· 1,4-dichlorobenzene 6.34 75 chloromethane 1.18 dichlorodifluoromethane 0.37 390...

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Page 1:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96
Page 2:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96
Page 3:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96
Page 4:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Table 1. Springs/Seeps near Fulton Class 3 Landfill, August 2005 Sampling Event.

Spring/Seep Sampled August

2005

Location Description (Approximate Location Shown in Figure 1)

Springs regularly sampled during past events

ES Spring 1 Yes Big spring south of landfill along Quail Road. North and east of Quail Road feeding gully adjacent to road. Can see from road unless covered with vegetation. Metal fence post with number “7” at spring. Located few hundred feet from pond at bottom of the hill.

ES Spring 2 Yes In hollow south of landfill, between landfill and Quail Road. Located a couple of hundred feet up hollow from Quail Road. Hoses and pipe lead to spring. No longer a metal fence post labeling the site due to major erosion - older pictures show post.

ES Spring 3 No – Could Not Locate

Map shows location in drainage to north-northeast of landfill. Could not locate, will attempt again during next sampling trip.

ADPC&E-3 No - Dry In drainage to northeast of landfill, normally discharges from rock shelf, metal fence post with number “1” at spring.

Additional seeps and springs sampled or noted during the current event

Seep A Yes Located in gully approx 30 feet upstream of ES Spring 1 discharge to gully.

Seep B Yes Coming out of deeply incised gully entering southern stream bank approximately 100 ft downstream of ADPC&E-3. Low flow. Stream is dry.

Spring C Yes Coming out of upper portion of northern stream bank approximately 220 ft downstream of ADPC&E-3. Approx 1 gpm. Stream was dry. Spring seen during April 2005 and was discharging on terrace above current discharge point.

Seep D Yes In hollow adjacent and to the north-northwest of the landfill. Found while looking for ES Spring 3. Followed hollow upstream until could no longer continue due to huge tangle of downed trees, limbs, vines, woody debris. Orange water flowing out of debris pile.

Seep E No - Dry Located in gully approximately 150 feet upstream of ES Spring 1, but on west side of Quail Road. Orange staining. Location pointed out by Mr. Lynn Fulton.

Page 5:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Table 2. Parameters Collected from Springs at Fulton Class 3 Landfill, August 2005.

Sample Location

Specific Conductivity

(uS/cm) pH

Turbidity (from lab)

(NTU) Comments

ES Spring 1 937 6.34 159* Water orange from iron precipitate; flow is several gpm

ES Spring 2 635 6.54 6 Water orange from iron precipitate; several seeps in bottom of hollow

Seep A 943 6.42 986* Water orange from iron precipitate

Seep B 757 6.72 534* Water orange from iron precipitate

Spring C 534 7.00 1 Water Clear

Seep D ------ ------ 87* Water orange from iron precipitate *Turbidity is from orange iron precipitate suspended in the water.

Page 6:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Sampling Parameter Concentration MCL HHMSSLLocation (ug/L) (ug/L) (ug/L)

1,1-Dichloroethane 3.64 8101,4-Dichlorobenzene 6.34 75Chloromethane 1.18Dichlorodifluoromethane 0.37 3901,1-Dichloroethane 3.65 8101,4-Dichlorobenzene 3.89 75Chloromethane 2.87Vinyl Chloride 0.96 2

Spring C Trichloroethene 4.41 5Seep D Chloromethane 1.24

MCL = Maximum Contaminant LevelHHMSSL = EPA Region 6 Human Health Medium-Specific Screening Level for tap water

ES Spring 1

Seep A

Table 3. Detections of VOCs and other Organic Compounds, August 2005, Fulton Class 3

Page 7:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Aluminum (ug/L)

Arsenic (ug/L)

Barium (ug/L)

Cadmium (ug/L)

Chloride (mg/L)

Iron (mg/L)

ES Spring 1 <20 4.20 265 <0.10 47.0 5.2ES Spring 2 814 4.44 138 0.32 5.6 9.5Seep A 27.8 8.16 344 <0.10 31.2 51.5Seep B 27.2 6.69 247 <0.10 17.6 20.6Spring C <20 1.20 67.3 <0.10 10.6 <0.02Seep D 802 4.91 184 0.20 22.3 20.8MCL 50* 2,000 5SDWS 200 250 0.3HHMSSL 37000 11

