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Page 1: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

'$- )+$M'$*#.%.#2+)#*+)1 )*+,-+./!01!234&4

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&'!ORKU!'&:2 G#N\! NXLN7!!:2&@:(2

PN-QL7!]2/293 &&

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9'9!G !>KKL.*+!EMNLLM

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1!QLNM-PU!MV*M!MVL!*+*KU,L,!WLNP#NSLX!TU!MVL!0A6B!6+Y-N#+SL+M*K!)*T#N*M#NU!ZLNL!Q#+XRQMLX!TU!SLMV#X,!

*WWN#YLX!TU!MVL![ E !6+Y-N#+SL+M*K!PN#MLQM-#+!>.L+QU!*+X!#MVLN!*WWN#WN-*ML!NL.RK*M#NU!*.L+Q-L,

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Page 1 of 25

Page 2: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!2!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

79:;<==9<L>?@A?B /$#3(456 >J>?9&?:9!7A?A?B!">@K:<K&=LM!L>N:!/LJ

C2C!"D!>EE(0 8!@5$((5 @G5(!L#'(6 S*,,,,RQ R !"# $%

,.T,2T2,*+L 8OG80!7AP!+QR,R /$#3(45!7 8 0($6 F(11!/G84HI (

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LMLL<B"!2,!*,U<*CU *+,-*.+<,* " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!2*!*,U<*CU *+,-*.+<,2 " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!22!*2U<*.U *+,-*.+<,S " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!2S!*,<*CU *+,-*.+<,+ " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!2+!*,<*CU *+,-*.+<,C " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!S.!RU<*+ *+,-*.+<,- " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!*R!*,<*CU *+,-*.+<,. " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!*Q!*,<*CU *+,-*.+<,Q " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL<B"!2C!RU<*+U *+,-*.+<,R " 5($ ,-T*2T2,*+ ,-T*ST2,*+

LMLL<B"!2-!RU<*+U *+,-*.+<*, " 5($ ,-T*2T2,*+ ,-T*ST2,*+

LMLL</LA!7"!*,Q> *+,-*.+<** " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL</LA!7"!*,QJ *+,-*.+<*2 " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL</LA!7"!**S *+,-*.+<*S " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL</LA!7"!**Q *+,-*.+<*+ " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL</LA!7"!*2, *+,-*.+<*C " 5($ ,-T**T2,*+ ,-T*ST2,*+

LMLL</LA!7"!**S!9V/ *+,-*.+<*- " 5($ ,-T**T2,*+ ,-T*ST2,*+

;!# 8*'6$*, 7161#1!68*

W2* =(X#$5G80!LGIG5O!Y=LZ!$ GO('!'H(!5#!I 5$G[!G85($1($(84(D

W*. /$# E(!X(5$#E(HI!X$#'H45YOZ!X$(O(85D

K =(X#$5('!\ EH(!GO!E(OO!5] 8!5](!$(X#$5G80!EGIG5!Y=LZD!!=(OHE5!GO!(O5GI 5('D

F> =(OHE5!GO!(O5GI 5('!'H(!5#!IHE5GXE(!>$#4E#$O!X$(O(85D

>,* =(OHE5YOZ! 8'!$(X#$5G80!EGIG5YOZ! $(!(O5GI 5('!'H(!5#!E#^!OH$$#0 5(!$(4#\($_D

?9 A8'G4 5(O!4#IX#H8'! 8 E_`('!1#$! H5!8#5!'(5(45('

=L =(X#$5G80!LGIG5

?> ?#5!>XXEG4 E(

L !"#$%!&$'($!)!*+,-*.+

Page 2 of 25

Page 3: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!S!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*F>*<>GA<HG

-'.*+,%*<=>?<@=A><

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138A& (14!)'#1) 8

R*<C.<- 2<7(5]_E8 X]5] E(8( ?9 CD, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

QS<S2<R >4(8 X]5](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,Q<R-<Q >4(8 X]5]_E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*2,<*2<. >85]$ 4(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

C-<CC<S J(8`b c 85]$ 4(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

C,<S2<Q J(8`#b cX_$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,C<RR<2 J(8`#b c1EH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*R*<2+<2 J(8`#b0P]PGcX($_E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,.<,Q<R J(8`#b%c1EH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2*Q<,*<R L]$_O(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

CS<.,<S 9G (8`b P]c 85]$ 4(8( ?9 2D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,-<++<, aEH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

Q-<.S<. aEH#$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*RS<SR<C A8'(8#Y*P2PS<4P'ZX_$(8( ?9 2D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

R*<2,<S ? X]5] E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

QC<,*<Q /](8 85]$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*2R<,,<, /_$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

'())*+,-./%2"01(*)*2345.671 $! 2%& 2 !"!!# :$;!9;! J+a*-*2 829:

'())*+,-./%<3-)*2.6=.6."># 8 :%& !9 8"!!# :$;!9;! J+a*-*2 829:

'())*+,-./%4"@.)45.671">! 9? 2%& ! 8"!!# :$;!9;! J+a*-*2 829:

I"J'6138AKBL8*'8*5"!3)!"8

*2-.+<**<2 >$#4E#$!*,*- ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***,+<2Q<2 >$#4E#$!*22* ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 #? :%& ?:"!#: :$;2!;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. ## ?%& ?:"!#: :$;2!;! J+a*.,* 8:8!;8:82

L !"#$%!&$'($!)!*+,-*.+

Page 3 of 25

Page 4: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!+!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*F>*<>GA<HG

-'.*+,%*<=>?<@=A><

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

+6!"J'6138A0 #')8

.+2R<R,<C 5):(161:( <M>> CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<S-<, 56#1(!6/ FNO *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SQ<2 5"8 613 PH *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SR<S L'"1:( @H CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+*<. J($_EEGHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+S<R L 'IGHI ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+.<S BQ"!(1:( ONH *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+Q<+ L# E5 ?9 CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<C,<Q B! " <P *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<QR<- +"!6 PH> 2, H0TL * ,-T2CT*+ J+a*-,S -,*,T2,,D.

.+SR<R2<* L( ' ?9 *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.+SR<R-<C 0'6J'6 8 <O CD, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<R.<- 7($4H$_ ?9 ,D2 H0TL * ,-T2CT*+ J+a2S,. .+.,T2+CD*

.++,<,2<, ;13R ) HN@ 2D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

..Q2<+R<2 & ) 61:( FN> *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<22<+ @GE\($ ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<--<- S163 F= CD, H0TL * ,-TS,T*+ J+a*-,S -,2,T2,,DQ

L !"#$%!&$'($!)!*+,-*.+

Page 4 of 25

Page 5: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!C!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*F<*<>GA<HG

-'.*+,%*<=>?<@=A>F

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138A& (14!)'#1) 8

R*<C.<- 2<7(5]_E8 X]5] E(8( ?9 CD, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

QS<S2<R >4(8 X]5](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,Q<R-<Q >4(8 X]5]_E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*2,<*2<. >85]$ 4(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

C-<CC<S J(8`b c 85]$ 4(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

C,<S2<Q J(8`#b cX_$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,C<RR<2 J(8`#b c1EH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*R*<2+<2 J(8`#b0P]PGcX($_E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,.<,Q<R J(8`#b%c1EH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2*Q<,*<R L]$_O(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

CS<.,<S 9G (8`b P]c 85]$ 4(8( ?9 2D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

2,-<++<, aEH#$ 85](8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

Q-<.S<. aEH#$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*RS<SR<C A8'(8#Y*P2PS<4P'ZX_$(8( ?9 2D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

R*<2,<S ? X]5] E(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

QC<,*<Q /](8 85]$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

*2R<,,<, /_$(8( ?9 *D, H0TL * ,-T*.T*+ J+a*-*2 Q2.,

'())*+,-./%2"01(*)*2345.671 $! :%& 2 !"!!# :$;!9;! J+a*-*2 829:

'())*+,-./%<3-)*2.6=.6."># 8 !%& !9 8"!!# :$;!9;! J+a*-*2 829:

'())*+,-./%4"@.)45.671">! 9! 2%& ! 8"!!# :$;!9;! J+a*-*2 829:

I"J'6138AKBL8*'8*5"!3)!"8

*2-.+<**<2 >$#4E#$!*,*- ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***,+<2Q<2 >$#4E#$!*22* ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T2*T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 ?# !%& ?:"!#: :$;2!;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. 8 %& ?:"!#: :$;2!;! J+a*.,* 8:8!;8:82

L !"#$%!&$'($!)!*+,-*.+

Page 5 of 25

Page 6: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!-!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*F<*<>GA<HG

-'.*+,%*<=>?<@=A>F

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

+6!"J'6138A0 #')8

.+2R<R,<C 5):(161:( ?>> CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<S-<, >85GI#8_ ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SQ<2 5"8 613 <P *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SR<S L'"1:( OO CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+*<. J($_EEGHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+S<R L 'IGHI ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+.<S BQ"!(1:( =N@ *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+Q<+ L# E5 ?9 CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<C,<Q B! " <O> *, H0TL *, ,-TS,T*+ J+a*-,S -,2,T2,,DQ

.+SR<QR<- +"!6 OO> 2, H0TL * ,-T2CT*+ J+a*-,S -,*,T2,,D.

.+SR<R2<* L( ' ?9 *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.+SR<R-<C 0'6J'6 8 FM CD, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<R.<- 7($4H$_ ?9 ,D2 H0TL * ,-T2CT*+ J+a2S,. .+.,T2+CD*

.++,<,2<, ;13R ) HN> 2D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

..Q2<+R<2 @(E(8GHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<22<+ @GE\($ ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<--<- S163 <=> C, H0TL *, ,-TS,T*+ J+a*-,S -,2,T2,,DQ

L !"#$%!&$'($!)!*+,-*.+

Page 6 of 25

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***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 #8 !%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. #8 ?%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

L !"#$%!&$'($!)!*+,-*.+

Page 11 of 25

Page 12: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!*2!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*O@*MGA<=

-'.*+,%*<=>?<@=A>?

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

+6!"J'6138A0 #')8

.+2R<R,<C 5):(161:( =O> CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<S-<, >85GI#8_ ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SQ<2 >$O(8G4 ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SR<S L'"1:( P= CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+*<. J($_EEGHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+S<R L 'IGHI ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+.<S BQ"!(1:( <N= *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+Q<+ L# E5 ?9 CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<C,<Q B! " HM *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<QR<- +"!6 PP> 2, H0TL * ,-T2CT*+ J+a*-,S -,*,T2,,D.

.+SR<R2<* - '$ @NM *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.+SR<R-<C 0'6J'6 8 <@ CD, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<R.<- 7($4H$_ ?9 ,D2 H0TL * ,-T2CT*+ J+a2S,. .+.,T2+CD*

.++,<,2<, ;13R ) HNF 2D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

..Q2<+R<2 @(E(8GHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<22<+ @GE\($ ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<--<- S163 @F CD, H0TL * ,-TS,T*+ J+a*-,S -,2,T2,,DQ

L !"#$%!&$'($!)!*+,-*.+

Page 12 of 25

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/ 0(!*S!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*<M*<>A<HG

-'.*+,%*<=>?<@=A>@

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138AKBL8*'8*5"!3)!"8

*2-.+<**<2 >$#4E#$!*,*- ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,+<2Q<2 >$#4E#$!*22* ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 # :%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. #2 :%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

+6!"J'6138A0 #')8

.+2R<R,<C 5):(161:( <O>> CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<S-<, >85GI#8_ ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SQ<2 5"8 613 <F *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SR<S L'"1:( FF CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+*<. J($_EEGHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+S<R B'$(1:( >NF ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+.<S BQ"!(1:( <= *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+Q<+ L# E5 ?9 CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<C,<Q B! " ==> *, H0TL *, ,-TS,T*+ J+a*-,S -,2,T2,,DQ

.+SR<QR<- +"!6 F@>>> 2,, H0TL *, ,-T2CT*+ J+a*-,S -,*,T2,,D.

.+SR<R2<* - '$ @NM *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.+SR<R-<C 0'6J'6 8 FO> CD, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<R.<- 7($4H$_ ?9 ,D2 H0TL * ,-T2CT*+ J+a2S,. .+.,T2+CD*

.++,<,2<, ;13R ) F< 2D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

..Q2<+R<2 @(E(8GHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<22<+ &1)4 " ON> ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<--<- S163 ?> CD, H0TL * ,-TS,T*+ J+a*-,S -,2,T2,,DQ

L !"#$%!&$'($!)!*+,-*.+

Page 13 of 25

Page 14: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!*+!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*<P*<>A<HG

-'.*+,%*<=>?<@=A>P

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138A& (14!)'#1) 8

R*<C.<- 2<7(5]_E8 X]5] E(8( ?9 CD* H0TL * ,-T*RT*+ J+a*-*2 Q2.,

QS<S2<R >4(8 X]5](8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

2,Q<R-<Q >4(8 X]5]_E(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

*2,<*2<. >85]$ 4(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

C-<CC<S J(8`b c 85]$ 4(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

C,<S2<Q J(8`#b cX_$(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

2,C<RR<2 J(8`#b c1EH#$ 85](8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

*R*<2+<2 J(8`#b0P]PGcX($_E(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

2,.<,Q<R J(8`#b%c1EH#$ 85](8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

2*Q<,*<R L]$_O(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

CS<.,<S 9G (8`b P]c 85]$ 4(8( ?9 2D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

2,-<++<, aEH#$ 85](8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

Q-<.S<. aEH#$(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

*RS<SR<C A8'(8#Y*P2PS<4P'ZX_$(8( ?9 2D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

R*<2,<S ? X]5] E(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

QC<,*<Q /](8 85]$(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

*2R<,,<, /_$(8( ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

'())*+,-./%2"01(*)*2345.671 ## %& 2 !"!!# :$;!E;! J+a*-*2 829:

'())*+,-./%<3-)*2.6=.6."># #2 !%& !9 8"!!# :$;!E;! J+a*-*2 829:

'())*+,-./%4"@.)45.671">! $2 E%& ! 8"!!# :$;!E;! J+a*-*2 829:

I"J'6138AKBL8*'8*5"!3)!"8

*2-.+<**<2 >$#4E#$!*,*- ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,+<2Q<2 >$#4E#$!*22* ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 #8 2%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. #2 2%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

L !"#$%!&$'($!)!*+,-*.+

Page 14 of 25

Page 15: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!*C!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*<P*<>A<HG

-'.*+,%*<=>?<@=A>P

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

+6!"J'6138A0 #')8

.+2R<R,<C 5):(161:( ?>>> C, H0TL *, ,-TS,T*+ J+a*-,S -,2,T2,,DQ

.++,<S-<, >85GI#8_ ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<SQ<2 5"8 613 <NM *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<SR<S L'"1:( PM CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+*<. J($_EEGHI ?9 *D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+S<R L 'IGHI ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<+.<S BQ"!(1:( <P *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<+Q<+ L# E5 ?9 CD, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<C,<Q B! " <P> *, H0TL *, ,-TS,T*+ J+a*-,S -,2,T2,,DQ

.+SR<QR<- +"!6 H@>> 2, H0TL * ,-T2CT*+ J+a*-,S -,*,T2,,D.

.+SR<R2<* - '$ O= *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.+SR<R-<C 0'6J'6 8 =@ CD, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.+SR<R.<- 7($4H$_ ?9 ,D2 H0TL * ,-T2CT*+ J+a2S,. .+.,T2+CD*

.++,<,2<, ;13R ) <F 2D, H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

..Q2<+R<2 @(E(8GHI ?9 *D, H0TL * ,-T2.T*+ J+a*-,S -,2,T2,,DQ

.++,<22<+ @GE\($ ?9 ,D2 H0TL * ,-T2-T*+ J+a*-,S -,2,T2,,DQ

.++,<--<- S163 O< CD, H0TL * ,-TS,T*+ J+a*-,S -,2,T2,,DQ

L !"#$%!&$'($!)!*+,-*.+

Page 15 of 25

Page 16: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!*-!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*FH*MGA<=G

-'.*+,%*<=>?<@=A>M

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138AKBL8*'8*5"!3)!"8

*2-.+<**<2 >$#4E#$!*,*- ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,+<2Q<2 >$#4E#$!*22* ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***+*<*-<C >$#4E#$!*2S2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

CS+-R<2*<R >$#4E#$!*2+2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

*2-.2<2R<- >$#4E#$!*2+Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R.<-R<* >$#4E#$!*2C+ ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

**,R-<Q2<C >$#4E#$!*2-, ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

S.S2+<2S<C >$#4E#$!*2-2 ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

***,,<*+<+ >$#4E#$!*2-Q ?9 ,D*, H0TL * ,-T22T*+ J+a*.,* Q,Q*TQ,Q2

'())*+,-./%A.B,B51*)*2345.671 $ #%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

'())*+,-./%@.-),B51*)*"C"D71.6. 9 8%& ?:"!#: :$;22;! J+a*.,* 8:8!;8:82

L !"#$%!&$'($!)!*+,-*.+

Page 16 of 25

Page 17: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

/ 0(!*.!#1!2+

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

B)1 6#*+,%*BC--ADE*F?*MGA<=G

-'.*+,%*<=>?<@=A<>

>8 E_`('bL>@!) >8 E_5( =(OHE5 =L V8G5O 9GEH5G#8 9 5( ;L!J 54] 7(5]#' ;H EG1G($b

I"J'6138A& (14!)'#1) 8

2<7(5]_E8 X]5] E(8(R*<C.<- ?9 CD* H0TL * ,-T*RT*+ J+a*-*2 Q2.,

>4(8 X]5](8(QS<S2<R ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

>4(8 X]5]_E(8(2,Q<R-<Q ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

>85]$ 4(8(*2,<*2<. ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

J(8`b c 85]$ 4(8(C-<CC<S ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

J(8`#b cX_$(8(C,<S2<Q ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

J(8`#b c1EH#$ 85](8(2,C<RR<2 ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

J(8`#b0P]PGcX($_E(8(*R*<2+<2 ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

J(8`#b%c1EH#$ 85](8(2,.<,Q<R ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

L]$_O(8(2*Q<,*<R ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

9G (8`b P]c 85]$ 4(8(CS<.,<S ?9 2D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

aEH#$ 85](8(2,-<++<, ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

aEH#$(8(Q-<.S<. ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

A8'(8#Y*P2PS<4P'ZX_$(8(*RS<SR<C ?9 2D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

? X]5] E(8(R*<2,<S ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

/](8 85]$(8(QC<,*<Q ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

/_$(8(*2R<,,<, ?9 *D, H0TL * ,-T*RT*+ J+a*-*2 Q2.,

'())*+,-./%2"01(*)*2345.671 2 8%& 2 !"!!# :$;!E;! J+a*-*2 829:

'())*+,-./%<3-)*2.6=.6."># $ 8%& !9 8"!!# :$;!E;! J+a*-*2 829:

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Page 24 of 25

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Page 25 of 25

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-LANSING

RE: ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing, MI 48909

525 W. Allegan Street

Jeff Pincumbe

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.

Sincerely,

03 July 2014 Work Order: 1406177

Price: $2,800.00

George Krisztian

Laboratory Director

Lab Work Order # 1406177

Page 1 of 13Page 1 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-LANSING

525 W. Allegan Street

Jeff Pincumbe

ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing MI, 48909

Site Code: 3100009807/03/2014

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1406177-01 Soil/Sediment 06/13/2014CHLL-SB 33 6''-12'' 06/11/2014

1406177-02 Soil/Sediment 06/13/2014CHLL-SB 33 1'-4' 06/11/2014

1406177-03 Soil/Sediment 06/13/2014CHLL-SB34 6''-12'' 06/11/2014

1406177-04 Soil/Sediment 06/13/2014CHLL-SB 34 1'-4' 06/11/2014

1406177-05 Soil/Sediment 06/13/2014CHLL-SB 34 1'-4' DUP 06/11/2014

1406177-06 Soil/Sediment 06/13/2014CHLL-SB35 1'-4' 06/11/2014

1406177-07 Soil/Sediment 06/13/2014CHLL-SB36 6''-12'' 06/11/2014

1406177-08 Soil/Sediment 06/13/2014CHLL-SB 36 1'-4' 06/11/2014

1406177-09 Soil/Sediment 06/13/2014CHLL-SB37 6''-12'' 06/11/2014

1406177-10 Soil/Sediment 06/13/2014CHLL-SB 37 1'-4' 06/11/2014

Notes and Definitions

Y21 Reporting Limits (RL) raised due to matrix interference.

X3 Spike recovery is not applicable due to large target analyte concentration in the source sample.

T Reported value is less than the reporting limit (RL). Result is estimated.

JA Result is estimated due to multiple Aroclors present.

I Dilution required due to matrix interference; reporting limit (RL) raised.

A09 Result is estimated due to high recovery of batch quality control.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

dry Sample results reported on a dry weight basis

Not ApplicableNA

Lab Work Order # 1406177

Page 2 of 13Page 2 of 13

Page 28: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-01

RLCAS #

Client ID: CHLL-SB 33 6''-12''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-15075.5 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15075.3 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1494.2 B4F1611

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1000 mg/kg dry 10000 6020/200.8Aluminium7429-90-5 07/02/1422000 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1415 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1440 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.9 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1439 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/1424 B4F1903

1000 mg/kg dry 10000 6020/200.8Copper7440-50-8 07/02/145300 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1430000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1417 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14740 B4F1903

0.05 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/140.06 B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1479 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.3 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/141.8 B4F1903

10 mg/kg dry 100 6020/200.8Zinc7440-66-6 07/01/14170 B4F1903

Lab Work Order # 1406177

Page 3 of 13Page 3 of 13

Page 29: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-02

RLCAS #

Client ID: CHLL-SB 33 1'-4'

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-150108 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15092.5 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1490.5 B4F1611

Lab Work Order # 1406177

Page 4 of 13Page 4 of 13

Page 30: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-03

RLCAS #

Client ID: CHLL-SB34 6''-12''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

110 JAug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14660 B4F1923

110 JAug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14250 B4F1923

260 Y21ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15038.2 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15056.7 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1489.8 B4F1611

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/1413000 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/1456 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/141600 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/14340 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.7 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/147.3 B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/14200 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/1413 B4F1903

100 mg/kg dry 1000 6020/200.8Copper7440-50-8 07/02/1463000 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1447000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/14660 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14440 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/140.4 B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1476 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/02/140.8 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/1413 B4F1903

100 mg/kg dry 1000 6020/200.8Zinc7440-66-6 07/02/143000 B4F1903

Lab Work Order # 1406177

Page 5 of 13Page 5 of 13

Page 31: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-04

RLCAS #

Client ID: CHLL-SB 34 1'-4'

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15069.6 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15076.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1493.3 B4F1611

Lab Work Order # 1406177

Page 6 of 13Page 6 of 13

Page 32: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-05

RLCAS #

Client ID: CHLL-SB 34 1'-4' DUP

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15056.9 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15057.1 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1494.1 B4F1611

Lab Work Order # 1406177

Page 7 of 13Page 7 of 13

Page 33: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-06

RLCAS #

Client ID: CHLL-SB35 1'-4'

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15075.2 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15064.0 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1492.4 B4F1611

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

10 mg/kg dry 100 6020/200.8Aluminium7429-90-5 07/02/143100 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/02/141.9 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1414 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/14ND B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1415 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/142.6 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/02/1421 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/146800 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/02/141.4 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1454 B4F1903

0.05 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/14ND B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/147.1 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/14ND B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/14ND B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1413 B4F1903

Lab Work Order # 1406177

Page 8 of 13Page 8 of 13

Page 34: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-07

RLCAS #

Client ID: CHLL-SB36 6''-12''

QC Batch

Organics-PCBs as Aroclors

100 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15064.0 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15063.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1499.5 B4F1611

0.10 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1000 mg/kg dry 10000 6020/200.8Aluminium7429-90-5 07/02/1433000 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/140.5 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/145.5 B4F1903

10 mg/kg dry 100 6020/200.8Barium7440-39-3 07/01/141400 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/141.4 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/14130 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/1411 B4F1903

1000 mg/kg dry 10000 6020/200.8Copper7440-50-8 07/02/1413000 B4F1903

50 A09mg/kg dry 100 6010/200.7Iron7439-89-6 06/27/14140000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1429 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14690 B4F1903

0.05 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/14ND B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1413 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.2 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/141.9 B4F1903

10 mg/kg dry 100 6020/200.8Zinc7440-66-6 07/01/14140 B4F1903

Lab Work Order # 1406177

Page 9 of 13Page 9 of 13

Page 35: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-08

RLCAS #

Client ID: CHLL-SB 36 1'-4'

QC Batch

Organics-PCBs as Aroclors

100 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15077.4 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15067.9 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1498.8 B4F1611

Lab Work Order # 1406177

Page 10 of 13Page 10 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-09

RLCAS #

Client ID: CHLL-SB37 6''-12''

QC Batch

Organics-PCBs as Aroclors

100 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

100 Tug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/1498 B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15040.5 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15059.0 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1495.7 B4F1611

1.0 Img/kg dry 10 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/1425000 B4F1903

0.3 A03mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/145.9 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1427 B4F1903

10 mg/kg dry 100 6020/200.8Barium7440-39-3 07/01/141000 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/141.6 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/1410 B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1488 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/149.2 B4F1903

100 mg/kg dry 1000 6020/200.8Copper7440-50-8 07/02/1410000 B4F1903

50 A09mg/kg dry 100 6010/200.7Iron7439-89-6 06/27/1490000 B4F1903

10 A03mg/kg dry 100 6020/200.8Lead7439-92-1 07/01/14210 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14580 B4F1903

0.05 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/140.06 B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1417 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.4 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/143.4 B4F1903

100 mg/kg dry 1000 6020/200.8Zinc7440-66-6 07/02/14690 B4F1903

Lab Work Order # 1406177

Page 11 of 13Page 11 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406177-10

RLCAS #

Client ID: CHLL-SB 37 1'-4'

QC Batch

Organics-PCBs as Aroclors

100 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

100 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15046.9 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15050.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1496.2 B4F1611

Lab Work Order # 1406177

Page 12 of 13Page 12 of 13

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Page 13 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-LANSING

RE: ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing, MI 48909

525 W. Allegan Street

Jeff Pincumbe

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.

