golder associates - cpr.ca · pdf filegolder associates may 15, 2017 metropolitan council...

. Golder Associates

May 15, 2017

Metropolitan Council Environmental Services Industrial Waste Division 390 Robert St. N. St. Paul, MN 55101

Attention: Ms. Ashley Corbeille

RE: APRIL 2017 SAMPLING RESULTS SMR INDUSTRIAL DISCHARGE PERMIT NUMBER 2289 SOUTHEAST PUMP AND TREAT SYSTEM CANADIAN PACIFIC SHOREHAM FACILITY

Dear Ms. Corbeille:

Project No.:023-6105.017

On behalf of Canadian Pacific, enclosed is the April 2017 Sampling Results Self-Monitoring Report for the site located at 281h & Central Avenue NE, Minneapolis MN. In accordance with the Metropolitan Council Environmental Services (MCES) Industrial Discharge Permit Number 2289, effective October 1, 2016 (MCES permit), this submittal documents the quality of water discharged from the groundwater pump and treat system owned by Canadian Pacific.

Required information for the discharge is provided as follows: • Attachment A - Sampling Results - SMR. • Attachment B - analytical data from Pace Analytical Services, LLC for the April 2017 monthly

sampling event. • Attachment C - Field Instrument pH Calibration Records

Analytical results from the April 2017 sampling event1 showed that the treated discharge water was in compliance with the MCES permit discharge limitations during this reporting period.

If you have any questions or comments, please do not hesitate to contact Barbara Johnson at (651) 697-9737. Thank you for your assistance in this matter.

Very truly yours,

GOLDER ASSOCIATES INC.

/{-!~,I c/!t_; Alan Phillips Project Geologist

Cc: Ms. Aimee Zack, CP Ms. Claire Mackler, Golder

k~ Barbara Johnson, PE Associate

1 Note that sample point SP-01 is identified as sample SE EFFLUENT in the analytical results from April 2017 (Attachmen_t_B...._~~~~~~~~~~~~~~~~~~~~~~~~~~~

Golder Associates Inc. 1751 West County Rd. B, Ste. 105

Roseville, MN USA 55113 Tel: (651) 697-9737 Fax: (651) 697-9737 www.golder.com

Golder Associates: Operations In Africa, Asia, Australasia, Europe, North America and South America

Attachment A

SAMPLING RESULTS – SELF-MONITORING REPORT

Metropolitan Council Environmental Services Industrial Waste & Pollution Prevention Section 390 North Robert Street St. Paul, Minnesota 55101-1805

For MCES Use Only

Permit No: Staff: 1

Received: 0 L 45 E -- j

SAMPLING RESULTS - SMR for Standard and Special Discharge Permits Please complete Page 2 of this form for each monitoring point with sampling requirements in Attachment A of the Permit.

1. Permittee Name: Canadian Pacific Railway Permit No: 2289 ------2. Facility Address: 28th Ave NE & Central Ave NE, Minneapolis, MN 55418

3. Reporting Period: Year: 20_1_7 ___ _ Choose applicable period below

D

Quarterly Reporter: 0 Jan-Mar

Semi-Annual Reporter: D Jan-Jun

Annual Reporter: D Jan-Dec

No discharge/No sampling this period.

0 Apr-Jun 0 Jul-Sep

D Jul-Dec

D Oct-Dec

If checked, proceed to section 9 below and do not complete page 2.

4. Proper Sampling: Were all samples collected and composited according to permit requirements?

['.!] Yes D No If No, add explanation below:

5. Proper Analysis: Were all analyses conducted per permit requirements? 0 Yes D No If No, add explanation below:

6. Representative Discha~: Are the an~ical results representative of the wastewater discharged during this monitoring event? L.!.J Yes LJ No If No, add explanation below:

7. Compliance Status: Compare the analytical results with the corresponding discharge limits in your Permit. Do any analytical results exceed the corresponding discharge limit(s) in your Permit? D Yes 0 No If Yes, add explanation below:

When did you become aware of the exceedance(s)?

8. General comments regarding submission:

9. Certification Statement: "I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties under law for submitting false information, including the possibility of fine and imprisonment for known violations. "

Name (print): Barbara Johnson, PE Title: Authorized Representative for Canadian Pacific

Signature Date: S-11 s-l l.D • ?

Email [email protected] Phone 651-697-9737

Report form help sheet

Page 1of2 SMR-SR-2016

Sample Results: Submit one result sheet for each sampling day per monitoring point. Enter daily values for each sampling event from one monitoring point, in accordance with requirements in the Industrial Discharge Permit (Section 8). Daily and long-term values shall be compared to Discharge Limitations in Permit Section A.1 for compliance determinations. Attach all laboratory data sheets and supporting calculations.