Lead (ug/L)

Manganese (mg/L)

Sulfate (mg/L)

TDS (mg/L)

TOC (mg/L)

Zinc (ug/L)

ES Spring 1 0.36 24.6 9.14 585 3.77 15.7ES Spring 2 3.91 10.1 1.41 380 1.07 41.1Seep A 0.44 23.3 3.48 568 2.76 11.6Seep B 0.40 4.7 4.72 471 7.18 4.31Spring C 0.36 0.0128 5.49 333 0.941 2.88Seep D 3.68 14.8 2.30 462 2.92 56.7MCL 15SDWS 0.05 250 500 5000HHMSSL 1.7MCL = Maximum Contaminant LevelSDWS = Secondary Drinking Water StandardHHMSSL = EPA Region 6 Human Health Medium-Specific Screening Level for tap water *MCL for arsenic will change from 50 ug/L to 10 ug/L as of 1/23/06

Table 4. Concentrations of Selected Parameters, August 2005, Fulton Class 3

Page 8:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96
Page 9:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

ATTACHMENT 1

LABORATORY WATER QUALITY

ANALYSES

Page 10:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2475 FAX: Your Sample ID: ES Spring1 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 159 NTU 9/1/2005 TDS Total dissolved solids 585 mg/L 9/1/2005 Anions Bromide 0.44 mg/L 9/7/2005 Chloride 47.0 mg/L 9/7/2005 Fluoride 0.11 mg/L 9/7/2005 Sulfate 9.14 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 103 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 89.7 %REC 9/6/2005 Toluene-d8(Surr.) 93.9 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 106 %REC 9/6/2005 Dichlorodifluoromethane 0.371 µg/L 9/6/2005 Chloromethane 1.18 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 26

Page 11:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2475 FAX: Your Sample ID: ES Spring1 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 27

Page 12:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2475 FAX: Your Sample ID: ES Spring1 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene 6.34 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 28

Page 13:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2475 FAX: Your Sample ID: ES Spring1 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane 3.64 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 3.77 mg/L 9/1/2005 ICP/MS-T Aluminum < 20.0 µg/L 10/4/2005 Antimony < 5.00 µg/L 10/4/2005 Arsenic 4.20 µg/L 10/4/2005 Barium 265 µg/L 10/4/2005 Beryllium < 0.10 µg/L 10/4/2005 Boron 59.3 µg/L 10/4/2005 Cadmium < 0.10 µg/L 10/4/2005 Calcium 180 mg/L 10/4/2005 Chromium 0.11 µg/L 10/4/2005 Cobalt 68.0 µg/L 10/4/2005 Copper 1.10 µg/L 10/4/2005

Reported by: Jeff Ruehr 29

Page 14:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2475 FAX: Your Sample ID: ES Spring1 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron 5220 µg/L 10/4/2005 Lead 0.36 µg/L 10/4/2005 Magnesium 6.96 mg/L 10/4/2005 Manganese 24600 µg/L 10/4/2005 Nickel 101 µg/L 10/4/2005 Potassium 3.62 mg/L 10/4/2005 Selenium < 0.50 µg/L 10/4/2005 Silicon Dioxide 15.7 µg/L 10/4/2005 Silver < 1.00 µg/L 10/4/2005 Sodium 38.2 mg/L 10/4/2005 Thallium < 0.50 µg/L 10/4/2005 Vanadium < 0.50 µg/L 10/4/2005 Zinc 15.7 µg/L 10/4/2005

Reported by: Jeff Ruehr 30

Page 15:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2476 FAX: Your Sample ID: Seep A Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 986 NTU 9/1/2005 TDS Total dissolved solids 568 mg/L 9/1/2005 Anions Bromide 0.33 mg/L 9/7/2005 Chloride 31.2 mg/L 9/7/2005 Fluoride 0.12 mg/L 9/7/2005 Sulfate 3.48 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 98.7 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 86.3 %REC 9/6/2005 Toluene-d8(Surr.) 90.5 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 108 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane 2.87 µg/L 9/6/2005 Vinyl Chloride 0.963 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 31

