8270D SIMFluoranthene 002 1 CE51403CYE0202051515 1038J 009 (019)

8270D SIMFluorene 003 1 CE51403CYE0202051515 1038J 004 (019)

8270D SIMIndeno(123-cd)Pyrene 002 1 CE51403CYE0202051515 1038J 003 (005)

8270D SIMNaphthalene 004 1 CE51403CYE0202051515 1038 ND (019)

8270D SIMPentachlorophenol 030 1 CE51403CYE0202051515 1038 ND (084)

8270D SIMPhenanthrene 004 1 CE51403CYE0202051515 1038J 006 (019)

8270D SIMPyrene 002 1 CE51403CYE0202051515 1038J 006 (019)


30-13054 Surrogate 12-Dichlorobenzene-d4

15-110124 Surrogate 246-Tribromophenol S+

30-1305 Surrogate 2-Fluorobiphenyl S-

30-13075 Surrogate Nitrobenzene-d5

30-13084 Surrogate p-Terphenyl-d14




Page 37 of 51







Percent Solids NA

Classical Chemistry

Analyte Results (MRL) MDL UnitsMethod Limit DF Analyst Analyzed Batch3000 mgLChloride 1000 EEM CE51118051115 2009 2320 (500)

4201 mgLPhenols 003 1 EEM CE51242051215 1605 ND (010)

4500 CN CE ugLTotal Cyanide (LL) 18 1 JLK CE51420051415 000J 27 (50)

1664A mgLTotal Petroleum Hydrocarbon 1 JLK CE50906051215 1119 ND (5)

2540D mgLTotal Suspended Solids 1 EEM CE51124051115 1630 316 (10)




Page 38 of 51







Prepared 51315 1222Analyst JXSInitial Volume 35

Final Volume 2

Percent Solids NA

Extraction Method 5048011

Units ugL

8011 12-Dibromoethane 12-Dibromo-3-chloropropane

Analyte Results (MRL) MDL Method Limit DF Analyst Analyzed Sequence Batch801112-Dibromoethane 0005 1 JXS CE51237051315 1447 ND (0015)


30-150102 Surrogate Pentachloroethane




Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank

010 ugLAroclor 1016 ND









005000 30-1507400371 ugLSurrogate Decachlorobiphenyl

005000 30-1507800389 ugLSurrogate Decachlorobiphenyl [2C]

005000 30-1505100253 ugLSurrogate Tetrachloro-m-xylene

005000 30-1504700237 ugLSurrogate Tetrachloro-m-xylene [2C]

LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank

10 ugL111-Trichloroethane ND


10 ugL11-Dichloroethane ND

10 ugL11-Dichloroethene ND

10 ugL12-Dichlorobenzene ND




100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B

10 ugLCarbon Tetrachloride ND

10 ugLcis-12-Dichloroethene ND

10 ugLEthylbenzene ND

10 ugLMethyl tert-Butyl Ether ND

20 ugLMethylene Chloride ND

10 ugLNaphthalene ND

10 ugLTertiary-amyl methyl ether ND

250 ugLTertiary-butyl Alcohol ND

10 ugLTetrachloroethene ND

10 ugLToluene ND

10 ugLTrichloroethene ND

10 ugLVinyl Chloride ND

10 ugLXylene O ND

20 ugLXylene PM ND

2500 70-13096239 ugLSurrogate 12-Dichloroethane-d4

2500 70-130102255 ugLSurrogate 4-Bromofluorobenzene

2500 70-13090225 ugLSurrogate Dibromofluoromethane

2500 70-13097242 ugLSurrogate Toluene-d8

LCS

1000 70-13091ugL111-Trichloroethane 91


1000 70-13089ugL11-Dichloroethane 89

1000 70-13092ugL11-Dichloroethene 92

1000 70-130103ugL12-Dichlorobenzene 103




5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96

1000 70-13096ugLCarbon Tetrachloride 96

1000 70-13093ugLcis-12-Dichloroethene 93

1000 70-13090ugLEthylbenzene 90

1000 70-13096ugLMethyl tert-Butyl Ether 96

1000 70-13080ugLMethylene Chloride 80

1000 70-130100ugLNaphthalene 100

1000 70-13093ugLTertiary-amyl methyl ether 93

5000 70-130122ugLTertiary-butyl Alcohol 611

1000 70-130113ugLTetrachloroethene 113

1000 70-13095ugLToluene 95

1000 70-13096ugLTrichloroethene 96

1000 70-13088ugLVinyl Chloride 88

1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup

1000 2570-13090 1ugL111-Trichloroethane 90


1000 2570-13088 1ugL11-Dichloroethane 88

1000 2570-13093 05ugL11-Dichloroethene 93

1000 2570-130100 3ugL12-Dichlorobenzene 100




5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95

1000 2570-13094 1ugLCarbon Tetrachloride 94

1000 2570-13094 04ugLcis-12-Dichloroethene 94

1000 2570-13090 06ugLEthylbenzene 90

1000 2570-13095 2ugLMethyl tert-Butyl Ether 95

1000 2570-13078 3ugLMethylene Chloride 78

1000 2570-13097 3ugLNaphthalene 97

1000 2570-13090 3ugLTertiary-amyl methyl ether 90

5000 2570-130112 8ugLTertiary-butyl Alcohol 562

1000 2570-130114 05ugLTetrachloroethene 114

1000 2570-13096 09ugLToluene 96

1000 2570-13095 05ugLTrichloroethene 95

1000 2570-13087 03ugLVinyl Chloride 87

1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04

5000 15-11583413 ugLSurrogate 14-Dioxane-d8

LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank

020 ugLAcenaphthene ND

020 ugLAcenaphthylene ND

020 ugLAnthracene ND

005 ugLBenzo(a)anthracene ND

005 ugLBenzo(a)pyrene ND

005 ugLBenzo(b)fluoranthene ND

020 ugLBenzo(ghi)perylene ND

005 ugLBenzo(k)fluoranthene ND

250 ugLbis(2-Ethylhexyl)phthalate ND

250 ugLButylbenzylphthalate ND

005 ugLChrysene ND

005 ugLDibenzo(ah)Anthracene ND

250 ugLDiethylphthalate ND

250 ugLDimethylphthalate ND

250 ugLDi-n-butylphthalate ND

250 ugLDi-n-octylphthalate ND

020 ugLFluoranthene ND

020 ugLFluorene ND

005 ugLIndeno(123-cd)Pyrene ND


090 ugLPentachlorophenol ND

020 ugLPhenanthrene ND

020 ugLPyrene ND

2500 30-13043107 ugLSurrogate 12-Dichlorobenzene-d4

3750 15-11085318 ugLSurrogate 246-Tribromophenol

2500 30-13057141 ugLSurrogate 2-Fluorobiphenyl

2500 30-13084211 ugLSurrogate Nitrobenzene-d5

2500 30-13082204 ugLSurrogate p-Terphenyl-d14

LCS

020 4000 40-14072ugLAcenaphthene 286

020 4000 40-14070ugLAcenaphthylene 281

020 4000 40-14080ugLAnthracene 321

005 4000 40-14075ugLBenzo(a)anthracene 302

005 4000 40-14081ugLBenzo(a)pyrene 323

005 4000 40-14081ugLBenzo(b)fluoranthene 325

020 4000 40-14082ugLBenzo(ghi)perylene 330

005 4000 40-14081ugLBenzo(k)fluoranthene 322

250 4000 40-140162ugLbis(2-Ethylhexyl)phthalate 647 B+

250 4000 40-14094ugLButylbenzylphthalate 375

005 4000 40-14076ugLChrysene 302

005 4000 40-14084ugLDibenzo(ah)Anthracene 337