Sincerely,

07 July 2014 Work Order: 1406230

Price: $1,350.00

George Krisztian

Laboratory Director

Lab Work Order # 1406230

Page 1 of 13Page 1 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-LANSING

525 W. Allegan Street

Jeff Pincumbe

ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing MI, 48909

Site Code: 3100009807/07/2014

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1406230-01 Soil/Sediment 06/18/2014CHLL-SD 50-0''-6'' 06/14/2014

1406230-02 Soil/Sediment 06/18/2014CHLL-SD 50-1'-3' 06/14/2014

1406230-03 Soil/Sediment 06/18/2014CHLL-SD 50-3'-5' 06/14/2014

1406230-04 Soil/Sediment 06/18/2014CHLL-SD 09-0''-6'' 06/15/2014

1406230-05 Soil/Sediment 06/18/2014CHLL-SD 09-1'-2.1' 06/15/2014

1406230-06 Soil/Sediment 06/18/2014CHLL-SD 09-1'-2.1' dup 06/15/2014

1406230-07 Soil/Sediment 06/18/2014CHLL-SD 10-0''-6'' 06/15/2014

1406230-08 Soil/Sediment 06/18/2014CHLL-SD 10-1'-2' 06/15/2014

1406230-09 Soil/Sediment 06/18/2014CHLL-SD 12-0''-6'' 06/15/2014

1406230-10 Soil/Sediment 06/18/2014CHLL-SD 12-1'-2.5' 06/15/2014

Notes and Definitions

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Lab Work Order # 1406230

Page 2 of 13Page 2 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-01

RLCAS #

Client ID: CHLL-SD 50-0''-6''

QC Batch

Organics-PCBs as Aroclors

190 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15066.8 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15073.1 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1453.2 B4F1909

Lab Work Order # 1406230

Page 3 of 13Page 3 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-02

RLCAS #

Client ID: CHLL-SD 50-1'-3'

QC Batch

Organics-PCBs as Aroclors

190 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

190 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15084.3 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15093.7 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1452.8 B4F1909

Lab Work Order # 1406230

Page 4 of 13Page 4 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-03

RLCAS #

Client ID: CHLL-SD 50-3'-5'

QC Batch

Organics-PCBs as Aroclors

180 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

180 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15077.7 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15084.8 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1455.3 B4F1909

Lab Work Order # 1406230

Page 5 of 13Page 5 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-04

RLCAS #

Client ID: CHLL-SD 09-0''-6''

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15078.0 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15069.5 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1473.1 B4F1909

Lab Work Order # 1406230

Page 6 of 13Page 6 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-05

RLCAS #

Client ID: CHLL-SD 09-1'-2.1'

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15084.0 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15070.5 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1474.9 B4F1909

Lab Work Order # 1406230

Page 7 of 13Page 7 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-06

RLCAS #

Client ID: CHLL-SD 09-1'-2.1' dup

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15068.2 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15060.4 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1474.0 B4F1909

Lab Work Order # 1406230

Page 8 of 13Page 8 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-07

RLCAS #

Client ID: CHLL-SD 10-0''-6''

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15074.2 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15068.5 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1469.5 B4F1909

Lab Work Order # 1406230

Page 9 of 13Page 9 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-08

RLCAS #

Client ID: CHLL-SD 10-1'-2'

QC Batch

Organics-PCBs as Aroclors

150 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15090.4 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15083.8 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1468.1 B4F1909

Lab Work Order # 1406230

Page 10 of 13Page 10 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-09

RLCAS #

Client ID: CHLL-SD 12-0''-6''

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15088.4 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15077.6 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1472.5 B4F1909

Lab Work Order # 1406230

Page 11 of 13Page 11 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406230-10

RLCAS #

Client ID: CHLL-SD 12-1'-2.5'

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15087.9 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15075.6 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1476.7 B4F1909

Lab Work Order # 1406230

Page 12 of 13Page 12 of 13

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Page 13 of 13

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-LANSING

RE: ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing, MI 48909

525 W. Allegan Street

Jeff Pincumbe

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.

Sincerely,

07 July 2014 Work Order: 1406229

Price: $2,700.00

George Krisztian

Laboratory Director

Lab Work Order # 1406229

Page 1 of 23Page 1 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-LANSING

525 W. Allegan Street

Jeff Pincumbe

ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing MI, 48909

Site Code: 3100009807/07/2014

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1406229-01 Soil/Sediment 06/18/2014CHLL-SD 70-0-6'' 06/14/2014

1406229-02 Soil/Sediment 06/18/2014CHLL-SD 70-1'-3' 06/14/2014

1406229-03 Soil/Sediment 06/18/2014CHLL-SD 70-3-'4.5' 06/14/2014

1406229-04 Soil/Sediment 06/18/2014CHLL-SD 66-0''-6'' 06/14/2014

1406229-05 Soil/Sediment 06/18/2014CHLL-SD 66-1'-1.5' 06/14/2014

1406229-06 Soil/Sediment 06/18/2014CHLL-SD 65-0''-6'' 06/14/2014

1406229-07 Soil/Sediment 06/18/2014CHLL-SD 65-.75'-1' 06/14/2014

1406229-08 Soil/Sediment 06/18/2014CHLL-SD 51-0''-6'' 06/14/2014

1406229-09 Soil/Sediment 06/18/2014CHLL-SD 51-1'-3' 06/14/2014

1406229-10 Soil/Sediment 06/18/2014CHLL-SD 51-3'-5' 06/14/2014

1406229-11 Soil/Sediment 06/18/2014CHLL-SD 13-0''-6'' 06/15/2014

1406229-12 Soil/Sediment 06/18/2014CHLL-SD 13-1'-2' 06/15/2014

1406229-13 Soil/Sediment 06/18/2014CHLL-SD 13-1'-2' dup 06/15/2014

1406229-14 Soil/Sediment 06/18/2014CHLL-SD 15-0-6'' 06/16/2014

1406229-15 Soil/Sediment 06/18/2014CHLL-SD 15-1'-2.7' 06/16/2014

1406229-16 Soil/Sediment 06/18/2014CHLL-SD 20-0-6'' 06/16/2014

1406229-17 Soil/Sediment 06/18/2014CHLL-SD 20-1'-2' 06/16/2014

1406229-18 Soil/Sediment 06/18/2014CHLL-SD 22-0-6'' 06/16/2014

1406229-19 Soil/Sediment 06/18/2014CHLL-SD 22-0-6'' dup 06/16/2014

1406229-20 Soil/Sediment 06/18/2014CHLL-SD 22-1'-1.5' 06/16/2014

Notes and Definitions

Y21 Reporting Limits (RL) raised due to matrix interference.

JA Result is estimated due to multiple Aroclors present.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

dry Sample results reported on a dry weight basis

Not ApplicableNA

Lab Work Order # 1406229

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-01

RLCAS #

Client ID: CHLL-SD 70-0-6''

QC Batch

Organics-PCBs as Aroclors

250 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

250 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15070.4 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15082.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1439.9 B4F1908

Lab Work Order # 1406229

Page 3 of 23Page 3 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-02

RLCAS #

Client ID: CHLL-SD 70-1'-3'

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15074.3 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15071.9 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1472.5 B4F1908

Lab Work Order # 1406229

Page 4 of 23Page 4 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-03

RLCAS #

Client ID: CHLL-SD 70-3-'4.5'

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15068.8 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15072.0 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1472.0 B4F1908

Lab Work Order # 1406229

Page 5 of 23Page 5 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-04

RLCAS #

Client ID: CHLL-SD 66-0''-6''

QC Batch

Organics-PCBs as Aroclors

170 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

170 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15073.6 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15073.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1457.6 B4F1908

Lab Work Order # 1406229

Page 6 of 23Page 6 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-05

RLCAS #

Client ID: CHLL-SD 66-1'-1.5'

QC Batch

Organics-PCBs as Aroclors

220 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

220 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15063.9 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15073.5 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1446.5 B4F1908

Lab Work Order # 1406229

Page 7 of 23Page 7 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-06

RLCAS #

Client ID: CHLL-SD 65-0''-6''

QC Batch

Organics-PCBs as Aroclors

210 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/28/14ND B4F1923

210 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/28/14ND B4F1923

30-15065.8 %Surrogate: Decachlorobiphenyl 8081/808206/28/14 B4F1923

30-15071.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/28/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1447.2 B4F1908

Lab Work Order # 1406229

Page 8 of 23Page 8 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-07

RLCAS #

Client ID: CHLL-SD 65-.75'-1'

QC Batch

Organics-PCBs as Aroclors

1000 Y21ug/kg dry 5 8081/8082Aroclor 101612674-11-2 06/30/14ND B4F1923

1000 Y21ug/kg dry 5 8081/8082Aroclor 122111104-28-2 06/30/14ND B4F1923

1000 Y21ug/kg dry 5 8081/8082Aroclor 123211141-16-5 06/30/14ND B4F1923

1000 Y21ug/kg dry 5 8081/8082Aroclor 124253469-21-9 06/30/14ND B4F1923

1000 Y21ug/kg dry 5 8081/8082Aroclor 124812672-29-6 06/30/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/29/14ND B4F1923

30-15054.1 %Surrogate: Decachlorobiphenyl 8081/808206/29/14 B4F1923

30-15065.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/29/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1449.7 B4F1908

Lab Work Order # 1406229

Page 9 of 23Page 9 of 24

Page 61: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-08

RLCAS #

Client ID: CHLL-SD 51-0''-6''

QC Batch

Organics-PCBs as Aroclors

190 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/29/14ND B4F1923

190 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/29/14ND B4F1923

30-15069.5 %Surrogate: Decachlorobiphenyl 8081/808206/29/14 B4F1923

30-15080.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/29/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1451.6 B4F1908

Lab Work Order # 1406229

Page 10 of 23Page 10 of 24

Page 62: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-09

RLCAS #

Client ID: CHLL-SD 51-1'-3'

QC Batch

Organics-PCBs as Aroclors

180 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/29/14ND B4F1923

180 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/29/14ND B4F1923

30-15077.5 %Surrogate: Decachlorobiphenyl 8081/808206/29/14 B4F1923

30-15081.9 %Surrogate: Tetrachloro-m-xylene 8081/808206/29/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1455.5 B4F1908

Lab Work Order # 1406229

Page 11 of 23Page 11 of 24

Page 63: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-10

RLCAS #

Client ID: CHLL-SD 51-3'-5'

QC Batch

Organics-PCBs as Aroclors

200 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/29/14ND B4F1923

200 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/29/14ND B4F1923

30-15070.4 %Surrogate: Decachlorobiphenyl 8081/808206/29/14 B4F1923

30-15072.3 %Surrogate: Tetrachloro-m-xylene 8081/808206/29/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1449.2 B4F1908

Lab Work Order # 1406229

Page 12 of 23Page 12 of 24

Page 64: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-11

RLCAS #

Client ID: CHLL-SD 13-0''-6''

QC Batch

Organics-PCBs as Aroclors

140 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/29/14ND B4F1923

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/29/14ND B4F1923

30-15073.4 %Surrogate: Decachlorobiphenyl 8081/808206/29/14 B4F1923

30-15067.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/29/14 B4F1923

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1470.9 B4F1908

Lab Work Order # 1406229

Page 13 of 23Page 13 of 24

Page 65: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-12

RLCAS #

Client ID: CHLL-SD 13-1'-2'

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15089.9 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15070.0 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1478.2 B4F1908

Lab Work Order # 1406229

Page 14 of 23Page 14 of 24

Page 66: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-13

RLCAS #

Client ID: CHLL-SD 13-1'-2' dup

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14ND B4F2608

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15077.9 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15050.5 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1478.9 B4F1908

Lab Work Order # 1406229

Page 15 of 23Page 15 of 24

Page 67: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-14

RLCAS #

Client ID: CHLL-SD 15-0-6''

QC Batch

Organics-PCBs as Aroclors

240 Y21ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

240 Y21ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

240 Y21ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

240 Y21ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

170 JAug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14230 B4F2608

170 JAug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14270 B4F2608

170 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

170 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14ND B4F2608

170 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15068.5 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15072.1 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1458.5 B4F1908

Lab Work Order # 1406229

Page 16 of 23Page 16 of 24

Page 68: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-15

RLCAS #

Client ID: CHLL-SD 15-1'-2.7'

QC Batch

Organics-PCBs as Aroclors

210 Y21ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

210 Y21ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

210 Y21ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

210 Y21ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

210 Y21ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14ND B4F2608

180 Y21ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14ND B4F2608

300 Y21ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14290 B4F2608

140 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15084.6 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15067.4 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1470.5 B4F1909

Lab Work Order # 1406229

Page 17 of 23Page 17 of 24

Page 69: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-16

RLCAS #

Client ID: CHLL-SD 20-0-6''

QC Batch

Organics-PCBs as Aroclors

150 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14ND B4F2608

150 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15091.1 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15073.9 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1468.1 B4F1909

Lab Work Order # 1406229

Page 18 of 23Page 18 of 24

Page 70: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-17

RLCAS #

Client ID: CHLL-SD 20-1'-2'

QC Batch

Organics-PCBs as Aroclors

120 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/01/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/01/14ND B4F2608

30-15080.5 %Surrogate: Decachlorobiphenyl 8081/808207/01/14 B4F2608

30-15066.0 %Surrogate: Tetrachloro-m-xylene 8081/808207/01/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1484.7 B4F1909

Lab Work Order # 1406229

Page 19 of 23Page 19 of 24

Page 71: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-18

RLCAS #

Client ID: CHLL-SD 22-0-6''

QC Batch

Organics-PCBs as Aroclors

120 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

120 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15079.5 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15064.4 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1486.0 B4F1909

Lab Work Order # 1406229

Page 20 of 23Page 20 of 24

Page 72: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-19

RLCAS #

Client ID: CHLL-SD 22-0-6'' dup

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15087.3 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15078.8 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1487.5 B4F1909

Lab Work Order # 1406229

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406229-20

RLCAS #

Client ID: CHLL-SD 22-1'-1.5'

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 07/02/14ND B4F2608

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 07/02/14ND B4F2608

30-15099.7 %Surrogate: Decachlorobiphenyl 8081/808207/02/14 B4F2608

30-15088.6 %Surrogate: Tetrachloro-m-xylene 8081/808207/02/14 B4F2608

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/19/1487.1 B4F1909

Lab Work Order # 1406229

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Page 23 of 24

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Page 24 of 24

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-LANSING

RE: ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing, MI 48909

525 W. Allegan Street

Jeff Pincumbe

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.

Sincerely,

08 July 2014 Work Order: 1406176

Price: $7,709.50

George Krisztian

Laboratory Director

Lab Work Order # 1406176

Page 1 of 42Page 1 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-LANSING

525 W. Allegan Street

Jeff Pincumbe

ABANDONED MINING WASTE-TORCH LAKE PCB

Lansing MI, 48909

Site Code: 3100009807/08/2014

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1406176-01 Soil/Sediment 06/13/2014CHLL-SB52 0-6'' 06/11/2014

1406176-02 Soil/Sediment 06/13/2014CHLL-SB52 6''-4' 06/11/2014

1406176-03 Soil/Sediment 06/13/2014CHLL-SB32 0-6'' 06/11/2014

1406176-04 Soil/Sediment 06/13/2014CHLL-SB32 6''-4' 06/11/2014

1406176-05 Soil/Sediment 06/13/2014CHLL-SB31 0-6'' 06/11/2014

1406176-06 Soil/Sediment 06/13/2014CHLL-SB31 6''-4' 06/11/2014

1406176-07 Soil/Sediment 06/13/2014CHLL-SB53 6''-12'' 06/12/2014

1406176-08 Soil/Sediment 06/13/2014CHLL-SB38 6''-12'' 06/12/2014

1406176-09 Soil/Sediment 06/13/2014CHLL-SB38 1'-4' 06/12/2014

1406176-10 Soil/Sediment 06/13/2014CHLL-SB39 6''-12'' 06/12/2014

1406176-11 Soil/Sediment 06/13/2014CHLL-SB39 1'-4' 06/12/2014

1406176-12 Soil/Sediment 06/13/2014CHLL-SB39 1'-4' DUP 06/12/2014

1406176-13 Soil/Sediment 06/13/2014CHLL-SB54 6''-18'' 06/12/2014

1406176-14 Soil/Sediment 06/13/2014CHLL-SB40 6''-12'' 06/12/2014

1406176-15 Soil/Sediment 06/13/2014CHLL-SB40 1'-4' 06/12/2014

1406176-16 Soil/Sediment 06/13/2014CHLL-SB41 6''-12'' 06/12/2014

1406176-17 Soil/Sediment 06/13/2014CHLL-SB41 1'-4' 06/12/2014

Lab Work Order # 1406176

Page 2 of 42Page 2 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Notes and Definitions

Y37 Raised RL due to possible laboratory contamination.

Y21 Reporting Limits (RL) raised due to matrix interference.

Y20 Reporting Limits (RL) raised due to matrix.

X3 Spike recovery is not applicable due to large target analyte concentration in the source sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene

have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

JA Result is estimated due to multiple Aroclors present.

A11 Result is estimated due to high initial verification standard criteria failure.

A10 Result and reporting limit are estimated due to low initial verification standard criteria failure.

A09 Result is estimated due to high recovery of batch quality control.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

dry Sample results reported on a dry weight basis

Not ApplicableNA

Lab Work Order # 1406176

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-01

RLCAS #

Client ID: CHLL-SB52 0-6''

QC Batch

Organics-Volatiles

70 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/18/14ND B4F1814

70 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/18/14ND B4F1814

70 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/18/14ND B4F1814

70 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/18/14ND B4F1814

70 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/18/14ND B4F1814

70 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/18/14ND B4F1814

350 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/18/14ND B4F1814

350 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/18/14110 B4F1814

350 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/18/14ND B4F1814

70 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/18/14ND B4F1814

70 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/18/14ND B4F1814

70 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/18/14ND B4F1814

70 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/18/14ND B4F1814

350 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/18/14ND B4F1814

350 ug/kg dry 50 82602-Hexanone591-78-6 06/18/14ND B4F1814

350 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/18/14ND B4F1814

1400 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/18/14ND B4F1814

350 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/18/14ND B4F1814

350 ug/kg dry 50 8260Acrylonitrile107-13-1 06/18/14ND B4F1814

70 ug/kg dry 50 8260Benzene71-43-2 06/18/14ND B4F1814

70 ug/kg dry 50 8260Bromobenzene108-86-1 06/18/14ND B4F1814

70 ug/kg dry 50 8260Bromochloromethane74-97-5 06/18/14ND B4F1814

70 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/18/14ND B4F1814

70 ug/kg dry 50 8260Bromoform75-25-2 06/18/14ND B4F1814

350 ug/kg dry 50 8260Bromomethane74-83-9 06/18/14ND B4F1814

70 ug/kg dry 50 8260Carbon disulfide75-15-0 06/18/14ND B4F1814

70 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/18/14ND B4F1814

70 ug/kg dry 50 8260Chlorobenzene108-90-7 06/18/14ND B4F1814

350 ug/kg dry 50 8260Chloroethane75-00-3 06/18/14ND B4F1814

70 ug/kg dry 50 8260Chloroform67-66-3 06/18/14ND B4F1814

350 ug/kg dry 50 8260Chloromethane74-87-3 06/18/14ND B4F1814

70 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/18/14ND B4F1814

70 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/18/14ND B4F1814

350 ug/kg dry 50 8260Cyclohexane110-82-7 06/18/14ND B4F1814

70 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/18/14ND B4F1814

Lab Work Order # 1406176

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-01

RLCAS #

Client ID: CHLL-SB52 0-6''

QC Batch

Organics-Volatiles

70 ug/kg dry 50 8260Dibromomethane74-95-3 06/18/14ND B4F1814

350 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/18/14ND B4F1814

350 ug/kg dry 50 8260Diethyl ether60-29-7 06/18/14ND B4F1814

350 A03, A05ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/18/14ND B4F1814

70 ug/kg dry 50 8260Ethylbenzene100-41-4 06/18/14ND B4F1814

350 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/18/14ND B4F1814

350 ug/kg dry 50 8260Hexachloroethane67-72-1 06/18/14ND B4F1814

70 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/18/14ND B4F1814

140 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/18/14210 B4F1814

280 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/18/14ND B4F1814

350 ug/kg dry 50 8260Methylene chloride75-09-2 06/18/14ND B4F1814

70 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/18/14ND B4F1814

350 Xug/kg dry 50 8260Naphthalene91-20-3 06/18/14ND B4F1814

70 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/18/14ND B4F1814

70 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/18/14ND B4F1814

70 ug/kg dry 50 8260o-Xylene95-47-6 06/18/14150 B4F1814

70 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/18/14ND B4F1814

70 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/18/14ND B4F1814

70 ug/kg dry 50 8260Styrene100-42-5 06/18/14ND B4F1814

70 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/18/14ND B4F1814

3500 A03ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/18/14ND B4F1814

350 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/18/14ND B4F1814

70 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/18/14ND B4F1814

350 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/18/14ND B4F1814

70 ug/kg dry 50 8260Toluene108-88-3 06/18/14190 B4F1814

70 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/18/14ND B4F1814

70 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/18/14ND B4F1814

350 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/18/14ND B4F1814

70 ug/kg dry 50 8260Trichloroethylene79-01-6 06/18/14ND B4F1814

70 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/18/14ND B4F1814

70 ug/kg dry 50 8260Vinyl chloride75-01-4 06/18/14ND B4F1814

50-15094.3 %Surrogate: Bromofluorobenzene 826006/18/14 B4F1814

50-15098.1 %Surrogate: Dibromofluoromethane 826006/18/14 B4F1814

50-15097.4 %Surrogate: Toluene-d8 826006/18/14 B4F1814

Lab Work Order # 1406176

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-01

RLCAS #

Client ID: CHLL-SB52 0-6''

QC Batch

Organics-Semivolatiles See note Y20, Y21

3000 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

2400 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

1200 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11571.2 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11582.9 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11585.2 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

120 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

330 Y21ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

210 Y21ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

210 Y21ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-15065.5 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15085.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Lab Work Order # 1406176

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-01

RLCAS #

Client ID: CHLL-SB52 0-6''

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1484.4 B4F1610

0.12 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1000 mg/kg dry 10000 6020/200.8Aluminium7429-90-5 07/02/148000 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/149.8 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/14120 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/14180 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.6 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/141.2 B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1434 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/147.1 B4F1903

1000 mg/kg dry 10000 6020/200.8Copper7440-50-8 07/01/1426000 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1419000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/141700 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14320 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.1 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1421 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/141.0 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/1410 B4F1903

1000 mg/kg dry 10000 6020/200.8Zinc7440-66-6 07/01/14ND B4F1903

Lab Work Order # 1406176

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-02

RLCAS #

Client ID: CHLL-SB52 6''-4'

QC Batch

Organics-Volatiles

61 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/18/14ND B4F1814

310 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/18/14ND B4F1814

310 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/18/14ND B4F1814

310 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/18/14ND B4F1814

61 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/18/14ND B4F1814

310 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/18/14ND B4F1814

310 ug/kg dry 50 82602-Hexanone591-78-6 06/18/14ND B4F1814

310 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/18/14ND B4F1814

1200 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/18/14ND B4F1814

310 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/18/14ND B4F1814

310 ug/kg dry 50 8260Acrylonitrile107-13-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Benzene71-43-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromobenzene108-86-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromochloromethane74-97-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromoform75-25-2 06/18/14ND B4F1814

310 ug/kg dry 50 8260Bromomethane74-83-9 06/18/14ND B4F1814

61 ug/kg dry 50 8260Carbon disulfide75-15-0 06/18/14ND B4F1814

61 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260Chlorobenzene108-90-7 06/18/14ND B4F1814

310 ug/kg dry 50 8260Chloroethane75-00-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260Chloroform67-66-3 06/18/14ND B4F1814

310 ug/kg dry 50 8260Chloromethane74-87-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/18/14ND B4F1814

310 ug/kg dry 50 8260Cyclohexane110-82-7 06/18/14ND B4F1814

61 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/18/14ND B4F1814

Lab Work Order # 1406176

Page 8 of 42Page 8 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-02

RLCAS #

Client ID: CHLL-SB52 6''-4'

QC Batch

Organics-Volatiles

61 ug/kg dry 50 8260Dibromomethane74-95-3 06/18/14ND B4F1814

310 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/18/14ND B4F1814

310 ug/kg dry 50 8260Diethyl ether60-29-7 06/18/14ND B4F1814

310 A05ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260Ethylbenzene100-41-4 06/18/14ND B4F1814

310 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/18/14ND B4F1814

310 ug/kg dry 50 8260Hexachloroethane67-72-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/18/14ND B4F1814

120 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/18/14ND B4F1814

61 A05, A10ug/kg dry 50 8260Methyl iodide74-88-4 06/18/14ND B4F1814

310 ug/kg dry 50 8260Methylene chloride75-09-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/18/14ND B4F1814

310 Xug/kg dry 50 8260Naphthalene91-20-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260o-Xylene95-47-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260Styrene100-42-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/18/14ND B4F1814

3100 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/18/14ND B4F1814

310 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/18/14ND B4F1814

310 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/18/14ND B4F1814

61 ug/kg dry 50 8260Toluene108-88-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/18/14ND B4F1814

310 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260Trichloroethylene79-01-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/18/14ND B4F1814

61 ug/kg dry 50 8260Vinyl chloride75-01-4 06/18/14ND B4F1814

50-15068.4 %Surrogate: Bromofluorobenzene 826006/18/14 B4F1814

50-15069.9 %Surrogate: Dibromofluoromethane 826006/18/14 B4F1814

50-15069.8 %Surrogate: Toluene-d8 826006/18/14 B4F1814

Lab Work Order # 1406176

Page 9 of 42Page 9 of 43

Page 85: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-02

RLCAS #

Client ID: CHLL-SB52 6''-4'

QC Batch

Organics-Semivolatiles See note Y20

560 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

230 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

230 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

230 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

230 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

230 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

450 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

230 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

230 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

450 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

230 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

230 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

230 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11581.1 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11597.4 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11584.2 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-15098.9 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15088.2 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Lab Work Order # 1406176

Page 10 of 42Page 10 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-02

RLCAS #

Client ID: CHLL-SB52 6''-4'

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1488.6 B4F1610

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/143300 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/140.4 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/143.4 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1429 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/148.0 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/142.6 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/141500 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/146100 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1428 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1487 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/14ND B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/147.5 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/14ND B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.6 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1423 B4F1903

Lab Work Order # 1406176

Page 11 of 42Page 11 of 43

Page 87: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-03

RLCAS #

Client ID: CHLL-SB32 0-6''

QC Batch

Organics-PCBs as Aroclors See note Y21

1200 ug/kg dry 5 8081/8082Aroclor 101612674-11-2 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 122111104-28-2 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 123211141-16-5 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 124253469-21-9 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 124812672-29-6 06/26/14ND B4F1720

1200 JAug/kg dry 5 8081/8082Aroclor 125411097-69-1 06/26/141400 B4F1720

1200 JAug/kg dry 5 8081/8082Aroclor 126011096-82-5 06/26/141900 B4F1720

2000 ug/kg dry 5 8081/8082Aroclor 126237324-23-5 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 126811100-14-4 06/26/14ND B4F1720