Monitoring Point: _s_P_-0_1 _________________ Description: Effluent discharge line

Sample Start Date & Time: 4/19/1714:05 Sample End Date & Time: _4_11_9_11_7_1_4_:0_5 ______ _

Discharge volume through monitoring point on sampling day: 28, 182 (estimated)

Sample collected by: D Permittee El Other, name: Golder Associates Inc.

gallons

Method of collection: 0 Manual D Automatic

Sample composited by: D Permittee D Other, name: ------------- Composite method: N_A _____________ _

Substance Analytical Result Unit Detection Limits Analysis Method Sample Method

Sample Laboratory Result Container Type Name

pH 6.4 S.U. 0-14 4500-H+ Grab-Single Other Field Measurement

Total Suspended Solids NS Grab - Single NA

Chemical Oxygen Demand NS Grab - Single NA

1, 1-Dichloroethane 0.0196 mg/I 0.00024 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

1, 1-Dichloroethene 0.0058 mg/I 0.00041 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

cis-1,2-Dichloroethene 0.0155 mg/I 0.00026 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

T etrachloroethene 0.0407 mg/I 0.00050 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

1, 1, 1-Trichloroethane 0.0182 mg/I 0.00050 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

Trichloroethane 0.0058 mg/I 0.00033 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

Page 2 of 2 SMR-SR-2016

Attachment B

ANALYTICAL DATA FROM PACE ANALYTICAL SERVICES, LLC

April 2017

#=CL#

April 24, 2017

LIMS USE: FR - ALISON ZOLLLIMS OBJECT ID: 40148633

40148633Project:Pace Project No.:

RE:

Alison ZollGolder Associates Inc.744 Broad Street25th FloorNewark, NJ 07102

023-6105-017 CP-SHOREHAM YARD

Dear Alison Zoll:Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2017. Theresults relate only to the samples included in this report. Results reported herein conform to the mostcurrent, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, whereapplicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Steven Mleczko for

[email protected]

Project Manager

Laurie Woelfel

(920)469-2436

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC1241 Bellevue Street - Suite 9

Green Bay, WI 54302(920)469-2436

Page 1 of 17

#=CP#

CERTIFICATIONS

Pace Project No.:Project:

40148633023-6105-017 CP-SHOREHAM YARD

Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky UST Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334New York Certification #: 12064North Dakota Certification #: R-150

Virginia VELAP ID: 460263South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1Wisconsin Certification #: 405132750Wisconsin DATCP Certification #: 105-444USDA Soil Permit #: P330-16-00157Federal Fish & Wildlife Permit #: LE51774A-0




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#=SS#

SAMPLE SUMMARY


40148633023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID Matrix Date Collected Date Received

40148633001 041917-0800-200 Water 04/19/17 08:00 04/20/17 08:55

40148633002 SE EFFLUENT Water 04/19/17 14:05 04/20/17 08:55




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Page 3 of 17

#=SA#

SAMPLE ANALYTE COUNT


40148633023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

40148633001 041917-0800-200 EPA 8260 71 PASI-GLAP

40148633002 SE EFFLUENT EPA 8260 71 PASI-GLAP




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Page 4 of 17

#=AR#

ANALYTICAL RESULTS


40148633023-6105-017 CP-SHOREHAM YARD

Sample: 041917-0800-200 Lab ID: 40148633001 Collected: 04/19/17 08:00 Received: 04/20/17 08:55 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Analytical Method: EPA 82608260 MSV

Acetone <3.0 ug/L 04/21/17 12:41 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 04/21/17 12:41 107-05-15.0 2.2 1Benzene <0.50 ug/L 04/21/17 12:41 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 04/21/17 12:41 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 04/21/17 12:41 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 04/21/17 12:41 75-27-41.0 0.50 1Bromoform <0.50 ug/L 04/21/17 12:41 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 04/21/17 12:41 74-83-95.0 2.4 12-Butanone (MEK) <3.0 ug/L 04/21/17 12:41 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 04/21/17 12:41 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 04/21/17 12:41 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 04/21/17 12:41 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 04/21/17 12:41 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 04/21/17 12:41 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 04/21/17 12:41 75-00-31.0 0.37 1Chloroform <2.5 ug/L 04/21/17 12:41 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 04/21/17 12:41 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 04/21/17 12:41 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 04/21/17 12:41 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 04/21/17 12:41 96-12-85.0 2.2 1Dibromochloromethane <0.50 ug/L 04/21/17 12:41 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 04/21/17 12:41 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 04/21/17 12:41 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 04/21/17 12:41 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 04/21/17 12:41 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 04/21/17 12:41 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 04/21/17 12:41 75-71-81.0 0.22 11,1-Dichloroethane <0.24 ug/L 04/21/17 12:41 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 04/21/17 12:41 107-06-21.0 0.17 11,1-Dichloroethene <0.41 ug/L 04/21/17 12:41 75-35-41.0 0.41 1cis-1,2-Dichloroethene <0.26 ug/L 04/21/17 12:41 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 04/21/17 12:41 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 04/21/17 12:41 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 04/21/17 12:41 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 04/21/17 12:41 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 04/21/17 12:41 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 04/21/17 12:41 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 04/21/17 12:41 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 04/21/17 12:41 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 04/21/17 12:41 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 04/21/17 12:41 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 04/21/17 12:41 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 04/21/17 12:41 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 04/21/17 12:41 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 04/21/17 12:41 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 04/21/17 12:41 108-10-15.0 2.1 1