250 4000 40-14077ugLDiethylphthalate 309

250 4000 40-14081ugLDimethylphthalate 324

250 4000 40-14085ugLDi-n-butylphthalate 338




Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

250 4000 40-14094ugLDi-n-octylphthalate 374

020 4000 40-14081ugLFluoranthene 324

020 4000 40-14074ugLFluorene 297

005 4000 40-14083ugLIndeno(123-cd)Pyrene 331

020 4000 40-14062ugLNaphthalene 246

090 4000 30-13060ugLPentachlorophenol 240

020 4000 40-14079ugLPhenanthrene 315

020 4000 40-14076ugLPyrene 304






LCS Dup

020 4000 2040-14070 3ugLAcenaphthene 279

020 4000 2040-14068 3ugLAcenaphthylene 273

020 4000 2040-14085 6ugLAnthracene 341

005 4000 2040-14084 10ugLBenzo(a)anthracene 335

005 4000 2040-14083 3ugLBenzo(a)pyrene 333

005 4000 2040-14083 2ugLBenzo(b)fluoranthene 331

020 4000 2040-14083 09ugLBenzo(ghi)perylene 333

005 4000 2040-14079 2ugLBenzo(k)fluoranthene 315

250 4000 2040-140162 003ugLbis(2-Ethylhexyl)phthalate 646 B+

250 4000 2040-14099 6ugLButylbenzylphthalate 396

005 4000 2040-14080 5ugLChrysene 319

005 4000 2040-14087 3ugLDibenzo(ah)Anthracene 348

250 4000 2040-14081 5ugLDiethylphthalate 325

250 4000 2040-14082 1ugLDimethylphthalate 327

250 4000 2040-14090 7ugLDi-n-butylphthalate 362

250 4000 2040-14093 02ugLDi-n-octylphthalate 374

020 4000 2040-14089 9ugLFluoranthene 355

020 4000 2040-14076 3ugLFluorene 305

005 4000 2040-14086 4ugLIndeno(123-cd)Pyrene 343

020 4000 2040-14057 8ugLNaphthalene 228

090 4000 2030-13059 2ugLPentachlorophenol 234

020 4000 2040-14082 4ugLPhenanthrene 327

020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank

5 mgLTotal Petroleum Hydrocarbon ND

LCS

5 1938 66-11488mgLTotal Petroleum Hydrocarbon 17


Blank

05 mgLChloride ND

LCS

2500 90-11094mgLChloride 23


Blank

5 mgLTotal Suspended Solids ND

LCS

6880 80-12099mgLTotal Suspended Solids 68


Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101

Batch CE51420 - TCN Prep

Blank

50 ugLTotal Cyanide (LL) ND

LCS

50 2006 90-11097ugLTotal Cyanide (LL) 194

LCS


LCS Dup

50 1504 2090-110104 07ugLTotal Cyanide (LL) 156


Batch CE51237 - 5048011

Blank

0015 ugL12-Dibromoethane ND

02000 30-150960191 ugLSurrogate Pentachloroethane

LCS

0015 02000 60-140122ugL12-Dibromoethane 0244





Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51





S+ Surrogate recovery(ies) above upper control limit (S+)

S- Surrogate recovery(ies) below lower control limit (S-)

J Reported between MDL and MRL

D Diluted

C+ Continuing Calibration recovery is above upper control limit (C+)

C- Continuing Calibration recovery is below lower control limit (C-)

B+ Blank Spike recovery is above upper control limit (B+)



MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B


Client CDW Consultants ESS Project ID 15050204 Client Project ID ---=-=-==------- Date Project Due 51515 ShippedDelivered Via ESS Courier Days For Project 5 Day


1 Air Bill Manifest Present Ibull No 10 Are the samples properly preserved Yes


2 Were Custody Seals Present No 12 Any air bubbles in the VOA vials Ibull Yes

3 Were Custody Seals Intact

4 Is Radiation count lt 100 CPM

NA

Yes

13 Holding times exceeded

14 Sufficient sample volumes

No

I Yes

5 Is a cooler present Yes 15 Any Subcontracting needed I No

I cooler Temp 29 16 Are ESS labels on correct containers Yes I No

I Iced With Ice 17 Were samples received intact ~0 6 Was COC included with samples Yes ESS Sample IDs

7 Was COC signed and dated by client Yes Sub Lab ~ 8 Does the COC match the sample

9 Is COC complete and correct

Yes

Yes

Analysis

TAT 7


(f(1 zpoundr fova~ fa__-ampbbtj cg f( ( s~ampfr



1 Yes 1 L Glass 2 H2S04 1 Yes 1 L Glass 6 NP 1 Yes 1 L Plastic 1 NP 1 Yes 250 ml Plastic 1 HN03 w- w-nol

250 ml Plastic NaOH jt7tyH=l gtto A 1 ~~ ~ t1irifJ)- HCL 5~---40mi-VOA ~ 831o DateTime ~Jo J r-~~-Completed By -7~7-~---Tt----shy 7Jyen37 Reviewed By ~ aliJL DateTime [L) ~