Page 16:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2476 FAX: Your Sample ID: Seep A Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 32

Page 17:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2476 FAX: Your Sample ID: Seep A Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene 3.89 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 33

Page 18:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2476 FAX: Your Sample ID: Seep A Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane 3.65 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 2.76 mg/L 9/1/2005 ICP/MS-T Aluminum 27.8 µg/L 10/4/2005 Antimony < 5.00 µg/L 10/4/2005 Arsenic 8.16 µg/L 10/4/2005 Barium 344 µg/L 10/4/2005 Beryllium 0.10 µg/L 10/4/2005 Boron 39.6 µg/L 10/4/2005 Cadmium < 0.10 µg/L 10/4/2005 Calcium 187 mg/L 10/4/2005 Chromium 0.26 µg/L 10/4/2005 Cobalt 37.9 µg/L 10/4/2005 Copper 0.90 µg/L 10/4/2005

Reported by: Jeff Ruehr 34

Page 19:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2476 FAX: Your Sample ID: Seep A Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron 51500 µg/L 10/4/2005 Lead 0.44 µg/L 10/4/2005 Magnesium 6.54 mg/L 10/4/2005 Manganese 23300 µg/L 10/4/2005 Nickel 48.0 µg/L 10/4/2005 Potassium 3.57 mg/L 10/4/2005 Selenium 0.59 µg/L 10/4/2005 Silicon Dioxide 18.6 µg/L 10/4/2005 Silver < 1.00 µg/L 10/4/2005 Sodium 26.4 mg/L 10/4/2005 Thallium < 0.50 µg/L 10/4/2005 Vanadium 0.89 µg/L 10/4/2005 Zinc 11.6 µg/L 10/4/2005

Reported by: Jeff Ruehr 35

Page 20:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2477 FAX: Your Sample ID: ES Spring 2 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 6.29 NTU 9/1/2005 TDS Total dissolved solids 380 mg/L 9/1/2005 Anions Bromide < 0.01 mg/L 9/7/2005 Chloride 5.57 mg/L 9/7/2005 Fluoride 0.11 mg/L 9/7/2005 Sulfate 1.41 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 96.3 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 92.5 %REC 9/6/2005 Toluene-d8(Surr.) 88.9 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 108 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane < 0.484 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 36

Page 21:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2477 FAX: Your Sample ID: ES Spring 2 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 37

Page 22:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2477 FAX: Your Sample ID: ES Spring 2 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene < 0.364 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 38

Page 23:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2477 FAX: Your Sample ID: ES Spring 2 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane < 0.300 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 1.07 mg/L 9/1/2005 ICP/MS-T Aluminum 814 µg/L 10/4/2005 Antimony < 5.00 µg/L 10/4/2005 Arsenic 4.44 µg/L 10/4/2005 Barium 138 µg/L 10/4/2005 Beryllium 0.22 µg/L 10/4/2005 Boron 12.5 µg/L 10/4/2005 Cadmium 0.32 µg/L 10/4/2005 Calcium 137 mg/L 10/4/2005 Chromium 1.22 µg/L 10/4/2005 Cobalt 18.9 µg/L 10/4/2005 Copper 1.59 µg/L 10/4/2005

Reported by: Jeff Ruehr 39

Page 24:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2477 FAX: Your Sample ID: ES Spring 2 Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron 9510 µg/L 10/4/2005 Lead 3.91 µg/L 10/4/2005 Magnesium 4.01 mg/L 10/4/2005 Manganese 10100 µg/L 10/4/2005 Nickel 68.0 µg/L 10/4/2005 Potassium 1.04 mg/L 10/4/2005 Selenium < 0.50 µg/L 10/4/2005 Silicon Dioxide 17.6 µg/L 10/4/2005 Silver < 1.00 µg/L 10/4/2005 Sodium 7.57 mg/L 10/4/2005 Thallium < 0.50 µg/L 10/4/2005 Vanadium 3.05 µg/L 10/4/2005 Zinc 41.1 µg/L 10/4/2005