without the written consent of Pace Analytical Services, LLC.Date: 04/24/2017 11:03 AM


Green Bay, WI 54302(920)469-2436

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#=AR#

ANALYTICAL RESULTS


40148633023-6105-017 CP-SHOREHAM YARD

Sample: 041917-0800-200 Lab ID: 40148633001 Collected: 04/19/17 08:00 Received: 04/20/17 08:55 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 04/21/17 12:41 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 04/21/17 12:41 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 04/21/17 12:41 103-65-11.0 0.50 1Styrene <0.50 ug/L 04/21/17 12:41 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 04/21/17 12:41 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 04/21/17 12:41 79-34-51.0 0.25 1Tetrachloroethene <0.50 ug/L 04/21/17 12:41 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 04/21/17 12:41 109-99-95.0 2.0 1Toluene <0.50 ug/L 04/21/17 12:41 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 04/21/17 12:41 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 04/21/17 12:41 120-82-15.0 2.2 11,1,1-Trichloroethane <0.50 ug/L 04/21/17 12:41 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 04/21/17 12:41 79-00-51.0 0.20 1Trichloroethene <0.33 ug/L 04/21/17 12:41 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 04/21/17 12:41 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 04/21/17 12:41 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 04/21/17 12:41 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 04/21/17 12:41 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 04/21/17 12:41 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 04/21/17 12:41 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 04/21/17 12:41 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 04/21/17 12:41 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 83 % 04/21/17 12:41 460-00-470-130 1Dibromofluoromethane (S) 105 % 04/21/17 12:41 1868-53-770-130 1Toluene-d8 (S) 95 % 04/21/17 12:41 2037-26-570-130 1




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#=AR#

ANALYTICAL RESULTS


40148633023-6105-017 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40148633002 Collected: 04/19/17 14:05 Received: 04/20/17 08:55 Matrix: Water



Acetone <3.0 ug/L 04/21/17 12:18 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 04/21/17 12:18 107-05-15.0 2.2 1Benzene <0.50 ug/L 04/21/17 12:18 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 04/21/17 12:18 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 04/21/17 12:18 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 04/21/17 12:18 75-27-41.0 0.50 1Bromoform <0.50 ug/L 04/21/17 12:18 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 04/21/17 12:18 74-83-95.0 2.4 12-Butanone (MEK) <3.0 ug/L 04/21/17 12:18 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 04/21/17 12:18 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 04/21/17 12:18 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 04/21/17 12:18 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 04/21/17 12:18 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 04/21/17 12:18 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 04/21/17 12:18 75-00-31.0 0.37 1Chloroform <2.5 ug/L 04/21/17 12:18 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 04/21/17 12:18 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 04/21/17 12:18 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 04/21/17 12:18 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 04/21/17 12:18 96-12-85.0 2.2 1Dibromochloromethane <0.50 ug/L 04/21/17 12:18 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 04/21/17 12:18 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 04/21/17 12:18 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 04/21/17 12:18 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 04/21/17 12:18 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 04/21/17 12:18 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 04/21/17 12:18 75-71-81.0 0.22 11,1-Dichloroethane 19.6 ug/L 04/21/17 12:18 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 04/21/17 12:18 107-06-21.0 0.17 11,1-Dichloroethene 5.8 ug/L 04/21/17 12:18 75-35-41.0 0.41 1cis-1,2-Dichloroethene 15.5 ug/L 04/21/17 12:18 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 04/21/17 12:18 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 04/21/17 12:18 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 04/21/17 12:18 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 04/21/17 12:18 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 04/21/17 12:18 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 04/21/17 12:18 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 04/21/17 12:18 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 04/21/17 12:18 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 04/21/17 12:18 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 04/21/17 12:18 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 04/21/17 12:18 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 04/21/17 12:18 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 04/21/17 12:18 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 04/21/17 12:18 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 04/21/17 12:18 108-10-15.0 2.1 1