30-150142 %Surrogate: Decachlorobiphenyl 8081/808206/26/14 B4F1720

30-15084.7 %Surrogate: Tetrachloro-m-xylene 8081/808206/26/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1486.5 B4F1610

0.12 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1000 mg/kg dry 10000 6020/200.8Aluminium7429-90-5 07/02/147500 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/1446 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1439 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/14950 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.5 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1422 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/146.5 B4F1903

1000 mg/kg dry 10000 6020/200.8Copper7440-50-8 07/01/1433000 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1430000 B4F1903

1000 mg/kg dry 10000 6020/200.8Lead7439-92-1 07/01/148800 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14300 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.2 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1427 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/142.5 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/146.9 B4F1903

1000 mg/kg dry 10000 6020/200.8Zinc7440-66-6 07/01/144700 B4F1903

Lab Work Order # 1406176

Page 12 of 42Page 12 of 43

Page 88: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-04

RLCAS #

Client ID: CHLL-SB32 6''-4'

QC Batch

Organics-PCBs as Aroclors See note Y21

1200 ug/kg dry 5 8081/8082Aroclor 101612674-11-2 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 122111104-28-2 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 123211141-16-5 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 124253469-21-9 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 124812672-29-6 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 125411097-69-1 06/26/14ND B4F1720

2000 ug/kg dry 5 8081/8082Aroclor 126011096-82-5 06/26/14ND B4F1720

2000 ug/kg dry 5 8081/8082Aroclor 126237324-23-5 06/26/14ND B4F1720

1200 ug/kg dry 5 8081/8082Aroclor 126811100-14-4 06/26/14ND B4F1720

30-15095.2 %Surrogate: Decachlorobiphenyl 8081/808206/26/14 B4F1720

30-15085.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/26/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1484.7 B4F1610

0.12 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/140.17 B4F1606

Inorganics-Metals

1.0 mg/kg dry 10 6020/200.8Aluminium7429-90-5 07/02/142000 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/141.1 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1410 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1460 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/147.2 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/142.9 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14480 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1415000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1441 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1478 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.5 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/146.4 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.4 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/141.3 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1438 B4F1903

Lab Work Order # 1406176

Page 13 of 42Page 13 of 43

Page 89: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-05

RLCAS #

Client ID: CHLL-SB31 0-6''

QC Batch

Organics-PCBs as Aroclors See note Y21

550 ug/kg dry 5 8081/8082Aroclor 101612674-11-2 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 122111104-28-2 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 123211141-16-5 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 124253469-21-9 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 124812672-29-6 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 125411097-69-1 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 126011096-82-5 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 126237324-23-5 06/26/14ND B4F1720

550 ug/kg dry 5 8081/8082Aroclor 126811100-14-4 06/26/14ND B4F1720

30-15072.6 %Surrogate: Decachlorobiphenyl 8081/808206/26/14 B4F1720

30-15081.7 %Surrogate: Tetrachloro-m-xylene 8081/808206/26/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1490.2 B4F1610

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

10 mg/kg dry 100 6020/200.8Aluminium7429-90-5 07/02/141400 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/142.9 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1448 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/14380 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1414 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/141.7 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/141100 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1426000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/14440 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1464 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.06 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/148.6 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/141.9 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/142.9 B4F1903

10 mg/kg dry 100 6020/200.8Zinc7440-66-6 07/01/14120 B4F1903

Lab Work Order # 1406176

Page 14 of 42Page 14 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-06

RLCAS #

Client ID: CHLL-SB31 6''-4'

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-15099.4 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15091.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1488.8 B4F1610

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1.0 mg/kg dry 10 6020/200.8Aluminium7429-90-5 07/02/14650 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/140.4 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/1464 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1486 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/14ND B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/143.4 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/140.7 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14180 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1441000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1444 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1420 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/14ND B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/142.1 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/141.2 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.5 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1414 B4F1903

Lab Work Order # 1406176

Page 15 of 42Page 15 of 43

Page 91: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-07

RLCAS #

Client ID: CHLL-SB53 6''-12''

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-150104 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15091.5 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1478.8 B4F1610

0.13 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

10 mg/kg dry 100 6020/200.8Aluminium7429-90-5 07/02/144700 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/141.0 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/147.5 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/14240 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.5 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1413 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/144.3 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14400 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1448000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/142100 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14340 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.1 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1410 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.4 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/142.1 B4F1903

10 mg/kg dry 100 6020/200.8Zinc7440-66-6 07/01/14250 B4F1903

Lab Work Order # 1406176

Page 16 of 42Page 16 of 43

Page 92: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-08

RLCAS #

Client ID: CHLL-SB38 6''-12''

QC Batch

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-15099.2 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-150101 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1478.4 B4F1610

0.13 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

10 mg/kg dry 100 6020/200.8Aluminium7429-90-5 07/02/144800 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/140.3 B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/149.3 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1468 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.6 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1410 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/144.2 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14890 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1413000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1446 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14250 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.1 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/148.9 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.4 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.4 B4F1903

10 mg/kg dry 100 6020/200.8Zinc7440-66-6 07/01/1467 B4F1903

Lab Work Order # 1406176

Page 17 of 42Page 17 of 43

Page 93: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-09

RLCAS #

Client ID: CHLL-SB38 1'-4'

QC Batch

Organics-Volatiles

61 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/18/14ND B4F1814

61 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/18/14ND B4F1814

300 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/18/14ND B4F1814

300 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/18/14ND B4F1814

300 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/18/14ND B4F1814

61 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/18/14ND B4F1814

61 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/18/14ND B4F1814

61 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/18/14ND B4F1814

61 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/18/14ND B4F1814

300 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/18/14ND B4F1814

300 ug/kg dry 50 82602-Hexanone591-78-6 06/18/14ND B4F1814

300 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/18/14ND B4F1814

1200 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/18/14ND B4F1814

300 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/18/14ND B4F1814

300 ug/kg dry 50 8260Acrylonitrile107-13-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Benzene71-43-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromobenzene108-86-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromochloromethane74-97-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/18/14ND B4F1814

61 ug/kg dry 50 8260Bromoform75-25-2 06/18/14ND B4F1814

300 ug/kg dry 50 8260Bromomethane74-83-9 06/18/14ND B4F1814

61 ug/kg dry 50 8260Carbon disulfide75-15-0 06/18/14ND B4F1814

61 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260Chlorobenzene108-90-7 06/18/14ND B4F1814

300 ug/kg dry 50 8260Chloroethane75-00-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260Chloroform67-66-3 06/18/14ND B4F1814

300 ug/kg dry 50 8260Chloromethane74-87-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/18/14ND B4F1814

300 ug/kg dry 50 8260Cyclohexane110-82-7 06/18/14ND B4F1814

61 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/18/14ND B4F1814

Lab Work Order # 1406176

Page 18 of 42Page 18 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-09

RLCAS #

Client ID: CHLL-SB38 1'-4'

QC Batch

Organics-Volatiles

61 ug/kg dry 50 8260Dibromomethane74-95-3 06/18/14ND B4F1814

300 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/18/14ND B4F1814

300 ug/kg dry 50 8260Diethyl ether60-29-7 06/18/14ND B4F1814

300 A05ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260Ethylbenzene100-41-4 06/18/14ND B4F1814

300 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/18/14ND B4F1814

300 ug/kg dry 50 8260Hexachloroethane67-72-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/18/14ND B4F1814

120 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/18/14ND B4F1814

240 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/18/14ND B4F1814

300 ug/kg dry 50 8260Methylene chloride75-09-2 06/18/14ND B4F1814

61 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/18/14ND B4F1814

300 Xug/kg dry 50 8260Naphthalene91-20-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/18/14ND B4F1814

61 ug/kg dry 50 8260o-Xylene95-47-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260Styrene100-42-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/18/14ND B4F1814

3000 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/18/14ND B4F1814

300 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/18/14ND B4F1814

61 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/18/14ND B4F1814

300 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/18/14ND B4F1814

61 ug/kg dry 50 8260Toluene108-88-3 06/18/14ND B4F1814

61 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/18/14ND B4F1814

61 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/18/14ND B4F1814

300 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260Trichloroethylene79-01-6 06/18/14ND B4F1814

61 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/18/14ND B4F1814

61 ug/kg dry 50 8260Vinyl chloride75-01-4 06/18/14ND B4F1814

50-150101 %Surrogate: Bromofluorobenzene 826006/18/14 B4F1814

50-150103 %Surrogate: Dibromofluoromethane 826006/18/14 B4F1814

50-150103 %Surrogate: Toluene-d8 826006/18/14 B4F1814

Lab Work Order # 1406176

Page 19 of 42Page 19 of 43

Page 95: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-09

RLCAS #

Client ID: CHLL-SB38 1'-4'

QC Batch

Organics-Semivolatiles See note Y20

560 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

220 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

220 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

220 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

220 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

450 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

220 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

450 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

220 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

220 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

450 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

220 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

220 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

220 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11568.9 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11583.5 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11593.9 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-150111 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15091.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Lab Work Order # 1406176

Page 20 of 42Page 20 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-09

RLCAS #

Client ID: CHLL-SB38 1'-4'

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1489.1 B4F1610

Lab Work Order # 1406176

Page 21 of 42Page 21 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-10

RLCAS #

Client ID: CHLL-SB39 6''-12''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-15091.9 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15084.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1489.1 B4F1610

0.11 mg/kg dry 1 ASTM D 7511-09Total Cyanide57-12-5 06/18/14ND B4F1606

Inorganics-Metals

1.0 mg/kg dry 10 6020/200.8Aluminium7429-90-5 07/02/141900 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/143.5 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1425 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.2 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/145.7 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/141.5 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14300 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/145700 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1414 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/1476 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/140.09 B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/144.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.2 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.1 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1429 B4F1903

Lab Work Order # 1406176

Page 22 of 42Page 22 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-11

RLCAS #

Client ID: CHLL-SB39 1'-4'

QC Batch

Organics-Volatiles

69 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/19/14ND B4F1825

69 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/19/14ND B4F1825

69 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/19/14ND B4F1825

69 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/19/14ND B4F1825

69 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/19/14ND B4F1825

69 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/19/14ND B4F1825

340 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/19/14ND B4F1825

340 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/19/14ND B4F1825

340 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/19/14ND B4F1825

69 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/19/14ND B4F1825

69 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/19/14ND B4F1825

69 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/19/14ND B4F1825

69 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/19/14ND B4F1825

340 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/19/14ND B4F1825

340 ug/kg dry 50 82602-Hexanone591-78-6 06/19/14ND B4F1825

340 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/19/14ND B4F1825

1400 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/19/14ND B4F1825

340 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/19/14ND B4F1825

340 ug/kg dry 50 8260Acrylonitrile107-13-1 06/19/14ND B4F1825

69 ug/kg dry 50 8260Benzene71-43-2 06/19/14ND B4F1825

69 ug/kg dry 50 8260Bromobenzene108-86-1 06/19/14ND B4F1825

69 ug/kg dry 50 8260Bromochloromethane74-97-5 06/19/14ND B4F1825

69 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/19/14ND B4F1825

69 ug/kg dry 50 8260Bromoform75-25-2 06/19/14ND B4F1825

340 ug/kg dry 50 8260Bromomethane74-83-9 06/19/14ND B4F1825

69 ug/kg dry 50 8260Carbon disulfide75-15-0 06/19/14ND B4F1825

69 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/19/14ND B4F1825

69 ug/kg dry 50 8260Chlorobenzene108-90-7 06/19/14ND B4F1825

340 ug/kg dry 50 8260Chloroethane75-00-3 06/19/14ND B4F1825

69 ug/kg dry 50 8260Chloroform67-66-3 06/19/14ND B4F1825

340 ug/kg dry 50 8260Chloromethane74-87-3 06/19/14ND B4F1825

69 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/19/14ND B4F1825

69 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/19/14ND B4F1825

340 ug/kg dry 50 8260Cyclohexane110-82-7 06/19/14ND B4F1825

69 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/19/14ND B4F1825

Lab Work Order # 1406176

Page 23 of 42Page 23 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-11

RLCAS #

Client ID: CHLL-SB39 1'-4'

QC Batch

Organics-Volatiles

69 ug/kg dry 50 8260Dibromomethane74-95-3 06/19/14ND B4F1825

340 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/19/14ND B4F1825

340 ug/kg dry 50 8260Diethyl ether60-29-7 06/19/14ND B4F1825

340 ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/19/14ND B4F1825

69 ug/kg dry 50 8260Ethylbenzene100-41-4 06/19/14ND B4F1825

340 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/19/14ND B4F1825

340 ug/kg dry 50 8260Hexachloroethane67-72-1 06/19/14ND B4F1825

69 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/19/14ND B4F1825

140 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/19/14ND B4F1825

480 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/19/14ND B4F1825

340 ug/kg dry 50 8260Methylene chloride75-09-2 06/19/14ND B4F1825

69 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/19/14ND B4F1825

340 Xug/kg dry 50 8260Naphthalene91-20-3 06/19/14ND B4F1825

69 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/19/14ND B4F1825

69 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/19/14ND B4F1825

69 ug/kg dry 50 8260o-Xylene95-47-6 06/19/14ND B4F1825

69 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/19/14ND B4F1825

69 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/19/14ND B4F1825

69 ug/kg dry 50 8260Styrene100-42-5 06/19/14ND B4F1825

69 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/19/14ND B4F1825

3400 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/19/14ND B4F1825

340 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/19/14ND B4F1825

69 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/19/14ND B4F1825

340 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/19/14ND B4F1825

69 ug/kg dry 50 8260Toluene108-88-3 06/19/14ND B4F1825

69 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/19/14ND B4F1825

69 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/19/14ND B4F1825

340 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/19/14ND B4F1825

69 ug/kg dry 50 8260Trichloroethylene79-01-6 06/19/14ND B4F1825

69 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/19/14ND B4F1825

69 ug/kg dry 50 8260Vinyl chloride75-01-4 06/19/14ND B4F1825

50-150128 %Surrogate: Bromofluorobenzene 826006/19/14 B4F1825

50-150121 %Surrogate: Dibromofluoromethane 826006/19/14 B4F1825

50-150123 %Surrogate: Toluene-d8 826006/19/14 B4F1825

Lab Work Order # 1406176

Page 24 of 42Page 24 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-11

RLCAS #

Client ID: CHLL-SB39 1'-4'

QC Batch

Organics-Semivolatiles See note Y20

590 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

240 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

240 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

240 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

240 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

240 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

470 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

240 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

240 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

470 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

240 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

240 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

240 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11573.0 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11592.0 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-115102 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

120 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-150103 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15086.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Lab Work Order # 1406176

Page 25 of 42Page 25 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-11

RLCAS #

Client ID: CHLL-SB39 1'-4'

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1484.4 B4F1610

Lab Work Order # 1406176

Page 26 of 42Page 26 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-12

RLCAS #

Client ID: CHLL-SB39 1'-4' DUP

QC Batch

Organics-Volatiles

78 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/19/14ND B4F1825

78 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/19/14ND B4F1825

78 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/19/14ND B4F1825

78 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/19/14ND B4F1825

78 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/19/14ND B4F1825

78 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/19/14ND B4F1825

390 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/19/14ND B4F1825

390 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/19/14ND B4F1825

390 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/19/14ND B4F1825

78 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/19/14ND B4F1825

78 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/19/14ND B4F1825

78 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/19/14ND B4F1825

78 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/19/14ND B4F1825

390 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/19/14ND B4F1825

390 ug/kg dry 50 82602-Hexanone591-78-6 06/19/14ND B4F1825

390 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/19/14ND B4F1825

1600 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/19/14ND B4F1825

390 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/19/14ND B4F1825

390 ug/kg dry 50 8260Acrylonitrile107-13-1 06/19/14ND B4F1825

78 ug/kg dry 50 8260Benzene71-43-2 06/19/14ND B4F1825

78 ug/kg dry 50 8260Bromobenzene108-86-1 06/19/14ND B4F1825

78 ug/kg dry 50 8260Bromochloromethane74-97-5 06/19/14ND B4F1825

78 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/19/14ND B4F1825

78 ug/kg dry 50 8260Bromoform75-25-2 06/19/14ND B4F1825

390 ug/kg dry 50 8260Bromomethane74-83-9 06/19/14ND B4F1825

78 ug/kg dry 50 8260Carbon disulfide75-15-0 06/19/14ND B4F1825

78 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/19/14ND B4F1825

78 ug/kg dry 50 8260Chlorobenzene108-90-7 06/19/14ND B4F1825

390 ug/kg dry 50 8260Chloroethane75-00-3 06/19/14ND B4F1825

78 ug/kg dry 50 8260Chloroform67-66-3 06/19/14ND B4F1825

390 ug/kg dry 50 8260Chloromethane74-87-3 06/19/14ND B4F1825

78 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/19/14ND B4F1825

78 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/19/14ND B4F1825

390 ug/kg dry 50 8260Cyclohexane110-82-7 06/19/14ND B4F1825

78 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/19/14ND B4F1825

Lab Work Order # 1406176

Page 27 of 42Page 27 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-12

RLCAS #

Client ID: CHLL-SB39 1'-4' DUP

QC Batch

Organics-Volatiles

78 ug/kg dry 50 8260Dibromomethane74-95-3 06/19/14ND B4F1825

390 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/19/14ND B4F1825

390 ug/kg dry 50 8260Diethyl ether60-29-7 06/19/14ND B4F1825

390 ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/19/14ND B4F1825

78 ug/kg dry 50 8260Ethylbenzene100-41-4 06/19/14ND B4F1825

390 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/19/14ND B4F1825

390 ug/kg dry 50 8260Hexachloroethane67-72-1 06/19/14ND B4F1825

78 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/19/14ND B4F1825

160 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/19/14ND B4F1825

470 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/19/14ND B4F1825

390 ug/kg dry 50 8260Methylene chloride75-09-2 06/19/14ND B4F1825

78 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/19/14ND B4F1825

390 Xug/kg dry 50 8260Naphthalene91-20-3 06/19/14ND B4F1825

78 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/19/14ND B4F1825

78 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/19/14ND B4F1825

78 ug/kg dry 50 8260o-Xylene95-47-6 06/19/14ND B4F1825

78 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/19/14ND B4F1825

78 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/19/14ND B4F1825

78 ug/kg dry 50 8260Styrene100-42-5 06/19/14ND B4F1825

78 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/19/14ND B4F1825

3900 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/19/14ND B4F1825

390 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/19/14ND B4F1825

78 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/19/14ND B4F1825

390 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/19/14ND B4F1825

78 ug/kg dry 50 8260Toluene108-88-3 06/19/14ND B4F1825

78 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/19/14ND B4F1825

78 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/19/14ND B4F1825

390 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/19/14ND B4F1825

78 ug/kg dry 50 8260Trichloroethylene79-01-6 06/19/14ND B4F1825

78 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/19/14ND B4F1825

78 ug/kg dry 50 8260Vinyl chloride75-01-4 06/19/14ND B4F1825

50-15087.6 %Surrogate: Bromofluorobenzene 826006/19/14 B4F1825

50-15089.0 %Surrogate: Dibromofluoromethane 826006/19/14 B4F1825

50-15088.2 %Surrogate: Toluene-d8 826006/19/14 B4F1825

Lab Work Order # 1406176

Page 28 of 42Page 28 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-12

RLCAS #

Client ID: CHLL-SB39 1'-4' DUP

QC Batch

Organics-Semivolatiles See note Y20

590 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

240 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

240 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

240 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

240 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

470 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

240 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

470 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

240 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

240 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

470 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

240 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

240 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

240 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11568.3 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11585.3 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11590.0 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

120 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

120 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-150111 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15093.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Lab Work Order # 1406176

Page 29 of 42Page 29 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-12

RLCAS #

Client ID: CHLL-SB39 1'-4' DUP

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1484.6 B4F1610

Lab Work Order # 1406176

Page 30 of 42Page 30 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-13

RLCAS #

Client ID: CHLL-SB54 6''-18''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/23/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/23/14ND B4F1720

30-150103 %Surrogate: Decachlorobiphenyl 8081/808206/23/14 B4F1720

30-15096.4 %Surrogate: Tetrachloro-m-xylene 8081/808206/23/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1487.3 B4F1610

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/143300 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/144.4 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1433 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/140.2 B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/146.8 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/143.0 B4F1903

1.0 mg/kg dry 10 6020/200.8Copper7440-50-8 07/01/14440 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/148200 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1427 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14120 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/14ND B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/146.9 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.3 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.2 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1434 B4F1903

Lab Work Order # 1406176

Page 31 of 42Page 31 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-14

RLCAS #

Client ID: CHLL-SB40 6''-12''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-15098.2 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15092.8 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1489.2 B4F1610

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/145300 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/145.0 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1432 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.4 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1410 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/144.2 B4F1903

100 mg/kg dry 1000 6020/200.8Copper7440-50-8 07/01/14530 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1411000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1426 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14180 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 06/27/14ND B4F2520

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/149.2 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.3 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/140.4 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1436 B4F1903

Lab Work Order # 1406176

Page 32 of 42Page 32 of 43

Page 108: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-15

RLCAS #

Client ID: CHLL-SB40 1'-4'

QC Batch

Organics-Volatiles

55 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/19/14ND B4F1825

55 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/19/14ND B4F1825

55 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/19/14ND B4F1825

55 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/19/14ND B4F1825

55 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/19/14ND B4F1825

55 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/19/14ND B4F1825

280 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/19/14ND B4F1825

280 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/19/14ND B4F1825

280 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/19/14ND B4F1825

55 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/19/14ND B4F1825

55 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/19/14ND B4F1825

55 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/19/14ND B4F1825

55 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/19/14ND B4F1825

280 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/19/14ND B4F1825

280 ug/kg dry 50 82602-Hexanone591-78-6 06/19/14ND B4F1825

280 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/19/14ND B4F1825

1100 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/19/14ND B4F1825

280 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/19/14ND B4F1825

280 ug/kg dry 50 8260Acrylonitrile107-13-1 06/19/14ND B4F1825

55 ug/kg dry 50 8260Benzene71-43-2 06/19/14ND B4F1825

55 ug/kg dry 50 8260Bromobenzene108-86-1 06/19/14ND B4F1825

55 ug/kg dry 50 8260Bromochloromethane74-97-5 06/19/14ND B4F1825

55 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/19/14ND B4F1825

55 ug/kg dry 50 8260Bromoform75-25-2 06/19/14ND B4F1825

280 ug/kg dry 50 8260Bromomethane74-83-9 06/19/14ND B4F1825

55 ug/kg dry 50 8260Carbon disulfide75-15-0 06/19/14ND B4F1825

55 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/19/14ND B4F1825

55 ug/kg dry 50 8260Chlorobenzene108-90-7 06/19/14ND B4F1825

280 ug/kg dry 50 8260Chloroethane75-00-3 06/19/14ND B4F1825

55 ug/kg dry 50 8260Chloroform67-66-3 06/19/14ND B4F1825

280 ug/kg dry 50 8260Chloromethane74-87-3 06/19/14ND B4F1825

55 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/19/14ND B4F1825

55 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/19/14ND B4F1825

280 ug/kg dry 50 8260Cyclohexane110-82-7 06/19/14ND B4F1825

55 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/19/14ND B4F1825

Lab Work Order # 1406176

Page 33 of 42Page 33 of 43

Page 109: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-15

RLCAS #

Client ID: CHLL-SB40 1'-4'

QC Batch

Organics-Volatiles

55 ug/kg dry 50 8260Dibromomethane74-95-3 06/19/14ND B4F1825

280 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/19/14ND B4F1825

280 ug/kg dry 50 8260Diethyl ether60-29-7 06/19/14ND B4F1825

280 ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/19/14ND B4F1825

55 ug/kg dry 50 8260Ethylbenzene100-41-4 06/19/14ND B4F1825

280 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/19/14ND B4F1825

280 ug/kg dry 50 8260Hexachloroethane67-72-1 06/19/14ND B4F1825

55 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/19/14ND B4F1825

110 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/19/14ND B4F1825

390 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/19/14ND B4F1825

280 ug/kg dry 50 8260Methylene chloride75-09-2 06/19/14ND B4F1825

55 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/19/14ND B4F1825

280 Xug/kg dry 50 8260Naphthalene91-20-3 06/19/14ND B4F1825

55 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/19/14ND B4F1825

55 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/19/14ND B4F1825

55 ug/kg dry 50 8260o-Xylene95-47-6 06/19/14ND B4F1825

55 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/19/14ND B4F1825

55 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/19/14ND B4F1825

55 ug/kg dry 50 8260Styrene100-42-5 06/19/14ND B4F1825

55 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/19/14ND B4F1825

2800 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/19/14ND B4F1825

280 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/19/14ND B4F1825

55 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/19/14ND B4F1825

280 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/19/14ND B4F1825

55 ug/kg dry 50 8260Toluene108-88-3 06/19/1470 B4F1825

55 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/19/14ND B4F1825

55 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/19/14ND B4F1825

280 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/19/14ND B4F1825

55 ug/kg dry 50 8260Trichloroethylene79-01-6 06/19/14ND B4F1825

55 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/19/14ND B4F1825

55 ug/kg dry 50 8260Vinyl chloride75-01-4 06/19/14ND B4F1825

50-150140 %Surrogate: Bromofluorobenzene 826006/19/14 B4F1825

50-150134 %Surrogate: Dibromofluoromethane 826006/19/14 B4F1825

50-150138 %Surrogate: Toluene-d8 826006/19/14 B4F1825

Lab Work Order # 1406176

Page 34 of 42Page 34 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-15

RLCAS #

Client ID: CHLL-SB40 1'-4'

QC Batch

Organics-Semivolatiles See note Y20

540 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

220 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

220 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

220 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

220 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

430 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

430 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

430 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

430 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

220 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

430 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

220 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

220 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

430 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

220 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

220 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

220 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11565.5 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11582.6 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11592.4 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-15099.1 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15081.9 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Lab Work Order # 1406176

Page 35 of 42Page 35 of 43

Page 111: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-15

RLCAS #

Client ID: CHLL-SB40 1'-4'

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1492.8 B4F1610

Lab Work Order # 1406176

Page 36 of 42Page 36 of 43

Page 112: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-16

RLCAS #

Client ID: CHLL-SB41 6''-12''

QC Batch

Organics-PCBs as Aroclors

110 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

110 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-15090.2 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15088.6 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1490.0 B4F1610

