12/27/2016 mr. curt lueckenhoff project12/27/2016 mr. curt lueckenhoff missouri dept. of natural...

12/27/2016Mr. Curt LueckenhoffMissouri Dept. of Natural Resources2710 West Main

Jefferson City MO 65109

Project Name: Bridgeton LandfillProject #:

Dear Mr. Curt Lueckenhoff

The following report includes the data for the above referenced project for sample(s) received on 12/13/2016 at Air Toxics Ltd.

The data and associated QC analyzed by Modified TO-15 are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative.

Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air Toxics Inc. is committed to providing accurate data of the highest quality. Please feel freeto contact the Project Manager: Brian Whittaker at 916-985-1000 if you have any questions regarding the data in this report.

Regards,

Brian Whittaker

Project Manager

Workorder #: 1612183

of 21

Mr. Curt LueckenhoffMissouri Dept. of Natural Resources2710 West MainJefferson City, MO 65109

WORK ORDER #: 1612183

CLIENT: BILL TO:

PHONE:

Accounts PayableMissouri Dept. of Natural ResourcesP.O Box 176Jefferson City, MO 65102

573-526-3363

573-526-335012/13/2016

DATE COMPLETED: 12/27/2016

P.O. # 3ESP170425

PROJECT # Bridgeton Landfill

Work Order Summary

FAX:

DATE RECEIVED: CONTACT: Brian Whittaker

NAMEFRACTION # TEST VAC./PRES.RECEIPT

PRESSUREFINAL

01A D1 (163931) Modified TO-15 4.3 "Hg 5 psi02A D2 (163932) Modified TO-15 5.3 "Hg 5.1 psi03A U1 (163933) Modified TO-15 4.5 "Hg 5.1 psi04A U2 (163934) Modified TO-15 4.9 "Hg 5 psi05A Lab Blank Modified TO-15 NA NA06A CCV Modified TO-15 NA NA07A LCS Modified TO-15 NA NA07AA LCSD Modified TO-15 NA NA

CERTIFIED BY:

Technical Director

DATE:

Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)Accreditation number: CA300005, Effective date: 10/18/2016, Expiration date: 10/17/2017.

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020

12/27/16

of 21

This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.

Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards

Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291, TX NELAP - T104704434-16-11, UT NELAP CA0093332016-7, VA NELAP - 8113, WA NELAP - C935

LABORATORY NARRATIVEModified TO-15

Missouri Dept. of Natural ResourcesWorkorder# 1612183

Four 6 Liter Summa Canister (100% Certified) samples were received on December 13, 2016. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the full scan mode.

This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control requirements and verification of all quantified amounts.

Method modifications taken to run these samples are summarized in the table below. Specific project requirements may over-ride the ATL modifications.

Requirement ATL ModificationsTO-15Initial Calibration </=30% RSD with 2

compounds allowed out to < 40% RSD

</=30% RSD with 4 compounds allowed out to < 40% RSD

Blank and standards Zero Air UHP Nitrogen provides a higher purity gas matrix than zero air

Receiving Notes

There were no receiving discrepancies.

All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag isdefined at the bottom of this Case Narrative and on each Sample Result Summary page.

Analytical Notes

Eight qualifiers may have been used on the data analysis sheets and indicates as follows: B - Compound present in laboratory blank greater than reporting limit (background subtractionnot performed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. Seedata page for project specific U-flag definition. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.

File extensions may have been used on the data analysis sheets and indicates as follows: a-File was requantified b-File was quantified by a second column and detector r1-File was requantified for the purpose of reissue

Definition of Data Qualifying Flags

of 21

MODIFIED EPA METHOD TO-15 GC/MS FULL SCANSummary of Detected Compounds

Client Sample ID: D1 (163931)

Lab ID#: 1612183-01A

(ug/m3)(ug/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit

0.16 0.49 0.77 2.4Freon 12

0.16 0.23 0.88 1.3Freon 11

0.78 1.3 1.5 2.4Ethanol

0.78 2.8 1.8 6.7Acetone

0.16 0.24 0.50 0.76Benzene

0.16 0.16 0.59 0.60Toluene

Client Sample ID: D2 (163932)