Reported by: Jeff Ruehr 40

Page 25:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2478 FAX: Your Sample ID: Seep B Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 534 NTU 9/1/2005 TDS Total dissolved solids 471 mg/L 9/1/2005 Anions Bromide 0.18 mg/L 9/7/2005 Chloride 17.6 mg/L 9/7/2005 Fluoride 0.15 mg/L 9/7/2005 Sulfate 4.72 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 107 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 90.6 %REC 9/6/2005 Toluene-d8(Surr.) 93.2 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 102 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane < 0.484 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 41

Page 26:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2478 FAX: Your Sample ID: Seep B Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 42

Page 27:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2478 FAX: Your Sample ID: Seep B Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene < 0.364 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 43

Page 28:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2478 FAX: Your Sample ID: Seep B Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane < 0.300 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 7.18 mg/L 9/1/2005 ICP/MS-T Aluminum 27.2 µg/L 10/4/2005 Antimony < 5.00 µg/L 10/4/2005 Arsenic 6.69 µg/L 10/4/2005 Barium 247 µg/L 10/4/2005 Beryllium < 0.10 µg/L 10/4/2005 Boron 334 µg/L 10/4/2005 Cadmium < 0.10 µg/L 10/4/2005 Calcium 154 mg/L 10/4/2005 Chromium 0.27 µg/L 10/4/2005 Cobalt 9.97 µg/L 10/4/2005 Copper 1.02 µg/L 10/4/2005

Reported by: Jeff Ruehr 44

Page 29:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2478 FAX: Your Sample ID: Seep B Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron 20600 µg/L 10/4/2005 Lead 0.40 µg/L 10/4/2005 Magnesium 5.98 mg/L 10/4/2005 Manganese 4650 µg/L 10/4/2005 Nickel 18.2 µg/L 10/4/2005 Potassium 4.27 mg/L 10/4/2005 Selenium < 0.50 µg/L 10/4/2005 Silicon Dioxide 14.2 µg/L 10/4/2005 Silver < 1.00 µg/L 10/4/2005 Sodium 25.9 mg/L 10/4/2005 Thallium < 0.50 µg/L 10/4/2005 Vanadium 1.14 µg/L 10/4/2005 Zinc 4.31 µg/L 10/4/2005

Reported by: Jeff Ruehr 45

Page 30:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2479 FAX: Your Sample ID: Spring C Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 1.25 NTU 9/1/2005 TDS Total dissolved solids 333 mg/L 9/1/2005 Anions Bromide 0.08 mg/L 9/7/2005 Chloride 10.6 mg/L 9/7/2005 Fluoride 0.12 mg/L 9/7/2005 Sulfate 5.49 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 115 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 97.2 %REC 9/6/2005 Toluene-d8(Surr.) 92.8 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 115 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane < 0.484 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 46

Page 31:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2479 FAX: Your Sample ID: Spring C Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene 4.41 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 47

Page 32:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2479 FAX: Your Sample ID: Spring C Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene < 0.364 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 48

Page 33:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2479 FAX: Your Sample ID: Spring C Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane < 0.300 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 0.941 mg/L 9/1/2005 ICP/MS-T Aluminum < 20.0 µg/L 9/21/2005 Antimony < 5.00 µg/L 9/21/2005 Arsenic 1.20 µg/L 9/21/2005 Barium 67.3 µg/L 9/21/2005 Beryllium < 0.10 µg/L 9/21/2005 Boron 71.6 µg/L 9/21/2005 Cadmium < 0.10 µg/L 9/21/2005 Calcium 145 mg/L 9/21/2005 Chromium 0.19 µg/L 9/21/2005 Cobalt < 0.50 µg/L 9/21/2005 Copper 0.79 µg/L 9/21/2005

Reported by: Jeff Ruehr 49

Page 34:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2479 FAX: Your Sample ID: Spring C Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron < 20.0 µg/L 9/21/2005 Lead 0.36 µg/L 9/21/2005 Magnesium 3.92 mg/L 9/21/2005 Manganese 12.8 µg/L 9/21/2005 Nickel 0.83 µg/L 9/21/2005 Potassium 2.96 mg/L 9/21/2005 Selenium 0.56 µg/L 9/21/2005 Silicon Dioxide 15.0 µg/L 9/21/2005 Silver < 1.00 µg/L 9/21/2005 Sodium 12.2 mg/L 9/21/2005 Thallium < 0.50 µg/L 9/21/2005 Vanadium < 0.50 µg/L 9/21/2005 Zinc 2.88 µg/L 9/21/2005