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#=AR#

ANALYTICAL RESULTS


40148633023-6105-017 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40148633002 Collected: 04/19/17 14:05 Received: 04/20/17 08:55 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 04/21/17 12:18 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 04/21/17 12:18 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 04/21/17 12:18 103-65-11.0 0.50 1Styrene <0.50 ug/L 04/21/17 12:18 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 04/21/17 12:18 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 04/21/17 12:18 79-34-51.0 0.25 1Tetrachloroethene 40.7 ug/L 04/21/17 12:18 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 04/21/17 12:18 109-99-95.0 2.0 1Toluene <0.50 ug/L 04/21/17 12:18 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 04/21/17 12:18 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 04/21/17 12:18 120-82-15.0 2.2 11,1,1-Trichloroethane 18.2 ug/L 04/21/17 12:18 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 04/21/17 12:18 79-00-51.0 0.20 1Trichloroethene 5.8 ug/L 04/21/17 12:18 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 04/21/17 12:18 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 04/21/17 12:18 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 04/21/17 12:18 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 04/21/17 12:18 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 04/21/17 12:18 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 04/21/17 12:18 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 04/21/17 12:18 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 04/21/17 12:18 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 88 % 04/21/17 12:18 460-00-470-130 1Dibromofluoromethane (S) 98 % 04/21/17 12:18 1868-53-770-130 1Toluene-d8 (S) 95 % 04/21/17 12:18 2037-26-570-130 1




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#=QC#

QUALITY CONTROL DATA


40148633023-6105-017 CP-SHOREHAM YARD

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

253431EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 40148633001, 40148633002

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1495114Associated Lab Samples: 40148633001, 40148633002

Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L <0.18 1.0 04/21/17 07:230.181,1,1-Trichloroethane ug/L <0.50 1.0 04/21/17 07:230.501,1,2,2-Tetrachloroethane ug/L <0.25 1.0 04/21/17 07:230.251,1,2-Trichloroethane ug/L <0.20 1.0 04/21/17 07:230.201,1,2-Trichlorotrifluoroethane ug/L <0.81 5.0 04/21/17 07:230.811,1-Dichloroethane ug/L <0.24 1.0 04/21/17 07:230.241,1-Dichloroethene ug/L <0.41 1.0 04/21/17 07:230.411,1-Dichloropropene ug/L <0.44 1.0 04/21/17 07:230.441,2,3-Trichlorobenzene ug/L <2.1 5.0 04/21/17 07:232.11,2,3-Trichloropropane ug/L <0.50 1.0 04/21/17 07:230.501,2,4-Trichlorobenzene ug/L <2.2 5.0 04/21/17 07:232.21,2,4-Trimethylbenzene ug/L <0.50 1.0 04/21/17 07:230.501,2-Dibromo-3-chloropropane ug/L <2.2 5.0 04/21/17 07:232.21,2-Dibromoethane (EDB) ug/L <0.18 1.0 04/21/17 07:230.181,2-Dichlorobenzene ug/L <0.50 1.0 04/21/17 07:230.501,2-Dichloroethane ug/L <0.17 1.0 04/21/17 07:230.171,2-Dichloropropane ug/L <0.23 1.0 04/21/17 07:230.231,3,5-Trimethylbenzene ug/L <0.50 1.0 04/21/17 07:230.501,3-Dichlorobenzene ug/L <0.50 1.0 04/21/17 07:230.501,3-Dichloropropane ug/L <0.50 1.0 04/21/17 07:230.501,4-Dichlorobenzene ug/L <0.50 1.0 04/21/17 07:230.502,2-Dichloropropane ug/L <0.48 1.0 04/21/17 07:230.482-Butanone (MEK) ug/L <3.0 20.0 04/21/17 07:233.02-Chlorotoluene ug/L <0.50 1.0 04/21/17 07:230.504-Chlorotoluene ug/L <0.21 1.0 04/21/17 07:230.214-Methyl-2-pentanone (MIBK) ug/L <2.1 5.0 04/21/17 07:232.1Acetone ug/L <3.0 20.0 04/21/17 07:233.0Allyl chloride ug/L <2.2 5.0 04/21/17 07:232.2Benzene ug/L <0.50 1.0 04/21/17 07:230.50Bromobenzene ug/L <0.23 1.0 04/21/17 07:230.23Bromochloromethane ug/L <0.34 1.0 04/21/17 07:230.34Bromodichloromethane ug/L <0.50 1.0 04/21/17 07:230.50Bromoform ug/L <0.50 1.0 04/21/17 07:230.50Bromomethane ug/L <2.4 5.0 04/21/17 07:232.4Carbon tetrachloride ug/L <0.50 1.0 04/21/17 07:230.50Chlorobenzene ug/L <0.50 1.0 04/21/17 07:230.50Chloroethane ug/L <0.37 1.0 04/21/17 07:230.37Chloroform ug/L <2.5 5.0 04/21/17 07:232.5Chloromethane ug/L <0.50 1.0 04/21/17 07:230.50cis-1,2-Dichloroethene ug/L <0.26 1.0 04/21/17 07:230.26cis-1,3-Dichloropropene ug/L <0.50 1.0 04/21/17 07:230.50