1

Page 51 of 51

ESS Laboratory CHAIN OF CUSTODY Page of Division oJThielsch Engineering Inc Reporting Limits ESS LAB PROJECT ID

185 Frances Avenue Cranston RI 02910-2211 Tel (401) 461-7181 Fax (401) 461-4486

f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name

I CD )j C61gtlgt-~yen ~( I Contact Person

Lc-wtlaquo-1 G~_ --r( -I

lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax

Collection ~ I ~ I ~ Time

Electronic Deliverable Yesf-c No s this project for any of the following 6C r

MAmiddotMCP Navy USACE OtheriJ2J~gt GG(1 Format Excel-A Access_ PDF Other

I Project _ I Project Name (20 Char or less) I I I if Circle andor Write Required Analysis

ffi)_ ~elaquoL~ SS- Ck-12e- l Address

4ltgt e ~middot Z1p PO 5 ) 10 ~gtJ- sect

I Email Address sect 1lt-llck)Ce~ llaquolls U

0M -8

Sample Identification (20 Char or less)

- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~

I 15r I 5 lct 1tO - G_lt M- I l gt ~ qAc- y_ I

lllloc~ z e _L middotq ~ ) X NoJir- ~ -D v he _l 1pound4~-(4gt~ y ~0lt~ Co G I)( lx

~

I ~~- middotr se r ( I No~~ 3 I d G X lo~s I X

No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~

ass $-Sterile V-VOA Matrix S-Soil SD-Solid D-Sludge WW-Waste Water GW-Ground Water SW-Surface Water DW-Drinking Water 0-0il W-Wipes F-Filters

Cooler Present - __ Yes ~No ~7Use0nly

Seals Intact ~Yes ~No middotNA __ [ ] Pickup

CoolecTe~~ ~esJ [ ] Technicians __

DateTime I Received by (Signature)

I~A zmiddot -~- knl lfl qo _L2

watillJraquoNWrJ- middotl5ftJSiiCW~ circling MA-MCP client acknlwledges sample~ w~cted

in accordance with MADEP CAM VII A

Preservation Code 1- NP 2- HCl 3- HzS04 4- HNOJ 5- NaOH 6- MeOH 7- Asorbic Acid 8- ZnAct 9-

Sampled by lo---Ilaquo-C Lc(e_~Tfj

Comment N eDrS ~ G r Date~Time I ~tDd by (Signature) flfu_I~q I ~ampfT R~

v~~TIamp 91 Relinquished by (Signature) bull - tiatet- I IRe~ervd by (SigmUui I Dateri~e

Please fax all changes to Chain of Custody in writing 1 (White) Lab Copy 2 (Yellow) Client Receipt

102604 A

Authorization Letter13

NOI13

Therefore the following limits will apply to the effluent of this treatment system

Total Suspended Solids (TSS) - 30 mg1 Total Group I Polycyclic Aromatic Hydrocarbons- 10 ug1 Total Group II Polycyclic Aromatic Hydrocarbons - 100 ug1 Chromium (+3) - 190 ug1 Copper - 70 ug1 Lead- 16 ug1 Zinc- 160 ug1 Iron - 1900 ugL and pH range of 65 - 85 standard units (su) Monitoring for chloride tertiary butyl alcohol 14 dioxane and acetone shall be conducted with no effluent limit

This EPA general permit and authorization to discharge will expire on September 9 2015 You have reported this project will terminate on October 1 2015 Please be aware you are required to reapply for coverage after the EPA expired permit has been reissued The reissuance date as well as the reapplication submittal date will be posted on the EPA web site at that time Regardless of your project termination date you are required to submit a Notice ofTermination (NOT) to the attention of the contact person indicated below within thirty (30) days of the termination of the discharge

Thank you in advance for your cooperation in this matter Please contact George Papadopoulos at 617-918-1579 or PapadopoulosGeorgeepagov ifyou have any questions