Reported by: Jeff Ruehr 50

Page 35:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2480 FAX: Your Sample ID: Seep D Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date TURBIDITY Turbidity 86.5 NTU 9/1/2005 TDS Total dissolved solids 462 mg/L 9/1/2005 Anions Bromide 0.12 mg/L 9/7/2005 Chloride 22.3 mg/L 9/7/2005 Fluoride 0.12 mg/L 9/7/2005 Sulfate 2.30 mg/L 9/7/2005 VOL/WATER Dibromofluoromethane(Surr.) 105 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 93.0 %REC 9/6/2005 Toluene-d8(Surr.) 97.9 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 101 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane 1.24 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005

Reported by: Jeff Ruehr 51

Page 36:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2480 FAX: Your Sample ID: Seep D Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005 Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005

Reported by: Jeff Ruehr 52

Page 37:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2480 FAX: Your Sample ID: Seep D Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005 n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene < 0.364 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005

Reported by: Jeff Ruehr 53

Page 38:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2480 FAX: Your Sample ID: Seep D Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane < 0.300 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005 TOC Total Organic Carbon 2.92 mg/L 9/1/2005 ICP/MS-T Aluminum 802 µg/L 10/4/2005 Antimony < 5.00 µg/L 10/4/2005 Arsenic 4.91 µg/L 10/4/2005 Barium 184 µg/L 10/4/2005 Beryllium 0.19 µg/L 10/4/2005 Boron 125 µg/L 10/4/2005 Cadmium 0.20 µg/L 10/4/2005 Calcium 161 mg/L 10/4/2005 Chromium 1.32 µg/L 10/4/2005 Cobalt 24.6 µg/L 10/4/2005 Copper 3.15 µg/L 10/4/2005

Reported by: Jeff Ruehr 54

Page 39:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2480 FAX: Your Sample ID: Seep D Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Iron 20800 µg/L 10/4/2005 Lead 3.68 µg/L 10/4/2005 Magnesium 5.47 mg/L 10/4/2005 Manganese 14800 µg/L 10/4/2005 Nickel 23.6 µg/L 10/4/2005 Potassium 4.96 mg/L 10/4/2005 Selenium 0.53 µg/L 10/4/2005 Silicon Dioxide 19.0 µg/L 10/4/2005 Silver < 1.00 µg/L 10/4/2005 Sodium 21.0 mg/L 10/4/2005 Thallium < 0.50 µg/L 10/4/2005 Vanadium 2.42 µg/L 10/4/2005 Zinc 56.7 µg/L 10/4/2005

Reported by: Jeff Ruehr 55

Page 40:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2481 FAX: Your Sample ID: Trip Blank Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date VOL/WATER Dibromofluoromethane(Surr.) 111 %REC 9/6/2005 1,2-Dichloroethane-d4(Surr) 104 %REC 9/6/2005 Toluene-d8(Surr.) 90.7 %REC 9/6/2005 4-Bromofluorobenzene(Surr.) 117 %REC 9/6/2005 Dichlorodifluoromethane < 0.188 µg/L 9/6/2005 Chloromethane < 0.484 µg/L 9/6/2005 Vinyl Chloride < 0.169 µg/L 9/6/2005 Bromomethane < 0.313 µg/L 9/6/2005 Chloroethane < 0.346 µg/L 9/6/2005 Trichlorofluoromethane < 0.104 µg/L 9/6/2005 1,1-Dichloroethene < 0.168 µg/L 9/6/2005 Methylene_chloride < 5.00 µg/L 9/6/2005 trans-1-2-Dichloroethene < 0.104 µg/L 9/6/2005 cis-1-2-Dichloroethene < 0.073 µg/L 9/6/2005 Methyl Tert-Butyl Ether < 0.300 µg/L 9/6/2005 Bromochloromethane < 0.212 µg/L 9/6/2005 Chloroform < 0.570 µg/L 9/6/2005 2,2-Dichloropropane < 0.169 µg/L 9/6/2005 1,2-Dichloroethane < 0.240 µg/L 9/6/2005 1,1,1-Trichloroethane < 0.129 µg/L 9/6/2005 1,1-Dichloropropene < 0.133 µg/L 9/6/2005 Carbon Tetrachloride < 0.098 µg/L 9/6/2005