Green Bay, WI 54302(920)469-2436

Page 9 of 17

#=QC#



40148633023-6105-017 CP-SHOREHAM YARD


Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1495114Associated Lab Samples: 40148633001, 40148633002

Matrix: Water

AnalyzedMDL

Dibromochloromethane ug/L <0.50 1.0 04/21/17 07:230.50Dibromomethane ug/L <0.43 1.0 04/21/17 07:230.43Dichlorodifluoromethane ug/L <0.22 1.0 04/21/17 07:230.22Dichlorofluoromethane ug/L <0.21 1.0 04/21/17 07:230.21Diethyl ether (Ethyl ether) ug/L <2.2 5.0 04/21/17 07:232.2Ethylbenzene ug/L <0.50 1.0 04/21/17 07:230.50Hexachloro-1,3-butadiene ug/L <2.1 5.0 04/21/17 07:232.1Isopropylbenzene (Cumene) ug/L <0.14 1.0 04/21/17 07:230.14m&p-Xylene ug/L <1.0 2.0 04/21/17 07:231.0Methyl-tert-butyl ether ug/L <0.17 1.0 04/21/17 07:230.17Methylene Chloride ug/L <0.23 1.0 04/21/17 07:230.23n-Butylbenzene ug/L <0.50 1.0 04/21/17 07:230.50n-Propylbenzene ug/L <0.50 1.0 04/21/17 07:230.50Naphthalene ug/L <2.5 5.0 04/21/17 07:232.5o-Xylene ug/L <0.50 1.0 04/21/17 07:230.50p-Isopropyltoluene ug/L <0.50 1.0 04/21/17 07:230.50sec-Butylbenzene ug/L <2.2 5.0 04/21/17 07:232.2Styrene ug/L <0.50 1.0 04/21/17 07:230.50tert-Butylbenzene ug/L <0.18 1.0 04/21/17 07:230.18Tetrachloroethene ug/L <0.50 1.0 04/21/17 07:230.50Tetrahydrofuran ug/L <2.0 5.0 04/21/17 07:232.0Toluene ug/L <0.50 1.0 04/21/17 07:230.50trans-1,2-Dichloroethene ug/L <0.26 1.0 04/21/17 07:230.26trans-1,3-Dichloropropene ug/L <0.23 1.0 04/21/17 07:230.23Trichloroethene ug/L <0.33 1.0 04/21/17 07:230.33Trichlorofluoromethane ug/L <0.18 1.0 04/21/17 07:230.18Vinyl chloride ug/L <0.18 1.0 04/21/17 07:230.184-Bromofluorobenzene (S) % 90 70-130 04/21/17 07:23Dibromofluoromethane (S) % 98 70-130 04/21/17 07:23Toluene-d8 (S) % 94 70-130 04/21/17 07:23

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1495115LABORATORY CONTROL SAMPLE:LCSSpike

1,1,1-Trichloroethane ug/L 55.050 110 70-1311,1,2,2-Tetrachloroethane ug/L 46.650 93 67-1301,1,2-Trichloroethane ug/L 52.850 106 70-1301,1,2-Trichlorotrifluoroethane ug/L 60.650 121 50-1501,1-Dichloroethane ug/L 51.650 103 70-1331,1-Dichloroethene ug/L 53.150 106 70-1301,2,4-Trichlorobenzene ug/L 43.950 88 70-1301,2-Dibromo-3-chloropropane ug/L 39.750 79 50-1501,2-Dibromoethane (EDB) ug/L 51.050 102 70-1301,2-Dichlorobenzene ug/L 51.950 104 70-130




Green Bay, WI 54302(920)469-2436

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#=QC#



40148633023-6105-017 CP-SHOREHAM YARD


Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1495115LABORATORY CONTROL SAMPLE:LCSSpike