Sincerely

lU~~yen Thelma Murphy Chief Storm Water and Construction Permits Section

Enclosure

cc Kathleen Campbell PE CDW Consultants Inc Robert Kubit MassDEP Stephen Shea B WSC

2










Parameter



Limit)













3

Parameter




























100 ugL


4

Parameter


Limit)



















5

Metal Parameters



Minimum levei-ML11



44 Copper 70 15


so Zinc 160 15

51 Iron 1900 20
















6














7


June 22 2015





























I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~





















Remediation General Permit Page 12 of22 Appendix V - NOI



Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13










Parameter



Limit)













3

Parameter




























100 ugL


4

Parameter


Limit)



















5

Metal Parameters



Minimum levei-ML11



44 Copper 70 15


so Zinc 160 15

51 Iron 1900 20
















6














7


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft


httpmapsmassgisstatemausimagesdepmcpmcphtm 5222015 of 51

LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

Parameter




























100 ugL


4

Parameter


Limit)



















5

Metal Parameters



Minimum levei-ML11



44 Copper 70 15


so Zinc 160 15

51 Iron 1900 20
















6














7


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

Parameter


Limit)



















5

Metal Parameters



Minimum levei-ML11



44 Copper 70 15


so Zinc 160 15

51 Iron 1900 20
















6














7


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

Metal Parameters



Minimum levei-ML11



44 Copper 70 15


so Zinc 160 15

51 Iron 1900 20
















6














7


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13














7


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13


June 22 2015









Page 2





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204






httpssdevcrusgsgovv3_betaFTreporthtmstate=MAampworkspaceID=MA20150508104 582015 of 51



Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13
















I


I


----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT



05272015 0154 IPaC Information for Planning and Conservation Page 2 Version 2019 of 51































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

----

I





N bull -

MA IRTN3-17917


II


bull



N~
























Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT







05272015 0154 IPaC Information for Planning and Conservation Page 3 Version 2019 of 51



























Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13














Remediation General Permit of22 Appendix V - NOI



Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004















I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



Parameter CAS


Believed Present

of Samlles

SamiJe ~ ~ 2rab)

Analvtical Method

Used met bod

Minimum Level

(MLof


concentration ygffi

mass ~

concentration gill

mass ~T est

Metbod




l06423 95476

1330207

El D


106934

IE] D I


1634044 EJ D I


75650 D El

I 1

I grab 82608 10 ugL 147 00008 147 0 0004


Remediatton General Pennir of 22 Appendix V - NOI













I


I





Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13













I


I


Remediation General Permit of22 Appendix V -NOt



Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D





Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



Believed Absent

Believed Present

of Samlles

Sam(le Im ~ erab)

Analvtical Method

Used (method tf)

Minimum LeYel

(ML) of


concentration gill

mass ow

concentration ruill

mass OYtlTest


75014 rJ D I




87865 rJ D i



117817

rJ D


rJ D I




193395 El D


pound] D


Remediation General Permit of 22 Appendix V- NOl



Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D








Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



Believed Absent

Believed Present

o( Samlles

Samlle Type

~ grab)

Analvtical Method

Used method)

Minimum Level

(MLof


concentration lgffi

~ fg

concentration giD

mass

~Test Method





85687 84742 I 17840 84662 131113 117817

El D






Other (describe) D D Remediation General Permit of22 Appendix V - NOI


Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0






























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13


Parameter CAS


Samoles


Analvtical Method

Minimum Level

ltMLof


concentration gill

mass ~

concentration gill

mass flgtl


llethod I

D D I

D D




DF DF







Chlorination D

De-chlorination 0


Remediatton General Permit of22 Appendix V - NOl




























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




























I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13










Remediation General Pennit of22 Appendix Y - NOi





I



Date~ 622115

r

I


Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

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middotx

K ~














102604 A


NOI13





I



Date~ 622115

r

I

Remediation General PenniE of22 Appendix V - NOI

Page

1 o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

o

f 51

l J

DISCHARGE PT 1


~-~~~ -- I I I IN FEET )