Reported by: Jeff Ruehr 56

Page 41:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2481 FAX: Your Sample ID: Trip Blank Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date Benzene < 0.169 µg/L 9/6/2005 Dibromomethane < 0.268 µg/L 9/6/2005 1,2-Dichloropropane < 0.140 µg/L 9/6/2005 Trichloroethene < 0.165 µg/L 9/6/2005 Bromodichloromethane < 0.142 µg/L 9/6/2005 cis-1-3-Dichloropropene < 0.272 µg/L 9/6/2005 trans-1-3-Dichloropropene < 0.224 µg/L 9/6/2005 1,1,2-Trichloroethane < 0.091 µg/L 9/6/2005 Toluene < 0.116 µg/L 9/6/2005 1,3-Dichloropropane < 0.216 µg/L 9/6/2005 Dibromochloromethane < 0.294 µg/L 9/6/2005 1,2-Dibromoethane < 0.165 µg/L 9/6/2005 Tetrachloroethene < 0.149 µg/L 9/6/2005 Chlorobenzene < 0.220 µg/L 9/6/2005 Ethylbenzene < 0.066 µg/L 9/6/2005 m+p_Xylene < 0.183 µg/L 9/6/2005 Bromoform < 0.323 µg/L 9/6/2005 Styrene < 0.158 µg/L 9/6/2005 1,1,2,2-Tetrachloroethane < 0.240 µg/L 9/6/2005 o-Xylene < 0.103 µg/L 9/6/2005 1,2,3-Trichloropropane < 0.937 µg/L 9/6/2005 Isopropylbenzene < 0.090 µg/L 9/6/2005 Bromobenzene < 0.224 µg/L 9/6/2005

Reported by: Jeff Ruehr 57

Page 42:  · 1,4-Dichlorobenzene 6.34 75 Chloromethane 1.18 Dichlorodifluoromethane 0.37 390 1,1-Dichloroethane 3.65 810 1,4-Dichlorobenzene 3.89 75 Chloromethane 2.87 Vinyl Chloride 0.96

Report Date: 06-Oct-05

- CERTIFICATE OF ANALYSIS - Attn: Phone: Our Lab#: 2005-2481 FAX: Your Sample ID: Trip Blank Description: Fulton Class 3 Sample Type: Special Sample Sample Water

Test Group Test Result Units Analysis Date n-Propylbenzene < 0.037 µg/L 9/6/2005 2-Chlorotoluene < 0.126 µg/L 9/6/2005 4-Chlorotoluene < 0.109 µg/L 9/6/2005 1,3,5-Trimethylbenzene < 0.124 µg/L 9/6/2005 tert-Butylbenzene < 0.131 µg/L 9/6/2005 1,2,4-Trimethylbenzene < 0.090 µg/L 9/6/2005 sec-Butylbenzene < 0.096 µg/L 9/6/2005 1,3-Dichlorobenzene < 0.164 µg/L 9/6/2005 1,4-Dichlorobenzene < 0.364 µg/L 9/6/2005 p-Isopropyltoluene < 0.136 µg/L 9/6/2005 1,2-Dichlorobenzene < 0.139 µg/L 9/6/2005 n-butylbenzene < 0.094 µg/L 9/6/2005 1,2-Dibromo-3-chloropropane < 0.797 µg/L 9/6/2005 1,2,4-Trichlorobenzene < 0.102 µg/L 9/6/2005 Naphthalene < 0.157 µg/L 9/6/2005 Hexachlorobutadiene < 0.106 µg/L 9/6/2005 1,1,1,2-Tetrachloroethane < 0.300 µg/L 9/6/2005 1,1-Dichloroethane < 0.300 µg/L 9/6/2005 1,2,3-Trichlorobenzene < 0.174 µg/L 9/6/2005 Acetone < 7.70 µg/L 9/6/2005 2-Butanone < 4.80 µg/L 9/6/2005 4-Methyl-2-pentanone < 4.90 µg/L 9/6/2005 2-Hexanone < 4.10 µg/L 9/6/2005

Reported by: Jeff Ruehr 58