Nanosize Surface Electromodification of Carbon Fibers by ConductivePolymers and Their CharacterizationsProf.Dr.A.Sezai.SARAIstanbul Technical UniversityDepartment of Chemistry & Polymer Science and TechnologyMaslak 80626Istanbul,Turkey

Carbon fiber reinforcement of polymeric composites

Carbon fibers(CF) are used in composites(i.e.,PAN based CF) in order to produce materials of lower density and greater strength. advanced structural materials: aircraft, spacecraft, and suspension bridges The most widely used composite material in tactical aircraft is a carbon fibre/epoxy A polymeric interface acting as a coupling agent, improve the interfacial properties between reinforcing (carbon) fibers and the polymeric matrix .

5-7A.S. Sarac, A. Bismarck, E. Kumru, J. Springer,Synth. Met. 123 (2001) 411-423E.Kumru,J.Springer,A.S.Sarac,A.Bismarck., Synth. Met. 123(2001)391-402

Biosensor Appl.

Electromodified carbon fibers also have potential for biosensor applications as microelectrodes -working in small volumes of solutions-

Homogeneous Conductive Polymer coated -surface functionalities is suitable for the miniaturization of electrode system for a particular analyte. Several copolymer and polymer coated electrodes(Cz based) were shown to be an effective disposable microelectrode system for the determination of p-aminophenol at low detection limits

M. Jamal, E. Magner, A.S.Sarac, Sensors and Actuators 97 (2004)59-66

Carbon Fiber Reinforcement applying force to a composite material, the brittle matrix cracks at low stress levels > fibres take over

Epoxy resin polymer matrixWoven fiber

The structure & comp. of copolymeric films, plays an important role on the final properties of modified carbon surface The coating parameters & characterization of these functionalised thin films are important .

Improving the interfacial adhesionAdvanced Composites- Interfacial adhesioncontrol the level of fiber/matrix adhesion

A.S.Sarac,M.Serantoni,,A.M.T.Syed,V.J.Cunnane ,Appl.Surface Sci.,(2004) 229,13-18A.S.Sarac,A.M.T.Syed,M.Serantoni,,V.J.Cunnane J.Mater.Sci.Lett.(2004) 39,2945-2950

Surface Analysis (the characterizations of electrografted thin polymeric film ~10-50nm film characterizations-Fast and simple for org. thin film coating & charac. -Nanosize Change of functionality of surface)

Spectroscopic FunctionalitiesFTIR-ATRRamanComposition - XPS,EDX,FIBSIMSElectrochemical Impedance Spectroscopic studiesMorphologicalSEMAFM

AFM of Electrogrowth of P[Cz-co-AAm] onto HOPG Graphite Higher scan rates (100mV/s) : thin (hf22nm) coatings .Lower scan rates (50mV/s) ~50nm A.Bismarck,A.Menner,J.Barner,A.F.Lee,K.Wilson,J.Springer,J.P.Rabe,A.S.Sarac, Surface Coat .Tech. 145(2001)164-175

Current density vs cycle number (): 1.53V (): 1.04 Vand the coating thickness () from the ellipsometric angles

Galvanostatic vs.Cyclic voltammetrypolymerization rate vs.film growth. CV : Galvanostatic process thin coating (hf15nm) & smoother (RMS=13nm),

polyethylenedioxythiophene(PEDOT)AFM of Untreated Carbon fiber(r~5.6 )

Polyterthiophene/CF

Chart1

0.0000212097-0.0004657898-0.0007727051-0.001163025-0.001700439-0.002423096-0.002782593-0.004216309-0.006079102-0.00798645

0.0000241089-0.0004277954-0.0007275391-0.001105652-0.001636353-0.002351074-0.00270874-0.004131165-0.005984497-0.007867432

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0.0000298462-0.0003755493-0.0006585693-0.001020508-0.001535339-0.002233887-0.00258606-0.003977966-0.005804443-0.007653809

0.0000311279-0.00036203-0.0006420898-0.0009991455-0.00151001-0.002204895-0.002554016-0.003938599-0.005758667-0.007589722

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0.0004011230.00018652340.0000006714-0.000186615-0.0005218506-0.0008453369-0.0009210205-0.001951294-0.003149719-0.004361572

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0.00043441770.00021142580.000022522-0.0001610107-0.0004925537-0.0008117676-0.000869751-0.001902161-0.003092957-0.004301758

0.00045098880.00022409060.0000348511-0.0001487427-0.0004760742-0.0007910156-0.0008432007-0.001875-0.003064575-0.004277954

0.00046856690.00023715210.0000463562-0.0001335144-0.0004608154-0.0007736206-0.0008166504-0.00184845-0.003043213-0.004240112

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0.00051971440.00027691650.0000832825-0.0000933533-0.0004135132-0.0007159424-0.0007357788-0.001768494-0.002955322-0.00414917

0.00053771970.00029153440.000095398-0.0000783081-0.0003763123-0.000696106-0.0007064819-0.001741943-0.002927246-0.004116211

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