Lab ID#: 1612183-02A


0.16 0.46 0.81 2.3Freon 12

0.16 0.21 0.92 1.2Freon 11

0.82 1.1 1.5 2.0Ethanol

0.82 3.0 1.9 7.2Acetone

0.16 0.22 0.58 0.77Hexane

0.16 0.25 0.52 0.80Benzene

0.16 0.21 0.67 0.84Heptane

0.16 0.26 0.62 0.99Toluene

Client Sample ID: U1 (163933)

Lab ID#: 1612183-03A


0.16 0.42 0.78 2.1Freon 12

0.16 0.17 0.89 0.96Freon 11

0.79 1.1 1.5 2.0Ethanol

0.79 2.2 1.9 5.2Acetone

0.16 0.16 0.56 0.57Hexane

0.16 0.20 0.50 0.63Benzene

0.16 0.16 0.60 0.60Toluene

of 21

MODIFIED EPA METHOD TO-15 GC/MS FULL SCANSummary of Detected Compounds

Client Sample ID: U2 (163934)

Lab ID#: 1612183-04A


0.16 0.49 0.79 2.4Freon 12

0.16 0.20 0.90 1.1Freon 11

0.80 1.4 1.5 2.6Ethanol

0.80 2.6 1.9 6.2Acetone

0.16 0.17 0.56 0.60Hexane

0.16 0.23 0.51 0.73Benzene

0.16 0.16 J 0.66 0.64 JHeptane

0.16 0.34 0.60 1.3Toluene

of 21

Client Sample ID: D1 (163931)Lab ID#: 1612183-01A

MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN

e121412File Name:Dil. Factor: 1.56

Date of Collection: 12/6/16 1:10:00 PMDate of Analysis: 12/14/16 05:49 PM


0.16 0.49 0.77 2.4Freon 120.16 Not Detected 1.1 Not DetectedFreon 1140.78 Not Detected 1.6 Not DetectedChloromethane0.16 Not Detected 0.40 Not DetectedVinyl Chloride0.16 Not Detected 0.34 Not Detected1,3-Butadiene0.78 Not Detected 3.0 Not DetectedBromomethane0.78 Not Detected 2.0 Not DetectedChloroethane0.16 0.23 0.88 1.3Freon 110.78 1.3 1.5 2.4Ethanol0.16 Not Detected 1.2 Not DetectedFreon 1130.16 Not Detected 0.62 Not Detected1,1-Dichloroethene0.78 2.8 1.8 6.7Acetone0.78 Not Detected 1.9 Not Detected2-Propanol0.78 Not Detected 2.4 Not DetectedCarbon Disulfide0.78 Not Detected 2.4 Not Detected3-Chloropropene0.31 Not Detected 1.1 Not DetectedMethylene Chloride0.16 Not Detected 0.56 Not DetectedMethyl tert-butyl ether0.16 Not Detected 0.62 Not Detectedtrans-1,2-Dichloroethene0.16 Not Detected 0.55 Not DetectedHexane0.16 Not Detected 0.63 Not Detected1,1-Dichloroethane0.78 Not Detected 2.3 Not Detected2-Butanone (Methyl Ethyl Ketone)0.16 Not Detected 0.62 Not Detectedcis-1,2-Dichloroethene0.78 Not Detected 2.3 Not DetectedTetrahydrofuran0.16 Not Detected 0.76 Not DetectedChloroform0.16 Not Detected 0.85 Not Detected1,1,1-Trichloroethane0.16 Not Detected 0.54 Not DetectedCyclohexane0.16 Not Detected 0.98 Not DetectedCarbon Tetrachloride0.78 Not Detected 3.6 Not Detected2,2,4-Trimethylpentane0.16 0.24 0.50 0.76Benzene0.16 Not Detected 0.63 Not Detected1,2-Dichloroethane0.16 Not Detected 0.64 Not DetectedHeptane0.16 Not Detected 0.84 Not DetectedTrichloroethene0.16 Not Detected 0.72 Not Detected1,2-Dichloropropane0.16 Not Detected 0.56 Not Detected1,4-Dioxane0.16 Not Detected 1.0 Not DetectedBromodichloromethane0.16 Not Detected 0.71 Not Detectedcis-1,3-Dichloropropene0.16 Not Detected 0.64 Not Detected4-Methyl-2-pentanone0.16 0.16 0.59 0.60Toluene0.16 Not Detected 0.71 Not Detectedtrans-1,3-Dichloropropene0.16 Not Detected 0.85 Not Detected1,1,2-Trichloroethane0.16 Not Detected 1.0 Not DetectedTetrachloroethene0.78 Not Detected 3.2 Not Detected2-Hexanone