Inorganics-Metals

100 mg/kg dry 1000 6020/200.8Aluminium7429-90-5 07/02/149900 B4F1903

0.3 mg/kg dry 10 6020/200.8Antimony7440-36-0 07/01/14ND B4F1913

0.5 mg/kg dry 10 6020/200.8Arsenic7440-38-2 07/01/144.5 B4F1903

1.0 mg/kg dry 10 6020/200.8Barium7440-39-3 07/01/1421 B4F1903

0.2 mg/kg dry 10 6020/200.8Beryllium7440-41-7 07/01/140.3 B4F1903

0.2 mg/kg dry 10 6020/200.8Cadmium7440-43-9 07/01/14ND B4F1903

2.0 mg/kg dry 10 6020/200.8Chromium7440-47-3 07/01/1421 B4F1903

0.5 mg/kg dry 10 6020/200.8Cobalt7440-48-4 07/01/149.4 B4F1903

100 mg/kg dry 1000 6020/200.8Copper7440-50-8 07/01/14630 B4F1903

5.0 A09mg/kg dry 10 6010/200.7Iron7439-89-6 06/27/1414000 B4F1903

1.0 mg/kg dry 10 6020/200.8Lead7439-92-1 07/01/1415 B4F1903

1.0 mg/kg dry 10 6020/200.8Manganese7439-96-5 07/01/14260 B4F1903

0.06 mg/kg dry 1 7471/245.5Mercury7439-97-6 07/02/14ND B4F3014

1.0 mg/kg dry 10 6020/200.8Nickel7440-02-0 07/01/1421 B4F1903

0.2 mg/kg dry 10 6020/200.8Selenium7782-49-2 07/01/140.3 B4F1903

0.1 mg/kg dry 10 6020/200.8Silver7440-22-4 07/01/141.0 B4F1903

1.0 mg/kg dry 10 6020/200.8Zinc7440-66-6 07/01/1443 B4F1903

Lab Work Order # 1406176

Page 37 of 42Page 37 of 43

Page 113: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-17

RLCAS #

Client ID: CHLL-SB41 1'-4'

QC Batch

Organics-Volatiles

80 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 06/19/14ND B4F1825

80 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 06/19/14ND B4F1825

80 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 06/19/14ND B4F1825

80 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 06/19/14ND B4F1825

80 ug/kg dry 50 82601,1-Dichloroethane75-34-3 06/19/14ND B4F1825

80 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 06/19/14ND B4F1825

400 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 06/19/14ND B4F1825

400 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 06/19/14ND B4F1825

400 ug/kg dry 50 82601,2-Dibromo-3-chloropropane96-12-8 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2-Dibromoethane106-93-4 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2-Dichloroethane107-06-2 06/19/14ND B4F1825

80 ug/kg dry 50 82601,2-Dichloropropane78-87-5 06/19/14ND B4F1825

80 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 06/19/14ND B4F1825

80 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 06/19/14ND B4F1825

80 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 06/19/14ND B4F1825

400 ug/kg dry 50 82602-Butanone (MEK)78-93-3 06/19/14ND B4F1825

400 ug/kg dry 50 82602-Hexanone591-78-6 06/19/14ND B4F1825

400 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 06/19/14ND B4F1825

1600 ug/kg dry 50 82602-Propanone (acetone)67-64-1 06/19/14ND B4F1825

400 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 06/19/14ND B4F1825

400 ug/kg dry 50 8260Acrylonitrile107-13-1 06/19/14ND B4F1825

80 ug/kg dry 50 8260Benzene71-43-2 06/19/14ND B4F1825

80 ug/kg dry 50 8260Bromobenzene108-86-1 06/19/14ND B4F1825

80 ug/kg dry 50 8260Bromochloromethane74-97-5 06/19/14ND B4F1825

80 ug/kg dry 50 8260Bromodichloromethane75-27-4 06/19/14ND B4F1825

80 ug/kg dry 50 8260Bromoform75-25-2 06/19/14ND B4F1825

400 ug/kg dry 50 8260Bromomethane74-83-9 06/19/14ND B4F1825

80 ug/kg dry 50 8260Carbon disulfide75-15-0 06/19/14ND B4F1825

80 ug/kg dry 50 8260Carbon tetrachloride56-23-5 06/19/14ND B4F1825

80 ug/kg dry 50 8260Chlorobenzene108-90-7 06/19/14ND B4F1825

400 ug/kg dry 50 8260Chloroethane75-00-3 06/19/14ND B4F1825

80 ug/kg dry 50 8260Chloroform67-66-3 06/19/14ND B4F1825

400 ug/kg dry 50 8260Chloromethane74-87-3 06/19/14ND B4F1825

80 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 06/19/14ND B4F1825

80 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 06/19/14ND B4F1825

400 ug/kg dry 50 8260Cyclohexane110-82-7 06/19/14ND B4F1825

80 ug/kg dry 50 8260Dibromochloromethane124-48-1 06/19/14ND B4F1825

Lab Work Order # 1406176

Page 38 of 42Page 38 of 43

Page 114: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-17

RLCAS #

Client ID: CHLL-SB41 1'-4'

QC Batch

Organics-Volatiles

80 ug/kg dry 50 8260Dibromomethane74-95-3 06/19/14ND B4F1825

400 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 06/19/14ND B4F1825

400 ug/kg dry 50 8260Diethyl ether60-29-7 06/19/14ND B4F1825

400 ug/kg dry 50 8260Diisopropyl Ether108-20-3 06/19/14ND B4F1825

80 ug/kg dry 50 8260Ethylbenzene100-41-4 06/19/14ND B4F1825

400 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 06/19/14ND B4F1825

400 ug/kg dry 50 8260Hexachloroethane67-72-1 06/19/14ND B4F1825

80 ug/kg dry 50 8260Isopropylbenzene98-82-8 06/19/14ND B4F1825

160 ug/kg dry 50 8260m & p - Xylene1330-20-7 06/19/14ND B4F1825

560 A05, A10,

Y37

ug/kg dry 50 8260Methyl iodide74-88-4 06/19/14ND B4F1825

400 ug/kg dry 50 8260Methylene chloride75-09-2 06/19/14ND B4F1825

80 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 06/19/14ND B4F1825

400 Xug/kg dry 50 8260Naphthalene91-20-3 06/19/14ND B4F1825

80 ug/kg dry 50 8260n-Butylbenzene104-51-8 06/19/14ND B4F1825

80 ug/kg dry 50 8260n-Propylbenzene103-65-1 06/19/14ND B4F1825

80 ug/kg dry 50 8260o-Xylene95-47-6 06/19/14ND B4F1825

80 ug/kg dry 50 8260p-Isopropyl toluene99-87-6 06/19/14ND B4F1825

80 ug/kg dry 50 8260sec-Butylbenzene135-98-8 06/19/14ND B4F1825

80 ug/kg dry 50 8260Styrene100-42-5 06/19/14ND B4F1825

80 ug/kg dry 50 8260tert-Butylbenzene98-06-6 06/19/14ND B4F1825

4000 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 06/19/14ND B4F1825

400 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 06/19/14ND B4F1825

80 ug/kg dry 50 8260Tetrachloroethylene127-18-4 06/19/14ND B4F1825

400 ug/kg dry 50 8260Tetrahydrofuran109-99-9 06/19/14ND B4F1825

80 ug/kg dry 50 8260Toluene108-88-3 06/19/14ND B4F1825

80 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 06/19/14ND B4F1825

80 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 06/19/14ND B4F1825

400 ug/kg dry 50 8260trans-1,4-Dichloro-2-butene110-57-6 06/19/14ND B4F1825

80 ug/kg dry 50 8260Trichloroethylene79-01-6 06/19/14ND B4F1825

80 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 06/19/14ND B4F1825

80 ug/kg dry 50 8260Vinyl chloride75-01-4 06/19/14ND B4F1825

50-150162 %Surrogate: Bromofluorobenzene 826006/19/14 B4F1825

50-150152 %Surrogate: Dibromofluoromethane 826006/19/14 B4F1825

50-150159 %Surrogate: Toluene-d8 826006/19/14 B4F1825

Lab Work Order # 1406176

Page 39 of 42Page 39 of 43

Page 115: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-17

RLCAS #

Client ID: CHLL-SB41 1'-4'

QC Batch

Organics-Semivolatiles See note Y20

630 ug/kg dry 1 82702-Methylnaphthalene91-57-6 06/25/14ND B4F1621

250 ug/kg dry 1 8270Acenaphthene83-32-9 06/25/14ND B4F1621

250 ug/kg dry 1 8270Acenaphthylene208-96-8 06/25/14ND B4F1621

250 ug/kg dry 1 8270Anthracene120-12-7 06/25/14ND B4F1621

250 ug/kg dry 1 8270Benz[a]anthracene56-55-3 06/25/14ND B4F1621

510 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 06/25/14ND B4F1621

510 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 06/25/14ND B4F1621

510 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 06/25/14ND B4F1621

510 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 06/25/14ND B4F1621

250 ug/kg dry 1 8270Chrysene218-01-9 06/25/14ND B4F1621

510 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 06/25/14ND B4F1621

250 ug/kg dry 1 8270Fluoranthene206-44-0 06/25/14ND B4F1621

250 ug/kg dry 1 8270Fluorene86-73-7 06/25/14ND B4F1621

510 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 06/25/14ND B4F1621

250 ug/kg dry 1 8270Naphthalene91-20-3 06/25/14ND B4F1621

250 ug/kg dry 1 8270Phenanthrene85-01-8 06/25/14ND B4F1621

250 ug/kg dry 1 8270Pyrene129-00-0 06/25/14ND B4F1621

32.9-11570.4 %Surrogate: 2-Fluorobiphenyl 827006/25/14 B4F1621

31.8-11582.6 %Surrogate: Nitrobenzene-d5 827006/25/14 B4F1621

38.5-11595.6 %Surrogate: p-Terphenyl-d14 827006/25/14 B4F1621

Organics-PCBs as Aroclors

130 ug/kg dry 1 8081/8082Aroclor 101612674-11-2 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 122111104-28-2 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 123211141-16-5 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124253469-21-9 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 124812672-29-6 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 125411097-69-1 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126011096-82-5 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126237324-23-5 06/24/14ND B4F1720

130 ug/kg dry 1 8081/8082Aroclor 126811100-14-4 06/24/14ND B4F1720

30-15093.5 %Surrogate: Decachlorobiphenyl 8081/808206/24/14 B4F1720

30-15085.3 %Surrogate: Tetrachloro-m-xylene 8081/808206/24/14 B4F1720

Lab Work Order # 1406176

Page 40 of 42Page 40 of 43

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1406176-17

RLCAS #

Client ID: CHLL-SB41 1'-4'

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 06/16/1479.0 B4F1611

Lab Work Order # 1406176

Page 41 of 42Page 41 of 43

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Page 42 of 43

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Page 3 of 39

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()**+,-./0&1/2-234+*+5673/894 "#$%&' 3 !" #: ;:!< K+e.S*S % %!:% %;

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Page 4 of 39

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/S/.+=./=D ?$#5F#$!*.-. @: *+, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *+, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

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Page 5 of 39

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()**+,-./0&1/2-234+*+5673/894 =!$ &' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ ==$<&' 3 !" #: 3:!< K+e.S*S % %!:% %;

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S++,=+/=R C'$(1:( >O@ ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( AS .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# <> ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <?>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 <?>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

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S+/R=R-=D 0'6H'6 8 @P> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,D J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) <S *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >O= ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 ?? *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 6 of 39

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0 1(!S!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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G"H'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/+=/ *Q*=:H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/D=+ *Q*=:H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

3S=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*3=+ *Q.Q/=L$H5^F#$#V$#V 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D.-=S/=3 *Q.Q/=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.,=3.=* *Q.Q+=L$H5^F#$# (9`(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*.=3 *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=R/=+ *Q.=:H $#J#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=D,=* *Q.=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=,-=. *Q.=:H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=3S=D *Q.=:H5^F#$#V$#V 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=-S=3 *Q/QD=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D+*=S/=* *Q/=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=+-=S *Q+=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=R/=/ .=KI6 9#9(!X8;OY @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

DR*=S3=- .=N(Z 9#9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=DS=- .=8(6^]F9 V^6^ F(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

-S=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *+,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=*/=* ?5$]F#9H6$HF( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=+/=. K(9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=3-=* K$#J# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=RS=D K$#J#5^F#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.S=+ K$#J#'H5^F#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.D=. K$#J#2#$J @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3/=R K$#J#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=*D=, M $ #9!'HPIF2H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=R,=S M^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,,=/ M^F#$#(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-S=--=/ M^F#$#2#$J @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3S=/ M^F#$#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*D-=DR=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

**,=3.=S M]5F#^(Z 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.+=+3=* :H $#J#5^F#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

L !"#$%!&$'($!)!*+,-./*

Page 7 of 39

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0 1(!3!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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S+=RD=/ :H $#J#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=S*=3 :H5^F#$#'H2FI#$#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-,=.R=S :H(6^]F!(6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=.,=/ :HHP#V$#V]F!;6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,=+*=+ ;6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-/S=R.=/ ;6^]F6($6H $] I6]F(6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-S=S.=* N(Z 5^F#$#(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R3=3.=3 BP#V$#V]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*//,=.,=S J!_!V!=![]F(9( @: *+, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=33=+ 8(6^]F!H#'H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,R=. 8(6^]F(9(!5^F#$H'( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*-/+=,+=+ 8(6^]F6($6H $] I6]F(6^($ @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=.,=/ @ V^6^ F(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

*,+=D*=3 9=KI6]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,/=-D=* 9=0$#V]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=+S=- #=[]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RR=3S=- V=BP#V$#V]F!6#FI(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*/D=R3=3 P(5=KI6]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,=+.=D A6]$(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R3=,-=- 6($6=KI6]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=-D=, 6($6H $]!KI6]F!?F5#^#F @: /-,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RR+=,D=3 6($6H $]?J]FJ(6^]F(6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.S=*3=+ L(6$ 5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,R=RR=R L(6$ ^]'$#2I$ 9 @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=33=/ L#FI(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*D-=-,=D 6$ 9P=*Q.=:H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,-*=,.=- 6$ 9P=*Q/=:H5^F#$#V$#V]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

**,=DS=- 6$ 9P=*Q+=:H5^F#$#=.= I6(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=,*=- L$H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=-R=+ L$H5^F#$#2FI#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,*=+ gH9]F!5^F#$H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

()**+,-./0&B*+@+C4)+*+5/8D/8/ ##$>&' " !" =:; :!< K+e.,,D %;=

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()**+,-./0&?+4)/8/ E% #%$ &' " !" =:; :!< K+e.,,D %;=

L !"#$%!&$'($!)!*+,-./*

Page 8 of 39

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0 1(!R!#2!/3

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Page 9 of 39

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S++,=,.=, ;13Q ) <A *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OA ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 T< *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 10 of 39

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0 1(!**!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*==*@FFB<@FF*$:

-'.*+,%*<=>?@A<B>T

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/+=/ *Q*=:H5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/D=+ *Q*=:H5^F#$#(6^]F(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

3S=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*3=+ *Q.Q/=L$H5^F#$#V$#V 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D.-=S/=3 *Q.Q/=L$HJ(6^]F (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.,=3.=* *Q.Q+=L$H5^F#$# (9`(9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*.=3 *Q.=:H $#J#=/=5^F#$#V$#V 9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=R/=+ *Q.=:H $#J#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=D,=* *Q.=:H5^F#$# (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=,-=. *Q.=:H5^F#$#(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=3S=D *Q.=:H5^F#$#V$#V 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=-S=3 *Q/QD=L$HJ(6^]F (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D+*=S/=* *Q/=:H5^F#$# (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=+-=S *Q+=:H5^F#$# (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=R/=/ .=KI6 9#9(!X8;OY @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

DR*=S3=- .=N(Z 9#9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=DS=- .=8(6^]F9 V^6^ F(9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

-S=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *-,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=*/=* ?5$]F#9H6$HF( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=+/=. K(9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=3-=* K$#J# (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=RS=D K$#J#5^F#$#J(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.S=+ K$#J#'H5^F#$#J(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.D=. K$#J#2#$J @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3/=R K$#J#J(6^ 9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=*D=, M $ #9!'HPIF2H'( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=R,=S M^F#$# (9`(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,,=/ M^F#$#(6^ 9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-S=--=/ M^F#$#2#$J @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3S=/ M^F#$#J(6^ 9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*D-=DR=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

**,=3.=S M]5F#^(Z 9( @: +*, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.+=+3=* :H $#J#5^F#$#J(6^ 9( @: 3. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

L !"#$%!&$'($!)!*+,-./*

Page 11 of 39

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0 1(!*.!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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:H $#J#J(6^ 9(S+=RD=/

:H5^F#$#'H2FI#$#J(6^ 9(SD=S*=3

:H(6^]F!(6^($-,=.R=S

:HHP#V$#V]F!;6^($*,3=.,=/

;6^]F (9`(9(*,,=+*=+

;6^]F6($6H $] I6]F(6^($-/S=R.=/

N(Z 5^F#$#(6^ 9(-S=S.=*

BP#V$#V]F (9`(9(R3=3.=3

J!_!V!=![]F(9(*//,=.,=S

8(6^]F!H#'H'(S+=33=+

8(6^]F(9(!5^F#$H'(SD=,R=.

8(6^]F6($6H $] I6]F(6^($*-/+=,+=+

@ V^6^ F(9(R*=.,=/

9=KI6]F (9`(9(*,+=D*=3

9=0$#V]F (9`(9(*,/=-D=*

#=[]F(9(RD=+S=-

V=BP#V$#V]F!6#FI(9(RR=3S=-

P(5=KI6]F (9`(9(*/D=R3=3

A6]$(9(*,,=+.=D

6($6=KI6]F (9`(9(R3=,-=-

6($6H $]!KI6]F!?F5#^#FSD=-D=,

6($6H $]?J]FJ(6^]F(6^($RR+=,D=3

L(6$ 5^F#$#(6^]F(9(*.S=*3=+

L(6$ ^]'$#2I$ 9*,R=RR=R

L#FI(9(*,3=33=/

6$ 9P=*Q.=:H5^F#$#(6^]F(9(*D-=-,=D

6$ 9P=*Q/=:H5^F#$#V$#V]F(9(*,,-*=,.=-

6$ 9P=*Q+=:H5^F#$#=.= I6(9(**,=DS=-

L$H5^F#$#(6^]F(9(SR=,*=-

L$H5^F#$#2FI#$#J(6^ 9(SD=-R=+

gH9]F!5^F#$H'(SD=,*=+

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,-T.,T*+

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K+e.,,D

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L !"#$%!&$'($!)!*+,-./*

Page 12 of 39

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0 1(!*/!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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M?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

G"H'6138B& (14!)'#1) 8 & *6!# *V@>

R*=DS=- .=8(6^]F9 V^6^ F(9( @: -+, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

3/=/.=R ?5(9 V^6^(9( @: .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

.,3=R-=3 ?5(9 V^6^]F(9( @: .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

*.,=*.=S ?96^$ 5(9( @: .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

D-=DD=/ E 6WX'Y'6#K"'3 6 <P> .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S, L

D,=/.=3 K(9`#h iV]$(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

.,D=RR=. K(9`#h i2FI#$ 96^(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

*R*=.+=. K(9`#h1Q^QHiV($]F(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

.,S=,3=R K(9`#h%i2FI#$ 96^(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

.*3=,*=R CK"/8 6 @@> .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S, L

D/=S,=/ :H (9`h Q^i 96^$ 5(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

.,-=++=, Z):!"'6#K 6 AN> .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

3-=S/=S eFI#$(9( @: .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

*R/=/R=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: D*, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

R*=.,=/ @ V^6^ F(9( @: .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

3D=,*=3 IK 6'6#K" 6 <?> .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S, L

*.R=,,=, I/" 6 @P> .D, I1T%1!'$] * ,-T.3T*+ K+e*R.. 3.S,

()**+,-./0&; F4)+*+5673/894 <3$3&' 3;$> !!" =:;%:!< K+e*R.. %;#

()**+,-./0&G6.*+5/8D/8/ E" " $>&' 3!$% !!" =:;%:!< K+e*R.. %;#

()**+,-./0&7 ?/*73/894 E!< <#$3&' 3%$" !!" =:;%:!< K+e*R.. %;#

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: */, I1T%1!'$] * ,ST,.T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 ""$%&' 3 !" #: ;:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ =3$;&' 3 !" #: ;:!< K+e.S*S % %!:% %;

L !"#$%!&$'($!)!*+,-./*

Page 13 of 39

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0 1(!*+!#2!/3

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+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 PNO? ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E*/ J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( SA>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 AO> ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( T? *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >O= ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R M 'JHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( @@ .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# NON ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " ?P> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 <A>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ T= *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 @>> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) <N *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( >O@ ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OP ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 ?? *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 14 of 39

Page 133: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*D!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=T*>FFBNFF

-'.*+,%*<=>?@A<B>?

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 ="$>&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ # $"&' 3 !" #: 3:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 NAOA ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D M!#')*C/'61$ >OP< ,E*. J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( <=>>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ >OA ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 TON ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( P> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >OT ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R C'$(1:( >O= ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( =A .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# <? ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <P>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 @=>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ <?> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 =<> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) @S *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( >O= ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OS ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 @A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 15 of 39

Page 134: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*-!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=?*?B<@FF

-'.*+,%*<=>?@A<B>P

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *-, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 "#$=&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ =>$=&' 3 !" #: 3:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 ?=O@ ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D M!#')*C/'61$ >O@< ,E*- J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( S@>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ AO= ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 A= ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( A?> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( <O@ ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R C'$(1:( <OP ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( @S .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# POA ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <?>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 T@>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ TA> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 <@>>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 0 "3:"/ >OA ,E,3 J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) <N *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( =O< .E, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OS ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 <A>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 16 of 39

Page 135: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*S!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=P*>B?FF

-'.*+,%*<=>?@A<B>N

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 =<$%&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ #%$<&' 3 !" #: 3:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 N>O= ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E*. J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( SP>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ >O= ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 TO@ ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( P@ *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >OP ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R C'$(1:( >ON ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( @T .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# <@ ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <A>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 <T>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ <A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 A>> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) @T *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( >OA ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >ON ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 <N> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 17 of 39

Page 136: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*3!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=P*?FFBA>FF

-'.*+,%*<=>?@A<B>S

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SR=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/+=/ *Q*=:H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=/D=+ *Q*=:H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

3S=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*3=+ *Q.Q/=L$H5^F#$#V$#V 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D.-=S/=3 *Q.Q/=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.,=3.=* *Q.Q+=L$H5^F#$# (9`(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R-=*.=3 *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=R/=+ *Q.=:H $#J#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RD=D,=* *Q.=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=,-=. *Q.=:H5^F#$#(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=3S=D *Q.=:H5^F#$#V$#V 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=-S=3 *Q/QD=L$HJ(6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D+*=S/=* *Q/=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=+-=S *Q+=:H5^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=R/=/ .=KI6 9#9(!X8;OY @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

DR*=S3=- .=N(Z 9#9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=DS=- .=8(6^]F9 V^6^ F(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

-S=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *+,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=*/=* ?5$]F#9H6$HF( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=+/=. K(9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=3-=* K$#J# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=RS=D K$#J#5^F#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.S=+ K$#J#'H5^F#$#J(6^ 9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.D=. K$#J#2#$J @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3/=R K$#J#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=*D=, M $ #9!'HPIF2H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=R,=S M^F#$# (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,,=/ M^F#$#(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-S=--=/ M^F#$#2#$J @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3S=/ M^F#$#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*D-=DR=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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SD=S*=3 :H5^F#$#'H2FI#$#J(6^ 9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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*,,=+*=+ ;6^]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-/S=R.=/ ;6^]F6($6H $] I6]F(6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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R3=3.=3 BP#V$#V]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*//,=.,=S J!_!V!=![]F(9( @: *+, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=33=+ 8(6^]F!H#'H'( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,R=. 8(6^]F(9(!5^F#$H'( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*-/+=,+=+ 8(6^]F6($6H $] I6]F(6^($ @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=.,=/ @ V^6^ F(9( @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

*,+=D*=3 9=KI6]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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RD=+S=- #=[]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RR=3S=- V=BP#V$#V]F!6#FI(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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*,,=+.=D A6]$(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R3=,-=- 6($6=KI6]F (9`(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=-D=, 6($6H $]!KI6]F!?F5#^#F @: /-,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

RR+=,D=3 6($6H $]?J]FJ(6^]F(6^($ @: /-, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.S=*3=+ L(6$ 5^F#$#(6^]F(9( @: S. I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

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Page 19 of 39

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Page 20 of 39

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Page 21 of 39

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Page 22 of 39

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*,3=-S=3 *Q/QD=L$HJ(6^]F (9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D+*=S/=* *Q/=:H5^F#$# (9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,-=+-=S *Q+=:H5^F#$# (9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S3=R/=/ .=KI6 9#9(!X8;OY @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

DR*=S3=- .=N(Z 9#9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

R*=DS=- .=8(6^]F9 V^6^ F(9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-, [

-S=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *+,, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,S=*/=* ?5$]F#9H6$HF( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S*=+/=. K(9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=3-=* K$#J# (9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=RS=D K$#J#5^F#$#J(6^ 9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.S=+ K$#J#'H5^F#$#J(6^ 9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=.D=. K$#J#2#$J @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3/=R K$#J#J(6^ 9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=*D=, M $ #9!'HPIF2H'( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,3=R,=S M^F#$# (9`(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

SD=,,=/ M^F#$#(6^ 9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

-S=--=/ M^F#$#2#$J @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

S+=3S=/ M^F#$#J(6^ 9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*D-=DR=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

**,=3.=S M]5F#^(Z 9( @: /D, I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

*.+=+3=* :H $#J#5^F#$#J(6^ 9( @: -R I1T%1!'$] D, ,-T.,T*+ K+e.,,D 3.-,

L !"#$%!&$'($!)!*+,-./*

Page 23 of 39

Page 142: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.+!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

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G"H'6138BU!)'#1) 8

:H $#J#J(6^ 9(S+=RD=/

:H5^F#$#'H2FI#$#J(6^ 9(SD=S*=3

:H(6^]F!(6^($-,=.R=S

:HHP#V$#V]F!;6^($*,3=.,=/

;6^]F (9`(9(*,,=+*=+

;6^]F6($6H $] I6]F(6^($-/S=R.=/

N(Z 5^F#$#(6^ 9(-S=S.=*

BP#V$#V]F (9`(9(R3=3.=3

J!_!V!=![]F(9(*//,=.,=S

8(6^]F!H#'H'(S+=33=+

8(6^]F(9(!5^F#$H'(SD=,R=.