1,2-Dichloroethane ug/L 51.850 104 70-1301,2-Dichloropropane ug/L 52.950 106 70-1301,3-Dichlorobenzene ug/L 49.550 99 70-1301,4-Dichlorobenzene ug/L 50.250 100 70-130Benzene ug/L 54.050 108 60-135Bromodichloromethane ug/L 53.950 108 70-130Bromoform ug/L 56.850 114 70-130Bromomethane ug/L 45.450 91 33-130Carbon tetrachloride ug/L 56.750 113 70-138Chlorobenzene ug/L 53.050 106 70-130Chloroethane ug/L 45.950 92 51-130Chloroform ug/L 51.050 102 70-130Chloromethane ug/L 45.550 91 25-132cis-1,2-Dichloroethene ug/L 53.350 107 69-130cis-1,3-Dichloropropene ug/L 49.350 99 70-130Dibromochloromethane ug/L 53.650 107 70-130Dichlorodifluoromethane ug/L 45.150 90 23-130Ethylbenzene ug/L 56.550 113 70-136Isopropylbenzene (Cumene) ug/L 57.250 114 70-140m&p-Xylene ug/L 116100 116 70-138Methyl-tert-butyl ether ug/L 50.950 102 66-138Methylene Chloride ug/L 48.850 98 70-130o-Xylene ug/L 57.250 114 70-134Styrene ug/L 57.850 116 70-133Tetrachloroethene ug/L 55.750 111 70-138Toluene ug/L 56.450 113 70-130trans-1,2-Dichloroethene ug/L 50.750 101 70-131trans-1,3-Dichloropropene ug/L 51.750 103 69-130Trichloroethene ug/L 58.650 117 70-130Trichlorofluoromethane ug/L 55.050 110 50-150Vinyl chloride ug/L 53.650 107 49-1304-Bromofluorobenzene (S) % 104 70-130Dibromofluoromethane (S) % 95 70-130Toluene-d8 (S) % 99 70-130

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1495155MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40148659001

1495156

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1-Trichloroethane ug/L 50 111 70-134109 2 20504.6 60.1 59.01,1,2,2-Tetrachloroethane ug/L 50 91 67-13097 6 2050<0.25 45.7 48.61,1,2-Trichloroethane ug/L 50 99 70-130101 2 2050<0.20 49.4 50.41,1,2-Trichlorotrifluoroethane ug/L 50 119 50-150114 5 2050<0.81 59.6 57.01,1-Dichloroethane ug/L 50 98 70-13497 0 205018.1 67.1 66.81,1-Dichloroethene ug/L 50 103 68-136103 0 2050<0.41 51.7 51.7




Green Bay, WI 54302(920)469-2436

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#=QC#



40148633023-6105-017 CP-SHOREHAM YARD


Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1495155MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40148659001

1495156

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L 50 90 62-13990 0 2050<2.2 45.0 45.11,2-Dibromo-3-chloropropane

ug/L 50 93 50-15095 2 2050<2.2 46.3 47.4

1,2-Dibromoethane (EDB) ug/L 50 94 70-130101 7 2050<0.18 47.2 50.71,2-Dichlorobenzene ug/L 50 98 70-13098 1 2050<0.50 49.1 48.81,2-Dichloroethane ug/L 50 100 70-130101 2 2050<0.17 49.8 50.61,2-Dichloropropane ug/L 50 103 70-130103 0 2050<0.23 51.4 51.51,3-Dichlorobenzene ug/L 50 95 70-13199 4 2050<0.50 47.6 49.61,4-Dichlorobenzene ug/L 50 97 70-13098 1 2050<0.50 48.7 49.1Benzene ug/L 50 106 57-138103 2 2050<0.50 52.8 51.7Bromodichloromethane ug/L 50 101 70-130109 7 2050<0.50 50.7 54.6Bromoform ug/L 50 108 70-130108 0 2050<0.50 53.8 54.0Bromomethane ug/L 50 94 33-13095 1 2750<2.4 47.1 47.5Carbon tetrachloride ug/L 50 109 70-138109 0 2050<0.50 54.6 54.5Chlorobenzene ug/L 50 97 70-130102 5 2050<0.50 48.5 50.8Chloroethane ug/L 50 93 51-13090 3 2050<0.37 46.6 45.1Chloroform ug/L 50 102 70-130102 0 2050<2.5 50.8 50.9Chloromethane ug/L 50 86 25-13287 1 2050<0.50 43.2 43.6cis-1,2-Dichloroethene ug/L 50 105 61-140101 4 20507.0 59.6 57.2cis-1,3-Dichloropropene ug/L 50 98 70-13096 3 2050<0.50 49.2 47.8Dibromochloromethane ug/L 50 101 70-130107 5 2050<0.50 50.6 53.3Dichlorodifluoromethane ug/L 50 87 23-13085 2 2050<0.22 43.7 42.7Ethylbenzene ug/L 50 105 70-138108 3 2050<0.50 52.4 54.1Isopropylbenzene (Cumene) ug/L 50 106 70-152110 4 2050<0.14 52.9 55.0m&p-Xylene ug/L 100 106 70-140108 1 20100<1.0 106 108Methyl-tert-butyl ether ug/L 50 100 66-139100 0 2050<0.17 49.9 49.9Methylene Chloride ug/L 50 101 70-13099 1 2050<0.23 50.3 49.7o-Xylene ug/L 50 108 70-134109 1 2050<0.50 54.0 54.6Styrene ug/L 50 106 70-138109 3 2050<0.50 52.9 54.3Tetrachloroethene ug/L 50 106 70-148110 3 20503.7 56.9 58.7Toluene ug/L 50 104 70-130110 6 2050<0.50 51.8 54.9trans-1,2-Dichloroethene ug/L 50 101 70-133103 3 2050<0.26 50.3 51.7trans-1,3-Dichloropropene ug/L 50 97 69-13099 2 2050<0.23 48.4 49.5Trichloroethene ug/L 50 109 70-131115 5 20501.2 55.6 58.7Trichlorofluoromethane ug/L 50 108 50-150107 1 2050<0.18 54.0 53.6Vinyl chloride ug/L 50 102 49-133100 2 2050<0.18 51.1 50.04-Bromofluorobenzene (S) % 96 70-13095Dibromofluoromethane (S) % 93 70-13094Toluene-d8 (S) % 92 70-13095