of 21






0.16 Not Detected 1.3 Not DetectedDibromochloromethane0.16 Not Detected 1.2 Not Detected1,2-Dibromoethane (EDB)0.16 Not Detected 0.72 Not DetectedChlorobenzene0.16 Not Detected 0.68 Not DetectedEthyl Benzene0.16 Not Detected 0.68 Not Detectedm,p-Xylene0.16 Not Detected 0.68 Not Detectedo-Xylene0.16 Not Detected 0.66 Not DetectedStyrene0.16 Not Detected 1.6 Not DetectedBromoform0.16 Not Detected 0.77 Not DetectedCumene0.16 Not Detected 1.1 Not Detected1,1,2,2-Tetrachloroethane0.16 Not Detected 0.77 Not DetectedPropylbenzene0.16 Not Detected 0.77 Not Detected4-Ethyltoluene0.16 Not Detected 0.77 Not Detected1,3,5-Trimethylbenzene0.16 Not Detected 0.77 Not Detected1,2,4-Trimethylbenzene0.16 Not Detected 0.94 Not Detected1,3-Dichlorobenzene0.16 Not Detected 0.94 Not Detected1,4-Dichlorobenzene0.16 Not Detected 0.81 Not Detectedalpha-Chlorotoluene0.16 Not Detected 0.94 Not Detected1,2-Dichlorobenzene0.78 Not Detected 5.8 Not Detected1,2,4-Trichlorobenzene0.78 Not Detected 8.3 Not DetectedHexachlorobutadiene

Container Type: 6 Liter Summa Canister (100% Certified)

Limits%RecoverySurrogatesMethod

112 70-1301,2-Dichloroethane-d4102 70-130Toluene-d895 70-1304-Bromofluorobenzene

of 21






0.16 0.46 0.81 2.3Freon 120.16 Not Detected 1.1 Not DetectedFreon 1140.82 Not Detected 1.7 Not DetectedChloromethane0.16 Not Detected 0.42 Not DetectedVinyl Chloride0.16 Not Detected 0.36 Not Detected1,3-Butadiene0.82 Not Detected 3.2 Not DetectedBromomethane0.82 Not Detected 2.2 Not DetectedChloroethane0.16 0.21 0.92 1.2Freon 110.82 1.1 1.5 2.0Ethanol0.16 Not Detected 1.2 Not DetectedFreon 1130.16 Not Detected 0.65 Not Detected1,1-Dichloroethene0.82 3.0 1.9 7.2Acetone0.82 Not Detected 2.0 Not Detected2-Propanol0.82 Not Detected 2.6 Not DetectedCarbon Disulfide0.82 Not Detected 2.6 Not Detected3-Chloropropene0.33 Not Detected 1.1 Not DetectedMethylene Chloride0.16 Not Detected 0.59 Not DetectedMethyl tert-butyl ether0.16 Not Detected 0.65 Not Detectedtrans-1,2-Dichloroethene0.16 0.22 0.58 0.77Hexane0.16 Not Detected 0.66 Not Detected1,1-Dichloroethane0.82 Not Detected 2.4 Not Detected2-Butanone (Methyl Ethyl Ketone)0.16 Not Detected 0.65 Not Detectedcis-1,2-Dichloroethene0.82 Not Detected 2.4 Not DetectedTetrahydrofuran0.16 Not Detected 0.80 Not DetectedChloroform0.16 Not Detected 0.89 Not Detected1,1,1-Trichloroethane0.16 Not Detected 0.56 Not DetectedCyclohexane0.16 Not Detected 1.0 Not DetectedCarbon Tetrachloride0.82 Not Detected 3.8 Not Detected2,2,4-Trimethylpentane0.16 0.25 0.52 0.80Benzene0.16 Not Detected 0.66 Not Detected1,2-Dichloroethane0.16 0.21 0.67 0.84Heptane0.16 Not Detected 0.88 Not DetectedTrichloroethene0.16 Not Detected 0.76 Not Detected1,2-Dichloropropane0.16 Not Detected 0.59 Not Detected1,4-Dioxane0.16 Not Detected 1.1 Not DetectedBromodichloromethane0.16 Not Detected 0.74 Not Detectedcis-1,3-Dichloropropene0.16 Not Detected 0.67 Not Detected4-Methyl-2-pentanone0.16 0.26 0.62 0.99Toluene0.16 Not Detected 0.74 Not Detectedtrans-1,3-Dichloropropene0.16 Not Detected 0.89 Not Detected1,1,2-Trichloroethane0.16 Not Detected 1.1 Not DetectedTetrachloroethene0.82 Not Detected 3.4 Not Detected2-Hexanone