8(6^]F6($6H $] I6]F(6^($*-/+=,+=+

@ V^6^ F(9(R*=.,=/

9=KI6]F (9`(9(*,+=D*=3

9=0$#V]F (9`(9(*,/=-D=*

#=[]F(9(RD=+S=-

V=BP#V$#V]F!6#FI(9(RR=3S=-

P(5=KI6]F (9`(9(*/D=R3=3

A6]$(9(*,,=+.=D

6($6=KI6]F (9`(9(R3=,-=-

6($6H $]!KI6]F!?F5#^#FSD=-D=,

6($6H $]?J]FJ(6^]F(6^($RR+=,D=3

L(6$ 5^F#$#(6^]F(9(*.S=*3=+

L(6$ ^]'$#2I$ 9*,R=RR=R

L#FI(9(*,3=33=/

6$ 9P=*Q.=:H5^F#$#(6^]F(9(*D-=-,=D

6$ 9P=*Q/=:H5^F#$#V$#V]F(9(*,,-*=,.=-

6$ 9P=*Q+=:H5^F#$#=.= I6(9(**,=DS=-

L$H5^F#$#(6^]F(9(SR=,*=-

L$H5^F#$#2FI#$#J(6^ 9(SD=-R=+

gH9]F!5^F#$H'(SD=,*=+

@:

@:

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D,

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,-T.,T*+

,-T.,T*+

,-T.,T*+

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,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

K+e.,,D

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3.-,

3.-,

3.-,

3.-,

3.-,

3.-,

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3.-,

3.-,

3.-,

3.-,

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()**+,-./0&B*+@+C4)+*+5/8D/8/

()**+,-./0&165*+@+C4)+*+@/.3-8/

()**+,-./0&?+4)/8/ E%

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L !"#$%!&$'($!)!*+,-./*

Page 24 of 39

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0 1(!.D!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=N*?B=NFF

-'.*+,%*<=>?@A<B<<

?9 F]6(M?A!) >(PIF6 >L :HFI6H#9d9H6P

?9 F]`('

: 6( <M!K 65^ 8(6^#' <I FH2H($

G"H'6138B& (14!)'#1) 8 & *6!# *V@>

.=8(6^]F9 V^6^ F(9(R*=DS=- @: -,, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

?5(9 V^6^(9(3/=/.=R @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

?5(9 V^6^]F(9(.,3=R-=3 @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

?96^$ 5(9(*.,=*.=S @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

K(9`h i 96^$ 5(9(D-=DD=/ @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

K(9`#h iV]$(9(D,=/.=3 @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

K(9`#h i2FI#$ 96^(9(.,D=RR=. @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

K(9`#h1Q^QHiV($]F(9(*R*=.+=. @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

K(9`#h%i2FI#$ 96^(9(.,S=,3=R @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

M^$]P(9(.*3=,*=R @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

:H (9`h Q^i 96^$ 5(9(D/=S,=/ @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

Z):!"'6#K 6 .,-=++=, @=> .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

eFI#$(9(3-=S/=S @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

B9'(9#X*Q.Q/=5Q'YV]$(9(*R/=/R=D @: +3, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

@ V^6^ F(9(R*=.,=/ @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

0^(9 96^$(9(3D=,*=3 @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

0]$(9(*.R=,,=, @: .+, I1T%1!'$] * ,-T/,T*+ K+e*R.. 3.S,

()**+,-./0&; F4)+*+5673/894 # $"&' 3;$> !!" =:3 :!< K+e*R.. %;#

()**+,-./0&G6.*+5/8D/8/ E" %!$ &' 3!$% !!" =:3 :!< K+e*R.. %;#

()**+,-./0&7 ?/*73/894 E!< #%$>&' 3%$" !!" =:3 :!< K+e*R.. %;#

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 ">$!&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ =%$"&' 3 !" #: 3:!< K+e.S*S % %!:% %;

L !"#$%!&$'($!)!*+,-./*

Page 25 of 39

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0 1(!.-!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*=N*?B=NFF

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?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 NAO> ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

L !"#$%!&$'($!)!*+,-./*

Page 26 of 39

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0 1(!.S!#2!/3

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G"H'6138BICE8*'8*5"!3)!"8 & *6!# *V@<

*.-S+=**=. ?$#5F#$!*,*- @: .., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: .., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: .., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: .., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: .., I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: ..,, I1T%1!'$] *, ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: ..,, I1T%1!'$] *, ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: ..,, I1T%1!'$] *, ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: ..,, I1T%1!'$] *, ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 !!!&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ %;$>&' 3 !" #: 3:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 NSOT ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( ?S>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 << ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >OA ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R M 'JHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( <A .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# ?O> ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " AS>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 <>>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ << *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 <P> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) <? *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OS ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 27 of 39

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0 1(!.3!#2!/3

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Page 28 of 39

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Page 29 of 39

Page 148: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 30 of 39

Page 149: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 31 of 39

Page 150: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 32 of 39

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S+/R=R.=* L( ' @: *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 NS> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,D J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) ?S *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( @O? .E, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " <O> ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 @=> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 33 of 39

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0 1(!/+!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*@P*>FFB?FF

-'.*+,%*<=>?@A<B<P

?9 F]`('

M?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

G"H'6138BICE8*'8*5"!3)!"8 & *6!# *V@<

*.-S+=**=. ?$#5F#$!*,*- @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 #;$"&' 3 !" #: #:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ %<$<&' 3 !" #: #:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 NTO? ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E*. J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( ==>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ >ON ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 ?O= ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( TS *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >O= ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R M 'JHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( <= .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# ?OP ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <>>> *, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 <>>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ P> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 <@> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 0 "3:"/ >O>? ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) <A *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: .E, J1T%1!'$] *,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " >OT ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 S@ *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 34 of 39

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0 1(!/D!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*@P*@=FFBA>FF

-'.*+,%*<=>?@A<B<N

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: **, I1T%1!'$] * ,ST,/T*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 =>$;&' 3 !" #: 3:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ #3$;&' 3 !" #: 3:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 NPO> ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( ?N> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. ?$P(9H5 @: ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( <P *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S K($]FFHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R M 'JHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ M^$#JHIJ @: .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ M# F6 @: ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 @P>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ @OA *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 @A *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 8($5I$] @: ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, @H5%(F @: *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ AHF\($ @: ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 NO< *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

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0 1(!/-!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*@?*>FFB?FF

-'.*+,%*<=>?@A<B<S

?9 F]`('

M?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

G"H'6138BICE8*'8*5"!3)!"8 & *6!# *V@<

*.-S+=**=. ?$#5F#$!*,*- @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *.,, I1T%1!'$] *, ,ST,ST*+ K+e.S*S 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 %!$3&' 3 !" #: #:!< K+e.S*S % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ %"$%&' 3 !" #: #:!< K+e.S*S % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 N?OP ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E*. J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( AA>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ >O? ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 <@ ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( TT *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >OT ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R C'$(1:( >O= ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( NON .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# AOP ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " @<>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 N>>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ =>> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 <>> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 0 "3:"/ >O>N ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) SO> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. & ) 61:( <O@ ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " <O@ ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 PA *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

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0 1(!/S!#2!/3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*@?*?FFBA>FF

-'.*+,%*<=>?@A<B@>

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L d9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

G"H'6138BICE8*'8*5"!3)!"8

*.-S+=**=. ?$#5F#$!*,*- @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

***,+=.3=. ?$#5F#$!*..* @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

***+*=*-=D ?$#5F#$!*./. @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

D/+-R=.*=R ?$#5F#$!*.+. @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

*.-S.=.R=- ?$#5F#$!*.+3 @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

**,RS=-R=* ?$#5F#$!*.D+ @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

**,R-=3.=D ?$#5F#$!*.-, @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

/S/.+=./=D ?$#5F#$!*.-. @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

***,,=*+=+ ?$#5F#$!*.-3 @: *., I1T%1!'$] * ,ST,+T*+ K+e/,.. 3,3*T3,3.

()**+,-./0&1/2-234+*+5673/894 ">$>&' 3 !" #: <:!< K+e/,.. % %!:% %;

()**+,-./0&?/.*-234+*+ @ A94/8/ =;$ &' 3 !" #: <:!< K+e/,.. % %!:% %;

+6!"H'6138BJ 6 "')*CK (18#"/

LA L*M!#')*&!)1$8 N?OS ,E* f * ,-T*RT*+ K+e*R*, .D+,!K

DS=*.=D L#6 F!M] 9H'( @: ,E*. J1T%1!'$] * ,-T.DT*+ K+e./*S ?AL8!:!SD**=,R

+6!"H'6138B0 #')8

S+.R=R,=D 5):(161:( AN>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S++,=/-=, 56#1(!6/ >OT ,E/ J1T%1!'$] *, ,ST,/T*+ K+e./,D -,.,T.,,E3

S++,=/3=. 5"8 613 @O< ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=/R=/ E'"1:( == *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+*=S E "/))1:( >OA ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+/=R M 'JHIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+S=/ CK"!(1:( NO> .E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=+3=+ C!.')# AOA ,ED J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=D,=3 C! " <<>> *,, J1T%1!'$] *,,, ,ST,/T*+ K+e./,* -,.,T.,,E3

S+/R=3R=- +"!6 PS>> DE, J1T%1!'$] *, ,-T.ST*+ K+e./,* -,*,T.,,ES

S+/R=R.=* - '$ A> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=R-=D 0'6H'6 8 <T> *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S+/R=RS=- 0 "3:"/ >O>P ,E,- J1T%1!'$] * ,ST,.T*+ K+e/,*D S+S*T.+DED

S++,=,.=, ;13Q ) POP *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

SS3.=+R=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=..=+ &1)4 " <O= ,E* J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

S++,=--=- R163 PS *E, J1T%1!'$] *, ,ST,.T*+ K+e./,* -,.,T.,,E3

L !"#$%!&$'($!)!*+,-./*

Page 37 of 39

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Page 38 of 39

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Page 39 of 39

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0 1(!*!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

'$- )+$M'$*#.%.#2+)#*+)1 )*+,-+./!01!234&4

56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

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0A6B<CCA<)>DE1DF

9'9!G !>KKL.*+!EMNLLM

)*+,-+./!01!234&4

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S*<CC<- *P*P*<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR</+<C *P*P.P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

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SC</C<+ *P*<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

QS<-*<- *P.P/<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*Q<+ *P.P/<K$G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

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,-T.,T*+

,-T.,T*+

J+d,+,C

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Q.S,

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>$#4E#$!*..****,+<.Q<.

>$#4E#$!*./.***+*<*-<C

>$#4E#$!*.+.C/+-R<.*<R

>$#4E#$!*.+Q*.-S.<.R<-

>$#4E#$!*.C+**,RS<-R<*

>$#4E#$!*.-,**,R-<Q.<C

>$#4E#$!*.-./S/.+<./<C

>$#4E#$!*.-Q***,,<*+<+

?9

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Page 6 of 47

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=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*A?*<@GB<HG

-'.*+,%*<=>?@A?B><

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+6!"J'6138B0 #')8

S+.R<R,<C 5):(161:( HA> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</-<, >85GI#8Y ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,</Q<. 5"8 613 <NA *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</R</ M'"1:( O> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+*<S J($YEEGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+S</ CP"!(1:( @N@ *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+Q<+ L# E5 ?9 CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<C,<Q C! " =N? *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<QR<- +"!6 @?>> ., H1TL * ,-T.-T*+ J+d*R,* -,*,T.,,DS

S+/R<R.<* - '$ =NO *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<R-<C 0'6J'6 8 AQ> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<RS<- 7($4H$Y ?9 ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) @> .D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<..<+ @GEX($ ?9 ,D. H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<--<- S163 T= CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-./-

Page 7 of 47

Page 165: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!Q!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*AT*OGB<A

-'.*+,%*<=>?@A?B>@

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I"J'6138BLCM8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 $7%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. "$7%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 8 of 47

Page 166: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!R!#2!+-

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)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

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>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

I"J'6138BK!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<CC<- *P*P*<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR</+<C *P*P.P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR<,,<C *P*P.<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</+</ *P*<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</C<+ *P*<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

QS<-*<- *P.P/<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*Q<+ *P.P/<K$G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C.-<S/<Q *P.P/<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*.,<Q.<* *P.P+<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<-/<- *P.P+<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*.<Q *P.<9G $#I#</<4ZE#$#V$#V 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<R/<+ *P.<9G $#I#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<C,<* *P.<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<,-<. *P.<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<QS<C *P.<9G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<-S<Q *P/PC<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C+*<S/<* *P/<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<+-<S *P+<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<R/</ .<JH5 8#8(!_7:N` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

CR*<SQ<- .<M(b 8#8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-, >,CP!W

-S<-+<* .<0$#V 8#8(!_ 4(5#8(` ?9 ., H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<*,<* +<7(5ZYE<.<V(85 8#8(!_7AJN` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<*/<* >4$YE#8G5$GE( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<+/<. J(8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<Q-<* J$#I# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<RS<C J$#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.S<+ J$#I#'G4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.C<. J$#I#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<Q/<R J$#I#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C-<./<C L $ #8!5(5$ 4ZE#$G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<R,<S LZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<,,</ LZE#$#(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

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S+<QS</ LZE#$#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*C-<CR<. 4GO<*P.<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,,-*<,*<C 4GO<*P/<9G4ZE#$#V$#VYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

**,<Q.<S LY4E#Z(b 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*.+<+Q<* 9G $#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

L !"#$%!&$'($!)!*+,-./-

Page 9 of 47

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0 1(!*,!#2!+-

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S+<RC</

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S+<QQ<+

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*,+<C*<Q

*,/<-C<*

RC<+S<-

RR<QS<-

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*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

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*C-<-,<C

*,,-*<,.<-

**,<CS<-

SR<,*<-

SC<-R<+

SC<,*<+

9G $#I#I(5Z 8(

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Page 10 of 47

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I"J'6138B& (14!)'#1) 8

.<7(5ZYE8 VZ5Z E(8(R*<CS<-

53 6' P#P 6 Q/</.<R

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Page 11 of 47

Page 169: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 12 of 47

Page 170: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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I"J'6138BK!)'#1) 8

-/,<.,<-

S*<CC<-

SR</+<C

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QS<-*<-

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Page 13 of 47

Page 171: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 14 of 47

Page 172: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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I"J'6138B& (14!)'#1) 8

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T.-T*+ J+d.,,* Q.S,

Q/</.<R >4(8 VZ5Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,Q<R-<Q >4(8 VZ5ZYE(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

*.,<*.<S >85Z$ 4(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

C-<CC</ J(8\f g 85Z$ 4(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

C,</.<Q J(8\#f gVY$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,C<RR<. J(8\#f g2EH#$ 85Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

*R*<.+<. J(8\#f1PZPGgV($YE(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,S<,Q<R J(8\#f%g2EH#$ 85Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.*Q<,*<R LZ$YO(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

C/<S,</ 9G (8\f PZg 85Z$ 4(8( ?9 .D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,-<++<, dEH#$ 85Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

Q-<S/<S dEH#$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

*R/</R<C A8'(8#_*P.P/<4P'`VY$(8( ?9 .D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

R*<.,</ ? VZ5Z E(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

QC<,*<Q 0Z(8 85Z$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

*.R<,,<, 0Y$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

'())*+,-./%7 B3(*)*4>C?.5D3 8$;%& 7;$! !! 98:78:!; J+d.,,* 87<9

'())*+,-./%E>-)*4.56.5. A "$<%& !<$8 !! 98:78:!; J+d.,,* 87<9

'())*+,-./%C @.)C?.5D3 A!; 8"$8%& ;!$8 !! 98:78:!; J+d.,,* 87<9

I"J'6138BLCM8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 ;;$<%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. 8$!%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 15 of 47

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0 1(!*-!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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-'.*+,%*<=>?@A?B>=

>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

+6!"J'6138B0 #')8

S+.R<R,<C 5):(161:( <>>>> C,, H1TL *,, ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</-<, >85GI#8Y ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,</Q<. 5"8 613 ?N= *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</R</ M'"1:( QT> C,, H1TL *,, ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<+*<S J($YEEGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+S</ CP"!(1:( =H *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+Q<+ C!.')# ?N? CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<C,<Q C! " <H>> *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<QR<- +"!6 OO>> ., H1TL * ,-T.-T*+ J+d*R,* -,*,T.,,DS

S+/R<R.<* - '$ HN? *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<R-<C 0'6J'6 8 A>> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<RS<- 7($4H$Y ?9 ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) @= .D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<..<+ &1)4 " ?N< ,D. H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<--<- S163 ?> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-./-

Page 16 of 47

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0 1(!*S!#2!+-

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-'.*+,%*<=>?@A?B>Q

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I"J'6138BK!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<CC<- *P*P*<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR</+<C *P*P.P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR<,,<C *P*P.<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</+</ *P*<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</C<+ *P*<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

QS<-*<- *P.P/<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*Q<+ *P.P/<K$G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C.-<S/<Q *P.P/<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*.,<Q.<* *P.P+<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<-/<- *P.P+<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*.<Q *P.<9G $#I#</<4ZE#$#V$#V 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<R/<+ *P.<9G $#I#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<C,<* *P.<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<,-<. *P.<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<QS<C *P.<9G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<-S<Q *P/PC<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C+*<S/<* *P/<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<+-<S *P+<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<R/</ .<JH5 8#8(!_7:N` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

CR*<SQ<- .<M(b 8#8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-, >,CP!W

-S<-+<* .<0$#V 8#8(!_ 4(5#8(` ?9 ., H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<*,<* +<7(5ZYE<.<V(85 8#8(!_7AJN` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<*/<* >4$YE#8G5$GE( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<+/<. J(8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<Q-<* J$#I# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<RS<C J$#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.S<+ J$#I#'G4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.C<. J$#I#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<Q/<R J$#I#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C-<./<C L $ #8!5(5$ 4ZE#$G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<R,<S LZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<,,</ LZE#$#(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

-S<--</ LZE#$#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<QS</ LZE#$#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*C-<CR<. 4GO<*P.<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,,-*<,*<C 4GO<*P/<9G4ZE#$#V$#VYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

**,<Q.<S LY4E#Z(b 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*.+<+Q<* 9G $#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

L !"#$%!&$'($!)!*+,-./-

Page 17 of 47

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RC<+S<-

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*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

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**,<CS<-

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SC<-R<+

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Page 18 of 47

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.<7(5ZYE8 VZ5Z E(8(R*<CS<- ?9 CD, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>4(8 VZ5Z(8(Q/</.<R ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

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'())*+,-./%7 B3(*)*4>C?.5D3 9$<%& 7;$! !! 98:78:!; J+d.,,* 87<9

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'())*+,-./%C @.)C?.5D3 A!; 8<$!%& ;!$8 !! 98:78:!; J+d.,,* 87<9

I"J'6138BLCM8*'8*5"!3)!"8

>$#4E#$!*,*-*.-S+<**<. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*..****,+<.Q<. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*./.***+*<*-<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.+.C/+-R<.*<R ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.+Q*.-S.<.R<- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.C+**,RS<-R<* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-,**,R-<Q.<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-./S/.+<./<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-Q***,,<*+<+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 <!$<%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. 7$8%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 19 of 47

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0 1(!.,!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*>H*<=GB<TG

-'.*+,%*<=>?@A?B>Q

>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

+6!"J'6138B0 #')8

S+.R<R,<C 5):(161:( <<> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</-<, >85GI#8Y ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,</Q<. 5"8 613 @NQ *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</R</ M'"1:( A?> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+*<S J($YEEGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+S</ LZ$#IGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+Q<+ L# E5 ?9 CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<C,<Q C! " QA> *, H1TL *, ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S+/R<QR<- +"!6 A?> ., H1TL * ,-T.-T*+ J+d*R,* -,*,T.,,DS

S+/R<R.<* L( ' ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<R-<C 0'6J'6 8 A< CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<RS<- 7($4H$Y ?9 ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) HN? .D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<..<+ &1)4 " >NA ,D. H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<--<- hG84 ?9 CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-./-

Page 20 of 47

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0 1(!.*!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*>H*<=GB<TG*$:

-'.*+,%*<=>?@A?B>?

>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

I"J'6138BLCM8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 8;$!%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. <$ %& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 21 of 47

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0 1(!..!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*>?*<?GB@<G

-'.*+,%*<=>?@A?B>H

>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

I"J'6138BK!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<CC<- *P*P*<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR</+<C *P*P.P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR<,,<C *P*P.<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</+</ *P*<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</C<+ *P*<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

QS<-*<- *P.P/<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*Q<+ *P.P/<K$G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C.-<S/<Q *P.P/<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*.,<Q.<* *P.P+<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<-/<- *P.P+<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*.<Q *P.<9G $#I#</<4ZE#$#V$#V 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<R/<+ *P.<9G $#I#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<C,<* *P.<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<,-<. *P.<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<QS<C *P.<9G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<-S<Q *P/PC<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C+*<S/<* *P/<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<+-<S *P+<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<R/</ .<JH5 8#8(!_7:N` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

CR*<SQ<- .<M(b 8#8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-, >,CP!W

-S<-+<* .<0$#V 8#8(!_ 4(5#8(` ?9 ., H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<*,<* +<7(5ZYE<.<V(85 8#8(!_7AJN` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<*/<* >4$YE#8G5$GE( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<+/<. J(8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<Q-<* J$#I# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<RS<C J$#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.S<+ J$#I#'G4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.C<. J$#I#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<Q/<R J$#I#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C-<./<C L $ #8!5(5$ 4ZE#$G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<R,<S LZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<,,</ LZE#$#(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

-S<--</ LZE#$#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<QS</ LZE#$#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*C-<CR<. 4GO<*P.<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,,-*<,*<C 4GO<*P/<9G4ZE#$#V$#VYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

**,<Q.<S LY4E#Z(b 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*.+<+Q<* 9G $#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

L !"#$%!&$'($!)!*+,-./-

Page 22 of 47

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0 1(!./!#2!+-

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I"J'6138BK!)'#1) 8

S+<RC</

SC<S*<Q

-,<.R<S

*,Q<.,</

*,,<+*<+

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RQ<Q.<Q

*//,<.,<S

S+<QQ<+

SC<,R<.

*-/+<,+<+

R*<.,</

*,+<C*<Q

*,/<-C<*

RC<+S<-

RR<QS<-

*/C<RQ<Q

*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

*,R<RR<R

*,Q<QQ</

*C-<-,<C

*,,-*<,.<-

**,<CS<-

SR<,*<-

SC<-R<+

SC<,*<+

9G $#I#I(5Z 8(

9G4ZE#$#'G2EH#$#I(5Z 8(

9G(5ZYE!(5Z($

9GGO#V$#VYE!:5Z($

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AO#V$#VYE (8\(8(

I![!V!<!WYE(8(

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7(5ZYE5($5G $Y H5YE(5Z($

? VZ5Z E(8(

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K(5$ ZY'$#2H$ 8

K#EH(8(

5$ 8O<*P.<9G4ZE#$#(5ZYE(8(

5$ 8O<*P/<9G4ZE#$#V$#VYE(8(

5$ 8O<*P+<9G4ZE#$#<.< H5(8(

K$G4ZE#$#(5ZYE(8(

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Page 23 of 47

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0 1(!.+!#2!+-

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I"J'6138B& (14!)'#1) 8

.<7(5ZYE8 VZ5Z E(8(R*<CS<- ?9 CD, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>4(8 VZ5Z(8(Q/</.<R ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>4(8 VZ5ZYE(8(.,Q<R-<Q ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>85Z$ 4(8(*.,<*.<S ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\f g 85Z$ 4(8(C-<CC</ ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

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A8'(8#_*P.P/<4P'`VY$(8(*R/</R<C ?9 .D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

? VZ5Z E(8(R*<.,</ ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

0Z(8 85Z$(8(QC<,*<Q ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

0Y$(8(*.R<,,<, ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

'())*+,-./%7 B3(*)*4>C?.5D3 9$;%& 7;$! !! 98:78:!; J+d.,,* 87<9

'())*+,-./%E>-)*4.56.5. A !$8%& !<$8 !! 98:78:!; J+d.,,* 87<9

'())*+,-./%C @.)C?.5D3 A!; <#$8%& ;!$8 !! 98:78:!; J+d.,,* 87<9

I"J'6138BLCM8*'8*5"!3)!"8

>$#4E#$!*,*-*.-S+<**<. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*..****,+<.Q<. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*./.***+*<*-<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.+.C/+-R<.*<R ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.+Q*.-S.<.R<- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.C+**,RS<-R<* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-,**,R-<Q.<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-./S/.+<./<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-Q***,,<*+<+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 8#$9%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. <$!%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 24 of 47

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0 1(!.C!#2!+-

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C)1 6#*+,%*CD--BEF*>?*<?GB@<G

-'.*+,%*<=>?@A?B>H

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+6!"J'6138B0 #')8

S+.R<R,<C 5):(161:( O= CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ >,+

S++,</-<, >85GI#8Y ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,</Q<. >$O(8G4 ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,</R</ M'"1:( <T> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+*<S J($YEEGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+S</ LZ$#IGHI ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<+Q<+ L# E5 ?9 CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S++,<C,<Q C! " ?@ *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<QR<- +"!6 H?> ., H1TL * ,-T.-T*+ J+d*R,* -,*,T.,,DS

S+/R<R.<* L( ' ?9 *D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<R-<C 0'6J'6 8 AT> CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

S+/R<RS<- 7($4H$Y ?9 ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) << .D, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<..<+ &1)4 " >N? ,D. H1TL * ,ST,*T*+ J+d*R,* -,.,T.,,DQ

S++,<--<- hG84 ?9 CD, H1TL * ,-T/,T*+ J+d*R,* -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-./-

Page 25 of 47

Page 183: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.-!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BK!)'#1) 8

-/,<.,<-

S*<CC<-

SR</+<C

SR<,,<C

SC</+</

SC</C<+

QS<-*<-

R-<*Q<+

C.-<S/<Q

*.,<Q.<*

RC<-/<-

R-<*.<Q

*,-<R/<+

RC<C,<*

*,S<,-<.

SQ<QS<C

*,Q<-S<Q

C+*<S/<*

*,-<+-<S

SQ<R/</

CR*<SQ<-

R*<CS<-

-S<-+<*

*,Q<*,<*

*,S<*/<*

S*<+/<.

*,Q<Q-<*

S+<RS<C

SC<.S<+

SC<.C<.