Green Bay, WI 54302(920)469-2436

Page 12 of 17

#=QL#

QUALIFIERS


40148633023-6105-017 CP-SHOREHAM YARD

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Green BayPASI-G




Green Bay, WI 54302(920)469-2436

Page 13 of 17

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE


40148633023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

40148633001 253431041917-0800-200 EPA 826040148633002 253431SE EFFLUENT EPA 8260




Green Bay, WI 54302(920)469-2436

Page 14 of 17

Pag

e 15

of 1

7

Company Name:

A=None B=HCL C=H2S04 D=HN03

Sampled By (Sign):

H=Sodium Bisulfate Solution

FILTERED? (YES/NO)

PRESERVATION (CODE)•

PO#: Regulatory Program:

MS/MSD On your sample

(billable) NOT needed on

your sample

Rush Turnaround Time Requested - Prelims (Rush TAT subject to approval/surcharge)

Date Needed: Transmit Prelim Rush Results by (complete what you want):

Emall#1:

Emall#2: Telephone:

Fax:

Samples on HOLD are subject to

special pricing and release of llablllty

C019a(27 Jun2006)

Matrix Codes W=Water OW = Drinking Water GW = Ground Water SW Surface Water

Relinquished By:

!::::Sodium Thiosulfate

Date/Time:

UPPER MIDWEST REGION

MN: 612-607-1700 WI: 920-469-2

F=Methanol G=NaOH J=Other

Received By:

I '1 J

LI Lf:> Received By:

Received By:

Quote#:

Mail To Contact:

Mail To Company:

Mail To Address:

invoice To Contact:

Invoice To Company:

Invoice To Address:

Invoice To Phone:

CLIENT COMMENTS

Datemme:

LAB COMMENTS (lab Use Only)

Profile#

PACE Project No.

L/QfL(~ -33 l.Q oc

Sample Receipt pH

OK I Adjusted

of 17

~eAnalytica!" Document Name: Revised Dale: 28Sep2016

Minneapolis Cooler Transfer Check List Page 1 of 1

Document Number: Issuing Authority: ( F-MN-C-214-Rev 01 Pace Minnesota Quality Office

Minneapolis Service Center Cooler Transfer Check List

Client:

Received with Custody Seal: Yes

Temp Read Corrected Temp Correction Factor

Temperature C: IR Gun

~ Samples on ice, cooling process has begun

Rush/Short Hold:

Containers Intact: No

Re-packed and Re-Iced:

Temp Blank Included: Yes No

Shipped By/Date:

Notes

of 17

Sample Condition Upon Receipt

ace Analytical'

Pace Analytical Services, Inc. 1241 Bellevue Street, Suite 9

Green Bay, WI 54302

1Client Name: (,to\d.e..r A~Soe.,~ u.:l~ Courier: r Fed Ex r UPS :- Client r Pace,ither: fA)olff!JJ

Project#: W0#:40148633 1111111111111111111111

Tracking#: I o3Ji '?:><ts-t 40148633

Custody Seal on Cooler/Box Present: r yes 7 no Seals intact: r yes r no

(!)custody Seal on Samples Present: r yes Y"no Seals intact: r yes - no

Packing Material: J7'Bubble Wrap r7Bubble Bags r~e r Other

Thermometer Used 'CJ R- "".)~ Type of Ice: Wet Blue Dry None P""'samples on ice, cooling process has begun

Cooler Temperature Uncorr: lQ /Corr: {Q Bio ogical Tissue is Frozen: r yes

Temp Blank Present: ryes J7'no r no Personi/..amining contents:

Temp should be above freezing to 6°C for all sample except Biota. Date: ~f/ Frozen Biota Samples should be received s 0°C. Comments: Initials: -~

Chain of Custody Present: ~es ONo ON/A 1.