of 21










of 21

Client Sample ID: U1 (163933)Lab ID#: 1612183-03A





0.16 0.42 0.78 2.1Freon 120.16 Not Detected 1.1 Not DetectedFreon 1140.79 Not Detected 1.6 Not DetectedChloromethane0.16 Not Detected 0.40 Not DetectedVinyl Chloride0.16 Not Detected 0.35 Not Detected1,3-Butadiene0.79 Not Detected 3.1 Not DetectedBromomethane0.79 Not Detected 2.1 Not DetectedChloroethane0.16 0.17 0.89 0.96Freon 110.79 1.1 1.5 2.0Ethanol0.16 Not Detected 1.2 Not DetectedFreon 1130.16 Not Detected 0.63 Not Detected1,1-Dichloroethene0.79 2.2 1.9 5.2Acetone0.79 Not Detected 1.9 Not Detected2-Propanol0.79 Not Detected 2.5 Not DetectedCarbon Disulfide0.79 Not Detected 2.5 Not Detected3-Chloropropene0.32 Not Detected 1.1 Not DetectedMethylene Chloride0.16 Not Detected 0.57 Not DetectedMethyl tert-butyl ether0.16 Not Detected 0.63 Not Detectedtrans-1,2-Dichloroethene0.16 0.16 0.56 0.57Hexane0.16 Not Detected 0.64 Not Detected1,1-Dichloroethane0.79 Not Detected 2.3 Not Detected2-Butanone (Methyl Ethyl Ketone)0.16 Not Detected 0.63 Not Detectedcis-1,2-Dichloroethene0.79 Not Detected 2.3 Not DetectedTetrahydrofuran0.16 Not Detected 0.77 Not DetectedChloroform0.16 Not Detected 0.86 Not Detected1,1,1-Trichloroethane0.16 Not Detected 0.54 Not DetectedCyclohexane0.16 Not Detected 0.99 Not DetectedCarbon Tetrachloride0.79 Not Detected 3.7 Not Detected2,2,4-Trimethylpentane0.16 0.20 0.50 0.63Benzene0.16 Not Detected 0.64 Not Detected1,2-Dichloroethane0.16 Not Detected 0.65 Not DetectedHeptane0.16 Not Detected 0.85 Not DetectedTrichloroethene0.16 Not Detected 0.73 Not Detected1,2-Dichloropropane0.16 Not Detected 0.57 Not Detected1,4-Dioxane0.16 Not Detected 1.0 Not DetectedBromodichloromethane0.16 Not Detected 0.72 Not Detectedcis-1,3-Dichloropropene0.16 Not Detected 0.65 Not Detected4-Methyl-2-pentanone0.16 0.16 0.60 0.60Toluene0.16 Not Detected 0.72 Not Detectedtrans-1,3-Dichloropropene0.16 Not Detected 0.86 Not Detected1,1,2-Trichloroethane0.16 Not Detected 1.1 Not DetectedTetrachloroethene0.79 Not Detected 3.2 Not Detected2-Hexanone