1 INCH = 50 FT


200

I



DISCHARGE PT 2

SEAL


u f--shylt(

2 w I u (J)

s 0 _j

LL

0 w f--shylt(

s

tshyw w ~ (f)

r 0 Wlt(


J[jJ rr ~U

FIGURE 1

14350

CDW CONSULTANTS INC



Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13


Frac Tank


Catch Basin

Influent Sample

Effluent Sample


CDW Consultants Inc

Figure 2


Chelsea MA

Page 2 of 51



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



500 m

1000 ft



LKonetzny
Text Box
LKonetzny
Polygon Line
LKonetzny
Callout
LKonetzny
Callout
Discharge Pt 113
LKonetzny
Callout
Discharge Pt 213
LKonetzny
Callout





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Page 4 of 51




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Barnstable



Northeastern beach



Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Berkshire


Northern Long-

eared Bat

Proposed

Endangered



Bristol



Westport

Northern Red-


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Dukes



Northeastern beach



Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 5 of 51




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Essex

Small whorled

Pogonia Threatened






Salisbury

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Franklin

Northeastern


Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampshire

Small whorled

Pogonia Threatened





Dwarf


Northern Long-

eared Bat

Proposed

Endangered



Hampden

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Middlesex

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered



Nantucket



American burying


Red Knot1



Northern Long-

eared Bat

Proposed

Endangered



Updated 01092015

Page 6 of 51






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13






Northern Red-




and Pembroke



Mattapoisett

Red Knot1



Northern Long-

eared Bat

Proposed

Endangered




Suffolk Red Knot

1 Threatened



Northern Long-

eared Bat

Proposed

Endangered



Worcester

Small whorled

Pogonia Threatened



Northern Long-

eared Bat

Proposed

Endangered





Updated 01092015

Page 7 of 51


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13


ft3s

ft3s

ft3s

ft3s



record


Min Max

BFWDTH 421 ft

BFDPTH 037 ft

BFAREA 153 ft2

BFFLOW 138 ft3s



record


Min Max



D70 00876 ft3s

D75 00811 ft3s

D80 011 ft3s

D85 00743 ft3s

D90 00854 ft3s

D95 00387 ft3s

D98 00283 ft3s

D99 0019

M7D2Y 00369

AUGD50 00924

M7D10Y 00204









Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



Page 9 of 51






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13






PROJECT CODE


LOCATION


DESCRIPTION






CRITICAL HABITAT


































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13































Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



























Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13












Page 13 of 51





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Page 14 of 51





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





DATA LIMITATIONS




DATA EXCLUSIONS


DATA PRECAUTIONS



Page 15 of 51






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13






Min Max


161)161 149




0 129






Min Max









Min Max


06)06 329



22 239





Min Max

D50 00866 ft3s

D60 00788 ft3s





No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



No Results Found


Page 17 of 51




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 18 of 51

SMorrell
Reviewed



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



SAMPLE RECEIPT








Page 19 of 51



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



PROJECT NARRATIVE
















Page 20 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 21 of 51







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13







Percent Solids NA


Units ugL

Total Metals





Page 22 of 51







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13







Percent Solids NA

Classical Chemistry


4500 H+ B SUpH 1 JLK CE50653050615 1812 738 (NA)






Page 23 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS


LCS Dup



Blank


LCS





Page 24 of 51










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13










MDLMRL


IVFV








DL Detection Limit





Page 25 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 26 of 51

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

Attachment B




















1 Yes 1 Yes



DateTimeqJ r

NP HN03

Page 27 of 51

Page 28 of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

~

i ~

~ ~

Address

Lo __sectD_Qe~ Zip

0170

S SVs e 3ol



bull lj ~ 0 ou

~ ~ middota c c

0 bullbull u ~ 0

0 u 13 0

sect 0

z ~


~


0 _ r06--- L I~ --

~~ N

~

~

0 ~-~ Od N ampl ~ ~~

~ ~

ESS LAB PROJECT ID



~ N 00~

~ au ~]

~ lR _ ~~

b ii-

~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








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middotx

K ~














102604 A


NOI13

of 51







Co Name



Comacr Person I




t

Date

llfJ r(frf rlt)