S+<Q/<R

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C-<./<C

*,Q<R,<S

SC<,,</

-S<--</

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*,,-*<,*<C

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*.+<+Q<*

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*P*P.<K$G4ZE#$#(5Z 8(

*P*<9G4ZE#$#(5Z 8(

*P*<9G4ZE#$#(5ZYE(8(

*P.P/<K$G4ZE#$# (8\(8(

*P.P/<K$G4ZE#$#V$#V 8(

*P.P/<K$GI(5ZYE (8\(8(

*P.P+<K$G4ZE#$# (8\(8(

*P.P+<K$GI(5ZYE (8\(8(

*P.<9G $#I#</<4ZE#$#V$#V 8(

*P.<9G $#I#(5Z 8(

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*P.<9G4ZE#$#(5Z 8(

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Page 26 of 47

Page 184: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.S!#2!+-

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I"J'6138BK!)'#1) 8

9G $#I#I(5Z 8(S+<RC</

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8<JH5YE (8\(8(*,+<C*<Q

8<0$#VYE (8\(8(*,/<-C<*

#<WYE(8(RC<+S<-

V<AO#V$#VYE!5#EH(8(RR<QS<-

O(4<JH5YE (8\(8(*/C<RQ<Q

@5Y$(8(*,,<+.<C

5($5<JH5YE (8\(8(RQ<,-<-

5($5G $Y!JH5YE!>E4#Z#ESC<-C<,

5($5G $Y>IYEI(5ZYE(5Z($RR+<,C<Q

K(5$ 4ZE#$#(5ZYE(8(*.S<*Q<+

K(5$ ZY'$#2H$ 8*,R<RR<R

K#EH(8(*,Q<QQ</

5$ 8O<*P.<9G4ZE#$#(5ZYE(8(*C-<-,<C

5$ 8O<*P/<9G4ZE#$#V$#VYE(8(*,,-*<,.<-

5$ 8O<*P+<9G4ZE#$#<.< H5(8(**,<CS<-

K$G4ZE#$#(5ZYE(8(SR<,*<-

K$G4ZE#$#2EH#$#I(5Z 8(SC<-R<+

eG8YE!4ZE#$G'(SC<,*<+

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Page 27 of 47

Page 185: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.Q!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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C)1 6#*+,%*CD--BEF*>Q*@>B@QG

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I"J'6138B& (14!)'#1) 8

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T.-T*+ J+d.,,* Q.S,

Q/</.<R >4(8 VZ5Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,Q<R-<Q >4(8 VZ5ZYE(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

*.,<*.<S >85Z$ 4(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

C-<CC</ J(8\f g 85Z$ 4(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

C,</.<Q J(8\#f gVY$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

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C/<S,</ 9G (8\f PZg 85Z$ 4(8( ?9 .D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

.,-<++<, dEH#$ 85Z(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

Q-<S/<S dEH#$(8( ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

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'())*+,-./%7 B3(*)*4>C?.5D3 9$8%& 7;$! !! 98:78:!; J+d.,,* 87<9

'())*+,-./%E>-)*4.56.5. A ;$"%& !<$8 !! 98:78:!; J+d.,,* 87<9

'())*+,-./%C @.)C?.5D3 A!; 8 $;%& ;!$8 !! 98:78:!; J+d.,,* 87<9

I"J'6138BLCM8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 <7$;%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

'())*+,-./%@.-),F?3*)* 1 GD3.5. 8$9%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

L !"#$%!&$'($!)!*+,-./-

Page 28 of 47

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0 1(!.R!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--BEF*>Q*@>B@QG

-'.*+,%*<=>?@A?B>O

>8 EY\('bL>@!) >8 EY5( =(OHE5 =L c8G5O 9GEH5G#8 9 5( ;L!J 54Z 7(5Z#' ;H EG2G($b

+6!"J'6138B0 #')8

S+.R<R,<C 5):(161:( O@ CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,</-<, >85GI#8Y ?9 *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,</Q<. 5"8 613 @N@ *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,</R</ M'"1:( ?A> CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<+*<S J($YEEGHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<+S</ LZ$#IGHI ?9 *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<+Q<+ L# E5 ?9 CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<C,<Q C! " ?>> *, H1TL *, ,ST,/T*+ J+d*R,. -,.,T.,,DQ

S+/R<QR<- +"!6 OA> ., H1TL * ,-T.-T*+ J+d*R,. -,*,T.,,DS

S+/R<R.<* L( ' ?9 *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S+/R<R-<C 0'6J'6 8 =Q CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S+/R<RS<- 7($4H$Y ?9 ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) TN? .D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

SSQ.<+R<. & ) 61:( <NA *D, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<..<+ &1)4 " >N@ ,D. H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S++,<--<- S163 QN@ CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-./-

Page 29 of 47

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0 1(!/,!#2!+-

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BK!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<CC<- *P*P*<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR</+<C *P*P.P.<K(5$ 4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SR<,,<C *P*P.<K$G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</+</ *P*<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC</C<+ *P*<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

QS<-*<- *P.P/<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*Q<+ *P.P/<K$G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C.-<S/<Q *P.P/<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*.,<Q.<* *P.P+<K$G4ZE#$# (8\(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<-/<- *P.P+<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

R-<*.<Q *P.<9G $#I#</<4ZE#$#V$#V 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<R/<+ *P.<9G $#I#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

RC<C,<* *P.<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<,-<. *P.<9G4ZE#$#(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<QS<C *P.<9G4ZE#$#V$#V 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<-S<Q *P/PC<K$GI(5ZYE (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C+*<S/<* *P/<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,-<+-<S *P+<9G4ZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SQ<R/</ .<JH5 8#8(!_7:N` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

CR*<SQ<- .<M(b 8#8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

R*<CS<- .<7(5ZYE8 VZ5Z E(8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-, >,CP!W

-S<-+<* .<0$#V 8#8(!_ 4(5#8(` ?9 ., H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<*,<* +<7(5ZYE<.<V(85 8#8(!_7AJN` ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*,S<*/<* >4$YE#8G5$GE( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

S*<+/<. J(8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<Q-<* J$#I# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<RS<C J$#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.S<+ J$#I#'G4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<.C<. J$#I#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<Q/<R J$#I#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

C-<./<C L $ #8!5(5$ 4ZE#$G'( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,Q<R,<S LZE#$# (8\(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

SC<,,</ LZE#$#(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

-S<--</ LZE#$#2#$I ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

S+<QS</ LZE#$#I(5Z 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*C-<CR<. 4GO<*P.<9G4ZE#$#(5ZYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

*,,-*<,*<C 4GO<*P/<9G4ZE#$#V$#VYE(8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

**,<Q.<S LY4E#Z(b 8( ?9 CD, H1TL * ,-T./T*+ J+d./*, Q.-,

*.+<+Q<* 9G $#I#4ZE#$#I(5Z 8( ?9 *D, H1TL * ,-T./T*+ J+d./*, Q.-,

L !"#$%!&$'($!)!*+,-./-

Page 30 of 47

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S+<RC</

SC<S*<Q

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RQ<Q.<Q

*//,<.,<S

S+<QQ<+

SC<,R<.

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*,+<C*<Q

*,/<-C<*

RC<+S<-

RR<QS<-

*/C<RQ<Q

*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

*,R<RR<R

*,Q<QQ</

*C-<-,<C

*,,-*<,.<-

**,<CS<-

SR<,*<-

SC<-R<+

SC<,*<+

9G $#I#I(5Z 8(

9G4ZE#$#'G2EH#$#I(5Z 8(

9G(5ZYE!(5Z($

9GGO#V$#VYE!:5Z($

:5ZYE (8\(8(

:5ZYE5($5G $Y H5YE(5Z($

M(b 4ZE#$#(5Z 8(

AO#V$#VYE (8\(8(

I![!V!<!WYE(8(

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7(5ZYE(8(!4ZE#$G'(

7(5ZYE5($5G $Y H5YE(5Z($

? VZ5Z E(8(

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5$ 8O<*P+<9G4ZE#$#<.< H5(8(

K$G4ZE#$#(5ZYE(8(

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Page 31 of 47

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0 1(!/.!#2!+-

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I"J'6138B& (14!)'#1) 8

.<7(5ZYE8 VZ5Z E(8(R*<CS<- ?9 CD, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>4(8 VZ5Z(8(Q/</.<R ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>4(8 VZ5ZYE(8(.,Q<R-<Q ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

>85Z$ 4(8(*.,<*.<S ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\f g 85Z$ 4(8(C-<CC</ ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\#f gVY$(8(C,</.<Q ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\#f g2EH#$ 85Z(8(.,C<RR<. ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\#f1PZPGgV($YE(8(*R*<.+<. ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

J(8\#f%g2EH#$ 85Z(8(.,S<,Q<R ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

LZ$YO(8(.*Q<,*<R ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

9G (8\f PZg 85Z$ 4(8(C/<S,</ ?9 .D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

dEH#$ 85Z(8(.,-<++<, ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

dEH#$(8(Q-<S/<S ?9 *D, H1TL * ,-T.-T*+ J+d.,,* Q.S,

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>$#4E#$!*..****,+<.Q<. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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>$#4E#$!*.+Q*.-S.<.R<- ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.C+**,RS<-R<* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-,**,R-<Q.<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-./S/.+<./<C ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

>$#4E#$!*.-Q***,,<*+<+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

'())*+,-./%=.F,F?3*)*4>C?.5D3 #<$#%& #9 ! 9 98:7<:!; J+d.C,* 898!:8987

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Page 32 of 47

Page 190: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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S++,<C,<Q C! " @A>> *, H1TL *, ,ST,/T*+ J+d*R,. -,.,T.,,DQ

S+/R<QR<- +"!6 @H>>> .,, H1TL *, ,-T.-T*+ J+d*R,. -,*,T.,,DS

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S+/R<R-<C 0'6J'6 8 OA> CD, H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

S+/R<RS<- 0 "3:"/ >N? ,D. H1TL * ,-T.CT*+ J+d./,Q S+S,T.+CD*

S++,<,.<, ;13R ) <@> ., H1TL *, ,ST,/T*+ J+d*R,. -,.,T.,,DQ

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S++,<..<+ &1)4 " @A ,D. H1TL * ,ST,*T*+ J+d*R,. -,.,T.,,DQ

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Page 33 of 47

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Page 34 of 47

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C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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Page 38 of 47

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***,+<.Q<. >$#4E#$!*..* ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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Page 39 of 47

Page 197: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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***+*<*-<C >$#4E#$!*./. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 ,D*, H1TL * ,-T.ST*+ J+d.C,* Q,Q*TQ,Q.

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Page 198: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 41 of 47

Page 199: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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I"J'6138BK!)'#1) 8

-/,<.,<-

S*<CC<-

SR</+<C

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SC</+</

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QS<-*<-

R-<*Q<+

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Page 42 of 47

Page 200: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 45 of 47

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Page 47 of 47

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J"K'6138CLDM8*'8*5"!3)!"8

*.-0+=**=. ?$#5F#$!*,*- @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

*.-0.=.S=- ?$#5F#$!*.+R @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

**,S0=-S=* ?$#5F#$!*.D+ @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

/0/.+=./=D ?$#5F#$!*.-. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

()**+,-./0&1/2-234+*+5673/894 "!$<&' 3 !" =;3 ;!# K+g.0,* : :!;: :<

()**+,-./0&?/.*-234+*+ @ A94/8/ ##$:&' 3 !" =;3 ;!# K+g.0,* : :!;: :<

L !"#$%!&$'($!)!*+,-./0

Page 4 of 32

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1 2(!D!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

D)1 6#*+,%*DE--CFG*<?*SIC<AI

-'.*+,%*<=>?@ABC>@

?9 FZ[('bM?A!) ?9 FZ6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65X 8(6X#' <I FH3H($b

+6!"K'6138C0 #')8

0+.S=S,=D 5):(161:( BH> DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/-=, ?96HJ#9Z @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/R=. ?$P(9H5 @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/S=/ M'"1:( ?B DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+*=0 K($ZFFHIJ @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+/=S M 'JHIJ @: ,E. I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+0=/ DO"!(1:( @NB *E, I2TL * ,0T,/T*+ K+g*S,. -,.,T.,,ER

0++,=+R=+ M# F6 @: DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=D,=R D! " AR *E, I2TL * ,0T,/T*+ K+g*S,. -,.,T.,,ER

0+/S=RS=- +"!6 A=>> ., I2TL * ,-T.-T*+ K+g*S,. -,*,T.,,E0

0+/S=S.=* L( ' @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0+/S=S-=D 0'6K'6 8 <<> DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0+/S=S0=- 8($5I$Z @: ,E. I2TL * ,-T.DT*+ K+g./,R 0+0,T.+DE*

0++,=,.=, ;13P ) RNA .E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

00R.=+S=. A(F(9HIJ @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=..=+ AHF\($ @: ,E. I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=--=- Q163 BNR DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./0

Page 5 of 32

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1 2(!-!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

D)1 6#*+,%*DE--CFG*<H*<>IC<HI

-'.*+,%*<=>?@ABC>A

?9 FZ[('bM?A!) ?9 FZ6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65X 8(6X#' <I FH3H($b

J"K'6138C& (14!)'#1) 8

.=8(6XZF9 VX6X F(9(S*=D0=-

?5(9 VX6X(9(R/=/.=S

?5(9 VX6XZF(9(.,R=S-=R

?96X$ 5(9(*.,=*.=0

K(9[h i 96X$ 5(9(D-=DD=/

K(9[#h iVZ$(9(D,=/.=R

K(9[#h i3FI#$ 96X(9(.,D=SS=.

K(9[#h2QXQHiV($ZF(9(*S*=.+=.

K(9[#h%i3FI#$ 96X(9(.,0=,R=S

MX$ZP(9(.*R=,*=S

:H (9[h QXi 96X$ 5(9(D/=0,=/

gFI#$ 96X(9(.,-=++=,

gFI#$(9(R-=0/=0

B9'(9#_*Q.Q/=5Q'`VZ$(9(*S/=/S=D

@ VX6X F(9(S*=.,=/

1X(9 96X$(9(RD=,*=R

1Z$(9(*.S=,,=,

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

@:

DE,

*E,

*E,

*E,

*E,

*E,

*E,

*E,

*E,

*E,

.E,

*E,

*E,

.E,

*E,

*E,

*E,

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

I2TL

*

*

*

*

*

*

*

*

*

*

*

*

*

*

*

*

*

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

,-T.,T*+

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

K+g,+,D

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

R.0,

?,D

()**+,-./0&< B4)+*+5673/894

()**+,-./0&C6.*+5/8D/8/ E"

()**+,-./0&7 ?/*73/894 E!#

":$:&'

>#$3&'

%#$"&'

<#$! !!"

!>$: !!"

#!$: !!"

=;< ;!#

=;< ;!#

=;< ;!#

K+g,+,D

K+g,+,D

K+g,+,D

:<>

:<>

:<>

J"K'6138CLDM8*'8*5"!3)!"8

*.-0+=**=. ?$#5F#$!*,*- @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

*.-0.=.S=- ?$#5F#$!*.+R @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

**,S0=-S=* ?$#5F#$!*.D+ @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

/0/.+=./=D ?$#5F#$!*.-. @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: ,E*, I2TL * ,-T/,T*+ K+g.0,* R,R*TR,R.

()**+,-./0&1/2-234+*+5673/894 ##$<&' 3 !" =;3 ;!# K+g.0,* : :!;: :<

()**+,-./0&?/.*-234+*+ @ A94/8/ #:$ &' 3 !" =;3 ;!# K+g.0,* : :!;: :<

L !"#$%!&$'($!)!*+,-./0

Page 6 of 32

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1 2(!0!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

D)1 6#*+,%*DE--CFG*<H*<>IC<HI

-'.*+,%*<=>?@ABC>A

?9 FZ[('bM?A!) ?9 FZ6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65X 8(6X#' <I FH3H($b

+6!"K'6138C0 #')8

0+.S=S,=D 5):(161:( B=> DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/-=, ?96HJ#9Z @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/R=. ?$P(9H5 @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=/S=/ M'"1:( =< DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+*=0 K($ZFFHIJ @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+/=S M 'JHIJ @: ,E. I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+0=/ DO"!(1:( <NR *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+R=+ M# F6 @: DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=D,=R D! " <B>> *,, I2TL *,, ,0T,/T*+ K+g*S,. -,.,T.,,ER

0+/S=RS=- +"!6 A?>> ., I2TL * ,-T.-T*+ K+g*S,. -,*,T.,,E0

0+/S=S.=* L( ' @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0+/S=S-=D 0'6K'6 8 @>> DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0+/S=S0=- 8($5I$Z @: ,E. I2TL * ,-T.DT*+ K+g./,R 0+0,T.+DE*

0++,=,.=, ;13P ) SNR .E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

00R.=+S=. A(F(9HIJ @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=..=+ AHF\($ @: ,E. I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=--=- Q163 HN< DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./0

Page 7 of 32

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1 2(!R!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

D)1 6#*+,%*DE--CFG*><*BIC<@I

-'.*+,%*<=>?@ABC>=

?9 FZ[('bM?A!) ?9 FZ6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65X 8(6X#' <I FH3H($b

J"K'6138CT!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0*=DD=- *Q*Q*=L$H5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0S=/+=D *Q*Q.Q.=L(6$ 5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0S=,,=D *Q*Q.=L$H5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=/+=/ *Q*=:H5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=/D=+ *Q*=:H5XF#$#(6XZF(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

R0=-*=- *Q.Q/=L$H5XF#$# (9[(9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

S-=*R=+ *Q.Q/=L$H5XF#$#V$#V 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

D.-=0/=R *Q.Q/=L$HJ(6XZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*.,=R.=* *Q.Q+=L$H5XF#$# (9[(9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

SD=-/=- *Q.Q+=L$HJ(6XZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

S-=*.=R *Q.=:H $#J#=/=5XF#$#V$#V 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*,-=S/=+ *Q.=:H $#J#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

SD=D,=* *Q.=:H5XF#$# (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,0=,-=. *Q.=:H5XF#$#(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0R=R0=D *Q.=:H5XF#$#V$#V 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,R=-0=R *Q/QD=L$HJ(6XZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

D+*=0/=* *Q/=:H5XF#$# (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,-=+-=0 *Q+=:H5XF#$# (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0R=S/=/ .=KI6 9#9(!_8;O` @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

DS*=0R=- .=N(b 9#9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

S*=D0=- .=8(6XZF9 VX6X F(9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-, ?,/Q!?,DQ!

W

-0=-+=* .=1$#V 9#9(!_ 5(6#9(` @: ., I2TL * ,-T./T*+ K+g./*, R.-,

*,R=*,=* +=8(6XZF=.=V(96 9#9(!_8BKO` @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*,0=*/=* ?5$ZF#9H6$HF( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

0*=+/=. K(9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,R=R-=* K$#J# (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0+=S0=D K$#J#5XF#$#J(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=.0=+ K$#J#'H5XF#$#J(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=.D=. K$#J#3#$J @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0+=R/=S K$#J#J(6X 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

0D=*D=, M $ #9!'HPIF3H'( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

D-=./=D M $ #9!6(6$ 5XF#$H'( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,R=S,=0 MXF#$# (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=,,=/ MXF#$#(6X 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

-0=--=/ MXF#$#3#$J @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0+=R0=/ MXF#$#J(6X 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*D-=DS=. 5HP=*Q.=:H5XF#$#(6XZF(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,,-*=,*=D 5HP=*Q/=:H5XF#$#V$#VZF(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

**,=R.=0 MZ5F#X(b 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

L !"#$%!&$'($!)!*+,-./0

Page 8 of 32

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1 2(!S!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

D)1 6#*+,%*DE--CFG*><*BIC<@I

-'.*+,%*<=>?@ABC>=

?9 FZ[('bM?A!) ?9 FZ6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65X 8(6X#' <I FH3H($b

J"K'6138CT!)'#1) 8

*.+=+R=* :H $#J#5XF#$#J(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0+=SD=/ :H $#J#J(6X 9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=0*=R :H5XF#$#'H3FI#$#J(6X 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

-,=.S=0 :H(6XZF!(6X($ @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*,R=.,=/ :HHP#V$#VZF!;6X($ @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*,,=+*=+ ;6XZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

-/0=S.=/ ;6XZF6($6H $Z I6ZF(6X($ @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

-0=0.=* N(b 5XF#$#(6X 9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

SR=R.=R BP#V$#VZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*//,=.,=0 J!Y!V!=!WZF(9( @: .E, I2TL * ,-T./T*+ K+g./*, R.-,

0+=RR=+ 8(6XZF!H#'H'( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=,S=. 8(6XZF(9(!5XF#$H'( @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

*-/+=,+=+ 8(6XZF6($6H $Z I6ZF(6X($ @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

S*=.,=/ @ VX6X F(9( @: DE, I2TL * ,-T./T*+ K+g./*, R.-, W

*,+=D*=R 9=KI6ZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,/=-D=* 9=1$#VZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

SD=+0=- #=WZF(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

SS=R0=- V=BP#V$#VZF!6#FI(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*/D=SR=R P(5=KI6ZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

*,,=+.=D A6Z$(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

SR=,-=- 6($6=KI6ZF (9[(9( @: *E, I2TL * ,-T./T*+ K+g./*, R.-,

0D=-D=, 6($6H $Z!KI6ZF!?F5#X#F @: D, I2TL * ,-T./T*+ K+g./*, R.-,

SS+=,D=R 6($6H $Z?JZFJ(6XZF(6X($ @: DE, I2TL * ,-T./T*+ K+g./*, R.-,

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Page 11 of 32

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/0/.+=./=D ?$#5F#$!*.-. @: ,E*, I2TL * ,0T,*T*+ K+g.0,* R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: ,E*, I2TL * ,0T,*T*+ K+g.0,* R,R*TR,R.

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L !"#$%!&$'($!)!*+,-./0

Page 17 of 32

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1 2(!*R!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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0++,=/S=/ M'"1:( =>> DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=+*=0 K($ZFFHIJ @: *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

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0++,=+0=/ DO"!(1:( @= *E, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

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0++,=..=+ &1)4 " @N< ,E. I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

0++,=--=- Q163 @A DE, I2TL * ,0T,*T*+ K+g*S,. -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./0

Page 18 of 32

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1 2(!*S!#3!/.

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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J"K'6138CT!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5XF#$#(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0*=DD=- *Q*Q*=L$H5XF#$#(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0S=/+=D *Q*Q.Q.=L(6$ 5XF#$#(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0S=,,=D *Q*Q.=L$H5XF#$#(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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SD=-/=- *Q.Q+=L$HJ(6XZF (9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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SD=D,=* *Q.=:H5XF#$# (9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

*,0=,-=. *Q.=:H5XF#$#(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0R=R0=D *Q.=:H5XF#$#V$#V 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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D+*=0/=* *Q/=:H5XF#$# (9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

*,-=+-=0 *Q+=:H5XF#$# (9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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-0=-+=* .=1$#V 9#9(!_ 5(6#9(` @: ., I2TL * ,-T.+T*+ K+g./** R.-,

*,R=*,=* +=8(6XZF=.=V(96 9#9(!_8BKO` @: DE, I2TL * ,-T.+T*+ K+g./** R.-,

*,0=*/=* ?5$ZF#9H6$HF( @: DE, I2TL * ,-T.+T*+ K+g./** R.-,

0*=+/=. K(9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

*,R=R-=* K$#J# (9[(9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0+=S0=D K$#J#5XF#$#J(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

0D=.0=+ K$#J#'H5XF#$#J(6X 9( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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0+=R/=S K$#J#J(6X 9( @: DE, I2TL * ,-T.+T*+ K+g./** R.-,

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D-=./=D M $ #9!6(6$ 5XF#$H'( @: *E, I2TL * ,-T.+T*+ K+g./** R.-,

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L !"#$%!&$'($!)!*+,-./0

Page 19 of 32

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1 2(!.,!#3!/.

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0+=SD=/

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Page 20 of 32

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1 2(!.*!#3!/.

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Page 227: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 25 of 32

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1 2(!.-!#3!/.

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Page 26 of 32

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Page 27 of 32

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Page 28 of 32

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Page 4 of 42

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0 1(!C!#2!+*

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-'.*+,%*<=>?@AAB>@

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*.-S+<**<. >$#4E#$!*,*- ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*+T*+ J+B,/.* Q,Q*TQ,Q.

'())*+,-./%0.1,123*)*4562.783 #=$A%& 3 !" #:!<:!< J+B,/.* 9 9!:9 9;

'())*+,-./%>.-),123*)* ? @83.7. ==$3%& 3 !" #:!<:!< J+B,/.* 9 9!:9 9;

+6!"I'6138BK 6 "')*CL (18#"/

K@ M*N!#')*&!)1$8 OAQR ,D* e * ,-T*RT*+ J+f*R** .C+,!J

CS<*.<C K#5 E!L] 8G'( ?9 ,D** I1T%1!'$] * ,-T.CT*+ J+f./*S >@K7!9!SC**<,R

+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( P>>> *,, I1T%1!'$] *,,, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S++,</-<, >85GI#8] ?9 ,D/ I1T%1!'$] *, ,ST,ST*+ J+f./,- -,.,T.,,DQ

S++,</Q<. 5"8 613 <Q< ,DC I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,</R</ E'"1:( OQ= *D, I1T%1!'$] *, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S++,<+*<S E "/))1:( >QF ,D. I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+S</ CL"!(1:( <A .D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+Q<+ C!.')# ?QR ,DC I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<C,<Q C! " =A>> *,, I1T%1!'$] *,,, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S+/R<QR<- +"!6 OO>> CD, I1T%1!'$] *, ,-T.ST*+ J+f./,. -,*,T.,,DS

S+/R<R.<* - '$ @QO *D, I1T%1!'$] *, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 <F> *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,C I1T%1!'$] * ,ST,RT*+ J+f/,*- S+S*T.+CDC

S++,<,.<, ;13S ) <? *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<..<+ &1)4 " AQ= ,D* I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<--<- T163 P@ *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 5 of 42

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0 1(!-!#2!+*

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)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

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-'.*+,%*<=>?@AAB>A

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H"I'6138BJCE8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 *., H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

'())*+,-./%0.1,123*)*4562.783 99$"%& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

'())*+,-./%>.-),123*)* ? @83.7. #"$!%& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

+6!"I'6138BK 6 "')*CL (18#"/

K@ M*N!#')*&!)1$8 FAQ< ,D* e * ,-T*RT*+ J+f*R** .C+,!J

CS<*.<C K#5 E!L] 8G'( ?9 ,D*. I1T%1!'$] * ,-T.CT*+ J+f./*S >@K7!9!SC**<,R

+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( F>>> *,, I1T%1!'$] *,,, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S++,</-<, >85GI#8] ?9 ,D/ I1T%1!'$] *, ,ST,ST*+ J+f./,- -,.,T.,,DQ

S++,</Q<. 5"8 613 @Q= ,DC I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,</R</ E'"1:( @< *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+*<S E "/))1:( >Q? ,D. I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f./,. -,.,T.,,DQ

S++,<+S</ CL"!(1:( <R .D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<+Q<+ C!.')# FQA ,DC I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<C,<Q C! " AA> *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S+/R<QR<- +"!6 <?>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f./,. -,*,T.,,DS

S+/R<R.<* - '$ PQ? *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 @P> *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ >,+

S+/R<RS<- 7($4H$] ?9 ,D,- I1T%1!'$] * ,ST,RT*+ J+f/,*- S+S*T.+CDC

S++,<,.<, ;13S ) @> *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<..<+ &1)4 " >QR ,D* I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

S++,<--<- T163 =? *D, I1T%1!'$] *, ,ST,/T*+ J+f./,. -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 6 of 42

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0 1(!S!#2!+*

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*.-S+<**<. >$#4E#$!*,*- ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

'())*+,-./%0.1,123*)*4562.783 9;$ %& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

'())*+,-./%>.-),123*)* ? @83.7. =9$A%& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

+6!"I'6138BK 6 "')*CL (18#"/

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CS<*.<C K#5 E!L] 8G'( ?9 ,D** I1T%1!'$] * ,-T.CT*+ J+f./*S >@K7!9!SC**<,R

+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( ?A>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,</-<, >85GI#8] ?9 ,D/ I1T%1!'$] *, ,ST,ST*+ J+f./,- -,.,T.,,DQ

S++,</Q<. 5"8 613 <QA ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,</R</ E'"1:( =P *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,<+*<S E "/))1:( >QF ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+S</ CL"!(1:( <O .D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+Q<+ C!.')# FQR ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<C,<Q C! " =<>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<QR<- +"!6 <<>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f.+,S -,*,T.,,DS

S+/R<R.<* - '$ =QO *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 @?> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,- I1T%1!'$] * ,ST,RT*+ J+f/,*- S+S*T.+CDC

S++,<,.<, ;13S ) @A *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

SSQ.<+R<. & ) 61:( >Q@ ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<..<+ &1)4 " <QF ,D* I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<--<- T163 PP *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 7 of 42

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Q,Q*TQ,Q.