of 21










of 21






0.16 0.49 0.79 2.4Freon 120.16 Not Detected 1.1 Not DetectedFreon 1140.80 Not Detected 1.6 Not DetectedChloromethane0.16 Not Detected 0.41 Not DetectedVinyl Chloride0.16 Not Detected 0.35 Not Detected1,3-Butadiene0.80 Not Detected 3.1 Not DetectedBromomethane0.80 Not Detected 2.1 Not DetectedChloroethane0.16 0.20 0.90 1.1Freon 110.80 1.4 1.5 2.6Ethanol0.16 Not Detected 1.2 Not DetectedFreon 1130.16 Not Detected 0.63 Not Detected1,1-Dichloroethene0.80 2.6 1.9 6.2Acetone0.80 Not Detected 2.0 Not Detected2-Propanol0.80 Not Detected 2.5 Not DetectedCarbon Disulfide0.80 Not Detected 2.5 Not Detected3-Chloropropene0.32 Not Detected 1.1 Not DetectedMethylene Chloride0.16 Not Detected 0.58 Not DetectedMethyl tert-butyl ether0.16 Not Detected 0.63 Not Detectedtrans-1,2-Dichloroethene0.16 0.17 0.56 0.60Hexane0.16 Not Detected 0.65 Not Detected1,1-Dichloroethane0.80 Not Detected 2.4 Not Detected2-Butanone (Methyl Ethyl Ketone)0.16 Not Detected 0.63 Not Detectedcis-1,2-Dichloroethene0.80 Not Detected 2.4 Not DetectedTetrahydrofuran0.16 Not Detected 0.78 Not DetectedChloroform0.16 Not Detected 0.87 Not Detected1,1,1-Trichloroethane0.16 Not Detected 0.55 Not DetectedCyclohexane0.16 Not Detected 1.0 Not DetectedCarbon Tetrachloride0.80 Not Detected 3.7 Not Detected2,2,4-Trimethylpentane0.16 0.23 0.51 0.73Benzene0.16 Not Detected 0.65 Not Detected1,2-Dichloroethane0.16 0.16 J 0.66 0.64 JHeptane0.16 Not Detected 0.86 Not DetectedTrichloroethene0.16 Not Detected 0.74 Not Detected1,2-Dichloropropane0.16 Not Detected 0.58 Not Detected1,4-Dioxane0.16 Not Detected 1.1 Not DetectedBromodichloromethane0.16 Not Detected 0.73 Not Detectedcis-1,3-Dichloropropene0.16 Not Detected 0.66 Not Detected4-Methyl-2-pentanone0.16 0.34 0.60 1.3Toluene0.16 Not Detected 0.73 Not Detectedtrans-1,3-Dichloropropene0.16 Not Detected 0.87 Not Detected1,1,2-Trichloroethane0.16 Not Detected 1.1 Not DetectedTetrachloroethene0.80 Not Detected 3.3 Not Detected2-Hexanone

of 21







J = Estimated value.Container Type: 6 Liter Summa Canister (100% Certified)



of 21

Client Sample ID: Lab BlankLab ID#: 1612183-05A



Date of Collection: NA Date of Analysis: 12/14/16 01:56 PM


0.10 Not Detected 0.49 Not DetectedFreon 120.10 Not Detected 0.70 Not DetectedFreon 1140.50 Not Detected 1.0 Not DetectedChloromethane0.10 Not Detected 0.26 Not DetectedVinyl Chloride0.10 Not Detected 0.22 Not Detected1,3-Butadiene0.50 Not Detected 1.9 Not DetectedBromomethane0.50 Not Detected 1.3 Not DetectedChloroethane0.10 Not Detected 0.56 Not DetectedFreon 110.50 Not Detected 0.94 Not DetectedEthanol0.10 Not Detected 0.77 Not DetectedFreon 1130.10 Not Detected 0.40 Not Detected1,1-Dichloroethene0.50 Not Detected 1.2 Not DetectedAcetone0.50 Not Detected 1.2 Not Detected2-Propanol0.50 Not Detected 1.6 Not DetectedCarbon Disulfide0.50 Not Detected 1.6 Not Detected3-Chloropropene0.20 Not Detected 0.69 Not DetectedMethylene Chloride0.10 Not Detected 0.36 Not DetectedMethyl tert-butyl ether0.10 Not Detected 0.40 Not Detectedtrans-1,2-Dichloroethene0.10 Not Detected 0.35 Not DetectedHexane0.10 Not Detected 0.40 Not Detected1,1-Dichloroethane0.50 Not Detected 1.5 Not Detected2-Butanone (Methyl Ethyl Ketone)0.10 Not Detected 0.40 Not Detectedcis-1,2-Dichloroethene0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.10 Not Detected 0.49 Not DetectedChloroform0.10 Not Detected 0.54 Not Detected1,1,1-Trichloroethane0.10 Not Detected 0.34 Not DetectedCyclohexane0.10 Not Detected 0.63 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.10 Not Detected 0.32 Not DetectedBenzene0.10 Not Detected 0.40 Not Detected1,2-Dichloroethane0.10 Not Detected 0.41 Not DetectedHeptane0.10 Not Detected 0.54 Not DetectedTrichloroethene0.10 Not Detected 0.46 Not Detected1,2-Dichloropropane0.10 Not Detected 0.36 Not Detected1,4-Dioxane0.10 Not Detected 0.67 Not DetectedBromodichloromethane0.10 Not Detected 0.45 Not Detectedcis-1,3-Dichloropropene0.10 Not Detected 0.41 Not Detected4-Methyl-2-pentanone0.10 Not Detected 0.38 Not DetectedToluene0.10 Not Detected 0.45 Not Detectedtrans-1,3-Dichloropropene0.10 Not Detected 0.54 Not Detected1,1,2-Trichloroethane0.10 Not Detected 0.68 Not DetectedTetrachloroethene0.50 Not Detected 2.0 Not Detected2-Hexanone