I State

~ I Fax

Collection Time

-()

bull 8 u

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Address

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bull lj ~ 0 ou

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ESS LAB PROJECT ID



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~ ~ ~~ bull rt ~ ~ egt N 00 i


bUill








DateTime

J DareTime

I I 1~~ivbd ~gna~re


I (DateTime





102604 A




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Lauren Konetzny

CDW Consultants Inc


Framingham MA 01701









Laurel Stoddard

Laboratory Director

Analytical Summary















Page 29 of 51

SMorrell
Reviewed



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



SAMPLE RECEIPT





7010 7470A 8011 8082A 8260B 8270D 8270D

SIM




Page 30 of 51



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13



PROJECT NARRATIVE


Acetone (190 70-130)


Acetone (177 70-130)












14-Dioxane-d8 (126 80-120)


14-Dioxane-d8 (125 80-120)













Page 31 of 51




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




Prep Methods














Analytical Methods

1010A - Flashpoint

6010C - ICP

6020A - ICP MS





8011 - EDBDBCPTCP

8015D - GRODRO

8081B - Pesticides

8082A - PCB

8100M - TPH

8151A - Herbicides

8260B - VOA

8270D - SVOA


9014 - Cyanide

9038 - Sulfate

9040C - Aqueous pH



9056A - Anions (IC)

9060A - TOC






Page 32 of 51







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13







Percent Solids NA


Units ugL

Total Metals


7010 50 10Arsenic 03 2 KJK CE50809051215 640 47 (40)

7010 50 10Cadmium 001 1 KJK CE50809051415 056 ND (02)

6010C 50 10Copper 16 2 JP CE50809050915 1516 74 (40)

6010C 50 10Iron 92 2 JP CE50809050915 1516 19700 (400)

7010 50 10Lead 02 1 KJK CE50809051315 423 67 (10)


6010C 50 10Nickel 08 2 JP CE50809050915 1516J 33 (80)


7010 50 10Silver 003 1 KJK CE50809051315 2254 ND (01)

6010C 50 10Zinc 36 2 JP CE50809050915 1516 349 (200)




Page 33 of 51








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








Final Volume 1

Percent Solids NA


Units ugL



8082AAroclor 1221 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1232 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1242 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1248 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1254 003 1 CE51547051515 1152J 006 (009)

8082AAroclor 1260 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1262 003 1 CE51547051515 1152 ND (009)

8082AAroclor 1268 003 1 CE51547051515 1152 ND (009)









Page 34 of 51








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








Percent Solids NA


Units ugL










8260BAcetone 27 1 CE51130CYE0137051115 1805 223 (100)

8260BBenzene 01 1 CE51130CYE0137051115 1805J 09 (10)










8260BToluene 01 1 CE51130CYE0137051115 1805J 01 (10)