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L !"#$%!&$'($!)!*+,-.//

Page 8 of 42

Page 245: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!R!#2!+*

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)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

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***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

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L !"#$%!&$'($!)!*+,-.//

Page 9 of 42

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Page 11 of 42

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Page 12 of 42

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Page 13 of 42

Page 250: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 14 of 42

Page 251: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 15 of 42

Page 252: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*P<*?GGBPG

-'.*+,%*<=>?@AAB<@

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

H"I'6138BZ!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

S*<CC<- *P*P*<K$G4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SR</+<C *P*P.P.<K(5$ 4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SR<,,<C *P*P.<K$G4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC</+</ *P*<9G4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC</C<+ *P*<9G4^E#$#(5^]E(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

QS<-*<- *P.P/<K$G4^E#$# (8`(8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

R-<*Q<+ *P.P/<K$G4^E#$#V$#V 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

C.-<S/<Q *P.P/<K$GI(5^]E (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*.,<Q.<* *P.P+<K$G4^E#$# (8`(8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

RC<-/<- *P.P+<K$GI(5^]E (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

R-<*.<Q *P.<9G $#I#</<4^E#$#V$#V 8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,-<R/<+ *P.<9G $#I#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

RC<C,<* *P.<9G4^E#$# (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,S<,-<. *P.<9G4^E#$#(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SQ<QS<C *P.<9G4^E#$#V$#V 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,Q<-S<Q *P/PC<K$GI(5^]E (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

C+*<S/<* *P/<9G4^E#$# (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,-<+-<S *P+<9G4^E#$# (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SQ<R/</ .<JH5 8#8(!X7:NY ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

CR*<SQ<- .<M(Z 8#8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

R*<CS<- .<7(5^]E8 V^5^ E(8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-, [

-S<-+<* .<0$#V 8#8(!X 4(5#8(Y ?9 *.,, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,Q<*,<* +<7(5^]E<.<V(85 8#8(!X7AJNY ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,S<*/<* >4$]E#8G5$GE( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

S*<+/<. J(8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,Q<Q-<* J$#I# (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

S+<RS<C J$#I#4^E#$#I(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC<.S<+ J$#I#'G4^E#$#I(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC<.C<. J$#I#2#$I ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

S+<Q/<R J$#I#I(5^ 8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

C-<./<C L $ #8!5(5$ 4^E#$G'( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,Q<R,<S L^E#$# (8`(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

SC<,,</ L^E#$#(5^ 8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

-S<--</ L^E#$#2#$I ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

S+<QS</ L^E#$#I(5^ 8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*C-<CR<. 4GO<*P.<9G4^E#$#(5^]E(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*,,-*<,*<C 4GO<*P/<9G4^E#$#V$#V]E(8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

**,<Q.<S L]4E#^(Z 8( ?9 /*, H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

*.+<+Q<* 9G $#I#4^E#$#I(5^ 8( ?9 -. H1T%1!'$] C, ,-T..T*+ J+f..,* Q.-,

L !"#$%!&$'($!)!*+,-.//

Page 16 of 42

Page 253: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*S!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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H"I'6138BZ!)'#1) 8

S+<RC</

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*,+<C*<Q

*,/<-C<*

RC<+S<-

RR<QS<-

*/C<RQ<Q

*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

*,R<RR<R

*,Q<QQ</

*C-<-,<C

*,,-*<,.<-

**,<CS<-

SR<,*<-

SC<-R<+

SC<,*<+

9G $#I#I(5^ 8(

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Page 17 of 42

Page 254: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 18 of 42

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S+/R<R-<C 0'6I'6 8 <R> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 0 "3:"/ >QA ,D,C I1T%1!'$] * ,ST,RT*+ J+B,S*/ S+S*T.+CDC

S++,<,.<, ;13S ) FQ= *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<..<+ &1)4 " >Q@ ,D* I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<--<- T163 <O *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 19 of 42

Page 256: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.,!#2!+*

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H"I'6138BJCE8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

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+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( <@>>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

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S++,</R</ E'"1:( @@ *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+*<S E "/))1:( >QP ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+S</ CL"!(1:( @R .D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+Q<+ C!.')# <P ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<C,<Q C! " FO> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<QR<- +"!6 <O>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f.+,S -,*,T.,,DS

S+/R<R.<* - '$ FQ@ *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 AR> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,- I1T%1!'$] * ,ST,RT*+ J+B,S*/ S+S*T.+CDC

S++,<,.<, ;13S ) @O *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<..<+ &1)4 " >QO ,D* I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<--<- T163 ?A *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 20 of 42

Page 257: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.*!#2!+*

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Page 21 of 42

Page 258: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 22 of 42

Page 259: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 23 of 42

Page 260: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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S++,<C,<Q C! " <P>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<QR<- +"!6 @<>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f.+,S -,*,T.,,DS

S+/R<R.<* - '$ RQ? *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 A?> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,C I1T%1!'$] * ,ST,RT*+ J+B,S*/ S+S*T.+CDC

S++,<,.<, ;13S ) @O *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

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Page 24 of 42

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H"I'6138BZ!)'#1) 8

-/,<.,<-

S*<CC<-

SR</+<C

SR<,,<C

SC</+</

SC</C<+

QS<-*<-

R-<*Q<+

C.-<S/<Q

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RC<-/<-

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RC<C,<*

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SQ<QS<C

*,Q<-S<Q

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*,-<+-<S

SQ<R/</

CR*<SQ<-

R*<CS<-

-S<-+<*

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Page 25 of 42

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K$G4^E#$#(5^]E(8(SR<,*<-

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Page 26 of 42

Page 263: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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S++,</Q<.

S++,</R</

S++,<+*<S

S++,<+/<R

S++,<+S</

S++,<+Q<+

S++,<C,<Q

S+/R<QR<-

S+/R<R.<*

S+/R<R-<C

S+/R<RS<-

S++,<,.<,

SSQ.<+R<.

S++,<..<+

S++,<--<-

5):(161:(

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*,,,

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,ST,ST*+

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,ST,ST*+

,ST,QT*+

,-T.ST*+

,ST,ST*+

,ST,ST*+

,ST,RT*+

,ST,ST*+

,ST,ST*+

,ST,ST*+

,ST,ST*+

J+f.+,S

J+f./,-

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

J+B,S*/

J+f.+,S

J+f.+,S

J+f.+,S

J+f.+,S

-,.,T.,,DQ

-,.,T.,,DQ

-,.,T.,,DQ

-,.,T.,,DQ

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S+S*T.+CDC

-,.,T.,,DQ

-,.,T.,,DQ

-,.,T.,,DQ

-,.,T.,,DQ

>,/

L !"#$%!&$'($!)!*+,-.//

Page 28 of 42

Page 265: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.R!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

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H"I'6138B& (14!)'#1) 8 & *6!# *U@>

R*<CS<- .<7(5^]E8 V^5^ E(8( ?9 CS, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

Q/</.<R >4(8 V^5^(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,Q<R-<Q >4(8 V^5^]E(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*.,<*.<S >85^$ 4(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C-<CC</ J(8`g h 85^$ 4(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C,</.<Q J(8`#g hV]$(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,C<RR<. J(8`#g h2EH#$ 85^(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*R*<.+<. J(8`#g1P^PGhV($]E(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S, >,C

.,S<,Q<R J(8`#g%h2EH#$ 85^(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.*Q<,*<R L^$]O(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C/<S,</ 9G (8`g P^h 85^$ 4(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,-<++<, fEH#$ 85^(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

Q-<S/<S fEH#$(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*R/</R<C A8'(8#X*P.P/<4P'YV]$(8( ?9 +-, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

R*<.,</ ? V^5^ E(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

QC<,*<Q 0^(8 85^$(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*.R<,,<, 0]$(8( ?9 ./, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

'())*+,-./%; B3(*)*4562.783 =!$#%& 3;$A !!" #: ;:!< J+f.C*/ 9;#

'())*+,-./%C5-)*4.7D.7. E" #=$;%& 3!$9 !!" #: ;:!< J+f.C*/ 9;#

'())*+,-./%6 >.)62.783 E!< =A$3%& 39$" !!" #: ;:!< J+f.C*/ 9;#

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*.-S+<**<. >$#4E#$!*,*- ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,/.* Q,Q*TQ,Q.

'())*+,-./%0.1,123*)*4562.783 #=$!%& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

'())*+,-./%>.-),123*)* ? @83.7. #<$3%& 3 !" #:!":!< J+B,/.* 9 9!:9 9;

L !"#$%!&$'($!)!*+,-.//

Page 29 of 42

Page 266: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!/,!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*>?*>GGB?GG

-'.*+,%*<=>?@AAB<R

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

+6!"I'6138BK 6 "')*CL (18#"/

K@ M*N!#')*&!)1$8 FRQP ,D* e * ,-T*RT*+ J+f*R*R .C+,!J

CS<*.<C K#5 E!L] 8G'( ?9 ,D** I1T%1!'$] * ,-T.CT*+ J+f./*S >@K7!9!SC**<,R

+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( =?>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,</-<, >85GI#8] ?9 ,D/ I1T%1!'$] *, ,ST,QT*+ J+f.C.- -,.,T.,,DQ

S++,</Q<. 5"8 613 <Q< ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,</R</ E'"1:( @@ *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,<+*<S E "/))1:( >Q? ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+S</ CL"!(1:( <@ .D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+Q<+ C!.')# PQ= ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<C,<Q C! " P@> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<QR<- +"!6 <@>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f.+,S -,*,T.,,DS

S+/R<R.<* - '$ ?QA *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 <F> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,- I1T%1!'$] * ,ST,RT*+ J+B,S*/ S+S*T.+CDC

S++,<,.<, ;13S ) <A *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<..<+ &1)4 " >Q? ,D* I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<--<- T163 AF *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

Page 30 of 42

Page 267: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!/*!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*>?*?GGB=FGG

-'.*+,%*<=>?@AAB<F

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

H"I'6138BZ!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S*<CC<- *P*P*<K$G4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SR</+<C *P*P.P.<K(5$ 4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SR<,,<C *P*P.<K$G4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC</+</ *P*<9G4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC</C<+ *P*<9G4^E#$#(5^]E(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

QS<-*<- *P.P/<K$G4^E#$# (8`(8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R-<*Q<+ *P.P/<K$G4^E#$#V$#V 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C.-<S/<Q *P.P/<K$GI(5^]E (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*.,<Q.<* *P.P+<K$G4^E#$# (8`(8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

RC<-/<- *P.P+<K$GI(5^]E (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R-<*.<Q *P.<9G $#I#</<4^E#$#V$#V 8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,-<R/<+ *P.<9G $#I#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

RC<C,<* *P.<9G4^E#$# (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,S<,-<. *P.<9G4^E#$#(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SQ<QS<C *P.<9G4^E#$#V$#V 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<-S<Q *P/PC<K$GI(5^]E (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C+*<S/<* *P/<9G4^E#$# (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,-<+-<S *P+<9G4^E#$# (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SQ<R/</ .<JH5 8#8(!X7:NY ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

CR*<SQ<- .<M(Z 8#8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R*<CS<- .<7(5^]E8 V^5^ E(8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-, [

-S<-+<* .<0$#V 8#8(!X 4(5#8(Y ?9 *.,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<*,<* +<7(5^]E<.<V(85 8#8(!X7AJNY ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,S<*/<* >4$]E#8G5$GE( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S*<+/<. J(8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<Q-<* J$#I# (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<RS<C J$#I#4^E#$#I(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<.S<+ J$#I#'G4^E#$#I(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<.C<. J$#I#2#$I ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<Q/<R J$#I#I(5^ 8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C-<./<C L $ #8!5(5$ 4^E#$G'( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<R,<S L^E#$# (8`(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<,,</ L^E#$#(5^ 8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

-S<--</ L^E#$#2#$I ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<QS</ L^E#$#I(5^ 8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*C-<CR<. 4GO<*P.<9G4^E#$#(5^]E(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,,-*<,*<C 4GO<*P/<9G4^E#$#V$#V]E(8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

**,<Q.<S L]4E#^(Z 8( ?9 /*, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*.+<+Q<* 9G $#I#4^E#$#I(5^ 8( ?9 -* H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

L !"#$%!&$'($!)!*+,-.//

Page 31 of 42

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0 1(!/.!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*>?*?GGB=FGG

-'.*+,%*<=>?@AAB<F

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H"I'6138BZ!)'#1) 8

S+<RC</

SC<S*<Q

-,<.R<S

*,Q<.,</

*,,<+*<+

-/S<R.</

-S<S.<*

RQ<Q.<Q

*//,<.,<S

S+<QQ<+

SC<,R<.

*-/+<,+<+

R*<.,</

*,+<C*<Q

*,/<-C<*

RC<+S<-

RR<QS<-

*/C<RQ<Q

*,,<+.<C

RQ<,-<-

SC<-C<,

RR+<,C<Q

*.S<*Q<+

*,R<RR<R

*,Q<QQ</

*C-<-,<C

*,,-*<,.<-

**,<CS<-

SR<,*<-

SC<-R<+

SC<,*<+

9G $#I#I(5^ 8(

9G4^E#$#'G2EH#$#I(5^ 8(

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Page 33 of 42

Page 270: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 34 of 42

Page 271: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 35 of 42

Page 272: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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Page 36 of 42

Page 273: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!/S!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<A*OGGBO?GG

-'.*+,%*<=>?@AAB@>

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

H"I'6138BZ!)'#1) 8

-/,<.,<- *P*P*P.<K(5$ 4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S*<CC<- *P*P*<K$G4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SR</+<C *P*P.P.<K(5$ 4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SR<,,<C *P*P.<K$G4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC</+</ *P*<9G4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC</C<+ *P*<9G4^E#$#(5^]E(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

QS<-*<- *P.P/<K$G4^E#$# (8`(8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R-<*Q<+ *P.P/<K$G4^E#$#V$#V 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C.-<S/<Q *P.P/<K$GI(5^]E (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*.,<Q.<* *P.P+<K$G4^E#$# (8`(8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

RC<-/<- *P.P+<K$GI(5^]E (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R-<*.<Q *P.<9G $#I#</<4^E#$#V$#V 8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,-<R/<+ *P.<9G $#I#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

RC<C,<* *P.<9G4^E#$# (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,S<,-<. *P.<9G4^E#$#(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SQ<QS<C *P.<9G4^E#$#V$#V 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<-S<Q *P/PC<K$GI(5^]E (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C+*<S/<* *P/<9G4^E#$# (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,-<+-<S *P+<9G4^E#$# (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SQ<R/</ .<JH5 8#8(!X7:NY ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

CR*<SQ<- .<M(Z 8#8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

R*<CS<- .<7(5^]E8 V^5^ E(8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-, [

-S<-+<* .<0$#V 8#8(!X 4(5#8(Y ?9 *.,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<*,<* +<7(5^]E<.<V(85 8#8(!X7AJNY ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,S<*/<* >4$]E#8G5$GE( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S*<+/<. J(8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<Q-<* J$#I# (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<RS<C J$#I#4^E#$#I(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<.S<+ J$#I#'G4^E#$#I(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<.C<. J$#I#2#$I ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<Q/<R J$#I#I(5^ 8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<*C<, L $ #8!'GOHE2G'( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

C-<./<C L $ #8!5(5$ 4^E#$G'( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,Q<R,<S L^E#$# (8`(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

SC<,,</ L^E#$#(5^ 8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

-S<--</ L^E#$#2#$I ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

S+<QS</ L^E#$#I(5^ 8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*C-<CR<. 4GO<*P.<9G4^E#$#(5^]E(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*,,-*<,*<C 4GO<*P/<9G4^E#$#V$#V]E(8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

**,<Q.<S L]4E#^(Z 8( ?9 /,, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

*.+<+Q<* 9G $#I#4^E#$#I(5^ 8( ?9 -, H1T%1!'$] C, ,-T.*T*+ J+f.*,* Q.-,

L !"#$%!&$'($!)!*+,-.//

Page 37 of 42

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0 1(!/Q!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<A*OGGBO?GG

-'.*+,%*<=>?@AAB@>

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

H"I'6138BZ!)'#1) 8

9G $#I#I(5^ 8(S+<RC</

9G4^E#$#'G2EH#$#I(5^ 8(SC<S*<Q

9G(5^]E!(5^($-,<.R<S

9GGO#V$#V]E!:5^($*,Q<.,</

:5^]E (8`(8(*,,<+*<+

:5^]E5($5G $] H5]E(5^($-/S<R.</

M(Z 4^E#$#(5^ 8(-S<S.<*

AO#V$#V]E (8`(8(RQ<Q.<Q

I!_!V!<![]E(8(*//,<.,<S

7(5^]E!G#'G'(S+<QQ<+

7(5^]E(8(!4^E#$G'(SC<,R<.

7(5^]E5($5G $] H5]E(5^($*-/+<,+<+

? V^5^ E(8(R*<.,</

8<JH5]E (8`(8(*,+<C*<Q

8<0$#V]E (8`(8(*,/<-C<*

#<[]E(8(RC<+S<-

V<AO#V$#V]E!5#EH(8(RR<QS<-

O(4<JH5]E (8`(8(*/C<RQ<Q

@5]$(8(*,,<+.<C

5($5<JH5]E (8`(8(RQ<,-<-

5($5G $]!JH5]E!>E4#^#ESC<-C<,

5($5G $]>I]EI(5^]E(5^($RR+<,C<Q

K(5$ 4^E#$#(5^]E(8(*.S<*Q<+

K(5$ ^]'$#2H$ 8*,R<RR<R

K#EH(8(*,Q<QQ</

5$ 8O<*P.<9G4^E#$#(5^]E(8(*C-<-,<C

5$ 8O<*P/<9G4^E#$#V$#V]E(8(*,,-*<,.<-

5$ 8O<*P+<9G4^E#$#<.< H5(8(**,<CS<-

K$G4^E#$#(5^]E(8(SR<,*<-

K$G4^E#$#2EH#$#I(5^ 8(SC<-R<+

iG8]E!4^E#$G'(SC<,*<+

?9

?9

?9

?9

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H1T%1!'$]

H1T%1!'$]

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H1T%1!'$]

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H1T%1!'$]

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H1T%1!'$]

H1T%1!'$]

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H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

H1T%1!'$]

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

C,

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

,-T.*T*+

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

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J+f.*,*

J+f.*,*

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J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

J+f.*,*

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

Q.-,

[

'())*+,-./%F)*?*G3(*)*4.7D.7.

'())*+,-./%054)*?*G3(*)*?.-2,7.

'())*+,-./%>*3(.7. E9

!<;%&

!= %&

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" !"

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=:;!:!<

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J+f.*,*

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J+f.*,*

9;=

9;=

9;=

L !"#$%!&$'($!)!*+,-.//

Page 38 of 42

Page 275: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!/R!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<A*OGGBO?GG

-'.*+,%*<=>?@AAB@>

>8 E]`('

L>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($

H"I'6138B& (14!)'#1) 8 & *6!# *U@>

R*<CS<- .<7(5^]E8 V^5^ E(8( ?9 CC, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

Q/</.<R >4(8 V^5^(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,Q<R-<Q >4(8 V^5^]E(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*.,<*.<S >85^$ 4(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C-<CC</ J(8`g h 85^$ 4(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C,</.<Q J(8`#g hV]$(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,C<RR<. J(8`#g h2EH#$ 85^(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*R*<.+<. J(8`#g1P^PGhV($]E(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S, >,C

.,S<,Q<R J(8`#g%h2EH#$ 85^(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.*Q<,*<R L^$]O(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

C/<S,</ 9G (8`g P^h 85^$ 4(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

.,-<++<, fEH#$ 85^(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

Q-<S/<S fEH#$(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*R/</R<C A8'(8#X*P.P/<4P'YV]$(8( ?9 ++, H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

R*<.,</ ? V^5^ E(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

QC<,*<Q 0^(8 85^$(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

*.R<,,<, 0]$(8( ?9 .., H1T%1!'$] * ,ST,.T*+ J+f.C*/ Q.S,

'())*+,-./%; B3(*)*4562.783 ==$=%& 3;$A !!" #: ;:!< J+f.C*/ 9;#

'())*+,-./%C5-)*4.7D.7. E" 9!$#%& 3!$9 !!" #: ;:!< J+f.C*/ 9;#

'())*+,-./%6 >.)62.783 E!< #<$=%& 39$" !!" #: ;:!< J+f.C*/ 9;#

H"I'6138BJCE8*'8*5"!3)!"8

*.-S+<**<. >$#4E#$!*,*- ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

***,+<.Q<. >$#4E#$!*..* ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

***+*<*-<C >$#4E#$!*./. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

C/+-R<.*<R >$#4E#$!*.+. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

*.-S.<.R<- >$#4E#$!*.+Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

**,RS<-R<* >$#4E#$!*.C+ ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

**,R-<Q.<C >$#4E#$!*.-, ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

/S/.+<./<C >$#4E#$!*.-. ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

***,,<*+<+ >$#4E#$!*.-Q ?9 **, H1T%1!'$] * ,ST*CT*+ J+B,Q*+ Q,Q*TQ,Q.

'())*+,-./%0.1,123*)*4562.783 # $3%& 3 !" #:!":!< J+B,Q*+ 9 9!:9 9;

'())*+,-./%>.-),123*)* ? @83.7. "=$#%& 3 !" #:!":!< J+B,Q*+ 9 9!:9 9;

L !"#$%!&$'($!)!*+,-.//

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0 1(!+,!#2!+*

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<A*OGGBO?GG

-'.*+,%*<=>?@AAB@>

>8 E]`('bL>@!) >8 E]5( =(OHE5 =L d8G5O 9GEH5G#8 9 5( ;L!J 54^ 7(5^#' ;H EG2G($b

+6!"I'6138BK 6 "')*CL (18#"/

K@ M*N!#')*&!)1$8 O>QO ,D* e * ,-T*RT*+ J+f*R*R .C+,!J

CS<*.<C K#5 E!L] 8G'( ?9 ,D** I1T%1!'$] * ,-T.-T*+ J+f./*Q >@K7!9!SC**<,R

+6!"I'6138B0 #')8

S+.R<R,<C 5):(161:( RF>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,</-<, >85GI#8] ?9 ,D/ I1T%1!'$] *, ,ST,QT*+ J+f.C.- -,.,T.,,DQ

S++,</Q<. 5"8 613 >QO ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,</R</ E'"1:( @< *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S++,<+*<S E "/))1:( >QF ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+/<R L 'IGHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+S</ CL"!(1:( @@ .D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<+Q<+ C!.')# <> ,DC I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<C,<Q C! " <@>> *,, I1T%1!'$] *,,, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<QR<- +"!6 <=>>> CD, I1T%1!'$] *, ,-T.ST*+ J+f.+,S -,*,T.,,DS

S+/R<R.<* - '$ <> *D, I1T%1!'$] *, ,ST,QT*+ J+f.+,S -,.,T.,,DQ

S+/R<R-<C 0'6I'6 8 @R> *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S+/R<RS<- 7($4H$] ?9 ,D,C I1T%1!'$] * ,ST,RT*+ J+B,S*/ S+S*T.+CDC

S++,<,.<, ;13S ) @F *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

SSQ.<+R<. @(E(8GHI ?9 ,D. I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<..<+ &1)4 " @QA ,D* I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

S++,<--<- T163 ?R *D, I1T%1!'$] *, ,ST,ST*+ J+f.+,S -,.,T.,,DQ

L !"#$%!&$'($!)!*+,-.//

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Page 42 of 42

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*WWN#YLX!TU!MVL![ E !6+Y-N#+SL+M*K!PN#MLQM-#+!>.L+QU!*+X!#MVLN!*WWN#WN-*ML!NL.RK*M#NU!*.L+Q-L,

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Page 1 of 48

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Page 2 of 48

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^ \(! #HFH91!V#H96P! #\(!.,,!bM! 9'! $(! (66($!PIH6('!6#! 9 F]PHP! ]!J(6^#'P!R.3,!_!-.D! P!P(JH\#F 6HF(!#$1 9H5PE

?*. >(PIF6!HP!(P6HJ 6('!'I(!6#!H96($=$(VFH5 6(!P JVF(! 9 F]PHP!>A:!c!*,dE

?** >(PIF6!HP!(P6HJ 6('!'I(!6#!^H1^!H9H6H F!\($H2H5 6H#9!P6 9' $'!5$H6($H !2 HFI$(E

?,S >(PIF6!HP!(P6HJ 6('!'I(!6#!^H1^!$(5#\($]!#2! 65^!eI FH6]!5#96$#FE

?,3 >(PIF6XPY! 9'!$(V#$6H91!FHJH6XPY! $(!(P6HJ 6('!'I(!6#!V##$!V$(5HPH#9Eb

?,- >(PIF6!HP!(P6HJ 6('!'I(!6#!^H1^!5#96H9IH91!5 FH $ 6H#9!P6 9' $'!5$H6($H !2 HFI$(Eb

?,D >(PIF6! 9'!$(V#$6H91!FHJH6! $(!(P6HJ 6('!'I(!6#!F#a!5#96H9IH91!5 FH $ 6H#9!P6 9' $'!5$H6($H !2 HFI$(Eb

?,+ >(PIF6!HP!(P6HJ 6('!'I(!6#!^H1^!J 6$HZ!PVH%(!$(5#\($]Eb

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*,, A JVF(!(Z6$ 56('!V P6!^#F'!6HJ(!'I(!6#!H9P6$IJ(96!2 HFI$(E!: 6 !HP!(P6HJ 6('Eb