of 21

Client Sample ID: Lab BlankLab ID#: 1612183-05A






Container Type: NA - Not Applicable



of 21

Client Sample ID: CCVLab ID#: 1612183-06A



Date of Collection: NA Date of Analysis: 12/14/16 11:14 AM

%RecoveryCompound

96Freon 1291Freon 114118Chloromethane94Vinyl Chloride1001,3-Butadiene92Bromomethane92Chloroethane93Freon 1189Ethanol86Freon 113841,1-Dichloroethene97Acetone1022-Propanol88Carbon Disulfide883-Chloropropene91Methylene Chloride82Methyl tert-butyl ether82trans-1,2-Dichloroethene94Hexane941,1-Dichloroethane832-Butanone (Methyl Ethyl Ketone)90cis-1,2-Dichloroethene114Tetrahydrofuran94Chloroform881,1,1-Trichloroethane86Cyclohexane92Carbon Tetrachloride942,2,4-Trimethylpentane108Benzene1111,2-Dichloroethane112Heptane96Trichloroethene1081,2-Dichloropropane991,4-Dioxane104Bromodichloromethane93cis-1,3-Dichloropropene1244-Methyl-2-pentanone104Toluene95trans-1,3-Dichloropropene961,1,2-Trichloroethane92Tetrachloroethene972-Hexanone

of 21

Client Sample ID: CCVLab ID#: 1612183-06A




%RecoveryCompound

101Dibromochloromethane961,2-Dibromoethane (EDB)94Chlorobenzene97Ethyl Benzene95m,p-Xylene94o-Xylene97Styrene98Bromoform97Cumene1121,1,2,2-Tetrachloroethane99Propylbenzene964-Ethyltoluene971,3,5-Trimethylbenzene871,2,4-Trimethylbenzene911,3-Dichlorobenzene951,4-Dichlorobenzene103alpha-Chlorotoluene961,2-Dichlorobenzene821,2,4-Trichlorobenzene95Hexachlorobutadiene

Container Type: NA - Not Applicable



of 21

Client Sample ID: LCSLab ID#: 1612183-07A




Limits%RecoveryCompoundMethod

106 70-130Freon 1299 70-130Freon 114

147 Q 70-130Chloromethane108 70-130Vinyl Chloride106 70-1301,3-Butadiene100 70-130Bromomethane102 70-130Chloroethane99 70-130Freon 1174 70-130Ethanol92 70-130Freon 11390 70-1301,1-Dichloroethene109 70-130Acetone115 70-1302-Propanol93 70-130Carbon Disulfide89 70-1303-Chloropropene96 70-130Methylene Chloride92 70-130Methyl tert-butyl ether95 70-130trans-1,2-Dichloroethene106 70-130Hexane101 70-1301,1-Dichloroethane96 70-1302-Butanone (Methyl Ethyl Ketone)90 70-130cis-1,2-Dichloroethene127 70-130Tetrahydrofuran101 70-130Chloroform96 70-1301,1,1-Trichloroethane97 70-130Cyclohexane75 70-130Carbon Tetrachloride105 70-1302,2,4-Trimethylpentane114 70-130Benzene119 70-1301,2-Dichloroethane124 70-130Heptane106 70-130Trichloroethene114 70-1301,2-Dichloropropane99 70-1301,4-Dioxane114 70-130Bromodichloromethane104 70-130cis-1,3-Dichloropropene