Chain of Custody Filled Out: i:;;rYes ONo ON/A 2.

Chain of Custody Relinquished: y{ves 0No ON/A 3.

Sampler Name & Signature on COC: r;<fves ONo ON/A 4.

Samples Arrived within Hold Time: pves ONo ON/A 5.

- VOA Samples frozen upon receipt OYes ONo Dateffime:

Short Hold Time Analysis (<72hr): OYes Qi(io ON/A 6.

Rush Turn Around Time Requested: 0Yes ~o ON/A 7.

Sufficient Volume: r/ves ONo ON/A 8.

Correct Containers Used: ~es ONo ON/A 9.

-Pace Containers Used: 'fves ONo ON/A

-Pace IR Containers Used: OYes ONo ~/A

Containers Intact: c;W'es ONo ON/A 10.

Filtered volume received for Dissolved tests OYes ONo ~/A 11.

Sample Labels match COC: OYes izf'No ON/A 12.00\ 1.. "\tl4 At-\~)used t°t3etlur -Includes date/time/ID/Analysis Matrix: ( 1..) ~\th \ \o}otl id- 4 \ t-()\ \

All containers needing preservation have been checked. ..!J!::. . (Non-Compliance noted in 13.) OYes 0No /A 13.

r HN03 r H2S04 rNaOH r NaOH +ZnAct

---------------- ----------------- ---All containers needing preservation are found to be in compliance with EPA recommendation. OYes ONo Ji'itA (HN03, H2S04 s2; NaOH+ZnAct :2:9, NaOH ~12) e;;ptlo;;; ~ ;oiif~~ ioC: TOX, TOH, - - - - - - - - - l/<~ -- --- -- Initial when I Lab Std #ID of lua1e1 O&G, WIDRO , Phenolics, OTHER: es 0No completed preservative Time:

Headspace in VOA Vials ( >6mm): OYes J2fNo ON/A 14.

Trip Blank Present: ~es ONo ON/A 15.

Trip Blank Custody Seals Present J"es ONo ON/A

Pace Trip Blank Lot# (if purchased):

Client Notification/ Resolution: If checked, see attached form for additional comments U Person Contacted: Date/Time:

Comments/ ResolutionlP""'""strap--...--.,,...-a-£0-u_iiC___./ ___ c_, 00-....-~

I

Project Manager Review: Date: _'-l .... \.,..u...,\~o-----F-GB-C-031-Rev.03 (9April2015) SCUR Form

Attachment C

FIELD INSTRUMENT pH CALIBRATION RECORDS

,.Golder \9Lsociates Field Instrument pH Calibration Records

Page _l_of_ l _

INSTRUMENT (MAKE/MODEL NO.) Sper Scientific/850051 INSTRUMENT NO .. _____ _

STANDARD INFORMATION

Project Number: 0236105017 Project Name: CP-Shoreham Yard

Standard Vendor: Field Environmental Instruments

Prepared Date: NA Where Prepared: NA

Purchase Date: 11 /17/2016 Expiration Date: Varies Grade: NIA Units: Standard Units

Standard 4.0@25°C Lot# F158-18 ExpDate 6/14/18

Standard 7.0@25 °c Lot# F172-18 Exp Date 6/29/18

Standard 10 0 ®25 °c Lot# F124-01 ExD Date 5/10/17 DATE TIME TEMP STD INSTRUMENT

%DEV PASS/ CALIBRATED SAMPLER

(mm/dd/w\ (hr.min! DEGC VALUE RESPONSE FAIL (YES, NO) INITIALS

it/11; 11 l)LfS 17.0 7 .() 7 .0 0 p y _fp '1/l't//7 ns-o 17.s- '1.0 Lf. .o 0 p y Aff

4 /l't( fl l lfOO 17,) lo.o l (). 0 d \ y 4-f

Acceptable calibration check is if the meter reads within +/- 0.2 pH units of the value of appropriate calibration standard.

\MIN 1-V-FS l\Projects Golder Projects 023 PROJECTS 023-61 OS Shoreham Yard File Review East Side Southeast P&T System Data\20 I 7\pH Calibration Fonn.doc

Golder Associates REV-2-03/07

golder associates - cpr.ca · pdf filegolder associates may 15, 2017 metropolitan council...

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