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Page 3 of 48

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0 1(!+!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138B& (14!)'#1) 8 & *6!# *K@>

S*=D3=- .=8(6^]F9 V^6^ F(9( @: D+, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +/, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

S*=.,=/ @ V^6^ F(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .*, I1T%1!'$] * ,3T,.T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 $! %&' 3 !"##$ ;:<; <#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ :% %&' 3# 9"##$ ;:<; <#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% @9 @&' 39 $"##$ ;:<; <#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :; :&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ $: &' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 4 of 48

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0 1(!D!#2!+3

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+6!"J'6138BM 6 "')*CN (18#"/

LA O*P!#')*&!)1$8 GAQ< ,E* d * ,-T*ST*+ K+g*S*S .D+,!K

D3=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.-T*+ K+g./*R ?AL8!:!3D**=,S

+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( FR>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <Q< ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=/S=/ E'"1:( => *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=+*=3 E "/))1:( >QR ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+3=/ CN"!(1:( <= .E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+R=+ C!.')# RQ> ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=D,=R C! " RR> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=RS=- +"!6 <@>>> DE, J1T%1!'$] *, ,-T.3T*+ K+g.+,3 -,*,T.,,E3

3+/S=S.=* - '$ A@ *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @=> *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3+/S=S3=- 0 "3:"/ >Q>? ,E,D J1T%1!'$] * ,3T,ST*+ K+C,3*/ 3+3*T.+DED

3++,=,.=, ;13S ) <? *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

33R.=+S=. & ) 61:( >QA ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=..=+ &1)4 " <Q= ,E* J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=--=- T163 ?@ *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 5 of 48

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0 1(!-!#2!+3

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I"J'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/+=/ *Q*=:H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/D=+ *Q*=:H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

R3=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, ?,D

S-=*R=+ *Q.Q/=L$H5^F#$#V$#V 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D.-=3/=R *Q.Q/=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.,=R.=* *Q.Q+=L$H5^F#$# (9`(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S-=*.=R *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=S/=+ *Q.=:H $#J#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=D,=* *Q.=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=,-=. *Q.=:H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=R3=D *Q.=:H5^F#$#V$#V 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=-3=R *Q/QD=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D+*=3/=* *Q/=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=+-=3 *Q+=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=S/=/ .=KI6 9#9(!X8;OY @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

DS*=3R=- .=N(Z 9#9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=D3=- .=8(6^]F9 V^6^ F(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

-3=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *+,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=*/=* ?5$]F#9H6$HF( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=+/=. K(9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=R-=* K$#J# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=S3=D K$#J#5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.3=+ K$#J#'H5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.D=. K$#J#2#$J @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R/=S K$#J#J(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=*D=, M $ #9!'HPIF2H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=S,=3 M^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,,=/ M^F#$#(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-3=--=/ M^F#$#2#$J @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R3=/ M^F#$#J(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*D-=DS=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

**,=R.=3 M]5F#^(Z 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.+=+R=* :H $#J#5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

L !"#$%!&$'($!)!*+,-./+

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0 1(!3!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BU!)'#1) 8

3+=SD=/ :H $#J#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=3*=R :H5^F#$#'H2FI#$#J(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-,=.S=3 :H(6^]F!(6^($ @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=.,=/ :HHP#V$#V]F!;6^($ @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,=+*=+ ;6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-/3=S.=/ ;6^]F6($6H $] I6]F(6^($ @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-3=3.=* N(Z 5^F#$#(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SR=R.=R BP#V$#V]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*//,=.,=3 J!_!V!=![]F(9( @: *+, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=RR=+ 8(6^]F!H#'H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,S=. 8(6^]F(9(!5^F#$H'( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*-/+=,+=+ 8(6^]F6($6H $] I6]F(6^($ @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=.,=/ @ V^6^ F(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

*,+=D*=R 9=KI6]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,/=-D=* 9=0$#V]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=+3=- #=[]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SS=R3=- V=BP#V$#V]F!6#FI(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*/D=SR=R P(5=KI6]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,=+.=D A6]$(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SR=,-=- 6($6=KI6]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=-D=, 6($6H $]!KI6]F!?F5#^#F @: /D,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SS+=,D=R 6($6H $]?J]FJ(6^]F(6^($ @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.3=*R=+ L(6$ 5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,S=SS=S L(6$ ^]'$#2I$ 9 @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=RR=/ L#FI(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*D-=-,=D 6$ 9P=*Q.=:H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,-*=,.=- 6$ 9P=*Q/=:H5^F#$#V$#V]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

**,=D3=- 6$ 9P=*Q+=:H5^F#$#=.= I6(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,*=- L$H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=-S=+ L$H5^F#$#2FI#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,*=+ jH9]F!5^F#$H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

()**+,-./0&F*+D+G2)+*+3/7>/7/ #$3&' $;"#$; ;@< 3<#% K+g./,/ 9 @;

()**+,-./0&B43*+D+G2)+*+D/.6-7/ #@ &' $;"#$; ;@< 3<#% K+g./,/ 9 @;

()**+,-./0&A+2)/7/"?9 #%%&' $;"#$; ;@< 3<#% K+g./,/ 9 @;

L !"#$%!&$'($!)!*+,-./+

Page 7 of 48

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0 1(!R!#2!+3

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Page 8 of 48

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0 1(!S!#2!+3

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3++,=/R=. 5"8 613 <Q< ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=/S=/ E'"1:( <G *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=+*=3 E "/))1:( >QG ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

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Page 9 of 48

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0 1(!*,!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/+=/ *Q*=:H5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/D=+ *Q*=:H5^F#$#(6^]F(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

R3=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, ?,D

S-=*R=+ *Q.Q/=L$H5^F#$#V$#V 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D.-=3/=R *Q.Q/=L$HJ(6^]F (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.,=R.=* *Q.Q+=L$H5^F#$# (9`(9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S-=*.=R *Q.=:H $#J#=/=5^F#$#V$#V 9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=S/=+ *Q.=:H $#J#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=D,=* *Q.=:H5^F#$# (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=,-=. *Q.=:H5^F#$#(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=R3=D *Q.=:H5^F#$#V$#V 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=-3=R *Q/QD=L$HJ(6^]F (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D+*=3/=* *Q/=:H5^F#$# (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=+-=3 *Q+=:H5^F#$# (9`(9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=S/=/ .=KI6 9#9(!X8;OY @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

DS*=3R=- .=N(Z 9#9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=D3=- .=8(6^]F9 V^6^ F(9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

-3=-+=* .=0$#V 9#9(!X 5(6#9(Y @: */,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

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3+=S3=D K$#J#5^F#$#J(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.3=+ K$#J#'H5^F#$#J(6^ 9( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.D=. K$#J#2#$J @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R/=S K$#J#J(6^ 9( @: //, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=*D=, M $ #9!'HPIF2H'( @: -D I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

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Page 10 of 48

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Page 11 of 48

Page 290: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

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/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

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Page 12 of 48

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Page 13 of 48

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Page 14 of 48

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M?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

I"J'6138B& (14!)'#1) 8 & *6!# *K@>

S*=D3=- .=8(6^]F9 V^6^ F(9( @: -,, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +R, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 @9 &' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @$ 3&' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% :@ :&' 39 $"##$ ;:<;#<#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: *., I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :@ #&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ @% %&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 15 of 48

Page 294: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!*-!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*>F*?HHB=VHH

-'.*+,%*<=>?@A=B>F

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

+6!"J'6138BM 6 "')*CN (18#"/

LA O*P!#')*&!)1$8 VAQ@ ,E* d * ,-T*ST*+ K+g*S., .D+,!K

D3=*.=D L#6 F!M] 9H'( @: ,E*. J1T%1!'$] * ,-T.-T*+ K+g./*R ?AL8!:!3D**=,S

+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( F>>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 >QG ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=/S=/ E'"1:( <R *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=+*=3 E "/))1:( >QV ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+3=/ CN"!(1:( <F .E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+R=+ C!.')# RQ? ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=D,=R C! " G?> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=RS=- +"!6 <>>>> DE, J1T%1!'$] *, ,-T.3T*+ K+g.+,3 -,*,T.,,E3

3+/S=S.=* - '$ AQ? *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @>> *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,- J1T%1!'$] * ,3T,ST*+ K+C,3*/ 3+3*T.+DED

3++,=,.=, ;13S ) <G *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

33R.=+S=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=..=+ &1)4 " <QR ,E* J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=--=- T163 F? *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 16 of 48

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0 1(!*3!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<>*?HHB=VHH

-'.*+,%*<=>?@A=B>?

?9 F]`('

M?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

I"J'6138B& (14!)'#1) 8 & *6!# *K@>

S*=D3=- .=8(6^]F9 V^6^ F(9( @: DD, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: ++, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 :; $&' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @$ %&' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% :! #&' 39 $"##$ ;:<;#<#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 9# #&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ @$ $&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 17 of 48

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0 1(!*R!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<>*?HHB=VHH

-'.*+,%*<=>?@A=B>?

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

+6!"J'6138BM 6 "')*CN (18#"/

LA O*P!#')*&!)1$8 G>Q< ,E* d * ,-T*ST*+ K+g*S., .D+,!K

D3=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.-T*+ K+g./*R ?AL8!:!3D**=,S

+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( F=>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <Q< ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=/S=/ E'"1:( @G *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3++,=+*=3 E "/))1:( >QV ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+3=/ CN"!(1:( <? .E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=+R=+ C!.')# RQG ,ED J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=D,=R C! " <A>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=RS=- +"!6 <<>>> DE, J1T%1!'$] *, ,-T.3T*+ K+g.+,3 -,*,T.,,E3

3+/S=S.=* - '$ AQ> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,3 -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @<> *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,- J1T%1!'$] * ,3T,ST*+ K+C,3*/ 3+3*T.+DED

3++,=,.=, ;13S ) <G *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

33R.=+S=. & ) 61:( >QA ,E. J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=..=+ &1)4 " <QV ,E* J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

3++,=--=- T163 FG *E, J1T%1!'$] *, ,3T,3T*+ K+g.+,3 -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 18 of 48

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0 1(!*S!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<>*=VHHBG?HH

-'.*+,%*<=>?@A=B>R

?9 F]`('

M?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($

I"J'6138B& (14!)'#1) 8 & *6!# *K@>

S*=D3=- .=8(6^]F9 V^6^ F(9( @: D+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 :# 3&' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @9 #&' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% 9; 3&' 39 $"##$ ;:<;#<#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :: #&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ @$ 9&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 19 of 48

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Page 21 of 48

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Page 22 of 48

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Page 23 of 48

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Page 24 of 48

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.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +/, I1T%1!'$] * ,3T,ST*+ K+C,**- R.3, ?,D

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +/, I1T%1!'$] * ,3T,ST*+ K+C,**- R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,ST*+ K+C,**- R.3,

()**+,-./0& "12)+*+3456/782 @! #&' 3 !"##$ ;:<;!<#% K+C,**- 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @% %&' 3# 9"##$ ;:<;!<#% K+C,**- 9 :;

()**+,-./0&5"A/*56/782"?#% :% $&' 39 $"##$ ;:<;!<#% K+C,**- 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 9; &' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ :; @&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 25 of 48

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0 1(!.-!#2!+3

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+6!"J'6138B0 #')8

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3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <Q< ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/S=/ E'"1:( @F *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+*=3 E "/))1:( >QG ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

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3++,=+3=/ CN"!(1:( <? .E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+R=+ C!.')# RQG ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=D,=R C! " <<>> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=RS=- +"!6 <<>>> DE, J1T%1!'$] *, ,3T,.T*+ K+g.+,R -,*,T.,,E3

3+/S=S.=* - '$ VQF *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @<> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,D J1T%1!'$] * ,3T,ST*+ K+C,3*/ 3+3*T.+DED

3++,=,.=, ;13S ) @> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

33R.=+S=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=..=+ &1)4 " @QF ,E* J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=--=- T163 FG *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 26 of 48

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0 1(!.3!#2!+3

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-,.,T.,,ER

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Page 27 of 48

Page 306: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!.R!#2!+3

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*.,=*.=3 ?96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +D, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 :; #&' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @% @&' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% :$ #&' 39 $"##$ ;:<;#<#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :! $&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ @9 @&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

Page 28 of 48

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0 1(!.S!#2!+3

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+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( ?>>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <Q< ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/S=/ E'"1:( <<> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+*=3 E "/))1:( >QG ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+3=/ CN"!(1:( <V .E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+R=+ C!.')# VQ= ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=D,=R C! " VG> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=RS=- +"!6 <A>>> DE, J1T%1!'$] *, ,3T,.T*+ K+g.+,R -,*,T.,,E3

3+/S=S.=* - '$ <@ *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @A> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S3=- 0 "3:"/ >Q>? ,E,- J1T%1!'$] * ,3T,ST*+ K+C,3*+ 3+3*T.+DED

3++,=,.=, ;13S ) @@ *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

33R.=+S=. & ) 61:( >Q= ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=..=+ &1)4 " @QR ,E* J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=--=- T163 <<> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 29 of 48

Page 308: ! NXLN7!!:2&@:(2 PN-QL7!]2/293 && OLPP!P …...Lansing, MI 48909 TEL: (517) 335-9800 FAX: (517) 335-9600 MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY ENVIRONMENTAL LABORATORY MDEQ-RRD-LANSING

0 1(!/,!#2!+3

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I"J'6138B& (14!)'#1) 8 & *6!# *K@>

S*=D3=- .=8(6^]F9 V^6^ F(9( @: D3, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

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*.,=*.=3 ?96^$ 5(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +-, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +-, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +-, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

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.*R=,*=S M^$]P(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +-, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +-, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: ./, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 :$ 3&' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ :; &' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&5"A/*56/782"?#% 9; #&' 39 $"##$ ;:<;#<#% K+g.D*/ 9 :;

I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :! &' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

()**+,-./0&A/.*-C62+*+"D"E82/7/ @9 $&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

L !"#$%!&$'($!)!*+,-./+

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0 1(!/*!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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C)1 6#*+,%*CD--B&E*>G*?HB<@H

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+6!"J'6138BM 6 "')*CN (18#"/

LA O*P!#')*&!)1$8 VRQG ,E* d * ,-T*ST*+ K+g*S., .D+,!K

D3=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.-T*+ K+g./*R ?AL8!:!3D**=,S

+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( ?G>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <Q> ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/S=/ E'"1:( @> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+*=3 E "/))1:( >QG ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+3=/ CN"!(1:( @@ .E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+R=+ C!.')# <> ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=D,=R C! " <@>> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=RS=- +"!6 <=>>> DE, J1T%1!'$] *, ,3T,.T*+ K+g.+,R -,*,T.,,E3

3+/S=S.=* - '$ FQG *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @?> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,- J1T%1!'$] * ,3T,ST*+ K+C,3*+ 3+3*T.+DED

3++,=,.=, ;13S ) @R *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

33R.=+S=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=..=+ &1)4 " AQ< ,E* J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=--=- T163 V? *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

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0 1(!/.!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<<*>B?HH

-'.*+,%*<=>?@A=B<F

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

+6!"J'6138BM 6 "')*CN (18#"/

LA O*P!#')*&!)1$8 VGQF ,E* d * ,-T*ST*+ K+g*S., .D+,!K

D3=*.=D L#6 F!M] 9H'( @: ,E** J1T%1!'$] * ,-T.-T*+ K+g./*R ?AL8!:!3D**=,S

+6!"J'6138B0 #')8

3+.S=S,=D 5):(161:( R=>> *,, J1T%1!'$] *,,, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,RT*+ K+g.D.- -,.,T.,,ER

3++,=/R=. 5"8 613 <QR ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/S=/ E'"1:( ?G *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+*=3 E "/))1:( >QR ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+/=S C'$(1:( >QA ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+3=/ CN"!(1:( <V .E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+R=+ C!.')# VQ> ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=D,=R C! " F<> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=RS=- +"!6 <=>>> DE, J1T%1!'$] *, ,3T,.T*+ K+g.+,R -,*,T.,,E3

3+/S=S.=* - '$ VR *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @=> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,- J1T%1!'$] * ,3T,ST*+ K+C,3*+ 3+3*T.+DED

3++,=,.=, ;13S ) @< *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

33R.=+S=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=..=+ &1)4 " <Q> ,E* J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=--=- T163 <R> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 32 of 48

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0 1(!//!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

)*+,-+./!01!234&4'$- )+$M'$*#.%.#2+)#*+)1 56)7!89:(;!%%9<43&&

=>?7!89:(;!%%9<4@&&

C)1 6#*+,%*CD--B&E*<<*?HHBVH

-'.*+,%*<=>?@A=B<?

?9 F]`('bM?A!) ?9 F]6( >(PIF6 >L f9H6P :HFI6H#9 : 6( <M!K 65^ 8(6^#' <I FH2H($b

I"J'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/+=/ *Q*=:H5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/D=+ *Q*=:H5^F#$#(6^]F(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

R3=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, ?,D

S-=*R=+ *Q.Q/=L$H5^F#$#V$#V 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D.-=3/=R *Q.Q/=L$HJ(6^]F (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.,=R.=* *Q.Q+=L$H5^F#$# (9`(9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S-=*.=R *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=S/=+ *Q.=:H $#J#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=D,=* *Q.=:H5^F#$# (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=,-=. *Q.=:H5^F#$#(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=R3=D *Q.=:H5^F#$#V$#V 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=-3=R *Q/QD=L$HJ(6^]F (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D+*=3/=* *Q/=:H5^F#$# (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=+-=3 *Q+=:H5^F#$# (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=S/=/ .=KI6 9#9(!X8;OY @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

DS*=3R=- .=N(Z 9#9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=D3=- .=8(6^]F9 V^6^ F(9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

-3=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *.,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=*/=* ?5$]F#9H6$HF( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=+/=. K(9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=R-=* K$#J# (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=S3=D K$#J#5^F#$#J(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.3=+ K$#J#'H5^F#$#J(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.D=. K$#J#2#$J @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R/=S K$#J#J(6^ 9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=*D=, M $ #9!'HPIF2H'( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=S,=3 M^F#$# (9`(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,,=/ M^F#$#(6^ 9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-3=--=/ M^F#$#2#$J @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R3=/ M^F#$#J(6^ 9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*D-=DS=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

**,=R.=3 M]5F#^(Z 9( @: /,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.+=+R=* :H $#J#5^F#$#J(6^ 9( @: -, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

L !"#$%!&$'($!)!*+,-./+

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0 1(!/+!#2!+3

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Page 34 of 48

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S*=D3=- .=8(6^]F9 V^6^ F(9( @: D+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 @@ &' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

()**+,-./0&=4.*+3/7>/7/"?$ @# 3&' 3# 9"##$ ;:<;#<#% K+g.D*/ 9 :;

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***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :% ;&' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

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Page 35 of 48

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Page 36 of 48

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0 1(!/3!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/+=/ *Q*=:H5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/D=+ *Q*=:H5^F#$#(6^]F(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

R3=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, ?,D

S-=*R=+ *Q.Q/=L$H5^F#$#V$#V 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D.-=3/=R *Q.Q/=L$HJ(6^]F (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.,=R.=* *Q.Q+=L$H5^F#$# (9`(9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S-=*.=R *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=S/=+ *Q.=:H $#J#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=D,=* *Q.=:H5^F#$# (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=,-=. *Q.=:H5^F#$#(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=R3=D *Q.=:H5^F#$#V$#V 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=-3=R *Q/QD=L$HJ(6^]F (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D+*=3/=* *Q/=:H5^F#$# (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=+-=3 *Q+=:H5^F#$# (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=S/=/ .=KI6 9#9(!X8;OY @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

DS*=3R=- .=N(Z 9#9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=D3=- .=8(6^]F9 V^6^ F(9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

-3=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *.,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=*/=* ?5$]F#9H6$HF( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=+/=. K(9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=R-=* K$#J# (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=S3=D K$#J#5^F#$#J(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.3=+ K$#J#'H5^F#$#J(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.D=. K$#J#2#$J @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R/=S K$#J#J(6^ 9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=*D=, M $ #9!'HPIF2H'( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=S,=3 M^F#$# (9`(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,,=/ M^F#$#(6^ 9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-3=--=/ M^F#$#2#$J @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R3=/ M^F#$#J(6^ 9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*D-=DS=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,,-*=,*=D 5HP=*Q/=:H5^F#$#V$#V]F(9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

**,=R.=3 M]5F#^(Z 9( @: /*, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.+=+R=* :H $#J#5^F#$#J(6^ 9( @: -. I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

L !"#$%!&$'($!)!*+,-./+

Page 37 of 48

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Page 38 of 48

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0 1(!/S!#2!+3

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S*=D3=- .=8(6^]F9 V^6^ F(9( @: D+, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R/=/.=S ?5(9 V^6^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,R=S-=R ?5(9 V^6^]F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.,=*.=3 ?96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D-=DD=/ K(9`h i 96^$ 5(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D,=/.=R K(9`#h iV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,D=SS=. K(9`#h i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S*=.+=. K(9`#h1Q^QHiV($]F(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

.,3=,R=S K(9`#h%i2FI#$ 96^(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.*R=,*=S M^$]P(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

D/=3,=/ :H (9`h Q^i 96^$ 5(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

.,-=++=, gFI#$ 96^(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

R-=3/=3 gFI#$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*S/=/S=D B9'(9#X*Q.Q/=5Q'YV]$(9( @: +/, I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3, ?,D

S*=.,=/ @ V^6^ F(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

RD=,*=R 0^(9 96^$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

*.S=,,=, 0]$(9( @: .., I1T%1!'$] * ,3T,*T*+ K+g.D*/ R.3,

()**+,-./0& "12)+*+3456/782 @; :&' 3 !"##$ ;:<;#<#% K+g.D*/ 9 :;

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I"J'6138BLCE8*'8*5"!3)!"8

*.-3+=**=. ?$#5F#$!*,*- @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,+=.R=. ?$#5F#$!*..* @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***+*=*-=D ?$#5F#$!*./. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

D/+-S=.*=S ?$#5F#$!*.+. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

*.-3.=.S=- ?$#5F#$!*.+R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S3=-S=* ?$#5F#$!*.D+ @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

**,S-=R.=D ?$#5F#$!*.-, @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

/3/.+=./=D ?$#5F#$!*.-. @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

***,,=*+=+ ?$#5F#$!*.-R @: **, I1T%1!'$] * ,3T*-T*+ K+C,R*+ R,R*TR,R.

()**+,-./0&B/C-C62+*+3456/782 :$ &' 3;"#$; ;:<#@<#% K+C,R*+ 9;9#<9;9

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L !"#$%!&$'($!)!*+,-./+

Page 39 of 48

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0 1(!+,!#2!+3

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+6!"J'6138B0 #')8

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3++,=/-=, ?96HJ#9] @: ,E/ J1T%1!'$] *, ,3T,ST*+ K+g.D.3 -,.,T.,,ER

3++,=/R=. 5"8 613 <QA ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=/S=/ E'"1:( @@ *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+*=3 E "/))1:( >QR ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+/=S M 'JHIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+3=/ CN"!(1:( <G .E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=+R=+ C!.')# GQ> ,ED J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=D,=R C! " <<>> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=RS=- +"!6 <@>>> DE, J1T%1!'$] *, ,3T,.T*+ K+g.+,R -,*,T.,,E3

3+/S=S.=* - '$ <F *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S-=D 0'6J'6 8 @A> *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3+/S=S3=- 8($5I$] @: ,E,D J1T%1!'$] * ,3T,ST*+ K+C,3*+ 3+3*T.+DED

3++,=,.=, ;13S ) @A *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

33R.=+S=. A(F(9HIJ @: ,E. J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=..=+ &1)4 " <QR ,E* J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

3++,=--=- T163 ?< *E, J1T%1!'$] *, ,3T,RT*+ K+g.+,R -,.,T.,,ER

L !"#$%!&$'($!)!*+,-./+

Page 40 of 48

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0 1(!+*!#2!+3

M ! "#$%&'(#)*M'$*%+,%'$- )+$M'$*#.%/0#. *1 P !"#$!%&'(&

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I"J'6138BU!)'#1) 8

-/,=.,=- *Q*Q*Q.=L(6$ 5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=DD=- *Q*Q*=L$H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=/+=D *Q*Q.Q.=L(6$ 5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3S=,,=D *Q*Q.=L$H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/+=/ *Q*=:H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=/D=+ *Q*=:H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

R3=-*=- *Q.Q/=L$H5^F#$# (9`(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, ?,D

S-=*R=+ *Q.Q/=L$H5^F#$#V$#V 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D.-=3/=R *Q.Q/=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.,=R.=* *Q.Q+=L$H5^F#$# (9`(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=-/=- *Q.Q+=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S-=*.=R *Q.=:H $#J#=/=5^F#$#V$#V 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=S/=+ *Q.=:H $#J#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

SD=D,=* *Q.=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=,-=. *Q.=:H5^F#$#(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=R3=D *Q.=:H5^F#$#V$#V 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=-3=R *Q/QD=L$HJ(6^]F (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D+*=3/=* *Q/=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,-=+-=3 *Q+=:H5^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3R=S/=/ .=KI6 9#9(!X8;OY @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

DS*=3R=- .=N(Z 9#9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

S*=D3=- .=8(6^]F9 V^6^ F(9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-, [

-3=-+=* .=0$#V 9#9(!X 5(6#9(Y @: *+,, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=*,=* +=8(6^]F=.=V(96 9#9(!X8BKOY @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,3=*/=* ?5$]F#9H6$HF( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3*=+/=. K(9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=R-=* K$#J# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=S3=D K$#J#5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.3=+ K$#J#'H5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=.D=. K$#J#2#$J @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R/=S K$#J#J(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=*D=, M $ #9!'HPIF2H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

D-=./=D M $ #9!6(6$ 5^F#$H'( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*,R=S,=3 M^F#$# (9`(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3D=,,=/ M^F#$#(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

-3=--=/ M^F#$#2#$J @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

3+=R3=/ M^F#$#J(6^ 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*D-=DS=. 5HP=*Q.=:H5^F#$#(6^]F(9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

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**,=R.=3 M]5F#^(Z 9( @: /D, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

*.+=+R=* :H $#J#5^F#$#J(6^ 9( @: 3, I1T%1!'$] D, ,-T./T*+ K+g./,/ R.-,

L !"#$%!&$'($!)!*+,-./+

Page 41 of 48

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