132 Q 70-1304-Methyl-2-pentanone110 70-130Toluene97 70-130trans-1,3-Dichloropropene106 70-1301,1,2-Trichloroethane98 70-130Tetrachloroethene98 70-1302-Hexanone

of 21

Client Sample ID: LCSLab ID#: 1612183-07A





103 70-130Dibromochloromethane102 70-1301,2-Dibromoethane (EDB)100 70-130Chlorobenzene103 70-130Ethyl Benzene102 70-130m,p-Xylene101 70-130o-Xylene101 70-130Styrene100 70-130Bromoform103 70-130Cumene112 70-1301,1,2,2-Tetrachloroethane105 70-130Propylbenzene101 70-1304-Ethyltoluene103 70-1301,3,5-Trimethylbenzene92 70-1301,2,4-Trimethylbenzene96 70-1301,3-Dichlorobenzene99 70-1301,4-Dichlorobenzene87 70-130alpha-Chlorotoluene99 70-1301,2-Dichlorobenzene73 70-1301,2,4-Trichlorobenzene98 70-130Hexachlorobutadiene

Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable



of 21

Client Sample ID: LCSDLab ID#: 1612183-07AA





103 70-130Freon 1296 70-130Freon 114

141 Q 70-130Chloromethane105 70-130Vinyl Chloride104 70-1301,3-Butadiene97 70-130Bromomethane92 70-130Chloroethane97 70-130Freon 1173 70-130Ethanol90 70-130Freon 11388 70-1301,1-Dichloroethene106 70-130Acetone112 70-1302-Propanol91 70-130Carbon Disulfide89 70-1303-Chloropropene95 70-130Methylene Chloride89 70-130Methyl tert-butyl ether94 70-130trans-1,2-Dichloroethene104 70-130Hexane97 70-1301,1-Dichloroethane92 70-1302-Butanone (Methyl Ethyl Ketone)87 70-130cis-1,2-Dichloroethene125 70-130Tetrahydrofuran98 70-130Chloroform93 70-1301,1,1-Trichloroethane93 70-130Cyclohexane73 70-130Carbon Tetrachloride103 70-1302,2,4-Trimethylpentane111 70-130Benzene113 70-1301,2-Dichloroethane123 70-130Heptane105 70-130Trichloroethene113 70-1301,2-Dichloropropane100 70-1301,4-Dioxane110 70-130Bromodichloromethane104 70-130cis-1,3-Dichloropropene130 70-1304-Methyl-2-pentanone108 70-130Toluene95 70-130trans-1,3-Dichloropropene102 70-1301,1,2-Trichloroethane97 70-130Tetrachloroethene98 70-1302-Hexanone

of 21

Client Sample ID: LCSDLab ID#: 1612183-07AA





101 70-130Dibromochloromethane103 70-1301,2-Dibromoethane (EDB)102 70-130Chlorobenzene103 70-130Ethyl Benzene102 70-130m,p-Xylene102 70-130o-Xylene100 70-130Styrene100 70-130Bromoform104 70-130Cumene112 70-1301,1,2,2-Tetrachloroethane105 70-130Propylbenzene102 70-1304-Ethyltoluene99 70-1301,3,5-Trimethylbenzene90 70-1301,2,4-Trimethylbenzene96 70-1301,3-Dichlorobenzene100 70-1301,4-Dichlorobenzene89 70-130alpha-Chlorotoluene100 70-1301,2-Dichlorobenzene74 70-1301,2,4-Trichlorobenzene97 70-130Hexachlorobutadiene

Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable



of 21

12/27/2016 mr. curt lueckenhoff project12/27/2016 mr. curt lueckenhoff missouri dept. of natural...

Documents