Page 35 of 51








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








Final Volume 1

Percent Solids NA


Units ugL








Page 36 of 51








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








Final Volume 025

Percent Solids NA


Units ugL


































Page 37 of 51







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13







Percent Solids NA

Classical Chemistry









Page 38 of 51








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








Final Volume 2

Percent Solids NA


Units ugL








Page 39 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Total Metals

Batch CE50809 - 3005A2007

Blank

20 ugLAntimony ND

20 ugLArsenic ND

02 ugLCadmium ND

20 ugLCopper ND

200 ugLIron ND

10 ugLLead ND

40 ugLNickel ND

20 ugLSelenium ND

10 ugLSilver ND

01 ugLSilver ND

100 ugLZinc ND

LCS

100 2500 80-120102ugLAntimony 254

100 2500 80-120110ugLArsenic 276

250 1250 80-120100ugLCadmium 125 J

50 2500 80-12098ugLCopper 244

500 1250 80-12098ugLIron 1220

500 2500 80-12099ugLLead 248

100 2500 80-12099ugLNickel 247

100 5000 80-120108ugLSelenium 538

250 1250 80-120106ugLSilver 132

25 1250 80-12099ugLSilver 124

250 2500 80-12096ugLZinc 241

LCS Dup

100 2500 2080-12092 10ugLAntimony 230

100 2500 2080-12099 11ugLArsenic 246

250 1250 2080-12093 7ugLCadmium 117 J

50 2500 2080-12095 2ugLCopper 239

500 1250 2080-12093 4ugLIron 1170

500 2500 2080-12091 9ugLLead 226

100 2500 2080-12096 3ugLNickel 240

100 5000 2080-12098 9ugLSelenium 490

250 1250 2080-120108 2ugLSilver 135

25 1250 2080-12096 3ugLSilver 121

250 2500 2080-12095 2ugLZinc 236

Batch CE50910 - 24517470A

Blank

0200 ugLMercury ND

LCS

0200 6000 80-120113ugLMercury 677

LCS Dup

0200 6000 2080-120111 2ugLMercury 665




Page 40 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51547 - 3510C

Blank














LCS

010 1000 40-14063ugLAroclor 1016 063

010 1000 40-14074ugLAroclor 1260 074





LCS Dup

010 1000 2040-14073 15ugLAroclor 1016 073

010 1000 2040-14076 2ugLAroclor 1260 076






Batch CE51130 - 5030B

Blank









100 ugLAcetone ND

10 ugLBenzene ND




Page 41 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B










10 ugLToluene ND



10 ugLXylene O ND

20 ugLXylene PM ND





LCS









5000 70-130190ugLAcetone 948 B+

1000 70-13096ugLBenzene 96










1000 70-13095ugLToluene 95



1000 70-13083ugLXylene O 83

2000 70-13088ugLXylene PM 177






Page 42 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51130 - 5030B



LCS Dup









5000 2570-130177 7ugLAcetone 884 B+

1000 2570-13095 1ugLBenzene 95










1000 2570-13096 09ugLToluene 96



1000 2570-13083 01ugLXylene O 83

2000 2570-13088 0ugLXylene PM 177






Batch CE51243 - 3520C

Blank

02 ugL14-Dioxane 04


LCS

02 1000 40-14084ugL14-Dioxane 84


LCS Dup

02 1000 2040-14078 8ugL14-Dioxane 78





Page 43 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C

Blank











005 ugLChrysene ND







020 ugLFluorene ND





020 ugLPyrene ND






LCS



020 4000 40-14080ugLAnthracene 321








005 4000 40-14076ugLChrysene 302








Page 44 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51403 - 3510C



020 4000 40-14074ugLFluorene 297





020 4000 40-14076ugLPyrene 304






LCS Dup



020 4000 2040-14085 6ugLAnthracene 341








005 4000 2040-14080 5ugLChrysene 319







020 4000 2040-14076 3ugLFluorene 305


020 4000 2040-14057 8ugLNaphthalene 228



020 4000 2040-14082 8ugLPyrene 329






Classical Chemistry





Page 45 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier

Classical Chemistry


Blank


LCS



Blank

05 mgLChloride ND

LCS



Blank


LCS



Blank

010 mgLPhenols ND

LCS

010 01000 80-12098mgLPhenols 010 J

LCS

010 1000 80-120101mgLPhenols 101


Blank


LCS


LCS


LCS Dup



Batch CE51237 - 5048011

Blank



LCS






Page 46 of 51





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13





Spike

Level

Source

Result REC

REC

Limits RPD

RPD

Limit Qualifier


Batch CE51237 - 5048011

LCS






Page 47 of 51








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13








D Diluted






MDLMRL


IVFV








DL Detection Limit





Page 48 of 51




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13




ENVIRONMENTAL





















CHEMISTRY




CPSC ID 1141






Page 49 of 51

Page 50 of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

of 51

Attachment B









NA

Yes



No

I Yes






Yes

Yes

Analysis

TAT 7







1

Page 51 of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

of 51



f-=~~=~~===~=-~N~gte (2Gr ISos-~o

wwwesslaboratorycom

Co Name



lc~ I t-r~lM Nrgt

ESSLAB Sample

s

Date

State

~-I Fax








0M -8


- ~ s ~ 0 I u z

~ ~

~ ~ reg

~ ~ 0 u u ~

b g g ggg ~ ~ ~~ ~



~


No~l_ 6 (

-I h( I F-

oJ

~ p s - J

middotx

K ~














102604 A


NOI13

145-155 beech street, chelsea, ma, mag910688 - us … beech street : facility/site ... 34. bis...

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